CN113979638A - Preparation method of protruded blood vessel-shaped transmutation glaze and transmutation glaze porcelain - Google Patents
Preparation method of protruded blood vessel-shaped transmutation glaze and transmutation glaze porcelain Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/20—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
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Abstract
The invention relates to a preparation method of raised blood vessel-shaped transmutation glaze and transmutation glaze porcelain, and belongs to the technical field of ceramics. The transmutation glaze comprises the following components in parts by weight: 18-22 parts of potash feldspar, 28-32 parts of calcite, 18-22 parts of zinc oxide, 4-8 parts of Guizhou soil, 24-27 parts of spodumene, 10-15 parts of frit, 3-5 parts of aluminum powder, 12-17 parts of a reactant and 10-12 parts of a chromophore.
Description
Technical Field
The invention belongs to the technical field of ceramics, and particularly relates to a preparation method of a protruded blood vessel-shaped transmutation glaze and transmutation glaze porcelain.
Background
The 'transmutation' is a name for deviating the glaze color from the original color generation phenomenon in the firing process, and modern researches show that the transmutation has both a chemical mechanism and a physical action, although the mechanism of the transmutation cannot be comprehensively mastered, the generation of the transmutation can be known, and one or all of the following conditions are required: 1) coloring elements in the glaze have various color generation capacities; 2) other trace coloring elements exist in the glaze; 3) the presence of elements in the base glaze which may promote an uneven distribution of the enamel layer; 4) the sintering temperature is higher, the time is long, and the cooling is proper and slow; 5) the glaze bottom and the overglaze have certain physical and chemical reactions and the like.
Most of the porcelain manufactured by the existing furnace transmutation glaze porcelain through natural furnace transmutation has different colors and stripes, has no higher artistry, obtains specific patterns through artificially drawing pigments, and has poor natural texture effect. The invention obtains a glaze surface which is interlaced vertically and horizontally and exactly like blood vessels under natural transmutation through unique glaze components, proportion and firing process.
Disclosure of Invention
In order to solve the technical problems mentioned in the background technology, the invention provides a raised blood vessel-shaped transmutation glaze and a preparation method of transmutation glaze porcelain.
The purpose of the invention can be realized by the following technical scheme:
the protruded vessel-shaped transmutation glaze comprises the following raw materials in parts by weight: 18-22 parts of potash feldspar, 28-32 parts of calcite, 18-22 parts of zinc oxide, 4-8 parts of Guizhou soil, 24-27 parts of spodumene, 10-15 parts of frit, 3-5 parts of aluminum powder, 12-17 parts of a reactant and 10-12 parts of a chromophore;
further, the protruded vessel-shaped transmutation glaze comprises the following raw materials in parts by weight: 20 parts of potash feldspar, 30 parts of calcite, 20 parts of zinc oxide, 5 parts of Guizhou soil, 25 parts of spodumene, 15 parts of frit, 5 parts of aluminum powder, 15 parts of a reactant and 10 parts of a chromophore;
the protruded vessel-shaped transmutation glaze is prepared by the following method:
step A1: crushing and grinding the raw materials respectively until the raw materials pass through a 80-mesh screen, weighing the materials in parts by weight, stirring and mixing to obtain prefabricated powder;
step A2: adding the prefabricated powder and water into a wet ball mill for repeated ball milling to obtain basic glaze slurry;
step A3: adding water into the basic glaze slip under the stirring state, adjusting the concentration of the glaze slip to 52-58 baume degrees, and preparing the protruding vessel-shaped transmutation glaze for later use.
Further, the chromophore comprises copper oxide and cobalt oxide, and the mass ratio of the copper oxide to the cobalt oxide is 1: 1.
Further, the reactant is rutile titanium dioxide.
Further, in step a2, the ball of the ball mill is controlled: material preparation: the water ratio is 1.5-1.8:1.1-1.3:0.5-0.7, and the fineness of ball milling glaze slurry of a ball mill is controlled to be 0.1-0.2 percent of the screen allowance of a 250-mesh screen.
A preparation method of the protruded vessel-shaped transmutation glazed porcelain comprises the following steps:
step S1: placing the trimmed porcelain blank into a kiln, and carrying out biscuit firing at the kiln temperature of 750-810 ℃ for 1-1.5h to obtain a biscuit;
step S2: immersing the biscuit in the transmutation glaze to carry out glaze immersion to obtain a glaze blank, and controlling the thickness of a glaze layer to be 0.3-0.5 mm;
step S3: and (3) placing the glaze blank into a kiln, firing in an oxidizing atmosphere, and cooling after firing to obtain the protruded vessel-shaped transmutation glaze porcelain.
