CN113925951B - 崖柏中药提取物及其提取方法和在洗护发产品中的应用 - Google Patents
崖柏中药提取物及其提取方法和在洗护发产品中的应用 Download PDFInfo
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Abstract
本发明公开了一种崖柏中药提取物及其提取方法和在洗护发产品中的应用。该提取物的原料为崖柏、姜、皂角、茶枯、何首乌、无患子、黄芪、侧柏叶、地肤子、白鲜皮、苦参和丹参。该提取方法的步骤为:1)将崖柏置于蒸馏锅中加水浸泡,煮沸后蒸馏,蒸馏产物油水分离后,获得崖柏精油和纯露,所得精油为组分A;2)将蒸馏锅中的料液过滤,滤液通入提取罐,提取罐内加其它原料组分,煎煮,过滤,将滤液和纯露混合浓缩成清膏,所得清膏为组分B。该崖柏中药提取物及含该提取物的洗护发产品香气怡人,控油祛屑,生发固发,能够有效抑制脱发,尤其是脂溢性脱发。
Description
技术领域
本发明属于天然植物提取物技术领域,具体涉及一种崖柏中药提取物及其提取方法和在洗护发产品中的应用。
背景技术
崖柏(Thuja Sutchuenensis)为柏科(Cupressaceae)崖柏属(Thuja)常绿乔木,是一类起源于恐龙时代的“活化石”。经研究发现,崖柏的根、茎、叶中含有罗汉柏烯、a-蒎烯、柠檬烯等萜类化合物,这些萜类化合物脂溶性佳,分子小,具有抗菌、抗氧化、抗肿瘤、降血压、驱虫、抗炎、利尿、祛痰和健身强体的功效。近年来,已进行了崖柏的人工种植试验,并获得成功,为对崖柏的研究开发提供了条件。
病理性脱发是指头发异常或过度的脱落,其原因很多。目前最常见的病理性脱发为脂溢性脱发。脂溢性脱发又称雄性激素性脱发,一般在20岁左右开始出现额、颞、顶部的进行性缓慢脱发。男女均可发生,但以男性患者更为常见。脂溢性脱发的临床表现为:初期常有头痒,搔抓或梳头时头发大量脱落,脱落之毛发毛根短小,毛球消失;脱发症状经过缓慢,可呈阶段性,时轻时重,数年后可致头顶或两鬓毛发稀疏,头皮光亮;头部油腻多脂或脱碎屑,毛发细软发黄。目前,还未发现将含有崖柏的中药提取物及其洗护发产品,用于防治脱发尤其是脂溢性脱发的报道。
发明内容
本发明的第一个目的为提供一种崖柏中药提取物。
该崖柏中药提取物的原料,包括如下重量份的组分:崖柏10~100份,姜0.1~30份,皂角0.1~30份,茶枯0.1~30份,何首乌0.1~30份,无患子10~40份,黄芪0.1~30份,侧柏叶0.1~30份,地肤子0.1~30份,白鲜皮0.1~30份,苦参0.1~30份,丹参0.1~30份。
优选地,所述组分的重量份为:崖柏30~100份,姜1~5份,皂角5~10份,茶枯10~20份,何首乌8~12份,无患子25~35份,黄芪5~10份,侧柏叶13~20份,地肤子8~12份,白鲜皮1~5份,苦参8~12份,丹参8~12份。
更优地,所述组分的重量份为:崖柏80份,姜3份,皂角8份,茶枯15份,何首乌8份,无患子30份,黄芪8,侧柏叶15份,地肤子10份,白鲜皮2份,苦参10份,丹参10份。
上述原料组分中,所述崖柏选自崖柏的根和\或茎和\或叶。其余原料则为中药材,具体的:姜,为姜科植物姜的根茎,可选用生姜或干姜;皂角,为豆科植物皂荚的果实;茶枯,又称枯饼、茶油粑、茶麸、茶子饼、茶子麸或茶油麸,为山茶科植物油茶种子榨去脂肪油后的渣滓;何首乌,为蓼科植物何首乌的块根;无患子,为无患子科植物无患树的种子;黄芪,为豆科植物蒙古黄芪或膜荚黄芪的根;侧柏叶,为柏科植物侧柏的枝与叶;地肤子,为藜科植物地肤子的干燥成熟果实;白鲜皮,为芸香科多年生草本植物白鲜或狭叶白鲜的根皮;苦参,为豆科植物苦参的干燥根;丹参,为唇形科植物丹参的根。
