CN108669103A - A kind of galangal fumigation preparation and preparation method thereof - Google Patents
A kind of galangal fumigation preparation and preparation method thereof Download PDFInfo
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- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/20—Combustible or heat-generating compositions
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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- A61K36/88—Liliopsida (monocotyledons)
- A61K36/906—Zingiberaceae (Ginger family)
- A61K36/9062—Alpinia, e.g. red ginger or galangal
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- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0002—Galenical forms characterised by the drug release technique; Application systems commanded by energy
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Abstract
The invention discloses a kind of galangal fumigation preparations and preparation method thereof, are related to essence and flavoring agent field.A kind of galangal fumigation preparation is mainly prepared by the following method to obtain：The first mixture will be obtained after mixing according to 1.5~3.5% adhesive, 1~4% jelly and 0.5~2 combustion adjuvant of mass percent meter；By according to the 90~95% of mass percent meter galangal leaf and the mixture of galangal fibrous root and the first mixture and surplus to obtain the second mixture after each material mixing of distilled water.This product has apparent galangal ginger taste and green grass perfume.It is safe and non-toxic its advantage is that simple for process, it is easy to use, there is expelling mosquito, air sterillization, moxibustion treatment to unsting, preservation and freshness and other effects after burning, can not only efficiently use accessory substance after galangal harvesting, improve its added value, reach environment amenable purpose；The application range of galangal product and abundant fumigant formulation products have also been enlarged simultaneously.
Description
Technical field
The present invention relates to a kind of essence and flavoring agent fields, and more particularly to a kind of galangal fumigation preparation and preparation method thereof.
Background technology
Galangal (Rhizoma Alpiniae Officinarum), the high cool ginger of alias, galingal, rough ginger and fingered citron root etc.,
For the rhizome of Zingiber Alpinia herbaceos perennial galangal (Alpinia officinarum Hance).Main product is in Guangdong
The counties and cities such as the Xuwen in Zhanjiang.Galangal medicinal history is long, and history tree is on the books, first recorded in《Mingyi Bielu》, in being classified as
Product；Go through version《Chinese Pharmacopoeia》Record.It is with special ginger fragrance, the fragrant restoring consciouness of energy, deodorization preventing or arresting vomiting.For treating gastral cavity abdomen
Crymodynia, gastrofrigid vomiting, belch acid regurgitation.Away from the unearthed galangal in modern 2,000 Mawangduis Duo Nianqian Western Han Dynastry ancient tombs confirm early in during the early years of Han Dynasty its
Be used as fragrance to use, by perfume with wear incense drug realization keep away it is dirty, get rid of evils, get rid of illness, mental-tranquilization the effects that.Modern galangal
Or Chinese patent drug processed is extracted after drying and crushing, or flavouring is done, or extraction essential oil and active material do daily necessities and cosmetics.
Invention content
The purpose of the present invention is to provide a kind of galangal fumigation preparation, this galangal fumigation preparation, which can be used for burning, to be driven
Mosquito, air sterillization, moxibustion treatment unsting, preservation and freshness, its is safe and non-toxic while easy to use, and preparation process is simple.
Another object of the present invention is to provide a kind of preparation method of galangal fumigation preparation, this preparation method simply may be used
Row, it is at low cost, high income is prepared, the galangal fumigation preparation being prepared can be used for burn expelling mosquito, air sterillization, moxibustion treatment
It unstings, preservation and freshness, its is safe and non-toxic.
The present invention solves its technical problem using following technical scheme to realize.
The present invention proposes a kind of galangal fumigation preparation, and galangal fumigation preparation is mainly by the original of following mass percent meter
Material is made：
The mixture of 90~95% galangal leaf and galangal fibrous root；
1.5~3.5% adhesive；
1~4% jelly；
0.5~2% combustion adjuvant；And
Surplus is distilled water.
The present invention proposes a kind of preparation method of galangal fumigation preparation, including：
It will be helped according to 1.5~3.5% adhesive of mass percent meter, 1~4% jelly and 0.5~2%
Combustion agent obtains the first mixture after mixing；
It will be mixed with the mixture of galangal fibrous root with first according to the 90~95% of mass percent meter galangal leaf
The second mixture is obtained after object and each material mixing that surplus is distilled water.
