CN113925989A - Application of storax and/or grafted storax in improvement of flammability of incense, incense and preparation method and application thereof - Google Patents
Application of storax and/or grafted storax in improvement of flammability of incense, incense and preparation method and application thereof Download PDFInfo
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- CN113925989A CN113925989A CN202111202227.0A CN202111202227A CN113925989A CN 113925989 A CN113925989 A CN 113925989A CN 202111202227 A CN202111202227 A CN 202111202227A CN 113925989 A CN113925989 A CN 113925989A
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- storax
- incense
- grafted
- parts
- flammability
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/015—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone
- A61L9/02—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone using substances evaporated in the air by heating or combustion
-
- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47G—HOUSEHOLD OR TABLE EQUIPMENT
- A47G33/00—Religious or ritual equipment in dwelling or for general use
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
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- Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention relates to the field of incense preparation, in particular to application of storax and/or grafted storax in improving incense flammability, incense and a preparation method and application thereof. The invention provides application of storax and/or grafted storax in improving fragrance flammability. The storax and/or the grafted storax have a combustion-supporting effect on noncombustible medicinal materials, and have a certain flame-retardant effect on combustible medicinal materials. And after storax and/or grafted storax are added, the cinnamic acid derivatives can not only congeal fragrance, but also can improve fragrance, and the substance can be metabolized in vivo after entering human body through breathing to have antibacterial, anti-inflammatory, blood circulation promoting and blood stasis removing effects, and also has resuscitation inducing, filth removing, qi circulation promoting, and pain relieving effects, and has pleasant and health promoting effects.
Description
Technical Field
The invention relates to the field of incense preparation, in particular to application of storax and/or grafted storax in improving incense flammability, incense and a preparation method and application thereof.
Background
In order to reduce the cost, most of the incense on the market at present consists of burning powder, chemical adhesives, chemical flame retardants and chemical essence, gas and particles harmful to human bodies can be generated in the burning process, and the incense cannot be used for mastering temperament and health preservation for a long time in the environment, so that the environment can be polluted and even sick.
At present, the incense prepared by pure plants in the market has unstable flammability, i.e. low or high flammability. Therefore, it is important to find a flammability regulator that improves the fragrance.
Disclosure of Invention
In order to solve the problems, the invention provides application of storax and/or grafted storax in improving incense flammability, incense, a preparation method and application thereof. The storax and/or the grafted storax can improve the flammability of the incense.
In order to achieve the above purpose, the invention provides the following technical scheme:
the invention provides application of storax and/or grafted storax in improving fragrance flammability.
Preferably, the grafted storax comprises grafted storax resin and/or grafted storax oil; the incense comprises a mixed incense.
Preferably, the flammability comprises combustion or flame retardancy.
The invention provides a regulator for improving the flammability of incense, which comprises storax and/or grafted storax.
Preferably, the grafted storax comprises grafted storax resin and/or grafted storax oil.
The invention provides a incense, which is prepared from the following raw materials in parts by mass: 3 to 10 parts of a perfume plant, 0.2 to 5 parts of the conditioner according to claim 4 or 5, and 2 to 5 parts of a binder.
Preferably, the adhesive comprises one or more of elm bark sticky powder, kenaf bark sticky powder, nanmu sticky powder, red bark sticky powder, indonesia sticky powder and white bark sticky powder.
The invention provides a preparation method of the incense, which comprises the following steps: mixing the perfume plant, the regulator and the binder with water to obtain the incense.
Preferably, the flavor plant, conditioning agent and binder are all sieved through a 100 mesh sieve.
The invention provides the application of the incense in improving human health. .
Has the advantages that: the invention provides application of storax and/or grafted storax in improving fragrance flammability. The storax and/or grafted storax has a combustion-supporting effect on noncombustible medicinal materials, and has a certain flame-retardant effect on combustible medicinal materials.
Furthermore, the invention provides a fragrance and its use in improving human health. During burning incense, storax and/or grafted storax has effects of condensing incense, inducing resuscitation, removing filth, promoting qi circulation, and relieving pain, and has effects of refreshing and promoting health. The results of the specific embodiments of the invention show that: after the storax is added and/or grafted, the fragrance of eugenol, caryophyllene and the like is increased.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the embodiments will be briefly described below.