上述中药材科学配伍,构成了用于养发护发、抑制脂溢性皮炎和脱发、减轻头屑和瘙痒的中药方。其中,无患子清热祛湿、消积杀虫,既能抑制头部皮脂分泌,又能抗菌消炎、祛屑止痒,其用量最大、功效全面,为君药;茶枯燥湿解毒,侧柏叶凉血祛湿,地肤子清热利湿、祛风止痒,白鲜皮清热燥湿、祛风解毒,苦参清热燥湿,姜散寒燥湿,主要为燥湿、止痒的组分,用于加强无患子之功效,为臣药;何首乌补益精血,黄芪补气生血、生发固发,丹参活血祛瘀、养血安神,除了能够用于滋养头皮、生发固发,还用于减轻无患子的溶血作用,以及避免使用较多抗菌消炎组分对头皮的刺激作用,为佐药;诸药合用,清热燥湿,止痒杀菌,养血祛风,具有显著的生发固发、控油祛屑功效。此外,本发明的原料还加有崖柏,崖柏主要用于提炼精油,崖柏精油含有罗汉柏烯、柏木烯、蒎烯等萜类化合物,芳香宜人、沁人心脾,崖柏中的萜类化合物被人体吸收后,调节呼吸和中枢神经系统,具有松弛精神、稳定情绪、改善失眠多梦的作用,其香味可提高血液含氧量使人精神愉悦,能够调和其余中药组分提取后的浓烈中药味,提高产品外用后的感观效果,而且崖柏精油具有抗菌、抗氧化、驱虫和抗炎的功效,能够增强提取物生发固发、控油祛屑的效果。
本发明的第二个目的为提供一种前述崖柏中药提取物的提取方法。
该提取方法包括以下步骤:
1)将崖柏置于蒸馏锅中加水浸泡0.1~5h,煮沸后蒸馏2~8h,蒸馏锅内保持崖柏和水的重量比为1:6~20,蒸馏产物经油水分离器处理后,获得崖柏精油和纯露,所得崖柏精油为崖柏中药提取物的组分A;
2)将蒸馏锅中的料液过滤,滤液通入提取罐,提取罐内加有崖柏之外的原料组分,煮沸后煎煮0.5~3h,过滤,将滤液通入浓缩器浓缩至原体积的30%~40%,然后通入步骤1)制得的纯露并一起浓缩成清膏,所得清膏为崖柏中药提取物的组分B。
进一步地,在步骤1)中,所述浸泡的时间为2h,所述蒸馏的时间为4h,所述崖柏和水的重量比为1:8;
进一步地,在步骤2)中,所述煎煮的时间为2h,所述清膏的含水量为15%~25%。
进一步地,为了收集更多的提取物,节省原料成本,步骤1)和步骤2)均重复两次用于处理同一份原料。
上述提取方法根据不同原料设置了不同的对应性的提取方法,其中,崖柏采用先水中蒸馏、后油水分离的方式提取精油,其余中药原料则用传统的水提和浓缩方式进行提取,水提时通入崖柏蒸馏后获得的滤液,浓缩时通入油水分离获得的纯露,既节约了水资源,而且利用余热降低了能耗,而且能够回收利用崖柏在蒸馏过程中的水溶物成分,获取更多的植物提取成分,提高整个提取物的保健价值。
本发明的第三个目的为提供前述崖柏中药提取物的应用。
具体为,该应用为所述崖柏中药提取物在洗护发产品中的应用。
更具体地,所述洗护发产品为洗发水或护发素;优选地,所述组分A在洗护发产品中添加量为0.1wt%~3wt%;所述组分B在洗护发产品中的添加量为1wt%~10wt%。
将上述崖柏中药提取物作为洗护发产品的组分后,所得的洗发水或护发素香气怡人,无强烈的中药味,而且控油祛屑、生发固发,有效抑制脱发,尤其是脂溢性皮炎引发的脱发。
附图说明
图1为本发明实施例的提取方法的流程图。
具体实施方式
下面结合附图对本发明进行说明,此处所描述的具体实施方式仅用于说明和解释本发明,并不用于限定本发明。
实施例1:崖柏中药提取物的制备
崖柏中药提取物的原料重量份为:崖柏(取枝叶)80份、生姜3份、皂角8份、茶枯15份、何首乌8份、无患子30份、黄芪8、侧柏叶15份、地肤子10份、白鲜皮2份、苦参10份、丹参10份。
