CN113842346A - Composite natural petal extract shower gel and preparation method thereof - Google Patents
Composite natural petal extract shower gel and preparation method thereof Download PDFInfo
- Publication number
- CN113842346A CN113842346A CN202111246698.1A CN202111246698A CN113842346A CN 113842346 A CN113842346 A CN 113842346A CN 202111246698 A CN202111246698 A CN 202111246698A CN 113842346 A CN113842346 A CN 113842346A
- Authority
- CN
- China
- Prior art keywords
- stirring
- parts
- extract
- essential oil
- surfactant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000002131 composite material Substances 0.000 title claims abstract description 9
- 238000002360 preparation method Methods 0.000 title abstract description 12
- 238000001879 gelation Methods 0.000 title description 2
- 239000000341 volatile oil Substances 0.000 claims abstract description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 13
- 229930195729 fatty acid Natural products 0.000 claims abstract description 13
- 239000000194 fatty acid Substances 0.000 claims abstract description 13
- 241000220317 Rosa Species 0.000 claims abstract description 12
- 244000178231 Rosmarinus officinalis Species 0.000 claims abstract description 12
- 150000004665 fatty acids Chemical class 0.000 claims abstract description 12
- 229940082892 tamarind seed extract Drugs 0.000 claims abstract description 12
- 235000019864 coconut oil Nutrition 0.000 claims abstract description 11
- 239000003240 coconut oil Substances 0.000 claims abstract description 11
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 10
- 239000003945 anionic surfactant Substances 0.000 claims abstract description 8
- 239000002888 zwitterionic surfactant Substances 0.000 claims abstract description 8
- 239000002738 chelating agent Substances 0.000 claims abstract description 7
- 239000003906 humectant Substances 0.000 claims abstract description 7
- 229910052751 metal Inorganic materials 0.000 claims abstract description 7
- 239000002184 metal Substances 0.000 claims abstract description 7
- 239000003755 preservative agent Substances 0.000 claims abstract description 7
- 230000002335 preservative effect Effects 0.000 claims abstract description 7
- 229940084750 sophora flavescens root extract Drugs 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims description 81
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical group CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 33
- -1 palmitoyl sarcosinate Chemical compound 0.000 claims description 33
- 239000000203 mixture Substances 0.000 claims description 17
- 238000001816 cooling Methods 0.000 claims description 16
- 229940117986 sulfobetaine Drugs 0.000 claims description 15
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical group C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 claims description 14
- ZUFONQSOSYEWCN-UHFFFAOYSA-M sodium;2-(methylamino)acetate Chemical compound [Na+].CNCC([O-])=O ZUFONQSOSYEWCN-UHFFFAOYSA-M 0.000 claims description 14
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims description 12
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims description 12
- 229940100555 2-methyl-4-isothiazolin-3-one Drugs 0.000 claims description 11
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical group OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims description 11
- BEGLCMHJXHIJLR-UHFFFAOYSA-N methylisothiazolinone Chemical group CN1SC=CC1=O BEGLCMHJXHIJLR-UHFFFAOYSA-N 0.000 claims description 11
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 8
- 239000008367 deionised water Substances 0.000 claims description 8
- 229910021641 deionized water Inorganic materials 0.000 claims description 8
- 239000002994 raw material Substances 0.000 claims description 8
- 229940071089 sarcosinate Drugs 0.000 claims description 8
- 229960003237 betaine Drugs 0.000 claims description 6
- 150000003839 salts Chemical class 0.000 claims description 6
- 150000002148 esters Chemical class 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 3
- FZKLLOBCECHTQV-UHFFFAOYSA-N 2-(methylamino)propanoyl dodecanoate Chemical compound CCCCCCCCCCCC(=O)OC(=O)C(C)NC FZKLLOBCECHTQV-UHFFFAOYSA-N 0.000 claims description 2
- NGOZDSMNMIRDFP-UHFFFAOYSA-N 2-[methyl(tetradecanoyl)amino]acetic acid Chemical compound CCCCCCCCCCCCCC(=O)N(C)CC(O)=O NGOZDSMNMIRDFP-UHFFFAOYSA-N 0.000 claims description 2
- 229910019142 PO4 Inorganic materials 0.000 claims description 2
- 150000003973 alkyl amines Chemical class 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- 150000002191 fatty alcohols Chemical class 0.000 claims description 2
- 229940071145 lauroyl sarcosinate Drugs 0.000 claims description 2
- 229940070782 myristoyl sarcosinate Drugs 0.000 claims description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 2