FIG. 1 is a GC-MS diagram of the clove Syzygium aromaticum No. 1 burning SPME probe after adsorption;
FIG. 2 is a GC-MS diagram of the clove Syzygium aromaticum No. 3 burning SPME probe after adsorption;
FIG. 3 is a GC-MS diagram of the ageratum odoratum No. 1 burning SPME probe after adsorption;
FIG. 4 is a GC-MS diagram of the ageratum odoratum No. 3 burning SPME probe after adsorption;
FIG. 5 is a GC-MS comparison of the adsorbed burning SPME probes of Agastache rugosa, Nos. 1 and 3, wherein the red line is Agastache rugosa, No. 3, and the black line is Agastache rugosa, No. 1.
Detailed Description
Hereinafter, unless otherwise specified, the perfume plants and components used in the present invention are those conventionally purchased by those skilled in the art.
The present invention provides the use of a storax and/or grafted storax to improve the flammability of a fragrance, preferably comprising a storax. In the present invention, the flammability preferably includes combustion or flame retardancy. In the present invention, the storax preferably comprises storax resin and/or storax oil; the grafted storax preferably comprises grafted storax resin and/or grafted storax oil, and more preferably grafted storax oil. The storax and/or grafted storax of the invention has combustion-supporting and fragrance-coagulating effects on incombustible perfume plants, and has certain flame-retardant and fragrance-coagulating effects on combustible perfume plants.
The source of the storax and the grafted storax is not specially limited, and the storax and the grafted storax are obtained by conventional purchase of technicians in the field; in a specific embodiment of the invention, the storax is preferably purchased from the bozhou medicinal market, imported from the uk; the grafted storax is preferably obtained by adopting a storax propagation method disclosed in the patent of application number 'CN 201510813643.2', and the specific steps are preferably as follows: taking a 20-year-old seedling (with the diameter of 10-20 cm) of the sweetgum as a stock, taking a twig of the styrax which does not germinate and has the growth capacity for 3-4 months as a scion, flattening the grafting part of the scion by using a knife (so that the scion can be closely attached to the stock for growth), cutting the head of the sweetgum seedling, cutting the phloem of the liquidgum seedling by using a sharp knife, inoculating the scion to the stock, fastening the scion by using a rope or a thread or a thin film, and covering the scion part by using the thin film or paper so as to prevent the liquidgum seedling from losing water. And when grafting is carried out for 1 to 2 months, cutting the film or paper sleeved with the scion part for ventilation, and loosening the scion and the stock after the binding rope grows and fuses for 1 year. In the invention, the storax has similar pharmacological action through comparison of volatile components and non-volatile components with the grafted storax, and the grafted storax also has the advantage of low cost.
In the invention, the method for obtaining the grafted storax resin is preferably as follows: and (3) cutting the grafted storax bark in 7-8 months, and collecting 9-10 parts in the current year to obtain the grafted storax resin. In the invention, the preferable method for obtaining the storax resin is to cut the bark of the storax in 7-8 months and collect 9-10 parts of the storax in the same year to obtain the storax resin; the storax resin may also be purchased commercially.
In the present invention, the preparation method of the grafted storax oil preferably comprises the following steps: mixing the grafted storax resin with an ethanol solution, and filtering to obtain a filtrate; and (4) concentrating the filtrate under reduced pressure to obtain the grafted storax oil. In the invention, the volume percentage of ethanol in the ethanol solution is 90-100%. The mixing, filtering and vacuum concentration method is not particularly limited in the present invention, and any method known to those skilled in the art may be used. In the present invention, the preparation method of the storax oil preferably comprises the following steps: mixing storax resin with ethanol solution, and filtering to obtain filtrate; concentrating the filtrate under reduced pressure to obtain storax oil; the storax resin may also be purchased commercially. In the invention, the volume percentage of ethanol in the ethanol solution is 90-100%. The manner of mixing, filtering and concentrating under reduced pressure is not particularly limited in the present invention, and may be any manner known to those skilled in the art.
The invention provides a regulator for improving the flammability of incense, which comprises storax and/or grafted storax. In the present invention, the grafted storax preferably comprises grafted storax resin and/or grafted storax oil, more preferably grafted storax oil; the obtaining method of the grafted storax resin and the preparation method of the grafted storax oil are described in detail in the foregoing, and are not described herein again. In the present invention, the flammability preferably includes combustion supporting properties and flame retardancy. The storax and/or the grafted storax have a combustion-supporting effect on nonflammable spice plants, and have a certain flame-retardant effect on combustible spice plants, so that the storax and/or the grafted storax can be used as a regulator for improving the flammability of the fragrance.
