CN113941027A - Injectable facial filler composition gel for cosmetic and plastic surgery and preparation method thereof - Google Patents
Injectable facial filler composition gel for cosmetic and plastic surgery and preparation method thereof Download PDFInfo
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- CN113941027A CN113941027A CN202111228824.0A CN202111228824A CN113941027A CN 113941027 A CN113941027 A CN 113941027A CN 202111228824 A CN202111228824 A CN 202111228824A CN 113941027 A CN113941027 A CN 113941027A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L27/00—Materials for grafts or prostheses or for coating grafts or prostheses
- A61L27/50—Materials characterised by their function or physical properties, e.g. injectable or lubricating compositions, shape-memory materials, surface modified materials
- A61L27/60—Materials for use in artificial skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L27/00—Materials for grafts or prostheses or for coating grafts or prostheses
- A61L27/02—Inorganic materials
- A61L27/12—Phosphorus-containing materials, e.g. apatite
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L27/00—Materials for grafts or prostheses or for coating grafts or prostheses
- A61L27/14—Macromolecular materials
- A61L27/20—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L27/00—Materials for grafts or prostheses or for coating grafts or prostheses
- A61L27/14—Macromolecular materials
- A61L27/22—Polypeptides or derivatives thereof, e.g. degradation products
- A61L27/24—Collagen
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L27/00—Materials for grafts or prostheses or for coating grafts or prostheses
- A61L27/36—Materials for grafts or prostheses or for coating grafts or prostheses containing ingredients of undetermined constitution or reaction products thereof, e.g. transplant tissue, natural bone, extracellular matrix
- A61L27/3604—Materials for grafts or prostheses or for coating grafts or prostheses containing ingredients of undetermined constitution or reaction products thereof, e.g. transplant tissue, natural bone, extracellular matrix characterised by the human or animal origin of the biological material, e.g. hair, fascia, fish scales, silk, shellac, pericardium, pleura, renal tissue, amniotic membrane, parenchymal tissue, fetal tissue, muscle tissue, fat tissue, enamel
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L27/00—Materials for grafts or prostheses or for coating grafts or prostheses
- A61L27/50—Materials characterised by their function or physical properties, e.g. injectable or lubricating compositions, shape-memory materials, surface modified materials
- A61L27/52—Hydrogels or hydrocolloids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L27/00—Materials for grafts or prostheses or for coating grafts or prostheses
- A61L27/50—Materials characterised by their function or physical properties, e.g. injectable or lubricating compositions, shape-memory materials, surface modified materials
- A61L27/54—Biologically active materials, e.g. therapeutic substances
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/10—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing inorganic materials
- A61L2300/112—Phosphorus-containing compounds, e.g. phosphates, phosphonates
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/20—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing organic materials
- A61L2300/30—Compounds of undetermined constitution extracted from natural sources, e.g. Aloe Vera
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2400/00—Materials characterised by their function or physical properties
- A61L2400/06—Flowable or injectable implant compositions
Abstract
The invention discloses an injection type face filler composition gel for cosmetic and plastic surgery, which belongs to the technical field of medical treatment and comprises the following components in parts by weight: 10-20 parts of sodium hyaluronate, 90-100 parts of an aqueous solution for injection, 2-5 parts of collagen powder, 5-8 parts of modified particles, 0.1-0.2 part of an extracting agent and 0.4-0.7 part of a vitamin complex. The composition gel is safe to use, does not cause the problems of red swelling, vascular embolism and the like, and the treated skin is beautiful and natural.
Description
Technical Field
The invention belongs to the technical field of medical treatment, and particularly relates to an injection type facial filler composition gel for cosmetic and plastic and a preparation method thereof.
Background
Over time, the skin naturally relaxes and wrinkles develop, especially facial contour aging becomes increasingly severe, including visible skin wrinkles, deep nasolabial folds, frown lines, puppet lines, buccal junctional lines, perioral wrinkles, temporal collapse, and the like. Also, collapse of the nose bridge due to congenital or trauma, and misalignment of the brow bone and chin all cause annoying pain to people. Beauty is a constant topic and a pursuit target of human beings, and the problem of continuously exploring and solving how to effectively delay skin aging and beautify the appearance of the skin is still solved.
The injection beautifying is a kind of non-operation shaping beautifying method, and the injection method is used to inject biological material or artificially synthesized material with good biocompatibility into dermis or subcutaneous layer, so as to reduce skin wrinkle or plasticity. The sodium hyaluronate is a polysaccharide biomaterial with very good biocompatibility, has clear research on the in-vivo degradation and metabolism process, is safe to human bodies, and is a preferred material for preparing gel products. Nowadays, gel products are well known as important products in the field of micro-plastic, and a plurality of gel products for injection are available on the market, wherein the hyaluronic acid products are widely used by plastic beauty institutions with good biocompatibility, little side effect after injection and relatively long-lasting plastic effect.