- 239000010452 phosphate Substances 0.000 claims description 2
- 241000222122 Candida albicans Species 0.000 abstract description 3
- 241000191967 Staphylococcus aureus Species 0.000 abstract description 3
- 229940095731 candida albicans Drugs 0.000 abstract description 3
- 230000002401 inhibitory effect Effects 0.000 abstract description 3
- 239000003112 inhibitor Substances 0.000 abstract description 2
- 239000000499 gel Substances 0.000 description 21
- 238000010438 heat treatment Methods 0.000 description 9
- 230000000844 anti-bacterial effect Effects 0.000 description 8
- 241000246044 Sophora flavescens Species 0.000 description 7
- 238000002156 mixing Methods 0.000 description 7
- 241000596504 Tamarindus Species 0.000 description 6
- 235000004298 Tamarindus indica Nutrition 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- 241000894006 Bacteria Species 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- KXDHJXZQYSOELW-UHFFFAOYSA-N Carbamic acid Chemical group NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011031 large-scale manufacturing process Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 229940051841 polyoxyethylene ether Drugs 0.000 description 2
- 241000186000 Bifidobacterium Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- QPCDCPDFJACHGM-UHFFFAOYSA-N N,N-bis{2-[bis(carboxymethyl)amino]ethyl}glycine Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(=O)O)CCN(CC(O)=O)CC(O)=O QPCDCPDFJACHGM-UHFFFAOYSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- AMTWCFIAVKBGOD-UHFFFAOYSA-N dioxosilane;methoxy-dimethyl-trimethylsilyloxysilane Chemical compound O=[Si]=O.CO[Si](C)(C)O[Si](C)(C)C AMTWCFIAVKBGOD-UHFFFAOYSA-N 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 229960001617 ethyl hydroxybenzoate Drugs 0.000 description 1
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 238000011081 inoculation Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 1
- MGFYIUFZLHCRTH-UHFFFAOYSA-N nitrilotriacetic acid Chemical compound OC(=O)CN(CC(O)=O)CC(O)=O MGFYIUFZLHCRTH-UHFFFAOYSA-N 0.000 description 1
- GYCKQBWUSACYIF-UHFFFAOYSA-N o-hydroxybenzoic acid ethyl ester Natural products CCOC(=O)C1=CC=CC=C1O GYCKQBWUSACYIF-UHFFFAOYSA-N 0.000 description 1
- 229960003330 pentetic acid Drugs 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 229940083037 simethicone Drugs 0.000 description 1
- 238000012430 stability testing Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/04—Antibacterial agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/10—Antimycotics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Birds (AREA)
- Pharmacology & Pharmacy (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dermatology (AREA)
- Epidemiology (AREA)
- Organic Chemistry (AREA)
- Communicable Diseases (AREA)
- Engineering & Computer Science (AREA)
- Oncology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The invention relates to the technical field of preparation of daily necessities, in particular to composite natural petal extract shower gel and a preparation method thereof. The shower gel consists of rose essential oil, rosemary essential oil, a sophora flavescens root extract, a tamarind seed extract, an anionic surfactant, a zwitterionic surfactant, a nonionic surfactant, a preservative, a humectant, a metal chelating agent and water. The tamarind seed extract is added and is compatible with the radix sophorae flavescentis extract, so that the inhibitor has a stronger inhibiting effect on staphylococcus aureus and candida albicans. The invention can effectively solve the problems of turbidity and layering when the tamarind seed extract and the radix sophorae flavescentis extract are compatible together by adding the coconut oil fatty acid diethanolamide serving as a nonionic surfactant.
Description
Technical Field
The invention relates to the technical field of preparation of daily necessities, in particular to composite natural petal extract shower gel and a preparation method thereof.
Background
The shower gel is one of the common washing and caring products in life, and has the characteristics of moistening, fine and smooth foam, lasting fragrance, bacteria inhibition and the like. Particularly, with the improvement of living standard and daily requirement of people, the shower gel needs more and more additional functions besides the basic function of cleaning skin, and in order to improve the using effect of the shower gel, components are added into the shower gel to improve the functionality of the shower gel, but at present, a lot of added components are chemical products, so that the shower gel is harmful to the body after long-term skin use and cannot play the effect of inhibiting bacteria and fungi, and a natural skin-care shower gel product is needed.