The invention provides a incense, which is prepared from the following raw materials in parts by mass: 3-10 parts of perfume plants, 0.2-5 parts of the regulator and 2-5 parts of adhesive in the technical scheme; preferably, the water-soluble paint also comprises 8-30 parts of water. In the present invention, the type of the incense preferably includes a mixed incense.
The incense provided by the invention comprises 3-10 parts by mass of spice plants, preferably 4-9 parts by mass, further preferably 5-8 parts by mass, and more preferably 6-7 parts by mass. In the present invention, the perfume plant preferably includes a perfume plant having poor flammability and a perfume plant having better flammability. The specific variety of the aromatic plant with poor flammability preferably includes galangal, Chinese pine knot, dried ginger, baked ginger, cacumen biotae, rhizoma kaempferiae, fructus amomi, elecampane, tsaoko amomum fruit, radix aucklandiae, radix aurantii, immature bitter orange, ligusticum wallichii, fructus caryophylli, rhizoma curcumae longae, fennel, bighead atractylodes rhizome, fructus alpiniae oxyphyllae, radix paeoniae alba, perilla fruit, radix angelicae dahuricae, citron, angelica sinensis, pepper, radix sileris, notopterygium root, radix angelicae pubescentis, exocarpium citri rubrum, pummelo peel, cortex moutan, cassia twig, curcuma longa, cinnamon, ligusticum sinense, alpinia katsumadai, sandalwood, nutmeg, agilawood, platycladi seed, lignum dalbergiae odoriferae and star anise, but is not limited thereto. The specific variety of the aromatic plant with better flammability is preferably China rose, Suqin flower, rose, peony, sweet osmanthus, jasmine flower, magnolia officinalis, peony, Chinese trumpet creeper, lotus, clove, white magnolia flower, magnolia grandiflora, chrysanthemum, Chinese flowering apple, wild chrysanthemum, elecampane, plum blossom, lavender, peach blossom, trachelospermi, cherry blossom, schizonepeta spike, woody flower, lavender, rosemary, elsholtzia, glechoma longituba, mint, fineleaf schizonepeta herb, sweet wormwood, folium artemisiae argyi, agastache rugosus, patchouli, oriental wormwood, benzoin, perilla leaf, stem perilla, sweetgum, eupatorium and myrrh, but not limited thereto. The perfume plant with poor flammability is not flammable, but has a combustion-supporting effect through the storax; the perfume plant with better flammability can be flammable, and the storax of the invention has a flame retardant effect on the perfume plant. The perfume plants in the incense provided by the invention can generate substances such as aroma and the like.
The perfume plant provided by the invention comprises 0.2-5 parts of the regulator by mass, preferably 0.4-4.8 parts of the regulator by mass, more preferably 0.6-4.6 parts of the regulator by mass, and more preferably 0.8-4.4 parts of the regulator by mass. The blending agent in the incense can improve the flammability of the incense, improve the flammability of the perfume plant with low flammability and reduce the flammability of the perfume plant with high flammability.
The perfume plant provided by the invention comprises 2-5 parts of the binder, preferably 2.5-4.5 parts of the binder, and more preferably 3-4 parts of the binder. In the invention, the adhesive preferably comprises one or more of elm bark sticky powder, kenaf bark sticky powder, nanmu sticky powder, red bark sticky powder, indonesia sticky powder and white bark sticky powder. When two or more of the binders are mixed, the ratio thereof is not particularly limited in the present invention. The prices of the elm bark sticky powder, the hemp bark sticky powder, the nanmu sticky powder, the red bark sticky powder, the Indonesia sticky powder and the white bark sticky powder are different, the elm bark sticky powder, the hemp bark sticky powder, the nanmu sticky powder, the red bark sticky powder, the Indonesia sticky powder and the white bark sticky powder can be selected according to self economic conditions, and the effects are equivalent. The adhesive in the incense of the invention bonds the components during incense production, and is helpful for molding.
The perfume provided by the invention preferably further comprises 8-30 parts of water, more preferably 10-25 parts of water, and even more preferably 13-20 parts of water based on the mass parts of the perfume plants.
The invention provides a preparation method of the incense, which comprises the following steps:
mixing the perfume plant, the regulator and the binder with water to obtain the incense.
