CN111233329A - Matte transmutation glaze and preparation method thereof - Google Patents
Matte transmutation glaze and preparation method thereof Download PDFInfo
- Publication number
- CN111233329A CN111233329A CN202010106243.9A CN202010106243A CN111233329A CN 111233329 A CN111233329 A CN 111233329A CN 202010106243 A CN202010106243 A CN 202010106243A CN 111233329 A CN111233329 A CN 111233329A
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- percent
- glaze
- matte
- transmutation
- ball
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/20—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
Abstract
The invention discloses a matte transmutation glaze and a preparation method thereof, and glaze used by the matte transmutation glaze comprises the following components in percentage by mass: 10% -30% of potash feldspar, and spodumene: 10% -30%, calcite: 5% -15%, quartz: 5% -20%, wollastonite: 10% -20%, talc: 10% -25%, zinc oxide: 2% -6%, Jiepai mud: 5% -10%, calcined kaolin: 5% -15%, anatase titanium dioxide: 5 to 10 percent of spinel type pigment, 0.5 to 8 percent of spinel type pigment, and the total content of the components is 100 percent. The glaze of the ceramic tile presents silky, fine and smooth matte glaze, generates natural flowing patterns, is matched with different shapes of the ceramic tiles to prepare artworks with different styles, and has the advantages of wide firing range, excellent thermal stability, environmental protection and green.
Description
Technical Field
The invention relates to a matte transmutation glaze and a preparation method thereof.
Background
At present, in the development process of daily and artistic ceramics, matte glaze is popular with more and more consumers, the matte transmutation glaze is more high-grade than the common matte glaze, the cost is reduced in the decoration process of ceramic products, various decoration procedures such as applique and the like are reduced, and the ceramic products are natural, environment-friendly and green new ceramic products.
Disclosure of Invention
The technical problem to be solved by the invention is to overcome the defects of the prior art and provide the matte transmutation glaze, the glaze surface of the glaze presents a silky, fine and smooth matte glaze surface and generates natural flowing patterns, artworks with different styles are manufactured by matching different models, and the glaze has the advantages of wide firing range, excellent thermal stability, environmental protection and green.
The technical scheme for solving the technical problem of the invention is as follows: a matte transmutation glaze comprises the following components in percentage by mass:
10% -30% of potash feldspar, and spodumene: 10% -30%, calcite: 5% -15%, quartz: 5% -20%, wollastonite: 10% -20%, talc: 10% -25%, zinc oxide: 2% -6%, Jiepai mud: 5% -10%, calcined kaolin: 5% -15%, anatase titanium dioxide: 5 to 10 percent of spinel type pigment, 0.5 to 8 percent of spinel type pigment, and the total content of the components is 100 percent.
Further, the glaze used by the method comprises the following components in percentage by mass:
15 percent of potash feldspar, 10 percent of spodumene, 10 percent of quartz, 10 percent of calcite, 10 percent of wollastonite, 13 percent of talcum, 4 percent of zinc oxide, 8 percent of Jiepai mud, 10 percent of calcined kaolin and 7 percent of anatase titanium dioxide; 3% of spinel type pigment.
The invention also provides a preparation method of the matte transmutation glaze, which comprises the following steps:
mixing potash feldspar, spodumene, quartz, calcite, wollastonite, talcum, zinc oxide, Jiepai mud and calcined kaolin which are measured according to a proportion;
putting the mixed raw materials into a ball mill, and mixing the raw materials: water: ball-milling for 8-12 hours by a wet method, wherein the mass ratio of the balls is 2:1: 4;
putting the anatase titanium dioxide and the spinel pigment which are weighed according to the proportion into a ball mill for ball milling to obtain a ball grinding material;
after the ball grinding material passes through a 200-mesh sieve, the glaze slurry with the Baume degree of 50-60 is prepared;
and after the blank is subjected to glaze dipping or glaze spraying, the blank is sintered into a product through a kiln.
After the technical scheme is adopted, the glaze of the matte transmutation glaze disclosed by the invention is a silky, fine and smooth matte glaze, natural flowing patterns are generated, artworks with different styles are prepared by matching different models, the firing range is wide, the thermal stability is excellent, the environment is protected, and the matte transmutation glaze with different colors can be prepared by adding different spinel pigments.