Further, in step S3, the firing process has three firing temperature control stages:
the first stage is as follows: the temperature of the kiln is increased from normal temperature to 550-600 ℃, and the temperature increasing rate is 30-40 ℃/h;
and a second stage: the temperature of the kiln is raised to 1150-1230 ℃, the temperature raising rate is 60-70 ℃/h, and the constant temperature firing is carried out for 2-2.5h after the preset furnace temperature is reached;
and a third stage: stopping heating, and after the furnace temperature is rapidly cooled to 680-700 ℃, controlling the cooling speed to be 10-20 ℃/h and cooling to the room temperature.
The invention has the beneficial effects that:
according to the invention, through unique glaze components and proportion, the prepared porcelain glaze presents semi-matte luster, all components interact, and the prepared porcelain glaze presents mutually interlaced longitudinal and transverse vein-shaped stripes by matching with a specific firing process, is exactly like raised blood vessels, is similar to a porcelain, has a common life, and greatly improves the artistry and commercial value of the porcelain.
Drawings
FIG. 1 is a schematic view of a porcelain glaze prepared in example 4 of the present invention;
FIG. 2 is a schematic view of a porcelain glaze prepared in example 5 of the present invention;
fig. 3 is a schematic view of a porcelain glaze obtained in example 6 of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the examples:
the reactant is commercially available rutile titanium dioxide;
the frit is a commercially available frit, and the type of the frit is JM 669;
crushing and grinding the raw materials, sieving the raw materials by a 80-mesh sieve, and taking the sieved powder;
the chromophore is prepared by mixing copper oxide and cobalt oxide according to the mass ratio of 1:1, and the mixture is used as the liquid.
Example 1
The preparation method of the raised blood vessel-shaped transmutation glaze comprises the following specific implementation processes:
step A1: taking 1.8kg of potash feldspar, 2.8kg of calcite, 1.8kg of zinc oxide, 0.4kg of Guizhou soil, 2.4kg of spodumene, 1kg of frit, 0.3kg of aluminum powder, 1.2kg of reactant and 1kg of chromophore, adding into a stirrer, and fully stirring and mixing for 20min at the rotating speed of 360r/min to obtain prefabricated powder;
step A2: adding the prefabricated powder and water into a wet ball mill, and controlling the ball: material preparation: setting the water ratio to be 1.5:1.1:0.5, and ball-milling the glaze slurry by a ball mill with the screen residue of a 250-mesh screen to be 0.1 percent to obtain basic glaze slurry;
step A3: and adding clear water into the basic glaze slip under the stirring state, adjusting the concentration of the glaze slip to 52 baume degrees, and preparing the protruding vessel-shaped transmutation glaze for later use.
Example 2
The preparation method of the raised blood vessel-shaped transmutation glaze comprises the following specific implementation processes:
step A1: adding 2kg of potash feldspar, 3kg of calcite, 2kg of zinc oxide, 0.5kg of Guizhou soil, 2.5kg of spodumene, 1.5kg of frit, 0.5kg of aluminum powder, 1.5kg of reactant and 1kg of chromophore into a stirrer, and fully stirring and mixing for 20min at the rotating speed of 360r/min to obtain prefabricated powder;
step A2: adding the prefabricated powder and water into a wet ball mill, and controlling the ball: material preparation: setting the water ratio to be 1.6:1.2:0.6, and ball-milling the glaze slurry by a ball mill with the screen allowance of 0.1 percent of a 250-mesh screen to obtain basic glaze slurry;
step A3: and adding clear water into the basic glaze slip under the stirring state, adjusting the concentration of the glaze slip to 55 baume degrees, and preparing the protruding vessel-shaped transmutation glaze for later use.