The invention mixes the perfume plant, the regulator and the adhesive with water to obtain the incense. The flavor plants, conditioning agents and binders described herein are all preferably screened through a 100 mesh screen. The invention preferably provides for a first mixing of the fragrance plant, conditioner and binder followed by a second mixing with water. The first mixing and second mixing means are not particularly limited in the present invention, and may be any means known to those skilled in the art; the second mixing mode is preferably to add water and stir simultaneously, so as to ensure that the individual materials are uniformly mixed; and the blank obtained by the second mixing is uniform in viscosity and does not scatter after being agglomerated according to the standard of finishing the second mixing. In the invention, the temperature of the water is preferably 30-100 ℃, more preferably 35-95 ℃, and more preferably 40-90 ℃, and the water at the temperature can make the adhesive have better adhesive property.
After the second mixing, the present invention preferably further comprises extruding, air drying and sub-packaging. In the present invention, the extrusion is preferably carried out in a fragrance maker or a fragrance maker, for the purpose of shaping. The airing is preferably carried out in a ventilated place; the airing temperature is preferably room temperature; need pay attention to when drying to press fragrant and prevent that the moisture evaporation is too fast, avoid appearing the condition appearance of fragrant perk. The dispensing of the present invention is not particularly limited and may be carried out in a manner known to those skilled in the art.
The invention provides the application of the incense in improving human health. The components and preparation method of the incense of the invention are discussed in detail in the foregoing, and are not repeated herein. During burning, storax and/or grafted storax release cinnamic acid derivatives, which can be metabolized in vivo after breathing into human body to have antibacterial, antiinflammatory, blood circulation promoting and blood stasis removing effects, and during burning, storax and/or grafted storax have fragrance condensing effect and can also be used for extracting fragrance; and can also release components for resuscitation, filth removal, qi circulation promotion and pain relief, and has the effects of joyful and health preservation. The results of the specific embodiments of the invention show that: after the storax and/or the grafted storax are added, the fragrance of eugenol, caryophyllene and the like is increased.
For further illustration of the present invention, the following detailed description of the use of the storax and/or grafted storax for improving the flammability of the incense, a incense and its preparation method and use are provided in the accompanying drawings and examples, which should not be construed as limiting the scope of the present invention.
Example 1
The method for obtaining the grafted storax resin comprises the following steps: the resin produced by grafting storax from plant research institute of Chinese academy of sciences of Jiangsu province is obtained by cutting and grafting the bark of storax at 18 days 7 and 7 months in 2020, and collecting the resin grafted with storax at 20 days 10 and 20 months in the year.
The method for obtaining the grafted storax oil comprises the following steps: the method comprises the steps of grafting the bark of storax by cutting in 7-18 days in 2020, and collecting the resin grafted with storax in 20 days in 10-20 months in the year from the plant research institute of Chinese academy of sciences in Jiangsu province; dissolving the resin in 90-100% ethanol at normal temperature, filtering, concentrating the filtrate under reduced pressure, and recovering the filtrate to obtain oily matter, namely the grafted storax oil.
The grafted storax resin or grafted storax oil used in the subsequent examples is the grafted storax resin or grafted storax oil prepared in this example.
Example 2
Firstly, screening the woody vetiver, the grafted styrax resin and the elm bark sticky powder by a 100-mesh sieve, weighing 10 parts (100g) of the woody vetiver, 0.2 part (2g) of the grafted styrax resin and 5 parts (50g) of the elm bark sticky powder, uniformly mixing, adding 15 parts (150g) of hot water at 90-100 ℃, stirring until the viscosity is uniform, and not dispersing after conglobation. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, drying the blank at room temperature in a ventilating way after finishing incense, pressing incense when drying the blank, and preventing the blank from tilting after water is evaporated too fast. And after drying, subpackaging to obtain the costustoot and Hexiang No. 2 incense.
Example 3
Firstly, screening the woody balsamroots, the grafted styrax resin and the elm bark sticky powder by a sieve of 100 meshes, weighing 10 parts (100g) of the woody roots, 2 parts (20g) of the grafted styrax resin and 5 parts (50g) of the elm bark sticky powder, uniformly mixing, adding 15 parts (150g) of hot water of 90-100 ℃, stirring until the viscosity is uniform, and not dispersing after conglobation. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, drying the blank at room temperature in a ventilating way after finishing incense, pressing incense when drying the blank, and preventing the blank from tilting after water is evaporated too fast. And after drying, subpackaging to obtain the costustoot and Hexiang No. 3 incense.
