CN111977981A - German white porcelain decorated by Jun porcelain textures and preparation method thereof - Google Patents
German white porcelain decorated by Jun porcelain textures and preparation method thereof Download PDFInfo
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- CN111977981A CN111977981A CN202010897595.0A CN202010897595A CN111977981A CN 111977981 A CN111977981 A CN 111977981A CN 202010897595 A CN202010897595 A CN 202010897595A CN 111977981 A CN111977981 A CN 111977981A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
- C03C8/08—Frit compositions, i.e. in a powdered or comminuted form containing phosphorus
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
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Abstract
The invention relates to the technical field of ceramic manufacturing, in particular to a denuded white porcelain decorated by Jun porcelain textures and a preparation method thereof. The prepared German white porcelain with the decorated Jun porcelain textures has the advantages that a strip of raised strip-shaped textures, such as grains allowing earthworms to climb, is displayed under the Jun porcelain texture surface glaze, the Jun porcelain texture surface glaze layer is bright, thick and jade-like, the Jun porcelain texture surface glaze is matched with the raw material of the earthworm-walking mud texture ground glaze, the combination of the raw materials and the earthworm-walking mud texture ground glaze is good, the firing rate is improved, the thickness of the glaze layers of the Jun porcelain texture surface glaze layer and the Jun porcelain texture surface glaze layer is limited, the prepared ceramic product can improve the jade effect of the German white porcelain and clearly express the earthworm-walking mud texture.
Description
Technical Field
The invention relates to the technical field of ceramic manufacturing, in particular to a denuded white porcelain decorated by Jun porcelain textures and a preparation method thereof.
Background
Jun porcelain is a unique style which is synthesized on the basis of the styles of kiln construction and Yaozhou kilns, and the earthworm mud-walking line is one of the main characteristics of the Jun porcelain. Jun porcelain, which has such a texture, is coated on the glaze surface as if the trace left by the earthworms walking and crawling in the soil. The book entitled "drink flow vegetarian said porcelain" (a book of writings): the glaze of the jun kiln is flat, the tear mark is called when the inner coarse grain is vertical and vertical, and the mud mark is called when the earthworms bend flatly. This is because the glaze layer cracks during drying or firing, and glaze flows into and fills up the glaze layer at a high temperature. The Jun glaze layer is particularly thick, and the porcelain body is subjected to biscuit firing before glazing, so that the phenomena of cracks, glaze shrinkage and the like occur.
Jun porcelain and German white porcelain are wonderful flowers in Chinese porcelain, the German porcelain industry is documented in Tang Dynasty, and the green and white porcelain is fired in Song and Yuan seasons, and is greatly developed after the Ming Dynasty, so that the Jun porcelain and the German white porcelain are famous for firing white porcelain. The German white porcelain has compact porcelain quality, excellent transmittance, pure white glaze surface, smooth and bright color, milky white like grease, and pink or milky white glaze in the perspective of near light, so the porcelain has the names of ivory white, goose down white and Chinese white.
Traditional german white porcelain uses the transmissivity fabulous, and the glaze is pure white, and the luster is smooth bright for the most outstanding characteristics, but along with the continuous development of society, people's aesthetic demand is also constantly your change, constantly improves the demand of innovation product, if can carry out a combination with the characteristics of german white porcelain with the characteristics of jun porcelain, provides a brand-new glaze effect, decorates the surface of german white porcelain, has positive meaning to the popularization and the inheritance of german white porcelain.
Disclosure of Invention
In order to solve the defects of the prior art, the invention provides a denuded white porcelain decorated by Jun porcelain textures and a preparation method thereof.
The invention provides a denuded white porcelain decorated by jun porcelain textures, which comprises a denuded white porcelain blank body, and also comprises a jun porcelain texture ground glaze and a jun porcelain texture surface glaze which are arranged outside the denuded white porcelain blank body, wherein the jun porcelain texture ground glaze comprises the following raw material components: 20-30 parts of frit, 30-40 parts of kaolin, 20-30 parts of montmorillonite, 5-10 parts of talc, 5-10 parts of sodium silicate and 1-5 parts of methanol; the Jun porcelain grain overglaze comprises the following raw material components: 30-40 parts of kaolin, 20-30 parts of quartz, 10-15 parts of melilite, 10-15 parts of agate, 1-5 parts of tin dioxide, 1-5 parts of calcium phosphate and 1-5 parts of polyethylene glycol.