参考图1,崖柏中药提取物的制备方法的步骤为:1)将崖柏置于蒸馏锅中加水浸泡2h,煮沸后蒸馏4h,蒸馏锅内保持崖柏和水的重量比为1:8,蒸馏产物经油水分离器处理后,获得崖柏精油和纯露,所得崖柏精油为崖柏中药提取物的组分A;2)将蒸馏锅中的料液过滤,滤液(煎煮液)通入提取罐,提取罐内加有崖柏之外的原料组分,煮沸后煎煮2h,过滤,将滤液(提取液)通入浓缩器浓缩至原体积的30%,然后通入步骤1)制得的纯露并一起浓缩成清膏(重量含水量20%),所得清膏为崖柏中药提取物的组分B;其中,步骤1)和步骤2)均重复两次用于处理同一份原料。
实施例2:崖柏中药提取物的制备
崖柏中药提取物的原料重量份为:崖柏(取枝叶)30份、生姜5份、皂角5份、茶枯20份、何首乌8份、无患子35份、黄芪5份、侧柏叶20份、地肤子8份、白鲜皮5份、苦参8份、丹参12份。
参考图1,崖柏中药提取物的制备方法的步骤为:1)将崖柏置于蒸馏锅中加水浸泡0.1h,煮沸后蒸馏8h,蒸馏锅内保持崖柏和水的重量比为1:6,蒸馏产物经油水分离器处理后,获得崖柏精油和纯露,所得崖柏精油为崖柏中药提取物的组分A;2)将蒸馏锅中的料液过滤,滤液(煎煮液)通入提取罐,提取罐内加有崖柏之外的原料组分,煮沸后煎煮3h,过滤,将滤液(提取液)通入浓缩器浓缩至原体积的40%,然后通入步骤1)制得的纯露并一起浓缩成清膏(重量含水量15%),所得清膏为崖柏中药提取物的组分B;其中,步骤1)和步骤2)均重复两次用于处理同一份原料。
实施例3:崖柏中药提取物的制备
崖柏中药提取物的原料重量份为:崖柏(取根部)100份、干姜1份、皂角10份、茶枯10份、何首乌12份、无患子25份、黄芪10份、侧柏叶13份、地肤子12份、白鲜皮1份、苦参12份、丹参8份。
参考图1,崖柏中药提取物的制备方法的步骤为:1)将崖柏置于蒸馏锅中加水浸泡5h,煮沸后蒸馏2h,蒸馏锅内保持崖柏和水的重量比为1:20,蒸馏产物经油水分离器处理后,获得崖柏精油和纯露,所得崖柏精油为崖柏中药提取物的组分A;2)将蒸馏锅中的料液过滤,滤液(煎煮液)通入提取罐,提取罐内加有崖柏之外的原料组分,煮沸后煎煮0.5h,过滤,将滤液(提取液)通入浓缩器浓缩至原体积的30%,然后通入步骤1)制得的纯露并一起浓缩成清膏(重量含水量25%),所得清膏为崖柏中药提取物的组分B。
实施例4:含有崖柏中药提取物的洗发水
将如下重量份的组分按照常规的制备工艺复配制成洗发水:
表面活性剂30份,其成分配比:月桂醇聚醚硫酸酯钠、椰油酰胺丙基甜菜碱、椰油酰两性基二乙酸二钠、椰油酰胺DEA、椰油酰甘氨酸钾的重量比为13:5:1.5:1:1;
调理剂1份,其成分配比:聚季铵盐-52、PPG-3辛基醚、瓜儿胶羟丙基三甲基氯化铵、聚季铵盐-10的重量比为0.3:2:1:1;
保湿剂(透明质酸)2.5份;
乳化剂(月桂醇聚醚-16)0.07份;
增稠剂(氯化钠)0.05份;
防腐剂(羟苯甲酯)0.05份;
pH调节剂(柠檬酸)0.5份;
去离子水45份;
组分A(实施例1)0.5份;
组分B(实施例1)3份。
实施例5:含有崖柏中药提取物的洗发水
将如下重量份的组分按照常规的制备工艺复配制成洗发水:
表面活性剂25份,其成分配比:月桂醇聚醚硫酸酯钠、椰油酰胺丙基甜菜碱、椰油酰两性基二乙酸二钠、椰油酰胺DEA、椰油酰甘氨酸钾的重量比为13.5:4:1.2:1:0.8;
调理剂1.1份,其成分配比:聚季铵盐-52、PPG-3辛基醚、瓜儿胶羟丙基三甲基氯化铵、聚季铵盐-10的重量比为0.2:2.5:0.6:1.1;
保湿剂(透明质酸)2份;
乳化剂(月桂醇聚醚-16)0.08份;
增稠剂(氯化钠)0.1份;
防腐剂(卡松防腐剂)0.05份;
pH调节剂(柠檬酸)0.2份;