Detailed Description
The invention provides a matte transmutation glaze and a preparation method thereof, and a person skilled in the art can appropriately improve process parameters by referring to the content. It is expressly intended that all such similar substitutes and modifications apparent to those skilled in the art are deemed to be within the scope of the invention. While the methods and applications of this invention have been described in terms of preferred embodiments, it will be apparent to those of ordinary skill in the art that variations and modifications in the methods and applications described herein, as well as other suitable variations and combinations, may be made to implement and use the techniques of this invention without departing from the spirit and scope of the invention.
In order that the present invention may be more clearly understood, the following detailed description of the present invention is given with reference to specific examples.
Example one
A matte transmutation glaze comprises the following components in percentage by mass:
15 percent of potash feldspar, 10 percent of spodumene, 10 percent of quartz, 10 percent of calcite, 10 percent of wollastonite, 13 percent of talcum, 4 percent of zinc oxide, 8 percent of Jiepai mud, 10 percent of calcined kaolin and 7 percent of anatase titanium dioxide; 3% of spinel type pigment.
The preparation method of the matte transmutation glaze comprises the following steps:
mixing potash feldspar, spodumene, quartz, calcite, wollastonite, talcum, zinc oxide, Jiepai mud and calcined kaolin which are measured according to a proportion;
putting the mixed raw materials into a ball mill, and mixing the raw materials: water: ball milling for 8 hours by a wet method, wherein the mass ratio of the balls is 2:1: 4;
putting the anatase titanium dioxide and the spinel pigment which are weighed according to the proportion into a ball mill for ball milling to obtain a ball grinding material;
after the ball grinding material passes through a 200-mesh sieve, the mixture is mixed into glaze slip with 50 baume degrees;
and after the blank is subjected to glaze dipping or glaze spraying, the blank is sintered into a product through a kiln.
Example two
A matte transmutation glaze comprises the following components in percentage by mass:
potash feldspar 10%, spodumene: 20%, calcite: 5%, quartz: 15%, wollastonite: 10%, talc: 10%, zinc oxide: 6 percent, Jiepai mud: 5%, calcined kaolin: 7%, anatase titanium dioxide: 5 percent of spinel type pigment, 7 percent of spinel type pigment,
the preparation method of the matte transmutation glaze comprises the following steps:
mixing potash feldspar, spodumene, quartz, calcite, wollastonite, talcum, zinc oxide, Jiepai mud and calcined kaolin which are measured according to a proportion;
putting the mixed raw materials into a ball mill, and mixing the raw materials: water: ball milling for 12 hours by a wet method, wherein the mass ratio of the balls is 2:1: 4;
putting the anatase titanium dioxide and the spinel pigment which are weighed according to the proportion into a ball mill for ball milling to obtain a ball grinding material;
after the ball grinding material passes through a 200-mesh sieve, the glaze slurry with 60 baume degrees is prepared;
and after the blank is subjected to glaze dipping or glaze spraying, the blank is sintered into a product through a kiln.
EXAMPLE III
A matte transmutation glaze comprises the following components in percentage by mass:
potassium feldspar 20%, spodumene: 10%, calcite: 5%, quartz: 5%, wollastonite: 10%, talc: 10%, zinc oxide: 6 percent, Jiepai mud: 10%, calcined kaolin: 10%, anatase titanium dioxide: 10 percent and 4 percent of spinel type pigment.
The preparation method of the matte transmutation glaze comprises the following steps:
mixing potash feldspar, spodumene, quartz, calcite, wollastonite, talcum, zinc oxide, Jiepai mud and calcined kaolin which are measured according to a proportion;
putting the mixed raw materials into a ball mill, and mixing the raw materials: water: ball-milling for 8-12 hours by a wet method, wherein the mass ratio of the balls is 2:1: 4;
putting the anatase titanium dioxide and the spinel pigment which are weighed according to the proportion into a ball mill for ball milling to obtain a ball grinding material;
after the ball grinding material passes through a 200-mesh sieve, the glaze slurry with the Baume degree of 50-60 is prepared;
and after the blank is subjected to glaze dipping or glaze spraying, the blank is sintered into a product through a kiln.
Observation shows that the glaze surface of the matte transmutation glaze prepared by the three embodiments has a good matte effect.
The above-mentioned embodiments are intended to illustrate the objects, technical solutions and advantages of the present invention in further detail, and it should be understood that the above-mentioned embodiments are only exemplary embodiments of the present invention, and are not intended to limit the present invention, and any modifications, equivalents, improvements and the like made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (3)
1. The matte transmutation glaze is characterized in that the glaze used by the matte transmutation glaze comprises the following components in percentage by mass:
10% -30% of potash feldspar, and spodumene: 10% -30%, calcite: 5% -15%, quartz: 5% -20%, wollastonite: 10% -20%, talc: 10% -25%, zinc oxide: 2% -6%, Jiepai mud: 5% -10%, calcined kaolin: 5% -15%, anatase titanium dioxide: 5 to 10 percent of spinel type pigment, 0.5 to 8 percent of spinel type pigment, and the total content of the components is 100 percent.