Further, the frit comprises the following raw material components: 40-45 parts of potash feldspar, 20-30 parts of limestone, 10-15 parts of dolomite, 5-10 parts of spodumene, 1-5 parts of zinc oxide, 1-5 parts of borax and 1-5 parts of ammonium tripolyphosphate.
Further, the raw material components of the de-whitened porcelain body are as follows: 50-60 parts of kaolin, 20-25 parts of anorthite, 15-20 parts of dolomite and 1-5 parts of spodumene.
Further, the Jun porcelain grain ground glaze comprises the following raw material components: 26 parts of frit, 34 parts of kaolin, 22 parts of montmorillonite, 6 parts of talc, 9 parts of sodium silicate and 3 parts of methanol.
Further, the Jun porcelain grain overglaze comprises the following raw material components: 36 parts of kaolin, 28 parts of quartz, 14 parts of melilite, 13 parts of agate, 4 parts of tin dioxide, 3 parts of calcium phosphate and 2 parts of polyethylene glycol.
Further, the thickness ratio of the jun porcelain grain ground glaze to the jun porcelain grain overglaze is 1: 2-3.
The preparation method of the denuded white porcelain decorated by the jun porcelain texture comprises the following steps:
step 1, preparing a ceramic body according to raw material components of a Dehua white ceramic body;
step 2, preparing a jun porcelain grain ground glaze and a jun porcelain grain surface glaze respectively according to the raw material groups of the glaze;
step 3, preparing a ceramic blank, applying a jun porcelain grain ground coat on the surface of the ceramic blank when the water content of the surface of the blank is 20-30%, wherein the thickness of the glaze is 2-3 mm;
step 4, when the water content of the surface of the glazed ceramic blank is 10-15%, applying Jun porcelain grain surface glaze on the surface of the ceramic blank;
and 5, putting the ceramic blank into a kiln for firing, wherein the kiln reaches the firing temperature of 1210-1215 ℃ after 10-12 hours, and taking out of the kiln for cooling to obtain the denuded white porcelain decorated by the Jun porcelain texture.
Further, when preparing the Jun porcelain grain ground glaze in the step 2, firstly preparing frits, mixing according to the proportion of the Jun porcelain grain ground glaze, carrying out mixed ball milling for 10-15 hours to obtain the Jun porcelain grain ground glaze, and mixing ball milling materials: water: the proportion of the balls is 2: 1-2: 1.
further, when preparing the jun porcelain grain ground glaze frit in the step 2, the raw materials are crushed according to the proportion and then melted in an electric furnace, when the temperature is increased to 1000-1010 ℃, the temperature is kept for 1-2 hours, after the temperature is kept, the raw materials are filtered to obtain the melt, and the molten liquid is separated from the unmelted solid to obtain the frit.
Further, after glazing the Jun porcelain grain ground coat in the step 3, heating the prepared ceramic blank to 40-50 ℃ for 10 minutes to ensure that the Jun porcelain grain ground coat is quickly flocculated, and standing until the Jun porcelain grain ground coat is flocculated.
The denuded white porcelain decorated by the Jun porcelain texture prepared by the invention has a strip of raised strip-shaped texture, such as the texture that earthworms climb, under the Jun porcelain texture glaze, but the texture appears under the Jun porcelain texture glaze, especially in the place with thick glaze, the texture is more concentrated and obvious like the bottom texture of a cup, the surface of a ceramic product is smooth, and the Jun porcelain texture glaze layer is glittering, moist, thick and has texture like muddy jade; the preparation method of the German white porcelain with the Jun porcelain texture decoration provided by the invention has the advantages that the Jun porcelain texture ground glaze contains high-purity kaolin, the viscosity of a blank body is effectively reduced by utilizing the dispersion effect of sodium silicate on slurry after a large amount of sodium silicate is introduced, the ground glaze containing the high-purity kaolin is dissociated into anions, insoluble salt is formed on the surface of a blank body and is adsorbed on the surface of the blank body, earthworm patterns are formed through flocculation, the raw material selected for the Jun porcelain pattern surface glaze is matched with the raw material of the earthworm mud pattern bottom glaze, the combination of the Jun porcelain pattern surface glaze and the earthworm mud pattern bottom glaze is good, the firing rate is improved, the glaze layer thickness of the Jun porcelain pattern surface glaze and the earthworm mud pattern bottom glaze is limited, the prepared ceramic product can show both the jade effect and the clear mud pattern of the German white porcelain, the invention provides a brand new glaze effect for the German white porcelain, the surface of the German white porcelain is decorated, and the method has positive significance for popularization and inheritance of the German white porcelain.
