CN113973956A - Eucommia ulmoides composite coffee solid beverage and preparation method thereof - Google Patents
Eucommia ulmoides composite coffee solid beverage and preparation method thereof Download PDFInfo
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- CN113973956A CN113973956A CN202111207162.9A CN202111207162A CN113973956A CN 113973956 A CN113973956 A CN 113973956A CN 202111207162 A CN202111207162 A CN 202111207162A CN 113973956 A CN113973956 A CN 113973956A
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- eucommia
- eucommia ulmoides
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/10—Treating roasted coffee; Preparations produced thereby
- A23F5/14—Treating roasted coffee; Preparations produced thereby using additives, e.g. milk, sugar; Coating, e.g. for preserving
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/24—Extraction of coffee; Coffee extracts; Making instant coffee
- A23F5/36—Further treatment of dried coffee extract; Preparations produced thereby, e.g. instant coffee
- A23F5/40—Further treatment of dried coffee extract; Preparations produced thereby, e.g. instant coffee using organic additives, e.g. milk, sugar
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- Food Science & Technology (AREA)
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- Tea And Coffee (AREA)
Abstract
The invention discloses a eucommia composite coffee solid beverage and a preparation method thereof. The eucommia composite coffee solid beverage comprises the following components: eucommia ulmoides leaf alcohol extract, resistant dextrin, black coffee powder, milk powder, stevioside and erythritol. The novel food raw material eucommia ulmoides leaves, the black coffee powder, the resistant dextrin and other ingredients are compounded, so that the novel food has multiple effects of relieving fatigue, reducing blood fat, reducing blood pressure, delaying senescence and the like, and sugar substitutes are selected as sweetening agents, so that the novel food is beneficial to controlling blood sugar rise and reducing calorie intake.
Description
Technical Field
The invention relates to the technical field of solid beverages, in particular to a eucommia composite coffee solid beverage and a preparation method thereof.
Background
The folium Eucommiae is leaf of eucommia ulmoides Oliver belonging to family Eucommiaceae. The eucommia leaves approved by the national health council can be used as new resource food. The eucommia leaves contain active ingredients such as chlorogenic acid, aucubin, polysaccharide, geniposide, various amino acids and the like, have the effects of resisting fatigue, reducing blood pressure, reducing blood fat, resisting bacteria, diminishing inflammation, enhancing immunity, resisting oxidation, delaying senescence and the like, and have special advantages in the aspect of developing health foods.
The resistant dextrin belongs to low-calorie glucan, has the total dietary fiber content of up to 82 percent, and is a low-calorie soluble food raw material. The product has the characteristics of no peculiar smell, easy dissolution in alcohol, heat resistance, acid resistance, freezing resistance and the like, and is widely used in food. The resistant dextrin has the function of resisting digestive enzyme, can not be digested and absorbed in the digestive tract, and can directly enter the large intestine, so that the resistant dextrin plays various physiological roles of dietary fiber, and has the functions of reducing blood sugar, blood fat, protecting the intestinal tract and the like due to the characteristics of high digestion tolerance, low glycemic index, low insulin index, low calorie, easy dissolution and the like.
In recent years, coffee is popular with young consumers as a beverage with unique taste, and workers engaged in mental activities and the like are main consumer groups of coffee products. Studies have shown that long-term consumption of beverages such as tea and caffeine in large quantities can induce caffeine intoxication. The symptoms of the disease include not only caffeine addiction, but also physical and psychological homeostasis such as anxiety, irritability, muscle twitch and sleep disorder. Therefore, reduction of caffeine intake is an effective measure. The folium Eucommiae has antifatigue effect, and can be mixed with coffee to reduce the consumption of coffee and thus reduce the intake of caffeine. At present, solid coffee beverages on the market are various, and mainly comprise instant coffee, three-in-one coffee and the like, but related research reports that an eucommia ulmoides leaf extract, resistant dextrin and coffee are simultaneously used as a solid beverage are not reported at present.
Disclosure of Invention
The eucommia ulmoides composite coffee solid beverage and the preparation method thereof solve the problems in the prior art, and the eucommia ulmoides composite coffee solid beverage are prepared by compounding new resource food raw materials, namely eucommia ulmoides leaves, black coffee powder, resistant dextrin and other components, have multiple effects of relieving fatigue, reducing blood fat, reducing blood pressure, delaying senescence and the like, and are beneficial to controlling blood sugar increase and reducing calorie intake by selecting sugar substitutes as sweetening agents.