Based on the situation, the invention provides the composite natural petal extract shower gel and the preparation method thereof, and the problems can be effectively solved.
Disclosure of Invention
The invention aims to provide composite natural petal extract shower gel and a preparation method thereof.
In order to achieve the purpose, the invention provides a composite natural petal extract shower gel which is composed of rose essential oil, rosemary essential oil, a sophora flavescens root extract, a tamarind seed extract, an anionic surfactant, a zwitterionic surfactant, a nonionic surfactant, a preservative, a humectant, a metal chelating agent and water.
Preferably, the shower gel consists of the following raw materials in parts by weight: 30-40 parts of rose essential oil, 10-20 parts of rosemary essential oil, 15-30 parts of sophora flavescens root extract, 25-35 parts of tamarind seed extract, 10-20 parts of anionic surfactant, 30-60 parts of zwitterionic surfactant, 5-10 parts of nonionic surfactant, 1-3 parts of preservative, 1-3 parts of humectant, 1-3 parts of metal chelating agent and 100-140 parts of water.
Preferably, the anionic surfactant is an N-acyl amino acid salt; the N-acyl amino acid salt comprises at least one or more of cocoyl sarcosinate, cocoyl sarcosinate TEA, lauroyl sarcosinate and salts thereof, myristoyl sarcosinate, palmitoyl sarcosinate, oleoyl sarcosinate and lauroyl methyl aminopropionate.
Preferably, the anionic surfactant is sodium cocoyl sarcosinate.
Preferably, the zwitterionic surfactant is a betaine derivative; the betaine derivative comprises at least one or more of alkyl dimethyl betaine, dodecyl ethoxy sulfobetaine, dodecyl hydroxypropyl sulfobetaine, dodecyl sulfopropyl betaine, tetradecylamidopropyl hydroxypropyl sulfobetaine, decyl hydroxypropyl sulfobetaine, cocamidopropyl betaine and phosphate ester betaine.
Preferably, the zwitterionic surfactant is a combination of cocamidopropyl betaine and tetradecanamidopropyl hydroxypropyl sulfobetaine.
Preferably, the nonionic surfactant is at least one or a combination of more than two of polyoxyethylene alkyl alcohol amide, polyoxyethylene alkylamine, polyoxyethylene fatty acid ester, alkylphenol polyoxyethylene ether, long-chain fatty alcohol polyoxyethylene ether, polyoxypropylene-polyoxyethylene copolymer and alkanolamide.
Preferably, the nonionic surfactant is coconut oil fatty acid diethanolamide.
Preferably, the preservative comprises one or a combination of more than two of methylisothiazolinone, nipagin ester, methyl hydroxybenzoate and ethyl hydroxybenzoate.
Preferably, the preservative is methylisothiazolinone.
Preferably, the humectant comprises one or a combination of more than two of simethicone, glycerol, propylene glycol and butanediol.
Preferably, the humectant is propylene glycol.
Preferably, the metal chelating agent is an aminocarboxylic acid; the aminocarboxylic acid is one of ethylenediamine tetraacetic acid, aminotriacetic acid and diethylenetriamine pentaacetic acid.
Preferably, the metal chelating agent is ethylenediaminetetraacetic acid.
In one embodiment, the tamarind seed extract is prepared by the following method:
(1) crushing tamarind seeds, adding 1-2% phosphoric acid aqueous solution which is 10-15 times of tamarind seeds in weight, heating to 70-80 ℃, and extracting for 30-40 min; filtering for later use;
(2) inoculating mixed bacteria consisting of acetic acid bacteria and bifidobacteria according to the inoculation amount of 6-8% in any proportion, and continuously fermenting for 5-8 days at the temperature of 25-35 ℃;
(3) after fermentation, instantly sterilizing at high temperature, and filtering by filter pressing method.
In one embodiment, the extract of the kuh-seng root is prepared by the following method:
crushing the sophora flavescens roots, adding an aqueous solution of which the weight is 10-15 times that of the sophora flavescens roots, heating to 100-110 ℃, and extracting for 45-60 min; filtering, and concentrating.