Detailed Description
The invention is further described below by means of specific embodiments.
The denuded white porcelain decorated by jun porcelain textures comprises a denuded white porcelain blank body, and further comprises a jun porcelain texture ground glaze and a jun porcelain texture surface glaze which are arranged outside the denuded white porcelain blank body, wherein the thickness ratio of the jun porcelain texture ground glaze to the jun porcelain texture surface glaze is 1: 2-3, the Jun porcelain grain ground glaze comprises the following raw material components:
20-30 parts of frit, 30-40 parts of kaolin, 20-30 parts of montmorillonite, 5-10 parts of talc, 5-10 parts of sodium silicate and 1-5 parts of methanol, wherein the frit comprises the following raw material components: 40-45 parts of potash feldspar, 20-30 parts of limestone, 10-15 parts of dolomite, 5-10 parts of spodumene, 1-5 parts of zinc oxide, 1-5 parts of borax and 1-5 parts of ammonium tripolyphosphate;
the Jun porcelain grain overglaze comprises the following raw material components: 30-40 parts of kaolin, 20-30 parts of quartz, 10-15 parts of melilite, 10-15 parts of agate, 1-5 parts of stannic oxide, 1-5 parts of calcium phosphate and 1-5 parts of polyethylene glycol;
the germanized white porcelain body comprises the following raw material components: 50-60 parts of kaolin, 20-25 parts of anorthite, 15-20 parts of dolomite and 1-5 parts of spodumene.
The preparation method of the denuded white porcelain decorated by the jun porcelain texture comprises the following steps:
step 1, preparing a ceramic body according to raw material components of a Dehua white ceramic body;
step 2, preparing a jun porcelain grain ground glaze and a jun porcelain grain surface glaze respectively according to the raw material groups of the glaze;
step 3, preparing a ceramic blank, applying a jun porcelain grain ground coat on the surface of the ceramic blank when the water content of the surface of the blank is 20-30%, wherein the thickness of the glaze is 2-3 mm;
step 4, when the water content of the surface of the glazed ceramic blank is 10-15%, applying Jun porcelain grain surface glaze on the surface of the ceramic blank;
and 5, putting the ceramic blank into a kiln for firing, wherein the kiln reaches the firing temperature of 1210-1215 ℃ after 10-12 hours, and taking out of the kiln for cooling to obtain the denuded white porcelain decorated by the Jun porcelain texture.
The specific embodiment is as follows:
the denuded white porcelain decorated by jun porcelain textures comprises a denuded white porcelain blank body, and further comprises a jun porcelain texture ground glaze and a jun porcelain texture surface glaze which are arranged outside the denuded white porcelain blank body, wherein the thickness ratio of the jun porcelain texture ground glaze to the jun porcelain texture surface glaze is 1: 2, the Jun porcelain grain ground glaze comprises the following raw material components:
26 parts of frit, 34 parts of kaolin, 22 parts of montmorillonite, 6 parts of talc, 9 parts of sodium silicate and 3 parts of methanol, wherein the frit comprises the following raw material components: 48 parts of potassium feldspar, 26 parts of limestone, 11 parts of dolomite, 6 parts of spodumene, 4 parts of zinc oxide, 3 parts of borax and 2 parts of ammonium tripolyphosphate;
the Jun porcelain grain overglaze comprises the following raw material components: 36 parts of kaolin, 28 parts of quartz, 14 parts of melilite, 13 parts of agate, 4 parts of tin dioxide, 3 parts of calcium phosphate and 2 parts of polyethylene glycol;
the germanized white porcelain body comprises the following raw material components: 56 parts of kaolin, 23 parts of anorthite, 18 parts of dolomite and 3 parts of spodumene.