去离子水40份;
组分A(实施例2)0.1份;
组分B(实施例2)2份。
实施例6:含有崖柏中药提取物的洗发水
将如下重量份的组分按照常规的制备工艺复配制成洗发水:
表面活性剂31份,其成分配比:月桂醇聚醚硫酸酯钠、椰油酰胺丙基甜菜碱、椰油酰两性基二乙酸二钠、椰油酰胺DEA、椰油酰甘氨酸钾的重量比为13:5:1.5:1:1;
调理剂0.9份,其成分配比:聚季铵盐-52、PPG-3辛基醚、瓜儿胶羟丙基三甲基氯化铵、聚季铵盐-10的重量份比为0.38:2.2:1.3:0.9;
保湿剂(PEG-7甘油椰油酸酯)2.5份;
乳化剂(月桂醇聚醚-16)0.07份;
增稠剂(羟乙基纤维素)0.08份;
防腐剂0.04份,其成分配比:羟苯甲酯、DMDM乙内酰脲和卡松防腐剂的重量比为1:0.5:2;
pH调节剂(山梨酸)0.1份;
去离子水30份;
组分A(实施例3)0.1份;
组分B(实施例3)1.5份。
实施例7:含有崖柏中药提取物的护发素
将如下重量份的组分按照常规的制备工艺复配制成护发素:
天然油脂2份,其成分配比为:山茶籽油、马油和蜂蜡的重量比为1:2:0.1;
硬脂酰胺丙基二甲胺3份;
鲸蜡硬脂醇4.3份;
乳酸0.5份;
泛醇3份;
乙二胺四乙酸二钠0.1份;
防腐剂(苯氧乙醇)0.5份;
去离子水60份;
组分A(实施例1)0.1份;
组分B(实施例1)5份。
实施例8:含有崖柏中药提取物的护发素
将如下重量份的组分按照常规的制备工艺复配制成护发素:
天然油脂1份,其成分配比为:山茶籽油、马油和蜂蜡的重量比为1:0.5:0.2;
硬脂酰胺丙基二甲胺1份;
鲸蜡硬脂醇5份;
乳酸0.5份;
泛醇5份;
乙二胺四乙酸二钠0.08份;
防腐剂(苯甲醇)0.3份;
去离子水70份;
组分A(实施例2)0.1份;
组分B(实施例2)4份。
实施例9:含有崖柏中药提取物的护发素
将如下重量份的组分按照常规的制备工艺复配制成护发素:
天然油脂1.5份,其成分配比为:山茶籽油、马油和蜂蜡的重量比为2:1:0.5;
硬脂酰胺丙基二甲胺1份;
鲸蜡硬脂醇4份;
乳酸1份;
泛醇5份;
乙二胺四乙酸二钠0.1份;
防腐剂(苯氧乙醇)0.5份;
去离子水50份;
组分A(实施例3)1份;
组分B(实施例3)3份。
最后,本发明将上述提取物、洗发水和护发素用于试验,以验证其护发效果。
试验例1:感官评价
洗发水分组和使用方法:选取60名志愿者,年龄分布在18~50岁,其中男、女各30名,头发普遍出现脱发、头油多、头屑多和头皮瘙痒的现象;将志愿者分为3组,每组20人,男女各10人;用5~10mL左右的洗发水洗发后,用清水冲洗干净即可。每个样品试用1月,测试者根据自己的感觉进行评分。
护发素分组和使用方法:选取60名志愿者,年龄分布在18~40岁的女性,头发普遍出现脱发、头屑多和头皮瘙痒的现象;将志愿者分为3组,每组20人;采用常规洗发水洗发后,擦干头发,根据发量,将护发素均匀涂抹在头发上,在头发上停留5分钟后,用清水冲洗干净即可。每个样品试用1月,测试者根据自己的感觉进行评分。
评分标准:采取10分制,1分最差,10分最好,分数越高效果越好,试验结果如下表1和表2所示。
表1.含有崖柏中药提取物的洗发水的感官评价效果
实施例 | 清洁效果 | 去屑效果 | 止痒效果 | 控油效果 | 固发效果 |
实施例4 | 9.15 | 8.80 | 9.15 | 7.80 | 7.50 |
实施例5 | 9.00 | 8.65 | 9.20 | 7.50 | 7.45 |
实施例6 | 8.90 | 8.30 | 9.30 | 7.65 | 7.15 |
表2.含有崖柏中药提取物的护发素的感官评价效果