However, the existing products usually have the defects that the product duration is not long, the injection needs to be performed again for several months, the phenomena of red and swollen after the operation and the like are easily caused, bad feeling is brought to operators, and great potential safety hazards exist.
Disclosure of Invention
The invention aims to solve the existing problems and provides an injection type face filler composition gel for cosmetic and plastic and a preparation method thereof.
The invention is realized by the following technical scheme:
an injection type face filler composition gel for cosmetic and plastic comprises the following components in parts by weight:
10-20 parts of sodium hyaluronate, 90-100 parts of an aqueous solution for injection, 2-5 parts of collagen powder, 5-8 parts of modified particles, 0.1-0.2 part of an extracting agent and 0.4-0.7 part of a vitamin complex.
Preferably, the composition comprises the following components in parts by weight:
15 parts of sodium hyaluronate, 95 parts of aqueous solution for injection, 4 parts of collagen powder, 7 parts of modified particles, 0.15 part of extractant and 0.6 part of vitamin complex.
Further, the water solution for injection is a sodium chloride solution with a mass concentration of 0.9%.
Further, the preparation method of the modified microparticle comprises the following steps:
(1) soaking apatite with a citric acid solution, filtering, washing with deionized water for 3-5 times for later use;
(2) immersing the apatite treated in the step (1) into a silane coupling agent solution, and filtering out for later use after immersing for 10-15 min;
(3) and (3) performing corona treatment on the apatite treated in the step (2), taking out the apatite after the corona treatment, washing the apatite with deionized water for 3-5 times, and drying the apatite.
Further, the mass concentration of the citric acid solution in the step (1) is 0.5-0.7%.
Further, the volume concentration of the silane coupling agent solution in the step (2) is 5-7%.
Further, the field intensity is controlled to be 500-520 kV/m during the corona treatment in the step (3).
Further, the preparation method of the extracting agent comprises the following steps:
a. firstly, the white atractylodes rhizome and the suberect spatholobus stem are mixed according to the weight ratio of 1: 2, mixing, then putting into an earthen pot filled with yellow core soil, stir-frying for 10-15 min, and taking out and crushing after completion;
b. and (3) putting the crushed materials into deionized water with the total mass being 8-10 times of that of the crushed materials, boiling the materials for 1-1.5 hours with strong fire, filtering the materials after the boiling, and finally concentrating the obtained filtrate to half of the original volume.
Furthermore, the compound vitamin contains vitamin A, vitamin B6, vitamin B9 and vitamin C.
A preparation method of an injectable facial filler composition gel for cosmetic and plastic surgery comprises the following steps:
firstly, adding sodium hyaluronate into an aqueous solution for injection, uniformly stirring at the rotating speed of 800-900 rpm, then adding collagen powder and modified particles, uniformly stirring at the rotating speed of 1200-1500 rpm, finally adding an extracting agent and multivitamins, and uniformly stirring at the rotating speed of 200-300 rpm.
Compared with the prior art, the invention has the following advantages:
the application provides an injection type facial filler composition gel for beauty and plastic, wherein the components are reasonably adjusted and compatible, and the added modified particles are formed by modifying apatite and have special active groups, so that the combination of sodium hyaluronate and tissues can be promoted, the natural filling effect can be improved, the natural filling effect cannot be eliminated by an immune system, and the using effect of the gel is enhanced; the added extractant can promote the hematopoietic function, improve the differentiation and proliferation capacity of cells, improve the natural fineness of the filled skin and further enhance the use effect of the gel. In addition, the method is simple, easy to popularize and apply and extremely high in market competitiveness.
Detailed Description
Example 1
An injection type face filler composition gel for cosmetic and plastic comprises the following components in parts by weight:
10 parts of sodium hyaluronate, 90 parts of aqueous solution for injection, 2 parts of collagen powder, 5 parts of modified particles, 0.1 part of extractant and 0.4 part of vitamin complex.
The water solution for injection is a sodium chloride solution with the mass concentration of 0.9%.
The preparation method of the modified particles comprises the following steps:
(1) firstly, soaking apatite with citric acid solution, then filtering and washing with deionized water for 3 times for later use; the mass concentration of the citric acid solution is 0.5 percent;
(2) immersing the apatite treated in the step (1) into a silane coupling agent solution, and filtering out for later use after immersing for 10 min; the volume concentration of the silane coupling agent solution is 5 percent;
(3) performing corona treatment on the apatite treated in the step (2), taking out the apatite after the corona treatment, washing the apatite for 3 times by using deionized water, and drying the apatite; the field intensity is controlled to be 500kV/m during corona treatment.