The preparation method of the denuded white porcelain decorated by the jun porcelain texture comprises the following steps:
step 1, preparing a ceramic body according to raw material components of a Dehua white ceramic body;
step 2, preparing a Jun porcelain grain ground glaze and a Jun porcelain grain surface glaze respectively according to the raw material groups of the glaze,
preparing frit when preparing the Jun porcelain grain ground glaze, melting the crushed raw materials in an electric furnace according to a proportion when preparing the frit, heating to 1008 ℃, preserving heat for 2 hours, filtering to obtain a melt of the raw materials after finishing the heat preservation, separating the molten liquid from unmelted solid to obtain the frit,
mixing the Jun porcelain grain ground glaze in proportion, mixing and ball-milling for 13 hours to obtain the Jun porcelain grain ground glaze, and mixing and ball-milling materials: water: the proportion of the balls is 2: 2: 1;
step 3, preparing a ceramic blank, applying a jun porcelain grain ground coat on the surface of the ceramic blank when the water content of the surface of the blank is 20%, wherein the thickness of the glaze is 3mm, heating the prepared ceramic blank at 45 ℃ for 10 minutes after glazing the jun porcelain grain ground coat, rapidly flocculating the jun porcelain grain ground coat, and standing the ceramic blank after flocculation;
step 4, when the water content of the surface of the glazed ceramic blank is 15%, applying a Jun porcelain grain overglaze on the surface of the ceramic blank, wherein the thickness of the overglaze is 6 mm;
and 5, putting the ceramic blank into a kiln for firing, wherein the kiln reaches the firing temperature after 12 hours, the firing temperature is 1213 ℃, and taking out of the kiln for cooling to obtain the denuded white porcelain decorated by the Jun porcelain texture.
The denuded white porcelain decorated by the Jun porcelain texture prepared by the invention has a strip of raised strip-shaped texture, such as the texture that earthworms climb, under the Jun porcelain texture glaze, but the texture appears under the Jun porcelain texture glaze, especially in the place with thick glaze, the texture is more concentrated and obvious like the bottom texture of a cup, the surface of a ceramic product is smooth, and the Jun porcelain texture glaze layer is glittering, moist, thick and has texture like muddy jade; the preparation method of the German white porcelain with the Jun porcelain texture decoration provided by the invention has the advantages that the Jun porcelain texture ground glaze contains high-purity kaolin, the viscosity of a blank body is effectively reduced by utilizing the dispersion effect of sodium silicate on slurry after a large amount of sodium silicate is introduced, the ground glaze containing the high-purity kaolin is dissociated into anions, insoluble salt is formed on the surface of a blank body and is adsorbed on the surface of the blank body, earthworm patterns are formed through flocculation, the raw material selected for the Jun porcelain pattern surface glaze is matched with the raw material of the earthworm mud pattern bottom glaze, the combination of the Jun porcelain pattern surface glaze and the earthworm mud pattern bottom glaze is good, the firing rate is improved, the glaze layer thickness of the Jun porcelain pattern surface glaze and the earthworm mud pattern bottom glaze is limited, the prepared ceramic product can show both the jade effect and the clear mud pattern of the German white porcelain, the invention provides a brand new glaze effect for the German white porcelain, the surface of the German white porcelain is decorated, and the method has positive significance for popularization and inheritance of the German white porcelain.
The above description is only an embodiment of the present invention, but the design concept of the present invention is not limited thereto, and any insubstantial modifications made by using the design concept should fall within the scope of infringing the present invention.
Claims (10)
1. The denuded white porcelain decorated by jun porcelain textures comprises a denuded white porcelain blank body and is characterized by further comprising a jun porcelain texture ground glaze and a jun porcelain texture surface glaze which are arranged outside the denuded white porcelain blank body, wherein the jun porcelain texture ground glaze comprises the following raw material components: 20-30 parts of frit, 30-40 parts of kaolin, 20-30 parts of montmorillonite, 5-10 parts of talc, 5-10 parts of sodium silicate and 1-5 parts of methanol; the Jun porcelain grain overglaze comprises the following raw material components: 30-40 parts of kaolin, 20-30 parts of quartz, 10-15 parts of melilite, 10-15 parts of agate, 1-5 parts of tin dioxide, 1-5 parts of calcium phosphate and 1-5 parts of polyethylene glycol.
