CN113818013A - 一种用于石英光纤的表面处理工艺 - Google Patents
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Abstract
本发明公开了一种用于石英光纤的表面处理工艺,本表面处理工艺采用先化学镀后电镀的方式进行镀层的镀覆,与只进行化学镀或电镀所产生的镀层相比,先化学镀后电镀所产生的外侧镀层更紧密,孔隙更小,耐磨性更好,内侧镀层与蓝宝石产品之间的结合能力更强,均匀性更高。
Description
技术领域
本发明涉及一种表面处理工艺,具体涉及一种用于石英光纤的表面处理工艺。
背景技术
电镀和化学镀是两种较为常见的金属表面处理技术,其具有防止金属氧化,提高耐磨性、导电性、反光性、抗腐蚀性及增进美观等作用。随着表面处理技术的不断发展,越来越多的镀覆制品改为在非金属材料表面上进行镀覆,以石英光纤为例,在其表面进行镀覆处理时为了增强产品的耐磨性,需要减少镀层的孔隙率,并且提高镀层与产品表面之间的结合能力。
发明内容
本发明是为了解决现有技术的不足,提供一种用于石英光纤的表面处理工艺。
一种用于石英光纤的表面处理工艺,包括一下步骤:
步骤一:将石英光纤放在温度为50~60℃的除油液中清洗,清洗时间为5~10min,所述除油液中除油粉的浓度为50g/L,清洗完成后用水去除石英光纤表面残留的除油液;
步骤二:将除油清洗后的石英光纤放在温度为40~45℃的粗化液中粗化,粗化时间为5~15min,所述粗化液的容积为200mL/L,粗化完成后用水去除石英光纤表面残留的粗化液;
步骤三:使用常温的10%硫酸液第一次活化去除石英光纤表面的氧化层,第一次活化的时间为1~5min;
步骤四:使用温度为38~45℃的硫酸钯溶液第二次活化石英光纤,增加石英光纤表面的张力,第二次活化的时间为2~8min,所述的硫酸钯溶液内离子钯和硫酸的质量分数均为5%;
步骤五:使用温度为78~80℃的酸性镍溶液对两次活化后的石英光纤进行化学镀镍,所述酸性镍溶液的PH值范围为4.5~4.8;
步骤六:使用电镀技术在石英光纤的表面上镀镍金;
步骤七:对电镀后的石英光纤依次进行拔检和外观全检。
优选地,步骤一中所述除油液的温度为60℃,清洗时间为5min。
优选地,步骤二中所述粗化液的温度为45℃,粗化时间为8min。
优选地,步骤三中所述第一次活化的时间为5min。
优选地,步骤四中所述硫酸钯溶液的温度为45℃,第二次活化的时间为3min。
优选地,步骤五中所述酸性镍溶液的温度为78℃,PH值为4.8。
有益效果:本发明公开了一种用于石英光纤的表面处理工艺,本表面处理工艺采用先化学镀后电镀的方式进行镀层的镀覆,与只进行化学镀或电镀所产生的镀层相比,先化学镀后电镀所产生的外侧镀层更紧密,孔隙更小,耐磨性更好,内侧镀层与蓝宝石产品之间的结合能力更强,均匀性更高。
具体实施方式
为了加深对本发明的理解,下面结合实施例对本发明作进一步详细详述,该实施例仅用于解释本发明,并不构成对本发明保护范围的限定。
一种用于石英光纤的表面处理工艺,包括一下步骤:
步骤一:将石英光纤放在温度为50~60℃的除油液中清洗,清洗时间为5~10min,所述除油液中除油粉的浓度为50g/L,清洗完成后用水去除石英光纤表面残留的除油液;
步骤二:将除油清洗后的石英光纤放在温度为40~45℃的粗化液中粗化,粗化时间为5~15min,所述粗化液的容积为200mL/L,粗化完成后用水去除石英光纤表面残留的粗化液;
步骤三:使用常温的10%硫酸液第一次活化去除石英光纤表面的氧化层,第一次活化的时间为1~5min;
步骤四:使用温度为38~45℃的硫酸钯溶液第二次活化石英光纤,增加石英光纤表面的张力,第二次活化的时间为2~8min,所述的硫酸钯溶液内离子钯和硫酸的质量分数均为5%;
步骤五:使用温度为78~80℃的酸性镍溶液对两次活化后的石英光纤进行化学镀镍,所述酸性镍溶液的PH值范围为4.5~4.8;
步骤六:使用电镀技术在石英光纤的表面上镀镍金;
步骤七:对电镀后的石英光纤依次进行拔检和外观全检。
于本实施例中,步骤一中所述除油液的温度为60℃,清洗时间为5min。
于本实施例中,步骤二中所述粗化液的温度为45℃,粗化时间为8min。
于本实施例中,步骤三中所述第一次活化的时间为5min。
于本实施例中,步骤四中所述硫酸钯溶液的温度为45℃,第二次活化的时间为3min。
于本实施例中,步骤五中所述酸性镍溶液的温度为78℃,PH值为4.8。
本表面处理工艺采用先化学镀后电镀的方式进行镀层的镀覆,与只进行化学镀或电镀所产生的镀层相比,先化学镀后电镀所产生的外侧镀层更紧密,孔隙更小,耐磨性更好,内侧镀层与蓝宝石产品之间的结合能力更强,均匀性更高。
以上所述仅为本发明的较佳实施例而已,并不用以限制本发明,凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。
Claims (6)
1.一种用于石英光纤的表面处理工艺,其特征在于,包括一下步骤:
步骤一:将石英光纤放在温度为50~60℃的除油液中清洗,清洗时间为5~10min,所述除油液中除油粉的浓度为50g/L,清洗完成后用水去除石英光纤表面残留的除油液;
步骤二:将除油清洗后的石英光纤放在温度为40~45℃的粗化液中粗化,粗化时间为5~15min,所述粗化液的容积为200mL/L,粗化完成后用水去除石英光纤表面残留的粗化液;
步骤三:使用常温的10%硫酸液第一次活化去除石英光纤表面的氧化层,第一次活化的时间为1~5min;
步骤四:使用温度为38~45℃的硫酸钯溶液第二次活化石英光纤,增加石英光纤表面的张力,第二次活化的时间为2~8min,所述的硫酸钯溶液内离子钯和硫酸的质量分数均为5%;
步骤五:使用温度为78~80℃的酸性镍溶液对两次活化后的石英光纤进行化学镀镍,所述酸性镍溶液的PH值范围为4.5~4.8;
步骤六:使用电镀技术在石英光纤的表面上镀镍金;
步骤七:对电镀后的石英光纤依次进行拔检和外观全检。
2.根据权利要求1所述的一种用于石英光纤的表面处理工艺,其特征在于,步骤一中所述除油液的温度为60℃,清洗时间为5min。
3.根据权利要求1所述的一种用于石英光纤的表面处理工艺,其特征在于,步骤二中所述粗化液的温度为45℃,粗化时间为8min。
4.根据权利要求1所述的一种用于石英光纤的表面处理工艺,其特征在于,步骤三中所述第一次活化的时间为5min。
5.根据权利要求1所述的一种用于石英光纤的表面处理工艺,其特征在于,步骤四中所述硫酸钯溶液的温度为45℃,第二次活化的时间为3min。
6.根据权利要求1所述的一种用于石英光纤的表面处理工艺,其特征在于,步骤五中所述酸性镍溶液的温度为78℃,PH值为4.8。
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