Example 3
The preparation method of the raised blood vessel-shaped transmutation glaze comprises the following specific implementation processes:
step A1: adding 2.2kg of potash feldspar, 3.2kg of calcite, 2.2kg of zinc oxide, 0.8kg of Guizhou soil, 2.7kg of spodumene, 1.5kg of frit, 0.5kg of aluminum powder, 1.7kg of reactant and 1.2kg of chromophore into a stirrer, and fully stirring and mixing for 20min at the rotating speed of 360r/min to obtain prefabricated powder;
step A2: adding the prefabricated powder and water into a wet ball mill, and controlling the ball: material preparation: setting the water ratio to be 1.8:1.3:0.7, and ball-milling the glaze slurry by a ball mill with the screen residue of a 250-mesh screen to be 0.2 percent to obtain basic glaze slurry;
step A3: and adding clear water into the basic glaze slip under the stirring state, adjusting the concentration of the glaze slip to 58 baume degrees, and preparing the protruded vessel-shaped transmutation glaze for later use.
Example 4
The embodiment prepares a protruding blood vessel form transmutation glaze porcelain, and the concrete implementation process is as follows:
step S1: placing the trimmed porcelain blank into a kiln, and carrying out biscuit firing at the kiln temperature of 750 ℃ for 1.5h to obtain a biscuit;
step S2: immersing the biscuit in transmutation glaze to carry out glaze immersion to obtain a glaze blank, and controlling the thickness of a glaze layer within 0.3-0.5 mm;
step S3: and (3) placing the glaze blank into a kiln, firing in an oxidizing atmosphere, and cooling after firing to obtain the protruded vessel-shaped transmutation glaze porcelain.
The firing process has three firing temperature control stages:
the first stage is as follows: the temperature of the kiln is increased from normal temperature to 550 ℃, and the temperature increasing rate is kept at 30 ℃/h;
and a second stage: the temperature of the kiln is increased to 1150 ℃, the temperature increasing rate is kept at 60 ℃/h, and the constant temperature firing is carried out for 2.5h after the preset furnace temperature is reached;
and a third stage: stopping heating, rapidly cooling to 680 deg.C, and cooling to room temperature at a cooling rate of 10 deg.C/h.
Example 5
The embodiment prepares a protruding blood vessel form transmutation glaze porcelain, and the concrete implementation process is as follows:
step S1: putting the trimmed porcelain blank into a kiln, and carrying out biscuit firing at the kiln temperature of 780 ℃ for 1.2h to obtain a biscuit;
step S2: immersing the biscuit in the transmutation glaze to carry out glaze immersion to obtain a glaze blank, and controlling the thickness of a glaze layer within 0.3-0.5 mm;
step S3: and (3) placing the glaze blank into a kiln, firing in an oxidizing atmosphere, and cooling after firing to obtain the protruded vessel-shaped transmutation glaze porcelain.
The firing process has three firing temperature control stages:
the first stage is as follows: the temperature of the kiln is increased from normal temperature to 600 ℃, and the temperature increasing rate is kept at 35 ℃/h;
and a second stage: the temperature of the kiln is raised to 1200 ℃, the temperature raising rate is kept to 65 ℃/h, and the constant temperature firing is carried out for 2h after the preset furnace temperature is reached;
and a third stage: stopping heating, rapidly cooling to 700 deg.C, and cooling to room temperature at 15 deg.C/h.
Example 6
The embodiment prepares a protruding blood vessel form transmutation glaze porcelain, and the concrete implementation process is as follows:
step S1: placing the trimmed porcelain blank into a kiln, and carrying out biscuit firing at the kiln temperature of 810 ℃ for 1h to obtain a biscuit;
step S2: immersing the biscuit in the transmutation glaze to carry out glaze immersion to obtain a glaze blank, and controlling the thickness of a glaze layer within 0.3-0.5 mm;
step S3: and (3) placing the glaze blank into a kiln, firing in an oxidizing atmosphere, and cooling after firing to obtain the protruded vessel-shaped transmutation glaze porcelain.
The firing process has three firing temperature control stages:
the first stage is as follows: the temperature of the kiln is raised from normal temperature to 600 ℃, and the temperature raising rate is kept at 40 ℃/h;
and a second stage: the temperature of the kiln is increased to 1230 ℃, the temperature increasing rate is kept at 70 ℃/h, and the kiln is fired for 2h at constant temperature after reaching the preset furnace temperature;
and a third stage: stopping heating, rapidly cooling to 700 deg.C, and cooling to room temperature at 20 deg.C/h.
Referring to fig. 1-3, the glaze of the porcelain prepared in examples 4-6 has semi-matte luster, and the glaze of the porcelain also has interlaced longitudinal and transverse vein-like stripes, which are similar to raised blood vessels, so that the porcelain has life, and the artistry and commercial value of the porcelain are greatly improved.