实施例 | 顺滑度 | 去屑效果 | 止痒效果 | 控油效果 | 固发效果 |
实施例7 | 8.65 | 7.25 | 7.20 | 7.95 | 8.65 |
实施例8 | 8.40 | 7.25 | 7.30 | 7.80 | 8.45 |
实施例9 | 8.35 | 7.00 | 6.95 | 7.60 | 8.50 |
由表1和表2可知,本发明含有崖柏中药提取物的洗发水、护发素均有一定的去屑、止痒、控油、固发的效果,而且在试用过程未发现过敏、头皮不适等副作用,说明了上述洗发水和护发素无毒副作用,具备安全性。
试验例2:临床实验
1.临床资料
1.1一般资料
50例患者均为门诊病人,其中男性31例,女性19例;年龄最小20岁,最大55岁;病程最长5年,最短1个月;均为脂溢性脱发患者。
1.2诊断标准
油脂分泌旺,头发油腻,或头皮屑较多,头发干燥,头发弥漫性缓慢脱落,伴有头皮瘙痒、头发稀疏。
2.治疗方法
外用实施实例1制得的提取物,按照组分A:组分B=1:5的重量比使用,先于脱发部位外擦组分B,再外擦组分A,擦至局部皮肤微红即可,2次/d,5~10mL/次,以1个月为1个疗程。治疗期间要保持按时作息,避免用脑过度和精神过度紧张,忌食油腻、辛辣之品。
3.治疗结果
3.1疗效标准
毛发脱落停止,脱发全部长出,皮脂分泌恢复正常,为治愈;毛发脱落停止,脱发再生达70%以上,皮脂分泌明显减少,为显效;毛发脱落停止,脱发再生达30%以上,皮脂分泌减少,为有效;毛发脱落仍有,脱发再生未达30%,为无效。
3.2治疗结果
治愈18例(男14例,女4例);显效9例(男7例,女2例);有效12例(男10例,女2例);无效11例(均为女性)。总有效率78%。疗程最长12个疗程,最短3个疗程。
由以上实验可知,本发明的崖柏中药提取物具有养发护发、控油去油的功效,可用于治疗和改善脂溢性脱发,可将其稀释后加入洗发水和护发素等洗护发产品中,用于增加洗护发产品的功效。
Claims (4)
1.崖柏中药提取物,其特征在于,制备该提取物的原料包括如下重量份的组分:崖柏30~100份,姜1~5份,皂角5~10份,茶枯10~20份,何首乌8~12份,无患子25~35份,黄芪5~10份,侧柏叶13~20份,地肤子8~12份,白鲜皮1~5份,苦参8~12份,丹参8~12份;
所述崖柏中药提取物的提取方法,包括以下步骤:1)将崖柏置于蒸馏锅中加水浸泡0.1~5h,煮沸后蒸馏2~8h,蒸馏锅内保持崖柏和水的重量比为1:6~20,蒸馏产物经油水分离器处理后,获得崖柏精油和纯露,所得崖柏精油为崖柏中药提取物的组分A;2)将蒸馏锅中的料液过滤,滤液通入提取罐,提取罐内加有崖柏之外的原料组分,煮沸后煎煮0.5~3h,过滤,将滤液通入浓缩器浓缩至原体积的30%~40%,然后通入步骤1)制得的纯露并一起浓缩成清膏,所得清膏为崖柏中药提取物的组分B。
2.根据权利要求1所述的崖柏中药提取物,其特征在于:步骤1)中,所述浸泡的时间为2h,所述蒸馏的时间为4h,所述崖柏和水的重量比为1:8;步骤2)中,所述煎煮的时间为2h,所述清膏的含水量为15%~25%。
3.根据权利要求1所述的崖柏中药提取物,其特征在于:步骤1)和步骤2)均重复两次用于处理同一份原料。
4.权利要求1~3中任一项所述崖柏中药提取物在洗护发产品中的应用,其特征在于:所述洗护发产品为洗发水或护发素;所述组分A在洗护发产品中添加量为0.1wt%~3wt%;所述组分B在洗护发产品中的添加量为1wt%~10wt%。
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