The invention also provides a preparation method of the composite natural petal extract shower gel, which comprises the following steps:
(1) mixing half of deionized water in formula amount with sodium cocoyl sarcosinate, cocamidopropyl betaine, tetradecylamidopropyl hydroxypropyl sulphobetaine and coconut oil fatty acid diethanolamide, heating and stirring uniformly, wherein the stirring temperature is 60-65 ℃, the stirring time is 10-15 min, and the stirring speed is 1000-1500 r/min;
(2) sequentially adding the sophora flavescens root extract, the tamarind seed extract and the ethylenediamine tetraacetic acid into the mixture obtained in the step (1), uniformly stirring, adding the rest water in the formula amount while stirring, wherein the stirring temperature is 70-75 ℃, and stirring for 30-40 min at constant temperature, and the stirring speed is 2000-2500 r/min;
(3) and (3) after cooling to below 50 ℃, sequentially adding propylene glycol, methylisothiazolinone, rose essential oil and rosemary essential oil into the mixture obtained in the step (2), uniformly stirring, cooling for 30-40 ℃ while stirring, stirring for 5-8 min at a stirring speed of 1500-1700 r/min, and standing for defoaming to obtain the product.
Compared with the prior art, the invention has the following beneficial effects:
1. the tamarind seed extract is added and is compatible with the radix sophorae flavescentis extract, so that the inhibitor has a stronger inhibiting effect on staphylococcus aureus and candida albicans.
2. The invention can effectively solve the problems of turbidity and layering when the tamarind seed extract and the radix sophorae flavescentis extract are compatible together by adding the coconut oil fatty acid diethanolamide serving as a nonionic surfactant.
3. The raw materials of the invention are sufficient in China and proper in price, so that the large-scale production of the invention is not limited by too high cost; meanwhile, the preparation method is simple, the total production cost is low, and the industrial large-scale production is facilitated.
Detailed Description
Example 1
The specific raw materials were weighed as in table 1, and the remaining steps were as follows:
(1) mixing half amount of deionized water with sodium cocoyl sarcosinate, cocamidopropyl betaine, tetradecylamidopropyl hydroxypropyl sulfobetaine and coconut oil fatty acid diethanolamide, heating and stirring uniformly at 65 deg.C for 15min at 1000 r/min;
(2) sequentially adding the extract of the root of the sophora flavescens ait, the extract of the tamarind seed and the ethylenediamine tetraacetic acid into the mixture obtained in the step (1), uniformly stirring, adding the rest water in the formula amount while stirring, wherein the stirring temperature is 75 ℃, and the stirring speed is 2500 r/min;
(3) and (3) after cooling to below 50 ℃, sequentially adding propylene glycol, methylisothiazolinone, rose essential oil and rosemary essential oil into the mixture obtained in the step (2), uniformly stirring, cooling while stirring at 40 ℃, stirring for 8min at the stirring speed of 1500r/min, and standing for defoaming to obtain the product.
Example 2
The specific raw materials were weighed as in table 1, and the remaining steps were as follows:
(1) mixing half amount of deionized water with sodium cocoyl sarcosinate, cocamidopropyl betaine, tetradecanamopropyl hydroxypropyl sulfobetaine and coconut oil fatty acid diethanolamide, heating and stirring uniformly at 60 deg.C for 15min at 1500 r/min;
(2) sequentially adding the extract of the root of the sophora flavescens ait, the extract of the tamarind seed and the ethylenediamine tetraacetic acid into the mixture obtained in the step (1), uniformly stirring, adding the rest water in the formula amount while stirring, wherein the stirring temperature is 70 ℃, and the stirring speed is 2500 r/min;
(3) and (3) after cooling to below 50 ℃, sequentially adding propylene glycol, methylisothiazolinone, rose essential oil and rosemary essential oil into the mixture obtained in the step (2), uniformly stirring, cooling while stirring for 30 ℃, stirring for 8min at the stirring speed of 1700r/min, and standing for defoaming to obtain the product.