In the description herein, references to the description of "one embodiment," "an example," "a specific example" or the like are intended to mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.
The foregoing is merely exemplary and illustrative of the principles of the present invention and various modifications, additions and substitutions of the specific embodiments described herein may be made by those skilled in the art without departing from the principles of the present invention or exceeding the scope of the claims set forth herein.
Claims (6)
1. The protruded vessel-shaped transmutation glaze is characterized by comprising the following raw materials in parts by weight: 18-22 parts of potash feldspar, 28-32 parts of calcite, 18-22 parts of zinc oxide, 4-8 parts of Guizhou soil, 24-27 parts of spodumene, 10-15 parts of frit, 3-5 parts of aluminum powder, 12-17 parts of a reactant and 10-12 parts of a chromophore;
the protruded vessel-shaped transmutation glaze is prepared by the following method:
step A1: respectively crushing, grinding and screening the raw materials, and stirring and mixing the materials under screening to obtain prefabricated powder;
step A2: adding the prefabricated powder and water into a wet ball mill according to the proportion for ball milling to obtain basic glaze slurry;
step A3: and adding water into the basic glaze slip under the stirring state, and adjusting the concentration of the glaze slip to 52-58 baume degrees to obtain the protruded vessel-shaped transmutation glaze.
2. The raised vessel-shaped transmutation glaze according to claim 1, characterized by comprising the following raw materials in parts by weight: 20 parts of potash feldspar, 30 parts of calcite, 20 parts of zinc oxide, 5 parts of Guizhou soil, 25 parts of spodumene, 15 parts of frit, 5 parts of aluminum powder, 15 parts of a reactant and 10 parts of a chromophore.
3. The raised vessel-shaped transmutation glaze according to claim 1, wherein the chromophore comprises copper oxide and cobalt oxide, and the mass ratio of the copper oxide to the cobalt oxide is 1: 1.
4. The raised vessel-shaped transmutation glaze according to claim 1, wherein in the step A2, the ball of the ball mill is controlled to have a ball: material preparation: the water ratio is 1.5-1.8:1.1-1.3:0.5-0.7, and the screen allowance of the glaze slip with the fineness of 250 meshes is 0.1-0.2%.
5. A preparation method of the protruded vessel-shaped transmutation glaze porcelain by adopting the protruded vessel-shaped transmutation glaze of claim 1 for firing is characterized by comprising the following steps:
step S1: placing the trimmed porcelain blank into a kiln, and carrying out biscuit firing at the kiln temperature of 750-810 ℃ for 1-1.5h to obtain a biscuit;
step S2: immersing the biscuit in the transmutation glaze to carry out glaze immersion to obtain a glaze blank, and controlling the thickness of a glaze layer to be 0.3-0.5 mm;
step S3: and (3) placing the glaze blank into a kiln, firing in an oxidizing atmosphere, and cooling after firing to obtain the protruded vessel-shaped transmutation glaze porcelain.
6. The method for preparing raised vessel-shaped fambe glazed porcelain according to claim 5, wherein in step S3, the firing process has three firing temperature control stages:
the first stage is as follows: the temperature of the kiln is increased from normal temperature to 550-600 ℃, and the temperature increasing rate is 30-40 ℃/h;
and a second stage: the temperature of the kiln is raised to 1150-1230 ℃, the temperature raising rate is 60-70 ℃/h, and the constant temperature firing is carried out for 2-2.5h after the preset furnace temperature is reached;
and a third stage: stopping heating, rapidly cooling to 680-700 ℃, and then cooling to room temperature at a cooling speed of 10-20 ℃/h.
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| CN111977981A (en) * | 2020-08-31 | 2020-11-24 | 福建省德化中发陶瓷有限公司 | German white porcelain decorated by Jun porcelain textures and preparation method thereof |
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| US6348425B1 (en) * | 1999-07-05 | 2002-02-19 | Ferro Corporation | Crystallizing glaze system |
| CN103253987A (en) * | 2013-05-24 | 2013-08-21 | 醴陵陶润实业发展有限公司 | Method for manufacturing metal glaze |
| CN107879630A (en) * | 2017-12-11 | 2018-04-06 | 程莉 | Particle flow track glaze glaze and preparation method thereof |
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| CN111003942A (en) * | 2020-01-08 | 2020-04-14 | 湖南泰鑫瓷业有限公司 | Frost crystal glaze and preparation method thereof |
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