The advantageous effect of the galangal fumigation preparation of the embodiment of the present invention and preparation method thereof is：
The galangal fumigation preparation that the embodiment of the present invention provides includes 90~95% height according to mass percent meter
The mixture of galingal leaf and galangal fibrous root, 1.5~3.5% adhesive, 1~4% jelly, 0.5~2% combustion adjuvant with
And surplus is distilled water.Galangal leaf and fibrous root are derived from the accessory substance of Alpinia Officinarum harvesting.These accessory substances be not subject to profit
With preceding frequently as waste ashing loam, there is only a large amount of waste inefficiencies, while causing centainly to pollute to atmospheric environment.
Therefore, galangal leaf and galangal fibrous root are rationally utilized by way of processing and recycling, can not only improve its added value,
Promote the industry development, and reaches environment amenable purpose.Meanwhile by galangal leaf and fibrous root volatile oil component and combustion
Composition analysis is burnt, it is similar to folium artemisiae argyi main pharmacodynamics substance containing ingredients such as 1, 8-Cineole, borneol, carypohyllenes, therefore carry
Show that it can similar folium artemisiae argyi be applied to burning expelling mosquito, air sterillization, moxibustion treatment are unsting, preservation and freshness etc..
In conclusion this galangal fumigation preparation be only environmentally friendly product, and burn after have expelling mosquito,
The effects that air sterillization, moxibustion treatment are unsting.Also, the agent is safe and non-toxic, easy to use, simple for process, is suitble to large-scale promotion.
A kind of preparation method of galangal fumigation preparation is provided, by will be according to 90~95% height of mass percent meter
The mixture of galingal leaf and galangal fibrous root, 1.5~3.5% adhesive, 1~4% jelly, 0.5~2% combustion adjuvant,
And surplus be distilled water each substance be simply mixed after can be prepared by galangal fumigation preparation.Therefore, this preparation method is simple
It is feasible, it is at low cost, high income is prepared, the galangal fumigation preparation being prepared can be used for burn expelling mosquito, air sterillization, moxibustion
Control unsting, preservation and freshness, its is safe and non-toxic.
Description of the drawings
In order to illustrate the technical solution of the embodiments of the present invention more clearly, below will be to needed in the embodiment attached
Figure is briefly described, it should be understood that the following drawings illustrates only certain embodiments of the present invention, therefore is not construed as pair
The restriction of range for those of ordinary skill in the art without creative efforts, can also be according to this
A little attached drawings obtain other relevant attached drawings.
Fig. 1 is that the PY-GC-MS (pyro-GC-MS) for the galangal sootiness product that the embodiment of the present invention provides is total
Ion flow graph；
Fig. 2 is the galangal leaf essential oil GC-MS total ion current figures that the embodiment of the present invention provides；
Fig. 3 is the galangal fibrous root essential oil GC-MS total ion current figures that the embodiment of the present invention provides.
Specific implementation mode
It in order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below will be in the embodiment of the present invention
Technical solution be clearly and completely described.The person that is not specified actual conditions in embodiment, builds according to normal condition or manufacturer
The condition of view carries out.Reagents or instruments used without specified manufacturer is the conventional production that can be obtained by commercially available purchase
Product.
Galangal fumigation preparation of the embodiment of the present invention and preparation method thereof is specifically described below.
The embodiment provides a kind of galangal fumigation preparations, and galangal fumigation preparation is mainly by following quality hundred
The raw material than meter is divided to be made：
The mixture of 90~95% galangal leaf and galangal fibrous root；
1.5~3.5% adhesive；
1~4% jelly；
0.5~2% combustion adjuvant；And
Surplus is distilled water.
Wherein, in an embodiment of the present invention, it is 1 that the mixture of galangal leaf and galangal fibrous root, which specifically includes weight ratio,
~3：1 galangal leaf and galangal fibrous root.The water content of galangal leaf is 25~35%, and the water content of galangal fibrous root is 40
~50%.Galangal leaf and fibrous root are derived from the accessory substance of Alpinia Officinarum harvesting.These accessory substances are often made before not being used
For waste ashing loam, there is only a large amount of waste inefficiencies, while causing centainly to pollute to environment.Therefore, by adding
The mode that work recycles rationally utilizes galangal leaf and galangal fibrous root, can not only improve its added value, promote the industry
Development, and reach environment amenable purpose.Meanwhile by galangal leaf and fibrous root volatile oil component and composition of combustion Product
Analysis, it is similar to folium artemisiae argyi main pharmacodynamics substance containing ingredients such as 1, 8-Cineole, borneol, carypohyllenes, therefore prompt it similar
Folium artemisiae argyi is applied to burning expelling mosquito, air sterillization, moxibustion treatment are unsting, preservation and freshness etc..