Example 3
The specific raw materials were weighed as in table 1, and the remaining steps were as follows:
(1) mixing half amount of deionized water with sodium cocoyl sarcosinate, cocamidopropyl betaine, tetradecanamopropyl hydroxypropyl sulfobetaine and coconut oil fatty acid diethanolamide, heating and stirring uniformly at 65 deg.C for 15min at 1500 r/min;
(2) sequentially adding the extract of the root of the sophora flavescens ait, the extract of the tamarind seed and the ethylenediamine tetraacetic acid into the mixture obtained in the step (1), uniformly stirring, adding the rest water in the formula amount while stirring, wherein the stirring temperature is 75 ℃, and the stirring speed is 2500 r/min;
(3) and (3) after cooling to below 50 ℃, sequentially adding propylene glycol, methylisothiazolinone, rose essential oil and rosemary essential oil into the mixture obtained in the step (2), uniformly stirring, cooling while stirring at 40 ℃, stirring for 8min at the stirring speed of 1700r/min, and standing for defoaming to obtain the product.
Comparative example 1
The specific raw materials were weighed as in table 1, and the preparation steps were as follows:
(1) mixing half amount of deionized water with sodium cocoyl sarcosinate, cocamidopropyl betaine, tetradecanamopropyl hydroxypropyl sulfobetaine and coconut oil fatty acid diethanolamide, heating and stirring uniformly at 65 deg.C for 15min at 1500 r/min;
(2) sequentially adding the extract of the roots of the sophora flavescens and the ethylenediamine tetraacetic acid into the mixture obtained in the step (1), uniformly stirring, adding the rest water in the formula amount while stirring, wherein the stirring temperature is 75 ℃, and stirring at the constant temperature for 40min at the stirring speed of 2500 r/min;
(3) and (3) after cooling to below 50 ℃, sequentially adding propylene glycol, methylisothiazolinone, rose essential oil and rosemary essential oil into the mixture obtained in the step (2), uniformly stirring, cooling while stirring at 40 ℃, stirring for 8min at the stirring speed of 1700r/min, and standing for defoaming to obtain the product.
Comparative example 2
The specific raw materials were weighed as in table 1, and the preparation steps were as follows:
(1) mixing half amount of deionized water with sodium cocoyl sarcosinate, cocamidopropyl betaine, tetradecanamopropyl hydroxypropyl sulfobetaine and coconut oil fatty acid diethanolamide, heating and stirring uniformly at 65 deg.C for 15min at 1500 r/min;
(2) sequentially adding the tamarind seed extract and the ethylenediamine tetraacetic acid into the mixture obtained in the step (1), uniformly stirring, adding the rest water in the formula amount while stirring, wherein the stirring temperature is 75 ℃, and stirring at the constant temperature for 40min at the stirring speed of 2500 r/min;
(3) and (3) after cooling to below 50 ℃, sequentially adding propylene glycol, methylisothiazolinone, rose essential oil and rosemary essential oil into the mixture obtained in the step (2), uniformly stirring, cooling while stirring at 40 ℃, stirring for 8min at the stirring speed of 1700r/min, and standing for defoaming to obtain the product.
Comparative example 3
(1) Mixing half of deionized water in formula amount with sodium cocoyl sarcosinate, cocamidopropyl betaine and tetradecylamidopropyl hydroxypropyl sulphobetaine, heating and stirring uniformly at 65 ℃ for 15min at 1500 r/min;
(2) sequentially adding the extract of the root of the sophora flavescens ait, the extract of the tamarind seed and the ethylenediamine tetraacetic acid into the mixture obtained in the step (1), uniformly stirring, adding the rest water in the formula amount while stirring, wherein the stirring temperature is 75 ℃, and the stirring speed is 2500 r/min;
(3) and (3) after cooling to below 50 ℃, sequentially adding propylene glycol, methylisothiazolinone, rose essential oil and rosemary essential oil into the mixture obtained in the step (2), uniformly stirring, cooling while stirring at 40 ℃, stirring for 8min at the stirring speed of 1700r/min, and standing for defoaming to obtain the product.
TABLE 1
Example 4 Performance testing
And (3) testing antibacterial ability: taking the shower gel prepared in the embodiments 1-3 and the comparative examples 1-2, testing the antibacterial capacity of the shower gel by referring to GB19877.2-2005, wherein the test strains are staphylococcus aureus and candida albicans; the antibacterial rate of the shower gel is defined to be more than or equal to 90 percent, the antibacterial capacity is strong, the antibacterial rate of the shower gel is 80 to 90 percent, the antibacterial capacity is general, and the antibacterial rate of the shower gel is less than or equal to 80 percent, and the antibacterial capacity is poor.