Example 4
Firstly, sieving clove buds and elm bark sticky powder by a 100-mesh sieve, weighing 10 parts (100g) of clove buds, 0.2 part (2g) of grafted storax oil and 5 parts (50g) of elm bark sticky powder, uniformly mixing, adding 15 parts (150g) of hot water at 90-100 ℃, stirring until the viscosity is uniform, and forming a dough without dispersing. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, drying the agglomerated blank at room temperature in a ventilated place after finishing incense, pressing the incense during drying, and preventing the moisture from being tilted after evaporating too fast. And after drying, subpackaging to obtain the clove and Hexiang No. 2 incense.
Example 5
Firstly, the clove bud and the elm bark sticky powder are sieved by a 100-mesh sieve, 10 parts (100g) of the clove bud, 2 parts (20g) of grafted storax oil and 5 parts (50g) of the elm bark sticky powder are weighed, and after being uniformly mixed, 15 parts (150g) and hot water at the temperature are added and stirred until the viscosity is uniform and the mixture is not scattered after being agglomerated. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, airing the blank at room temperature in a ventilating place after finishing incense, and paying attention to the aroma pressing during airing to prevent the blank from tilting after the moisture is evaporated too fast. And after drying, subpackaging to obtain the clove and Hexiang No. 3 incense.
Example 6
Firstly, sieving the overground part of the agastache rugosus and the elm bark sticky powder by a sieve of 100 meshes, weighing 10 parts (100g) of the overground part of the agastache rugosus, 0.2 part (2g) of storax oil and 5 parts (50g) of the elm bark sticky powder, uniformly mixing, adding 15 parts (150g) of hot water at 90-100 ℃, stirring until the viscosity is uniform, and not dispersing after agglomeration. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, drying the blank at room temperature in a ventilating way after finishing incense, pressing incense when drying the blank, and preventing the blank from tilting after water is evaporated too fast. And after drying, subpackaging to obtain the ageratum hexiang No. 2 incense.
Example 7
After sieving the overground part of the agastache rugosus and the elm bark sticky powder by a sieve of 100 meshes, weighing 10 parts (100g) of the overground part of the agastache rugosus, 2 parts (20g) of storax oil and 5 parts (50g) of the elm bark sticky powder, adding 15 parts (150g) of hot water at 90-100 ℃ after uniformly mixing, stirring until the viscosity is uniform, and not dispersing after conglobation. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, drying the blank at room temperature in a ventilating way after finishing incense, pressing incense when drying the blank, and preventing the blank from tilting after water is evaporated too fast. And after drying, subpackaging to obtain the ageratum hedyotis 3 incense.
Example 8
Firstly, screening rose and elm bark sticky powder by a 100-mesh sieve, weighing 10 parts (100g) of rose, 0.2 part (2g) of grafted storax oil and 5 parts (50g) of elm bark sticky powder, uniformly mixing, adding 15 parts (150g) of hot water at 90-100 ℃, stirring until the viscosity is uniform, and not dispersing after conglobation. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, drying the blank at room temperature in a ventilating way after finishing incense, pressing incense when drying the blank, and preventing the blank from tilting after water is evaporated too fast. And after the rose leaves are dried, subpackaging to obtain the rose mixed fragrance No. 2.
Example 9
Firstly, screening rose, grafted storax and elm bark sticky powder by a 100-mesh sieve, weighing 10 parts (100g) of rose, 2 parts (20g) of grafted storax oil and 5 parts (g) of elm bark sticky powder, uniformly mixing, adding 15 parts (150g) of hot water at 90-100 ℃, stirring until the viscosity is uniform, and not dispersing after conglobation. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, drying the blank at room temperature in a ventilating way after finishing incense, and paying attention to press incense when drying the blank, and preventing the blank from tilting after water is evaporated too fast. And after the rose leaves are dried, subpackaging to obtain the rose combined incense No. 3.