In detail, galangal fumigation preparation is subjected to thermal cracking-gas chromatograph tandem mass spectrum detection.Instrument is Agilent
7890A-5975C gas chromatography-mass spectrometries (Agilent company of the U.S.) FRONTIER LAB PY-2020ID thermal crackers
(Japanese Frontier companies).PY-GC-MS analysis conditions be chromatographic column be UA+-5 superalloy petrochemical industry column (30m × 0.25mm ×
0.25 μm, Japanese Frontier companies)；Thermal cracking temperature：300 DEG C, 5s；Temperature programming：60 DEG C of initial temperature keeps 6min,
160 DEG C are risen to the speed of 10 DEG C/min, keeps 5min, 240 DEG C is risen to the speed of 20 DEG C/min, keeps 5min；It does not shunt
Sample introduction, 250 DEG C of injector temperature；Mass spectrum uses electron bombardment (EI) ion source, 250 DEG C of interface temperature, ion source temperature 230
DEG C, scan mode：Full scan, mass scan range 40-450m/z.Meanwhile it is legal using mass spectrum, gas-chromatography carries out opposite
Quantitative (area normalization method).Mass spectrum retrieval using NIST Chemical Structures (American National Standards Institute, 14
Year version) library and Wiley Library (William's spectrum library, the 9th edition), it is qualitative to carry out component in conjunction with related data.The result is shown in Figure 1,
Substance such as table 1 in figure representated by peak number.
The title of main volatile compounds and effect in 1 Fig. 1 of table
It can obviously be learnt from Fig. 1 and data recorded in table 1, galangal of the present invention can be applied to burning and drive
The fields such as mosquito, air sterillization, moxibustion treatment unsting, preservation and freshness, and effect is preferable.
Meanwhile point of its essential oil is carried out extracting respectively with galangal fibrous root to the galangal leaf in the embodiment of the present invention
Analysis.Analysis result is shown in Fig. 2 and Fig. 3, wherein Fig. 2 is the galangal leaf essential oil GC-MS total ion currents that the embodiment of the present invention provides
Figure, Fig. 3 are the galangal fibrous root essential oil GC-MS total ion current figures that the embodiment of the present invention provides.Also, to galangal leaf and height
The title of the main volatile compounds of galingal fibrous root essential oil is recorded with effect, such as table 2.
The title of main volatile compounds and effect in 2 Fig. 2 of table, 3
From the data of table 2, Fig. 2 and Fig. 3 as it can be seen that remaining a certain amount of volatile oil in combustion product, they can adhere to
On skin, or through respiration, is permeated from skin, nasal cavity, play the therapeutic effects such as sterilizing, disinfection, also can adhere to fruit
Play sterilization, preservation in surface.
As a preferred option, in an embodiment of the present invention, adhesive is in honey, rosin, the bletilla striata and nanmu tree powder
One kind, two or more.Adhesive can provide enough bond properties.Certainly, in other embodiments of the invention, bond
The type of agent can also be selected according to demand, and the embodiment of the present invention does not limit.
As a preferred option, in an embodiment of the present invention, jelly is galactomannans powder.Certainly, in the present invention
Other embodiment in, the type of jelly can also be selected according to demand, and the embodiment of the present invention does not limit.
As a preferred option, in an embodiment of the present invention, combustion adjuvant garden burnet powdered carbon or rheum officinale powdered carbon.Combustion adjuvant can carry
For combustion-supporting performance.Certainly, in other embodiments of the invention, the type of combustion adjuvant can also be selected according to demand, this
The embodiment of invention does not limit.
The embodiments of the present invention also provide a kind of preparation methods of galangal fumigation preparation, including：
It will be helped according to 1.5~3.5% adhesive of mass percent meter, 1~4% jelly and 0.5~2%
Combustion agent obtains the first mixture after mixing；
It will be mixed with the mixture of galangal fibrous root with first according to the 90~95% of mass percent meter galangal leaf
The second mixture is obtained after object and each material mixing that surplus is distilled water.