The preparation method of the extractant comprises the following steps:
a. firstly, the white atractylodes rhizome and the suberect spatholobus stem are mixed according to the weight ratio of 1: 2, mixing, then putting into a marmite containing yellow core soil, stir-frying for 10min, taking out and crushing after completion;
b. and (3) putting the crushed materials into deionized water with the mass 8 times of the total mass of the materials, boiling the materials for 1 hour with strong fire, filtering the materials after the boiling is finished, and finally concentrating the obtained filtrate to be half of the original volume.
The compound vitamin contains vitamin A, vitamin B6, vitamin B9, and vitamin C.
A preparation method of an injectable facial filler composition gel for cosmetic and plastic surgery comprises the following steps:
firstly, adding sodium hyaluronate into an aqueous solution for injection, uniformly stirring at the rotating speed of 800rpm, then adding collagen powder and modified particles, uniformly stirring at the rotating speed of 1200rpm, finally adding an extracting agent and multivitamins, and uniformly stirring at the rotating speed of 200 rpm.
Example 2
An injection type face filler composition gel for cosmetic and plastic comprises the following components in parts by weight:
15 parts of sodium hyaluronate, 95 parts of aqueous solution for injection, 4 parts of collagen powder, 7 parts of modified particles, 0.15 part of extractant and 0.6 part of vitamin complex.
The water solution for injection is a sodium chloride solution with the mass concentration of 0.9%.
The preparation method of the modified particles comprises the following steps:
(1) firstly, soaking apatite with citric acid solution, and then filtering and washing with deionized water for 4 times for later use; the mass concentration of the citric acid solution is 0.6 percent;
(2) immersing the apatite treated in the step (1) into a silane coupling agent solution, and filtering out for later use after immersion treatment for 13 min; the volume concentration of the silane coupling agent solution is 6 percent;
(3) performing corona treatment on the apatite treated in the step (2), taking out the apatite after the corona treatment, washing the apatite with deionized water for 4 times, and drying the apatite; the field intensity is controlled to be 510kV/m during corona treatment.
The preparation method of the extractant comprises the following steps:
a. firstly, the white atractylodes rhizome and the suberect spatholobus stem are mixed according to the weight ratio of 1: 2, mixing, then putting into a marmite containing yellow core soil, stir-frying for 14min, taking out and crushing after completion;
b. and (3) putting the crushed materials into deionized water with the mass 9 times of the total mass of the materials, boiling the materials for 1.3 hours with strong fire, filtering the materials after the boiling is finished, and finally concentrating the obtained filtrate to half of the original volume.
The compound vitamin contains vitamin A, vitamin B6, vitamin B9, and vitamin C.
A preparation method of an injectable facial filler composition gel for cosmetic and plastic surgery comprises the following steps:
firstly, adding sodium hyaluronate into an injection water solution, uniformly stirring at the rotating speed of 860rpm, then adding collagen powder and modified particles, uniformly stirring at the rotating speed of 1400rpm, finally adding an extracting agent and multivitamins, and uniformly stirring at the rotating speed of 250 rpm.
Example 3
An injection type face filler composition gel for cosmetic and plastic comprises the following components in parts by weight:
20 parts of sodium hyaluronate, 100 parts of aqueous solution for injection, 5 parts of collagen powder, 8 parts of modified particles, 0.2 part of extractant and 0.7 part of vitamin complex.
The water solution for injection is a sodium chloride solution with the mass concentration of 0.9%.
The preparation method of the modified particles comprises the following steps:
(1) firstly, soaking apatite with citric acid solution, then filtering and washing with deionized water for 5 times for later use; the mass concentration of the citric acid solution is 0.7%;
(2) immersing the apatite treated in the step (1) into a silane coupling agent solution, and filtering out for later use after immersion treatment for 15 min; the volume concentration of the silane coupling agent solution is 7 percent;
(3) performing corona treatment on the apatite treated in the step (2), taking out the apatite after the corona treatment, washing the apatite for 5 times by using deionized water, and drying the apatite; the control field intensity during corona treatment is 520 kV/m.
The preparation method of the extractant comprises the following steps:
a. firstly, the white atractylodes rhizome and the suberect spatholobus stem are mixed according to the weight ratio of 1: 2, mixing, then putting into a marmite containing yellow core soil, stir-frying for 15min, taking out and crushing after completion;
b. and (3) putting the crushed materials into deionized water with the weight 10 times of the total weight of the materials, boiling the materials for 1.5 hours with strong fire, filtering the materials after the boiling is finished, and finally concentrating the obtained filtrate to half of the original volume.
The compound vitamin contains vitamin A, vitamin B6, vitamin B9, and vitamin C.
