CN113914117A - 一种透气荧光腈纶面料的染整工艺 - Google Patents
一种透气荧光腈纶面料的染整工艺 Download PDFInfo
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Abstract
本发明公开了一种透气荧光腈纶面料的染整工艺,属于面料染整技术领域。所述染整工艺包括以下步骤:将腈纶放入水缸中,加入质量分数为6‑10%的处理液,于40‑50℃温度下浸泡1‑1.5h,加入清洗剂搅拌15‑20min,再使用清水充分水洗至pH值为中性,在100℃下烘培25min;将烘干后的腈纶放入处理浴中进行染色和整理,在处理浴中加入荧光剂和含酸性基团组成的染色剂,调节pH为2‑5,将腈纶按浴比1:10‑100投入处理浴中,以0.5‑5℃/min的升温速度升温至80‑100℃,保温10‑60min,以0.5‑3℃/min的降温速度降温至50℃,加入抗黄变剂并浸轧后再进行汽蒸,最后将腈纶水洗、烘干或晾干。本发明工艺能显著提高面料的固色性能,同时也能改善面料的透气性和透湿性,提高面料的穿着舒适度。
Description
技术领域
本发明属于面料染整技术领域,具体为一种透气荧光腈纶面料的染整工艺。
背景技术
目前,我国一些特殊工种制服面料主要以黄色或橘红色的荧光涂料涂层腈纶面料为主,腈纶因手感柔软、蓬松,保暖性好,体积密度比羊毛低,广泛用于替代羊毛或与羊毛混纺,有“合成羊毛”之称,但由于腈纶是合成纤维,属于疏水性纤维,大分子中缺乏亲水性基团,分子链结构紧密,结晶度和取向度均较高,其亲水性差,从而导致透气性差,易产生静电、易沾污等问题。同时,面料中普遍存在基材面料荧光度不足、亮度系数低以及反光装饰材料可视性差等问题。即使新衣服的可视性能达到要求,但由于工作性质关系,工作人员需勤换勤洗,致使荧光的警示效果降低,甚至丧失警示效果,导致交通事故的。因此,需要采取有效的染整方法来提高面料的固色性能,延长面料的使用寿命。
发明内容
本发明的目的在于克服现有技术的缺点,提供一种透气荧光腈纶面料的染整工艺,本发明工艺能显著提高面料的固色性能,同时也能改善面料的透气性和透湿性,提高面料的穿着舒适度。
本发明的目的通过以下技术方案来实现:
一种透气荧光腈纶面料的染整工艺,包括以下步骤:
步骤一、将腈纶放入水缸中,加入质量分数为6-10%的处理液,于40-50℃温度下浸泡1-1.5h,加入清洗剂搅拌15-20min,再使用清水充分水洗至pH值为中性,在100℃下烘培25min;
步骤二、将烘干后的腈纶放入处理浴中进行染色和整理,在处理浴中加入荧光剂和含酸性基团组成的染色剂,调节pH为2-5,将腈纶按浴比1:10-100投入处理浴中,以0.5-5℃/min的升温速度升温至80-100℃,保温10-60min,以0.5-3℃/min的降温速度降温至50℃,加入抗黄变剂并浸轧后再进行汽蒸,最后将腈纶水洗、烘干或晾干。
进一步地,所述步骤一中的处理液为甲基丙烯磺酸钠和甲基乙烯基吡啶的混合溶液。
进一步地,所述步骤一中的清洗剂为烷基酚聚氧乙烯醚。
进一步地,所述步骤二中染色剂中荧光剂和含酸性基团的含量比为5:2。
进一步地,所述荧光剂为分散荧光染料荧光黄10G、荧光艳橙G、荧光红G和荧光红B。
进一步地,所述含酸性基团为磺酸基或磺酸钠盐或羧酸钠盐。
本发明的有益效果为:本发明中的处理成分为甲基丙烯磺酸钠和甲基乙烯基吡啶,甲基丙烯磺酸钠能够很好的改善腈纶面料的染色性和耐热性,同时也能增加腈纶面料的手感,甲基乙烯基吡啶则能与甲基丙烯磺酸钠产生协同作用,显著增强腈纶面料的染色性能;然而提高腈纶面料染色性的同时还需要进一步地提高其固色性,因此,本发明所采用的染色剂为分散荧光染料荧光黄10G、荧光艳橙G、荧光红G和荧光红B,同时对染色温度以及时间进行调整,在低于100℃的染色温度下,分散荧光染料荧光黄10G、荧光艳橙G、荧光红G和荧光红这些染料能够很好的固定于腈纶面料上,除此之外,本发明还在染色后加入抗黄变剂并浸轧后再进行汽蒸,能够有效抑制腈纶面料在使用过程中所产生的黄变,同时也能进一步高染料的固色性能;本发明中采用烷基酚聚氧乙烯醚作为清洗剂,除了其高乳化性能能够很好的清洗面料中常常含有的润滑油以及硅油等,烷基酚聚氧乙烯醚还具有良好的抗静电功能,能够提升面料的抗静电性能。
具体实施方式
下面结合具体实施例进一步详细描述本发明的技术方案,但本发明的保护范围不局限于以下所述。
实施例1
一种透气荧光腈纶面料的染整工艺,包括以下步骤:
首先将腈纶放入水缸中,加入质量分数为6%的甲基丙烯磺酸钠和甲基乙烯基吡啶混合而成的处理液,于40℃温度下浸泡1h,加入烷基酚聚氧乙烯醚搅拌15min,再使用清水充分水洗至pH值为中性,在100℃下烘培25min;其次,将烘干后的腈纶放入处理浴中进行染色和整理,在处理浴中加入荧光剂和磺酸基组成的染色剂,调节pH为2,其中荧光剂和含酸性基团的含量比为5:2,所述荧光剂为分散荧光红G,将腈纶按浴比1:10投入处理浴中,以0.5℃/min的升温速度升温至80℃,保温10min,以0.5℃/min的降温速度降温至50℃,加入抗黄变剂并浸轧后再进行汽蒸,最后将腈纶水洗、烘干或晾干。