In order to achieve the purpose, the invention adopts the technical scheme that: an eucommia composite coffee solid beverage comprises the following components: eucommia ulmoides leaf alcohol extract, resistant dextrin, black coffee powder, milk powder, stevioside and erythritol.
At present, the preparation method of the functional beverage taking the eucommia leaves as the core raw material mainly comprises the steps of taking water as a solvent for extraction, and then preparing the functional beverage according to the requirements of the beverage or the compound beverage. The invention adopts a certain proportion of alcohol and water as the extraction solvent, and can extract the effective components in the eucommia leaves to a greater extent, thereby ensuring the health care effect of the beverage.
Preferably, the eucommia ulmoides leaf alcohol extract is prepared by the following steps: placing the cleaned eucommia leaves into an extraction container, adding 50% volume fraction edible ethanol, and leaching at constant temperature, wherein the mass volume ratio of the material liquid is 1: 10-20 ℃, extracting at the temperature of 90-100 ℃, filtering after 2-3 h, adding 50% edible ethanol into filter residue, extracting for 2-3 h again, extracting at the temperature of 90-100 ℃, filtering and combining extracting solutions, and concentrating and drying under reduced pressure to obtain the eucommia leaf alcohol extract.
Further preferably, the eucommia ulmoides leaf alcohol extract is prepared by the following steps: placing the cleaned eucommia leaves into an extraction container, adding 50% volume fraction edible ethanol, and leaching at constant temperature, wherein the mass volume ratio of the material liquid is 1: 15, extracting at the temperature of 95 ℃ for 2.5h, filtering, adding 50% edible ethanol into filter residues, extracting for 2.5h again, extracting at the temperature of 95 ℃, filtering, combining extracting solutions, concentrating under reduced pressure and drying to obtain the eucommia leaf alcohol extract. The unit of the mass-to-volume ratio is g/mL.
Preferably, the eucommia composite coffee solid beverage comprises the following components in parts by mass: 0.25-0.60 part of eucommia ulmoides leaf alcohol extract, 4.0-6.0 parts of resistant dextrin, 0.2-0.7 part of black coffee powder, 1.5-2.5 parts of milk powder, 0.05-0.15 part of stevioside and 2.5-3.5 parts of erythritol.
Further preferably, the eucommia composite coffee solid beverage comprises the following components in parts by mass: 0.5 part of eucommia ulmoides leaf alcohol extract, 5.0 parts of resistant dextrin, 0.5 part of black coffee powder, 2.0 parts of milk powder, 0.10 part of stevioside and 3.0 parts of erythritol.
The invention also provides a preparation method of the eucommia ulmoides composite coffee solid beverage, which comprises the following steps: mixing the eucommia ulmoides leaf alcohol extract, resistant dextrin, black coffee powder, milk powder, stevioside and erythritol uniformly, sterilizing, subpackaging and packaging to obtain the eucommia ulmoides composite coffee solid beverage.
Preferably, the eucommia ulmoides leaf alcohol extract is prepared by the following steps: placing the cleaned eucommia leaves into an extraction container, adding 50% volume fraction edible ethanol, and leaching at constant temperature, wherein the mass volume ratio of the material liquid is 1: 10-20 ℃, extracting at the temperature of 90-100 ℃, filtering after 2-3 h, adding 50% edible ethanol into filter residue, extracting for 2-3 h again, extracting at the temperature of 90-100 ℃, filtering and combining extracting solutions, and concentrating and drying under reduced pressure to obtain the eucommia leaf alcohol extract.
Compared with the prior art, the invention has the beneficial effects that: the eucommia ulmoides composite coffee solid beverage provided by the invention is prepared by compounding new resource food raw materials, namely eucommia ulmoides leaves, black coffee powder, resistant dextrin and the like, has multiple effects of relieving fatigue, reducing blood fat, reducing blood pressure, delaying senescence and the like, and is beneficial to controlling blood sugar increase and reducing heat intake by selecting sugar substitutes as sweetening agents.
Detailed Description
The following examples are further illustrative of the present invention and are not intended to be limiting thereof. The equipment and reagents used in the present invention are, unless otherwise specified, conventional commercial products in the art.