A preparation method of an injectable facial filler composition gel for cosmetic and plastic surgery comprises the following steps:
firstly, adding sodium hyaluronate into an aqueous solution for injection, uniformly stirring at the rotating speed of 900rpm, then adding collagen powder and modified particles, uniformly stirring at the rotating speed of 1500rpm, finally adding an extracting agent and multivitamins, and uniformly stirring at the rotating speed of 300 rpm.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing description, it will be apparent to one skilled in the art that various changes, modifications, equivalents, and improvements may be made without departing from the spirit and scope of the invention.
Claims (10)
1. An injection type face filler composition gel for cosmetic and plastic, which is characterized by comprising the following components in parts by weight:
10-20 parts of sodium hyaluronate, 90-100 parts of an aqueous solution for injection, 2-5 parts of collagen powder, 5-8 parts of modified particles, 0.1-0.2 part of an extracting agent and 0.4-0.7 part of a vitamin complex.
2. The injectable facial filler composition gel for cosmetic and cosmetic use according to claim 1, comprising the following components in parts by weight:
15 parts of sodium hyaluronate, 95 parts of aqueous solution for injection, 4 parts of collagen powder, 7 parts of modified particles, 0.15 part of extractant and 0.6 part of vitamin complex.
3. The injectable facial filler composition gel for cosmetic and cosmetic use according to claim 1 or 2, wherein the aqueous solution for injection is a sodium chloride solution having a mass concentration of 0.9%.
4. The injectable facial filler composition gel for cosmetic and cosmetic use according to claim 1 or 2, wherein the modified fine particles are prepared by a method comprising the steps of:
(1) soaking apatite with a citric acid solution, filtering, washing with deionized water for 3-5 times for later use;
(2) immersing the apatite treated in the step (1) into a silane coupling agent solution, and filtering out for later use after immersing for 10-15 min;
(3) and (3) performing corona treatment on the apatite treated in the step (2), taking out the apatite after the corona treatment, washing the apatite with deionized water for 3-5 times, and drying the apatite.
5. The injectable facial filler composition gel for cosmetic and cosmetic use according to claim 4, wherein the citric acid solution in the step (1) has a mass concentration of 0.5 to 0.7%.
6. The injectable facial filler composition gel for cosmetic and cosmetic use according to claim 4, wherein the silane coupling agent solution in the step (2) has a volume concentration of 5 to 7%.
7. The injectable facial filler composition gel for cosmetic and cosmetic use according to claim 4, wherein the field strength during corona treatment in step (3) is controlled to be 500 to 520 kV/m.
8. The injectable facial filler composition gel for cosmetic and cosmetic use according to claim 1 or 2, wherein the extraction agent is prepared by a method comprising the steps of:
a. firstly, the white atractylodes rhizome and the suberect spatholobus stem are mixed according to the weight ratio of 1: 2, mixing, then putting into an earthen pot filled with yellow core soil, stir-frying for 10-15 min, and taking out and crushing after completion;
b. and (3) putting the crushed materials into deionized water with the total mass being 8-10 times of that of the crushed materials, boiling the materials for 1-1.5 hours with strong fire, filtering the materials after the boiling, and finally concentrating the obtained filtrate to half of the original volume.
9. The injectable gel of a cosmetic pack composition according to claim 1 or 2, wherein the vitamin complex comprises vitamin A, vitamin B6, vitamin B9, and vitamin C.
10. A preparation method of an injectable facial filler composition gel for cosmetic and plastic surgery is characterized by comprising the following steps:
firstly, adding sodium hyaluronate into an aqueous solution for injection, uniformly stirring at the rotating speed of 800-900 rpm, then adding collagen powder and modified particles, uniformly stirring at the rotating speed of 1200-1500 rpm, finally adding an extracting agent and multivitamins, and uniformly stirring at the rotating speed of 200-300 rpm.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111228824.0A CN113941027A (en) | 2021-10-21 | 2021-10-21 | Injectable facial filler composition gel for cosmetic and plastic surgery and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202111228824.0A CN113941027A (en) | 2021-10-21 | 2021-10-21 | Injectable facial filler composition gel for cosmetic and plastic surgery and preparation method thereof |
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| CN113941027A true CN113941027A (en) | 2022-01-18 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115252896A (en) * | 2022-08-11 | 2022-11-01 | 成都恒美盛生物科技有限公司 | Material mixing method for producing facial filler |
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- 2021-10-21 CN CN202111228824.0A patent/CN113941027A/en active Pending
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| CN106659639A (en) * | 2014-07-11 | 2017-05-10 | 三井化学株式会社 | Dental prosthesis |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115252896A (en) * | 2022-08-11 | 2022-11-01 | 成都恒美盛生物科技有限公司 | Material mixing method for producing facial filler |
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