2. The curdled white porcelain with Jun porcelain texture decoration according to claim 1, wherein the frit comprises the following raw material components: 40-45 parts of potash feldspar, 20-30 parts of limestone, 10-15 parts of dolomite, 5-10 parts of spodumene, 1-5 parts of zinc oxide, 1-5 parts of borax and 1-5 parts of ammonium tripolyphosphate.
3. The German white porcelain with Jun porcelain texture decoration according to claim 1, wherein the German white porcelain body comprises the following raw material components: 50-60 parts of kaolin, 20-25 parts of anorthite, 15-20 parts of dolomite and 1-5 parts of spodumene.
4. The German white porcelain decorated by Jun porcelain textures of claim 1 or 3 is characterized in that the Jun porcelain texture ground glaze comprises the following raw material components: 26 parts of frit, 34 parts of kaolin, 22 parts of montmorillonite, 6 parts of talc, 9 parts of sodium silicate and 3 parts of methanol.
5. The curdled white porcelain decorated by jun porcelain textures of claim 1 or 3 is characterized in that the jun porcelain texture overglaze comprises the following raw material components: 36 parts of kaolin, 28 parts of quartz, 14 parts of melilite, 13 parts of agate, 4 parts of tin dioxide, 3 parts of calcium phosphate and 2 parts of polyethylene glycol.
6. The chequered white porcelain decorated by jun porcelain textures of claim 1, wherein the thickness ratio of the jun porcelain texture ground glaze to the jun porcelain texture overglaze is 1: 2-3.
7. The preparation method of the German white porcelain decorated by the Jun porcelain texture comprises the following steps of:
step 1, preparing a ceramic body according to raw material components of a Dehua white ceramic body;
step 2, preparing a jun porcelain grain ground glaze and a jun porcelain grain surface glaze respectively according to the raw material groups of the glaze;
step 3, preparing a ceramic blank, applying a jun porcelain grain ground coat on the surface of the ceramic blank when the water content of the surface of the blank is 20-30%, wherein the thickness of the glaze is 2-3 mm;
step 4, when the water content of the surface of the glazed ceramic blank is 10-15%, applying Jun porcelain grain surface glaze on the surface of the ceramic blank;
and 5, putting the ceramic blank into a kiln for firing, wherein the kiln reaches the firing temperature of 1210-1215 ℃ after 10-12 hours, and taking out of the kiln for cooling to obtain the denuded white porcelain decorated by the Jun porcelain texture.
8. The method for preparing the denuded white porcelain decorated by the Jun porcelain textures as claimed in claim 7, wherein when preparing the Jun porcelain texture ground glaze in step 2, firstly preparing a frit, mixing the jun porcelain texture ground glaze in proportion, mixing and ball-milling for 10-15 hours to obtain the Jun porcelain texture ground glaze, and mixing and ball-milling materials: water: the proportion of the balls is 2: 1-2: 1.
9. the method for preparing a German white porcelain decorated with Jun porcelain textures as claimed in claim 8, is characterized in that: and 2, when preparing the jun porcelain grain ground glaze frit in the step 2, melting the crushed raw materials in an electric furnace according to the proportion, heating to 1000-1010 ℃, preserving heat for 1-2 hours, filtering to obtain a melt of the raw materials after finishing the heat preservation, and separating the molten liquid from the unmelted solid to obtain the frit.
10. The method for preparing a German white porcelain decorated with Jun porcelain textures as claimed in claim 7, is characterized in that: and 3, after glazing the Jun porcelain grain ground coat, heating the prepared ceramic blank at 40-50 ℃ for 10 minutes to ensure that the Jun porcelain grain ground coat is quickly flocculated, and standing until the Jun porcelain grain ground coat is flocculated.
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| CN113620691A (en) * | 2021-08-13 | 2021-11-09 | 德化月记窑陶瓷有限责任公司 | High-quality thick-body ultrahigh-thickness-ring-foot white porcelain tableware and manufacturing process thereof |
| CN113979638A (en) * | 2021-11-19 | 2022-01-28 | 醴陵市观前瓷业有限公司 | Preparation method of protruded blood vessel-shaped transmutation glaze and transmutation glaze porcelain |
| CN115557702A (en) * | 2022-11-10 | 2023-01-03 | 福建省德化非凡陶瓷有限公司 | Earthworm mud-streak-running multilayer composite thick-glaze white porcelain and manufacturing process thereof |
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