Example 10
Firstly, after the lavender flower and elm bark sticky powder is sieved by a 100-mesh sieve, 10 parts (100g) of lavender, 0.2 part (2g) of grafted storax oil and 5 parts (50g) of nanmu sticky powder are weighed, and after the lavender flower and elm bark sticky powder are uniformly mixed, 15 parts (150g) of hot water at 90-100 ℃ is added and stirred until the viscosity is uniform and the mixture is not scattered after being agglomerated. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, drying the agglomerated blank at room temperature in a ventilated place after finishing incense, pressing the incense during drying, and preventing the moisture from being tilted after evaporating too fast. And after the lavender is dried, subpackaging to obtain the lavender fragrance No. 2.
Example 11
Firstly, after the lavender flower and elm bark sticky powder are sieved by a 100-mesh sieve, 10 parts (100g) of lavender flower, 2 parts (20g) of grafted storax oil and 5 parts (50g) of nanmu sticky powder are weighed, and after the lavender flower and the elm bark sticky powder are uniformly mixed, 15 parts (150g) of water with the temperature of 90-100 ℃ are added and stirred until the viscosity is uniform and the mixture is not scattered after being agglomerated. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, drying the blank at room temperature in a ventilating way after finishing incense, pressing incense when drying the blank, and preventing the blank from tilting after water is evaporated too fast. And after drying, subpackaging to obtain the lavender fragrance No. 3.
Comparative example 1
Firstly, screening the woody balsamroot and the elm bark sticky powder by a 100-mesh sieve, weighing 10 parts (100g) of the woody balsamroot and 5 parts (50g) of the elm bark sticky powder, uniformly mixing, adding 15 parts (150g) of hot water at 90-100 ℃, stirring until the viscosity is uniform, and not dispersing after conglobation. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, drying the blank at room temperature in a ventilating way after finishing incense, pressing incense when drying the blank, and preventing the blank from tilting after water is evaporated too fast. And after drying, subpackaging to obtain the costustoot and Hexiang No. 1 incense.
Comparative example 2
Firstly, sieving clove buds and elm bark sticky powder by a sieve of 100 meshes, weighing 10 parts (100g) of clove buds and 5 parts (50g) of elm bark sticky powder, uniformly mixing, adding 15 parts (150g) of hot water at 90-100 ℃, stirring until the viscosity is uniform, and not dispersing after conglobation. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, airing the blank at a ventilation place at room temperature after finishing the incense, and pressing the incense when airing the blank to prevent the moisture from tilting after evaporating too fast. And after drying, subpackaging to obtain the clove mixed incense No. 1 incense.
Comparative example 3
Firstly, sieving the overground part of the agastache rugosus and the elm bark sticky powder by a sieve of 100 meshes, weighing 10 parts (100g) of the overground part of the agastache rugosus and 5 parts (50g) of the elm bark sticky powder, uniformly mixing, adding 15 parts (150g) of hot water at 90-100 ℃, stirring until the viscosity is uniform, and not dispersing after the mixture is agglomerated. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, drying the blank at normal temperature in a ventilation place after finishing incense, pressing incense when drying the blank, and preventing the blank from tilting after water is evaporated too fast. After drying, subpackaging to obtain the ageratum hexiang No. 1 incense.
Comparative example 4
Firstly, screening rose and elm bark sticky powder by a 100-mesh sieve, weighing 10 parts (100g) of rose and 5 parts (50g) of elm bark sticky powder, uniformly mixing, adding 15 parts (150g) of hot water at 90-100 ℃, stirring until the viscosity is uniform, and not dispersing after agglomeration. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, drying the blank at normal temperature in a ventilation place after finishing incense, pressing incense when drying the blank, and preventing the blank from tilting after water is evaporated too fast. And after the rose leaves are dried, subpackaging to obtain the rose mixed fragrance No. 1 fragrance.
Comparative example 5
Firstly, after the lavender flower and nanmu sticky powder are sieved by a 100-mesh sieve, 10 parts (100g) of lavender flower and 5 parts (50g) of nanmu sticky powder are weighed, and after the lavender flower and the nanmu sticky powder are uniformly mixed, 15 parts (150g) of hot water at 90-100 ℃ is added and stirred until the lavender flower and the nanmu sticky powder are uniformly sticky and do not scatter after being agglomerated. Extruding and molding the agglomerated blank by using a incense maker or an incense maker, after finishing incense, airing the blank at normal temperature in a ventilation place, and paying attention to pressing incense during airing to prevent the blank from tilting after water is evaporated too fast. And after drying, subpackaging to obtain the lavender fragrance No. 1.