Specifically, galangal leaf and the mixture of galangal fibrous root are prepared especially by following steps：
By weight ratio 1~3：1 galangal leaf crushes processing with galangal fibrous root and obtains galangal leaf powder respectively
With galangal fibrous root powder, and sieving for standby；
The mixture of galangal leaf and galangal fibrous root is obtained after galangal leaf powder is mixed with galangal fibrous root powder.
Also, as a preferred option, the preparation method of galangal fumigation preparation further includes：
It will be mixed with the mixture of galangal fibrous root with first according to the 90~95% of mass percent meter galangal leaf
The second mixture obtained after object and each material mixing that surplus is distilled water is squeezed.
To sum up, this preparation method simple possible, it is at low cost, high income is prepared, the galangal fumigation preparation being prepared can
It unstings for the expelling mosquito that burns, air sterillization, moxibustion treatment, preservation and freshness, its is safe and non-toxic.
The feature and performance of the present invention are described in further detail with reference to embodiments.
Embodiment 1
A kind of galangal fumigation preparation is present embodiments provided, is prepared by the following method to obtain：
By weight ratio 1:1 galangal leaf (moisture 35%) carries out respectively with galangal fibrous root (moisture 50%)
Pulverization process obtains galangal leaf powder and galangal fibrous root powder, and sieving for standby；
The mixture of galangal leaf and galangal fibrous root is obtained after galangal leaf powder is mixed with galangal fibrous root powder；
It will be uniformly mixed according to 1.5% nanmu tree powder, 1% galactomannans powder, the 2% garden burnet powdered carbon of mass percent meter
After obtain the first mixture；
By according to the 95% of mass percent meter galangal leaf and the mixture of galangal fibrous root and the first mixture with
And obtain the second mixture after each material mixing that surplus is distilled water；
Sootiness product is obtained after second mixture is squeezed.
Embodiment 2
A kind of galangal fumigation preparation is present embodiments provided, is prepared by the following method to obtain：
By weight ratio 2：1 galangal leaf (moisture 25%) and galangal fibrous root (moisture 40%) difference
It crushes processing and obtains galangal leaf powder and galangal fibrous root powder, and sieving for standby；
The mixture of galangal leaf and galangal fibrous root is obtained after galangal leaf powder is mixed with galangal fibrous root powder；
It will be according to 2% rosin of mass percent meter and the bletilla striata (1:1) mixture, 1.5% galactomannans powder, 1%
Garden burnet powdered carbon obtains the first mixture after mixing；
By according to the 95% of mass percent meter galangal leaf and the mixture of galangal fibrous root and the first mixture with
And obtain the second mixture after each material mixing that surplus is distilled water；
Sootiness product is obtained after second mixture is squeezed.
Embodiment 3
A kind of galangal fumigation preparation is present embodiments provided, is prepared by the following method to obtain：
By weight ratio 2：1 galangal leaf crushes processing with galangal fibrous root and obtains galangal leaf powder and height respectively
Galingal fibrous root powder, and sieving for standby；
The mixture of galangal leaf and galangal fibrous root is obtained after galangal leaf powder is mixed with galangal fibrous root powder；
It will be according to 3.5% honey and rosin (1 of mass percent meter:2) mixture, 4% galactomannans powder,
0.5% rheum officinale powdered carbon obtains the first mixture after mixing；
By according to the 90% of mass percent meter galangal leaf and the mixture of galangal fibrous root and the first mixture with
And obtain the second mixture after each material mixing that surplus is distilled water；
Sootiness product is obtained after second mixture is squeezed.
Simultaneously, it should be noted that the made galangal fumigation preparation of above three embodiments, color and luster is uniform, Wen Zhiyou
Refrigerant sense, special ginger fragrance and herbaceous taste.It is seted off using time point and sets required space, child is accompanied using Ying You adult and superintended and directed
It leads, please don't eat.
Experimental example 1
By the embodiment of the present invention 1 to embodiment 3, carried out production practices, using conventional use of mosquito repellent fumigant as
Positive control passes through the repelling effect of the repellent experiment test of the mosquito fumigant.Choose the both hands of at least 3 qualified volunteers
Each exposure of back 4cm × 4cm skin areas therein, tightly cover rest part, are put into the experiment cage after sootiness, are put into attack
The aedes albopictus of power qualification, first mosquito of record come to bite the period and as walk quickly and keep away the term of validity, the results are shown in Table 3.