2. The matte transmutation glaze of claim 1, wherein,
the glaze used by the method comprises the following components in percentage by mass:
15 percent of potash feldspar, 10 percent of spodumene, 10 percent of quartz, 10 percent of calcite, 10 percent of wollastonite, 13 percent of talcum, 4 percent of zinc oxide, 8 percent of Jiepai mud, 10 percent of calcined kaolin and 7 percent of anatase titanium dioxide; 3% of spinel type pigment.
3. A process for the preparation of a matte transmutation glaze according to claim 1 or 2, characterized in that the process comprises the steps of:
mixing potash feldspar, spodumene, quartz, calcite, wollastonite, talcum, zinc oxide, Jiepai mud and calcined kaolin which are measured according to a proportion;
putting the mixed raw materials into a ball mill, and mixing the raw materials: water: ball-milling for 8-12 hours by a wet method, wherein the mass ratio of the balls is 2:1: 4;
putting the anatase titanium dioxide and the spinel pigment which are weighed according to the proportion into a ball mill for ball milling to obtain a ball grinding material;
after the ball grinding material passes through a 200-mesh sieve, the glaze slurry with the Baume degree of 50-60 is prepared;
and after the blank is subjected to glaze dipping or glaze spraying, the blank is sintered into a product through a kiln.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010106243.9A CN111233329A (en) | 2020-02-21 | 2020-02-21 | Matte transmutation glaze and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010106243.9A CN111233329A (en) | 2020-02-21 | 2020-02-21 | Matte transmutation glaze and preparation method thereof |
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| CN111233329A true CN111233329A (en) | 2020-06-05 |
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| CN202010106243.9A Pending CN111233329A (en) | 2020-02-21 | 2020-02-21 | Matte transmutation glaze and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111943724A (en) * | 2020-08-11 | 2020-11-17 | 佛山市三水新明珠建陶工业有限公司 | Method for manufacturing matt transparent glazed ceramic chip |
| CN112225455A (en) * | 2020-10-19 | 2021-01-15 | 湖南华联瓷业股份有限公司 | Phosphorus-based zinc and titanium crystallization high-temperature matte reaction flow glaze decoration daily ceramic and preparation method thereof |
| CN112358183A (en) * | 2020-11-25 | 2021-02-12 | 湖南华联瓷业股份有限公司 | High-temperature dark green transmutation reaction glaze and preparation method thereof |
| CN113800951A (en) * | 2021-09-01 | 2021-12-17 | 湖南泉湘陶瓷有限公司 | Matte antique crystal glaze and preparation method thereof |
| CN113979638A (en) * | 2021-11-19 | 2022-01-28 | 醴陵市观前瓷业有限公司 | Preparation method of protruded blood vessel-shaped transmutation glaze and transmutation glaze porcelain |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111943724A (en) * | 2020-08-11 | 2020-11-17 | 佛山市三水新明珠建陶工业有限公司 | Method for manufacturing matt transparent glazed ceramic chip |
| CN112225455A (en) * | 2020-10-19 | 2021-01-15 | 湖南华联瓷业股份有限公司 | Phosphorus-based zinc and titanium crystallization high-temperature matte reaction flow glaze decoration daily ceramic and preparation method thereof |
| CN112358183A (en) * | 2020-11-25 | 2021-02-12 | 湖南华联瓷业股份有限公司 | High-temperature dark green transmutation reaction glaze and preparation method thereof |
| CN113800951A (en) * | 2021-09-01 | 2021-12-17 | 湖南泉湘陶瓷有限公司 | Matte antique crystal glaze and preparation method thereof |
| CN113979638A (en) * | 2021-11-19 | 2022-01-28 | 醴陵市观前瓷业有限公司 | Preparation method of protruded blood vessel-shaped transmutation glaze and transmutation glaze porcelain |
| CN113979638B (en) * | 2021-11-19 | 2023-05-26 | 醴陵市观前瓷业有限公司 | Preparation method of protruding blood tube-shaped transmutation glaze and transmutation glaze porcelain |
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Application publication date: 20200605 |