The flammability of the woody incense prepared in the examples 2, 3 and 1 is examined by the following specific method: the incense with the same length and diameter is simultaneously ignited in parallel, the time is calculated, and the burnt length is measured.
The results show that after 77.36min of burning, the incense of aucklandia No. 1 (comparative example 1) is incombustible, the incense of aucklandia No. 2 (example 2) is remained for 6.5cm, and the incense of wood No. 3 (example 3) is remained for 5cm, so that the resin or oil of the storax can be seen, or the resin or oil of the storax can be grafted, and the incense has certain combustion supporting effect on the incombustible perfume plants (traditional Chinese medicine incense), and can improve the combustibility of the incombustible perfume plants; and as the content thereof increases, the combustion ability increases.
The flammability of the clove aroma prepared in the embodiment 4, the embodiment 5 and the comparative example 2 is examined, and the specific method is as follows: the incense with the same length and diameter is simultaneously ignited in parallel, the time is calculated, and the burnt length is measured.
The results show that after 55.23min of combustion, the clove mixed incense No. 1 (comparative example 2) leaves 5.3cm, the clove mixed incense No. 2 (example 4) leaves 6.5cm, and the clove mixed incense No. 3 (example 5) leaves 7.8cm, so that the grafted storax can be seen, and the combustible spice plants (traditional Chinese medicine incense) have certain flame retardant effect, and the flame retardant capability is enhanced along with the increase of the content of the combustible spices, so that the combustible spices are prevented from being burnt out quickly, and the combustion time of the combustible spices can be prolonged.
The content of the main chemical components of the clove aroma prepared in the comparative example 2 and the example 5 is detected, and the specific detection method comprises the following steps:
the fiber end of a Supelco SPME (solid phase Microextraction) probe, model 57300-U, was exposed to a 2000mL inverted beaker, the fragrance was ignited and timed for 10min, the probe was removed and manually injected, and the data collected by GC-MS. GC: agilent 7890A; MS: agilent 5975C; capillary column type number: DB-1701(0.25mm 60M, 0.25 μ M); temperature programming: starting at 50 deg.C, 10 deg.C/min, and heating to 250 deg.C; the injection port temperature is 250 ℃, the interface temperature is 250 ℃, the EI is 230 ℃, the electron bombardment is 70Ev, and the identification of the compound is from a NIST database.
The detection results are shown in fig. 1 and fig. 2, the main chemical components of the burnt clove are Eugenol (Eugenol) of 10.837min and Caryophyllene (caryophylelene) of 11.764min, and after the storax is added, the clove oil phenol and the Caryophyllene are both increased, wherein the Caryophyllene is obviously increased, the Eugenol has the effects of resisting bacteria, reducing blood pressure and anesthetizing, and the Caryophyllene has the effects of local anesthesia and treating colitis.
The flammability of the agastache incense prepared in example 6, example 7 and comparative example 3 was investigated by the following specific method: the same length and diameter of incense were ignited simultaneously, the time was calculated, and the length after burning was measured.
The results show that after 67.27min of burning, the incense stick No. 1 (comparative example 3) of the agastache rugosa with the same diameter (2mm) and the same length (28.4cm) is 5.8cm, the incense stick No. 2 (example 6) of the agastache rugosa with the same length is 6.7cm, and the incense stick No. 3 (example 7) of the agastache rugosa with the same length (example 7), the storax plays a certain flame retardant role for the combustible traditional Chinese medicine incense, thereby increasing the lasting burning time of the incense; and the flame retardant capability is enhanced with the increase of the content, and the combustion time can be increased more obviously.
The content of the main chemical components of the agastache rugosa compound incense prepared by the comparative example 3 and the example 7 is detected, and the specific detection method comprises the following steps:
the fiber end of a Supelco model 57300-U SPME (solid Phase Microextraction) probe was exposed in a 2000mL inverted beaker, the fragrance was ignited and timed for 10min, the probe was removed and manually injected, and the data collected by GC-MS. GC: agilent 7890A; MS: agilent 5975C; the capillary column model: DB-1701(0.25mm 60M, 0.25 μ M); temperature programming: starting at 50 deg.C, 10 deg.C/min, and heating to 280 deg.C; the sample inlet temperature is 250 ℃, the interface temperature is 280 ℃, the EI is 230 ℃, the electron bombardment is 70eV, and the identification of the compound is from a NIST database.