And (3) stability testing: the shower gels prepared in examples 1 to 3 and comparative examples 1 to 2 were used, and 10 parallel samples were set for each sample. The samples are sequentially placed at 50 ℃, 40 ℃, 26 ℃ and-4 ℃ for one week respectively, and then are taken out to observe whether the shower gel has the phenomena of layering, turbidity, discoloration and peculiar smell. And recording the number of samples with layering, turbidity, color change and peculiar smell.
The test results are shown in Table 2.
Table 2 results of performance testing
The foregoing descriptions of specific exemplary embodiments of the present invention have been presented for purposes of illustration and description. It is not intended to limit the invention to the precise form disclosed, and obviously many modifications and variations are possible in light of the above teaching. The exemplary embodiments were chosen and described in order to explain certain principles of the invention and its practical application to enable one skilled in the art to make and use various exemplary embodiments of the invention and various alternatives and modifications as are suited to the particular use contemplated. It is intended that the scope of the invention be defined by the claims and their equivalents.
Claims (9)
1. The composite natural petal extract shower gel is characterized by comprising the following raw materials in parts by weight: 30-40 parts of rose essential oil, 10-20 parts of rosemary essential oil, 15-30 parts of sophora flavescens root extract, 25-35 parts of tamarind seed extract, 10-20 parts of anionic surfactant, 30-60 parts of zwitterionic surfactant, 5-10 parts of nonionic surfactant, 1-3 parts of preservative, 1-3 parts of humectant, 1-3 parts of metal chelating agent and 100-140 parts of water.
2. The body wash of claim 1, wherein the anionic surfactant is an N-acyl amino acid salt; the N-acyl amino acid salt comprises at least one or more of cocoyl sarcosinate, cocoyl sarcosinate TEA, lauroyl sarcosinate and salts thereof, myristoyl sarcosinate, palmitoyl sarcosinate, oleoyl sarcosinate and lauroyl methyl aminopropionate.
3. The body wash of claim 2, wherein the anionic surfactant is sodium cocoyl sarcosinate.
4. The body wash of claim 1, wherein the zwitterionic surfactant is a betaine derivative; the betaine derivative comprises at least one or more of alkyl dimethyl betaine, dodecyl ethoxy sulfobetaine, dodecyl hydroxypropyl sulfobetaine, dodecyl sulfopropyl betaine, tetradecylamidopropyl hydroxypropyl sulfobetaine, decyl hydroxypropyl sulfobetaine, cocamidopropyl betaine and phosphate ester betaine.
5. The body wash of claim 4, wherein the zwitterionic surfactant is a combination of cocamidopropyl betaine and tetradecanamidopropyl hydroxypropyl sulfobetaine.
6. The body wash of claim 1, wherein the nonionic surfactant is at least one of polyoxyethylene alkylolamides, polyoxyethylene alkylamines, fatty acid polyoxyethylene esters, alkylphenol ethoxylates, long-chain fatty alcohol polyoxyethylene ethers, polyoxypropylene-polyoxyethylene copolymers, and alkanolamides, or a combination of two or more thereof.
7. The body wash of claim 6, wherein the non-ionic surfactant is coconut oil fatty acid diethanolamide.
8. The body wash of claim 1, wherein the preservative is methylisothiazolinone; the humectant is propylene glycol; the metal chelating agent is ethylenediamine tetraacetic acid.
9. A method of preparing the body wash of any one of claims 1 to 8, comprising the steps of:
(1) half of deionized water in formula amount is mixed with sodium cocoyl sarcosinate, cocamidopropyl betaine, tetradecylamidopropyl hydroxypropyl sulphobetaine and coconut oil fatty acid diethanolamide, the mixture is heated and stirred uniformly, the stirring temperature is 60-65 ℃, the stirring time is 10-15 min, and the stirring speed is 1000-1500 r/min.
(2) And (2) sequentially adding the sophora flavescens root extract, the tamarind seed extract and the ethylenediamine tetraacetic acid into the mixture obtained in the step (1), uniformly stirring, adding the rest water in the formula amount while stirring, wherein the stirring temperature is 70-75 ℃, and stirring for 30-40 min at a constant temperature, and the stirring speed is 2000-2500 r/min.