The eucommia composite coffee solid beverage comprises the following components in parts by weight: 0.25-0.60 part of eucommia ulmoides leaf alcohol extract, 4.0-6.0 parts of resistant dextrin, 0.2-0.7 part of black coffee powder, 1.5-2.5 parts of milk powder, 0.05-0.15 part of stevioside and 2.5-3.5 parts of erythritol.
Preferably, in the following examples, the alcoholic extract of eucommia ulmoides leaves is prepared by the following steps: placing the cleaned eucommia leaves into an extraction container, adding 50% volume fraction edible ethanol, and leaching at constant temperature, wherein the mass volume ratio of the material liquid is 1: 10-20 ℃, extracting at the temperature of 90-100 ℃, filtering after 2-3 h, adding 50% edible ethanol into filter residue, extracting for 2-3 h again, extracting at the temperature of 90-100 ℃, filtering and combining extracting solutions, and concentrating and drying under reduced pressure to obtain the eucommia leaf alcohol extract.
More preferably, the eucommia ulmoides leaf alcohol extract is prepared by the following steps: placing the cleaned eucommia leaves into an extraction container, adding 50% volume fraction edible ethanol, and leaching at constant temperature, wherein the mass volume ratio of the material liquid is 1: 15, extracting at the temperature of 95 ℃ for 2.5h, filtering, adding 50% edible ethanol into filter residues, extracting for 2.5h again, extracting at the temperature of 95 ℃, filtering, combining extracting solutions, concentrating under reduced pressure and drying to obtain the eucommia leaf alcohol extract.
In the following preferred embodiments, the eucommia ulmoides composite coffee solid beverage comprises the following components in parts by weight: 0.5 part of eucommia ulmoides leaf alcohol extract, 5.0 parts of resistant dextrin, 0.5 part of black coffee powder, 2.0 parts of milk powder, 0.10 part of stevioside and 3.0 parts of erythritol.
The preparation method of the eucommia ulmoides composite coffee solid beverage comprises the following steps: and uniformly mixing the eucommia ulmoides leaf alcohol extract, resistant dextrin, black coffee powder, milk powder, stevioside and erythritol in parts by weight, sterilizing, subpackaging and packaging to obtain the eucommia ulmoides composite coffee solid beverage.
Example 1
The preparation method of the eucommia ulmoides leaf alcohol extract comprises the following steps: selecting qualified and high-quality eucommia leaves, cleaning, removing surface soil impurities and the like, weighing 1kg of eucommia leaves after drying, placing the eucommia leaves in an extraction container, adding 15L of edible ethanol with the volume fraction of 50%, placing the eucommia leaves in a constant-temperature water bath kettle for extraction, extracting at the extraction temperature of 95 ℃, filtering the eucommia leaves by using multilayer gauze after 2.5h of extraction, adding 10L of 50% edible ethanol into filter residues, extracting for 2.5h again at the extraction temperature of 95 ℃, filtering and combining extracting solutions, drying the concentrated solution by spray drying after reduced pressure concentration, and obtaining the eucommia leaf alcohol extract, wherein the air inlet temperature is 160 ℃, and the air outlet temperature is 91 ℃.
The eucommia composite coffee solid beverage comprises the following components: 0.5g of eucommia ulmoides leaf alcohol extract, 0.5g of black coffee powder, 5.0g of resistant dextrin, 2.0g of milk powder, 0.1g of stevioside and 3.0g of erythritol.
The eucommia composite coffee solid beverage is prepared by the following steps: taking the eucommia leaf alcohol extract, black coffee powder, resistant dextrin, milk powder, stevioside and erythritol, uniformly mixing, and sterilizing to obtain the eucommia leaf composite coffee solid beverage.
Example 2
The preparation method of the eucommia ulmoides leaf alcohol extract and the eucommia ulmoides composite coffee solid beverage is the same as that of example 1.
The eucommia composite coffee solid beverage comprises the following components: 0.25g of eucommia ulmoides leaf alcohol extract, 0.2g of black coffee powder, 4.0g of resistant dextrin, 1.5g of milk powder, 0.05g of stevioside and 2.5g of erythritol.
Example 3
The preparation method of the eucommia ulmoides leaf alcohol extract and the eucommia ulmoides composite coffee solid beverage is the same as that of example 1.