The detection results are shown in fig. 3-4, the content of some components in the storax is changed by adding storax, and the substance with retention time of 7.04min is identified as 2-Phenol, 2-Methoxy-compound, the substance with retention time of 8.59min is identified as 2-Methoxy-5-methylphenol compound, the substance with retention time of 9.90min is identified as 1-Tridecene compound, the substance with retention time of 11.34min is identified as tetradecanoe compound, the substance with retention time of 14.82min is identified as Patchouli alcohol, the substance with retention time of 21.00min is identified as 3-phenylpropyl cinnamate, and the substance with retention time of 21.84min is identified as cinnamyl cinnamate; after the storax is added, the relative content of Tetracan compounds and Patchouli alcohol is obviously reduced, the content of 3-phenylpropyl cinnamate and cinnamyl cinnamate is greatly increased, the two are famous perfume components and are commonly used for preparing perfume and raising fragrance, and the two substances can be metabolized into cinnamic acid with the effects of resisting bacteria, resisting inflammation, promoting blood circulation and removing blood stasis in a human body after entering the human body through breathing. Therefore, the storax and/or grafted storax has the effects of condensing fragrance, releasing components for resuscitation, removing dirt, promoting circulation of qi and relieving pain, and has the effects of joyful and health preservation.
The flammability of the rose bengal prepared in example 8, example 9 and comparative example 4 was investigated by the following specific method: the same length and diameter of incense were ignited simultaneously, the time was calculated, and the length after burning was measured.
The results show that after 54.77min of burning, the incense of the agastache 1 (comparative example 4) and the incense of the rose 2 (example 8) are 4.8cm, the incense of the rose 3 (example 9) are 6.0cm and the grafted storax also has a certain flame retardant effect on the combustible traditional Chinese medicine incense, so that the incense can continuously burn for a long time.
The flammability of the lavender fragrances prepared in example 10, example 11 and comparative example 5 was investigated, specifically by: the same length and diameter of incense were ignited simultaneously, the time was calculated, and the length after combustion was measured.
The results showed that after burning for 48.46min, the lavender fragrance No. 1 (comparative example 5) remained 4.5cm, the lavender fragrance No. 2 (example 10) remained 5.5cm, and the lavender fragrance No. 3 (example 11) remained 6.5cm, all of the same diameter and same length (26.5 cm); the grafted storax has certain flame retardant effect on the combustible traditional Chinese medicine incense, and the flame retardant capability is enhanced along with the increase of the content of the incense, so that the combustion time of the incense can be prolonged.
According to the embodiments, the storax and/or the grafted storax have a combustion-supporting effect on noncombustible medicinal materials, and have a certain flame-retardant effect on combustible medicinal materials. Moreover, the storax and/or the grafted storax have the effects of condensing the fragrance in the process of burning the fragrance, can also release components for resuscitation, dirt removal, qi circulation promotion and pain relief, has the effects of joyful and health preservation, and cannot cause environmental pollution.
Although the present invention has been described with reference to the preferred embodiments, it should be understood that various changes and modifications can be made therein by those skilled in the art without departing from the spirit and scope of the invention as defined in the appended claims.
Claims (10)
1. Use of storax and/or grafted storax for improving the flammability of the incense.
2. Use according to claim 1, wherein the grafted storax comprises grafted storax resin and/or grafted storax oil; the incense comprises a mixed incense.
3. Use according to claim 1, wherein the flammability comprises combustion or flame retardancy.
4. A modifier for improving the flammability of a fragrance, wherein said modifier comprises a storax and/or a grafted storax.
5. The modulator of claim 4, wherein said grafted storax comprises grafted storax resin and/or grafted storax oil.
6. The incense is characterized in that the preparation raw materials of the incense comprise the following components in parts by mass: 3 to 10 parts of a perfume plant, 0.2 to 5 parts of the conditioner according to claim 4 or 5, and 2 to 5 parts of a binder.
7. Incense as claimed in claim 6, wherein the adhesive comprises one or more of elm bark powder, kenaf bark powder, nanmu powder, red bark powder, indonesia powder and white bark powder.
8. A process for the preparation of a fragrance as claimed in claim 6 or 7, characterized in that it comprises the following steps: mixing the perfume plant, the regulator and the binder with water to obtain the incense.
9. The method of claim 8, wherein the flavor plant, conditioning agent, and binder are all sieved through a 100 mesh sieve.
10. Use of a fragrance according to any one of claims 6 to 9 for improving human health.
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