3 galangal fumigant mosquito of table walks quickly and keeps away experiment effect
Experimental example 2
By the embodiment of the present invention 1 to embodiment 3, production practices have been carried out, fresh-keeping fumigant sec-butylamine is used with conventional
As positive control, using banana as experiment material, after fumigating 2h, the fresh-keeping of the fumigant is tested using mycelial growth rate method
Effect the results are shown in Table 4.
The 4 fresh-keeping experiment effect of galangal fumigant of table
According to table 3 with the data shown by table 4 it is found that the galangal fumigation preparation of the embodiment of the present invention offer is with good
Good fresh-keeping and sootiness anthelminthic effect.
In conclusion galangal fumigation preparation that the embodiment of the present invention provides and preparation method thereof has the beneficial effect that：
This product has apparent galangal ginger taste and green grass perfume.Its advantage is that simple for process, safe and non-toxic, easy to use, burning
It unstings afterwards with expelling mosquito, air sterillization, moxibustion treatment, preservation and freshness, can not only efficiently use accessory substance after galangal harvesting,
Its added value is improved, environment amenable purpose is reached；The application range of galangal product and abundant sootiness has also been enlarged simultaneously
Agent formulation product.
Embodiments described above is a part of the embodiment of the present invention, instead of all the embodiments.The reality of the present invention
The detailed description for applying example is not intended to limit the range of claimed invention, but is merely representative of the selected implementation of the present invention
Example.Based on the embodiments of the present invention, those of ordinary skill in the art are obtained without creative efforts
Every other embodiment, shall fall within the protection scope of the present invention.
Claims (10)
1. a kind of galangal fumigation preparation, which is characterized in that the galangal fumigation preparation is mainly by following mass percent meter
Raw material be made：
The mixture of 90~95% galangal leaf and galangal fibrous root；
1.5~3.5% adhesive；
1~4% jelly；
0.5~2% combustion adjuvant；And
Surplus is distilled water.
2. galangal fumigation preparation according to claim 1, it is characterised in that：
It is 1~3 that the mixture of the galangal leaf and galangal fibrous root, which specifically includes weight ratio,：1 galangal leaf and galangal
Fibrous root.
3. galangal fumigation preparation according to claim 2, it is characterised in that：
The water content of the galangal leaf is 25~35%.
4. galangal fumigation preparation according to claim 3, it is characterised in that：
The water content of the galangal fibrous root is 40~50%.
5. galangal fumigation preparation according to claim 1, it is characterised in that：
Described adhesive be honey, rosin, the bletilla striata and one kind in nanmu tree powder, two or more.
6. galangal fumigation preparation according to claim 1, it is characterised in that：
The jelly is galactomannans powder.
7. galangal fumigation preparation according to claim 1, it is characterised in that：
The combustion adjuvant garden burnet powdered carbon or rheum officinale powdered carbon.
8. a kind of preparation method of galangal fumigation preparation, which is characterized in that including：
It will be mixed according to 1.5~3.5% adhesive, 1~4% jelly and 0.5~2% combustion adjuvant of mass percent meter
The first mixture is obtained after closing uniformly；
It will be mixed with the mixture of galangal fibrous root with described first according to the 90~95% of mass percent meter galangal leaf
The second mixture is obtained after object and each material mixing that surplus is distilled water.
9. the preparation method of galangal fumigation preparation according to claim 8, which is characterized in that galangal leaf and galangal
The mixture of fibrous root is prepared especially by following steps：
By weight ratio 1~3：1 galangal leaf crushes processing with galangal fibrous root and obtains galangal leaf powder and height respectively
Galingal fibrous root powder, and sieving for standby；
The galangal leaf and galangal fibrous root are obtained after the galangal leaf powder is mixed with the galangal fibrous root powder
Mixture.
10. the preparation method of galangal fumigation preparation according to claim 8, which is characterized in that further include：
It will be mixed with the mixture of galangal fibrous root with described first according to the 90~95% of mass percent meter galangal leaf
Second mixture obtained after object and each material mixing that surplus is distilled water is squeezed.
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| CN201810426593.6A CN108669103A (en) | 2018-05-07 | 2018-05-07 | A kind of galangal fumigation preparation and preparation method thereof |
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| CN112868681A (en) * | 2021-01-12 | 2021-06-01 | 中国农业大学 | Application of tupelo pterodonis in aspects of mite killing and insect killing, biological control medicament and preparation method thereof |
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