The eucommia composite coffee solid beverage comprises the following components: 0.6g of eucommia ulmoides leaf alcohol extract, 0.7g of black coffee powder, 6.0g of resistant dextrin, 2.5g of milk powder, 0.15g of stevioside and 3.5g of erythritol.
Experimental example 1
1. Laboratory animal
40 healthy male KM mice with the weight of 18-22g are bred adaptively for 5 days at the room temperature of 23-25 ℃ and the relative humidity of 55-60 percent before the experiment. Alternate light and shade for 12h, freely drink water, freely eat standard feed, and the treatment of the animal in the experimental process accords with the animal ethical standard.
2. Experimental groups and methods of administration
The eucommia ulmoides leaf alcohol extract group comprises 6g of eucommia ulmoides leaf alcohol extract, 2.0g of milk powder, 0.1g of stevioside and 3.0g of erythritol.
The black coffee group comprises 6g of black coffee, 2.0g of milk powder, 0.1g of stevioside and 3.0g of erythritol.
The food comprises 6g of resistant dextrin, 2.0g of milk powder, 0.1g of stevioside and 3.0g of erythritol.
The eucommia ulmoides composite coffee solid beverage group specifically comprises the following components: 0.5g of black coffee powder, 0.5g of eucommia ulmoides leaf alcohol extract, 5.0g of resistant dextrin, 2.0g of milk powder, 0.1g of stevioside and 3.0g of erythritol.
40 mice were randomly divided into 5 groups, namely a normal group, an eucommia leaf alcohol extract group, a black coffee group, a resistant dextrin group, and an eucommia composite coffee solid beverage group (example 1), and 8 mice were each group. The normal group does not do anything. The administration dose of the mouse was obtained by converting the equivalent dose according to the body surface area, and the administration was carried out in a 10-fold manner of the equivalent dose, and each administration group was administered alone to the mouse test substance. The administration method comprises the following steps: the administration is carried out by gavage for 1 time at 9 am every day for 30 days, and the corresponding volume of distilled water is gavage in a normal group.
3. Observation indexes are as follows:
3.1 judge the fatigue degree of the mice by the time of exhaustion of swimming. The mice were given a load of 6% and were forced to swim to exhaustion, and were judged to be exhausted when they were submerged in water for 10 seconds and could not emerge from the water surface, and the exhaustion swimming time was recorded.
3.2 serum lactate assay: collecting blood by an eyeball-picking method 1h after the mouse exhaustive swimming is finished, collecting the blood into a centrifuge tube, standing for 1h, centrifuging for 10min at 4 ℃ 4000r/min, taking supernatant, and storing in a refrigerator at-80 ℃ for later use. Detection was performed according to the kit instructions.
3.3 data were processed using software GaphPad Prism 8.0.2, Kolmogorov-Smirnov test for normal test, and Brown-Forsythe test for homogeneity of variance. One-way ANOVA is adopted for data which are in accordance with normal distribution and uniform in variance, and Tukey is adopted for pairwise comparison; normal distribution but variable data were obtained using Brown-Forythe and Welch ANOVA, and Dunnett's T3 for pairwise comparisons. Data are expressed as mean ± standard deviation.
4. Results of the experiment
The experimental results show that: the eucommia composite coffee solid beverage has obvious anti-fatigue effect; compared with the eucommia ulmoides leaf alcohol extract or black coffee powder or resistant dextrin which is singly given, the eucommia ulmoides composite coffee solid beverage can improve the exhaustion swimming time and can also obviously reduce the serum lactic acid level, and the fact that the eucommia ulmoides leaf alcohol extract, the black coffee powder and the resistant dextrin are compounded shows a certain synergistic effect.
Table 1: experiment of exhaustive swimming time and serum lactic acid levels in groups of mice
Note: p < 0.05, P < 0.01, compared to normal group
The above examples are only preferred embodiments of the present invention, and it should be noted that the above preferred embodiments should not be considered as limiting the present invention, and the protection scope of the present invention should be subject to the scope defined by the claims. It will be apparent to those skilled in the art that various modifications and adaptations can be made without departing from the spirit and scope of the invention, and these modifications and adaptations should be considered within the scope of the invention.
Claims (7)
1. The eucommia ulmoides composite coffee solid beverage is characterized by comprising the following components: eucommia ulmoides leaf alcohol extract, resistant dextrin, black coffee powder, milk powder, stevioside and erythritol.