(3) And (3) after cooling to below 50 ℃, sequentially adding propylene glycol, methylisothiazolinone, rose essential oil and rosemary essential oil into the mixture obtained in the step (2), uniformly stirring, cooling for 30-40 ℃ while stirring, stirring for 5-8 min at a stirring speed of 1500-1700 r/min, and standing for defoaming to obtain the product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111246698.1A CN113842346A (en) | 2021-10-26 | 2021-10-26 | Composite natural petal extract shower gel and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111246698.1A CN113842346A (en) | 2021-10-26 | 2021-10-26 | Composite natural petal extract shower gel and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN113842346A true CN113842346A (en) | 2021-12-28 |
Family
ID=78983013
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202111246698.1A Pending CN113842346A (en) | 2021-10-26 | 2021-10-26 | Composite natural petal extract shower gel and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN113842346A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105616322A (en) * | 2016-01-20 | 2016-06-01 | 惠州市明荃化妆品有限公司 | Antibacterial whitening and relaxing shower gel and preparation method thereof |
| CN108498436A (en) * | 2018-05-12 | 2018-09-07 | 大理大学 | A kind of skin care bacteriostatic hand sanitizer and preparation method thereof |
| CN111317693A (en) * | 2020-03-04 | 2020-06-23 | 刘志强 | Antibacterial and antiviral agilawood hand sanitizer and preparation method thereof |
-
2021
- 2021-10-26 CN CN202111246698.1A patent/CN113842346A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105616322A (en) * | 2016-01-20 | 2016-06-01 | 惠州市明荃化妆品有限公司 | Antibacterial whitening and relaxing shower gel and preparation method thereof |
| CN108498436A (en) * | 2018-05-12 | 2018-09-07 | 大理大学 | A kind of skin care bacteriostatic hand sanitizer and preparation method thereof |
| CN111317693A (en) * | 2020-03-04 | 2020-06-23 | 刘志强 | Antibacterial and antiviral agilawood hand sanitizer and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN114869815B (en) | Anti-dandruff antibacterial shampoo and preparation method thereof | |
| CN113398029B (en) | Antibacterial and anti-dandruff shampoo and preparation method thereof | |
| CN113842346A (en) | Composite natural petal extract shower gel and preparation method thereof | |
| CN109010193A (en) | A kind of Pudilan shower cream and preparation method thereof | |
| CN108125798A (en) | A kind of mild disposable foam liquid soap with bacteria resistance function | |
| CN107811897A (en) | A kind of Ju You treatment oil repairs the shampoo of effect | |
| CN112156060A (en) | Propolis wash-free long-acting antibacterial gel and preparation method thereof | |
| CN106420406A (en) | Velvet smoothening liquid shampoo | |
| KR102107772B1 (en) | Composition for cleaning dead skin | |
| CN110585081A (en) | Antibacterial and itching-relieving shampoo containing folium artemisiae argyi essential oil and preparation method thereof | |
| CN113368290B (en) | Rose fragrance fumigant | |
| CN111643440B (en) | Liquid soap containing goat milk and preparation method thereof | |
| CN112006954B (en) | Shampoo and preparation method thereof | |
| CN110123698B (en) | Soapberry enzyme shampoo with inhibiting effect on hair-related pathogenic bacteria and preparation method thereof | |
| CN104257563A (en) | Creeping falsepimpernel herb hand sanitizer and preparation method thereof | |
| CN107595683A (en) | The preparation method that one main laminaria ENZYME WASH becomes visible | |
| CN106491411A (en) | One kind is rich in natural Flos Matricariae chamomillae petal and its hydrosol | |
| CN113318021A (en) | Hand sanitizer | |
| CN112494393A (en) | Shampoo and preparation method thereof | |
| CN108559669A (en) | A kind of bacteria inhibiting composition and the preparation method and application thereof | |
| CN109431833A (en) | A kind of fermented juice shower cream and preparation method thereof | |
| CN102920629A (en) | Rose mask and preparation method thereof | |
| CN108998292A (en) | A kind of newborn soap and preparation method thereof that repelling effect is good | |
| CN114190276B (en) | Tissue culture and rapid propagation method for producing Panlongshen seedlings by using leaves | |
| CN107693482A (en) | A kind of special anti-bacteria wet keeping wet tissue of infant |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20211228 |