实施例2
一种透气荧光腈纶面料的染整工艺,包括以下步骤:
首先将腈纶放入水缸中,加入质量分数为8%的甲基丙烯磺酸钠和甲基乙烯基吡啶混合而成的处理液,于45℃温度下浸泡1.3h,加入烷基酚聚氧乙烯醚搅拌17min,再使用清水充分水洗至pH值为中性,在100℃下烘培25min;其次,将烘干后的腈纶放入处理浴中进行染色和整理,在处理浴中加入荧光剂和磺酸钠盐组成的染色剂,调节pH为3,其中荧光剂和含酸性基团的含量比为5:2,所述荧光剂为分散荧光艳橙G,将腈纶按浴比1:80投入处理浴中,以4.5℃/min的升温速度升温至90℃,保温10-60min,以2.3℃/min的降温速度降温至50℃,加入抗黄变剂并浸轧后再进行汽蒸,最后将腈纶水洗、烘干或晾干。
实施例3
一种透气荧光腈纶面料的染整工艺,包括以下步骤:
首先将腈纶放入水缸中,加入质量分数为10%的甲基丙烯磺酸钠和甲基乙烯基吡啶混合而成的处理液,于50℃温度下浸泡1.5h,加入烷基酚聚氧乙烯醚搅拌15-20min,再使用清水充分水洗至pH值为中性,在100℃下烘培25min;其次,将烘干后的腈纶放入处理浴中进行染色和整理,在处理浴中加入荧光剂和羧酸钠盐组成的染色剂,调节pH为5,其中荧光剂和含酸性基团的含量比为5:2,所述荧光剂为分散荧光染料荧光黄10G,将腈纶按浴比1:100投入处理浴中,以5℃/min的升温速度升温至100℃,保温60min,以3℃/min的降温速度降温至50℃,加入抗黄变剂并浸轧后再进行汽蒸,最后将腈纶水洗、烘干或晾干。
对比例
本对比例与实施例2的工艺以及参数基本一致,不同之处在于本对比例没有加入抗黄变剂并浸轧后再进行汽蒸的后处理步骤。
通过对实施例1-实施例3以及对比例所染整处理后的腈纶面料进行断裂强度、色牢度进行检测,所得结果如下表1所示:
表1检测结果
项目 | 实施例1 | 实施例2 | 实施例3 | 对比例 |
断裂强度cN·dtex<sup>-1</sup> | 2.23 | 2.25 | 2.22 | 2.18 |
耐水洗色牢度/级 | 4 | 4 | 4 | 3 |
耐酸汗渍色牢度/级 | 5 | 5 | 5 | 3 |
耐碱汗渍色牢度/级 | 4 | 4 | 4 | 4 |
从上表1可以看出实施例2的各方面检测数据均较为优异,为最优实施方案,同时加入抗黄变剂并浸轧后再进行汽蒸的后处理步骤也对腈纶面料的色牢度有直接影响。
其中,断裂强度的测试方法为:GB/T 3923.2-2013《纺织品织物拉伸性能第2部分:断裂强力的测定(抓样法)》。
耐水洗色牢度、耐酸汗渍色牢度、耐碱汗渍色牢度测试方法均参照GB 18401-2010《国家纺织产品基本安全技术规范》。
以上所述仅是本发明的优选实施方式,应当理解本发明并非局限于本文所披露的形式,不应看作是对其他实施例的排除,而可用于各种其他组合、修改和环境,并能够在本文所述构想范围内,通过上述教导或相关领域的技术或知识进行改动。而本领域人员所进行的改动和变化不脱离本发明的精神和范围,则都应在本发明所附权利要求的保护范围内。
Claims (6)
1.一种透气荧光腈纶面料的染整工艺,其特征在于,包括以下步骤:
步骤一、将腈纶放入水缸中,加入质量分数为6-10%的处理液,于40-50℃温度下浸泡1-1.5h,加入清洗剂搅拌15-20min,再使用清水充分水洗至pH值为中性,在100℃下烘培25min;
步骤二、将烘干后的腈纶放入处理浴中进行染色和整理,在处理浴中加入荧光剂和含酸性基团组成的染色剂,调节pH为2-5,将腈纶按浴比1:10-100投入处理浴中,以0.5-5℃/min的升温速度升温至80-100℃,保温10-60min,以0.5-3℃/min的降温速度降温至50℃,加入抗黄变剂并浸轧后再进行汽蒸,最后将腈纶水洗、烘干或晾干。
2.根据权利要求1所述的一种透气荧光腈纶面料的染整工艺,其特征在于,所述步骤一中的处理液为甲基丙烯磺酸钠和甲基乙烯基吡啶的混合溶液。
3.根据权利要求1所述的一种透气荧光腈纶面料的染整工艺,其特征在于,所述步骤一中的清洗剂为烷基酚聚氧乙烯醚。
4.根据权利要求1所述的一种透气荧光腈纶面料的染整工艺,其特征在于,所述步骤二中染色剂中荧光剂和含酸性基团的含量比为5:2。
5.根据权利要求1或4中所述的一种透气荧光腈纶面料的染整工艺,其特征在于,所述荧光剂为分散荧光染料荧光黄10G、荧光艳橙 G、荧光红 G 和荧光红 B。
6.根据权利要求1或4中所述的一种透气荧光腈纶面料的染整工艺,其特征在于,所述含酸性基团为磺酸基或磺酸钠盐或羧酸钠盐。
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