2. The eucommia ulmoides composite coffee solid beverage of claim 1, wherein the eucommia ulmoides leaf alcohol extract is prepared by the following steps: placing the cleaned eucommia leaves into an extraction container, adding 50% volume fraction edible ethanol, and leaching at constant temperature, wherein the mass volume ratio of the material liquid is 1: 10-20 ℃, extracting at the temperature of 90-100 ℃, filtering after 2-3 h, adding 50% edible ethanol into filter residue, extracting for 2-3 h again, extracting at the temperature of 90-100 ℃, filtering and combining extracting solutions, and concentrating and drying under reduced pressure to obtain the eucommia leaf alcohol extract.
3. The eucommia ulmoides composite coffee solid beverage of claim 2, wherein the eucommia ulmoides leaf alcohol extract is prepared by the following steps: placing the cleaned eucommia leaves into an extraction container, adding 50% volume fraction edible ethanol, and leaching at constant temperature, wherein the mass volume ratio of the material liquid is 1: 15, extracting at the temperature of 95 ℃ for 2.5h, filtering, adding 50% edible ethanol into filter residues, extracting for 2.5h again, extracting at the temperature of 95 ℃, filtering, combining extracting solutions, concentrating under reduced pressure and drying to obtain the eucommia leaf alcohol extract.
4. The eucommia ulmoides composite coffee solid beverage of claim 1, which comprises the following components in parts by mass: 0.25-0.60 part of eucommia ulmoides leaf alcohol extract, 4.0-6.0 parts of resistant dextrin, 0.2-0.7 part of black coffee powder, 1.5-2.5 parts of milk powder, 0.05-0.15 part of stevioside and 2.5-3.5 parts of erythritol.
5. The eucommia ulmoides composite coffee solid beverage of claim 4, which comprises the following components in parts by mass: 0.5 part of eucommia ulmoides leaf alcohol extract, 5.0 parts of resistant dextrin, 0.5 part of black coffee powder, 2.0 parts of milk powder, 0.10 part of stevioside and 3.0 parts of erythritol.
6. The preparation method of the eucommia ulmoides composite coffee solid beverage of claim 1, which comprises the following steps: mixing the eucommia ulmoides leaf alcohol extract, resistant dextrin, black coffee powder, milk powder, stevioside and erythritol uniformly, sterilizing, subpackaging and packaging to obtain the eucommia ulmoides composite coffee solid beverage.
7. The preparation method of the eucommia ulmoides composite coffee solid beverage as claimed in claim 6, wherein the eucommia ulmoides leaf alcohol extract is prepared by the following steps: placing the cleaned eucommia leaves into an extraction container, adding 50% volume fraction edible ethanol, and leaching at constant temperature, wherein the mass volume ratio of the material liquid is 1: 10-20 ℃, extracting at the temperature of 90-100 ℃, filtering after 2-3 h, adding 50% edible ethanol into filter residue, extracting for 2-3 h again, extracting at the temperature of 90-100 ℃, filtering and combining extracting solutions, and concentrating and drying under reduced pressure to obtain the eucommia leaf alcohol extract.
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| CN102670696A (en) * | 2012-05-03 | 2012-09-19 | 中国药科大学 | Eucommia ulmoids leaf extracts and preparation method and application thereof |
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| CN110193034A (en) * | 2019-05-06 | 2019-09-03 | 普正药业集团股份有限公司 | A kind of eucommia leaf extract and its application in alleviation physical fatigue product |
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2021
- 2021-10-15 CN CN202111207162.9A patent/CN113973956A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102670696A (en) * | 2012-05-03 | 2012-09-19 | 中国药科大学 | Eucommia ulmoids leaf extracts and preparation method and application thereof |
| CN107156586A (en) * | 2017-06-02 | 2017-09-15 | 江苏朸健生命科技发展有限公司 | Advantageously reduce solid beverage of blood glucose and regulation blood fat and preparation method thereof |
| CN107114627A (en) * | 2017-06-13 | 2017-09-01 | 浙江丰岛食品有限公司 | A kind of coffee carnitine pulp juice drink and preparation method thereof |
| CN109730181A (en) * | 2018-12-26 | 2019-05-10 | 陕西乾宁健康食品有限公司 | A kind of companion eucommia bark coffee solid drink and preparation method thereof |
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