CN113786359A - Perfume containing plant natural components and preparation method thereof - Google Patents

Perfume containing plant natural components and preparation method thereof Download PDF

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Publication number
CN113786359A
CN113786359A CN202111109303.3A CN202111109303A CN113786359A CN 113786359 A CN113786359 A CN 113786359A CN 202111109303 A CN202111109303 A CN 202111109303A CN 113786359 A CN113786359 A CN 113786359A
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pipe
plate
tank
water
distillation
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CN113786359B (en
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王蕾
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Zhejiang Jing Hui Cosmetics Co ltd
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Individual
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/35Ketones, e.g. benzophenone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00Formulations or additives for perfume preparations
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/022Refining
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/027Recovery of volatiles by distillation or stripping
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Emergency Medicine (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses a perfume containing plant natural components, which comprises the following components: 15-55% of plant essential oil, 5-20% of essence and 30-60% of alcohol, wherein the plant essential oil comprises the following components: 5-7 parts of lavender, 3-4 parts of mint, 2-3 parts of wormwood, 2-3 parts of camphor, 4-6 parts of jasmine flower, 4-5 parts of clove and 4-7 parts of tea leaves, and compared with the prior art, the invention has the following beneficial effects: through the mixed processing of various plants, the health of the perfume is improved, the harm to a human body is avoided, meanwhile, through the mutual matching of the lavender, the mint and the camphor, the mosquito repelling effect of the perfume is improved, the refreshing effect and the consciousness restoring effect can be realized, the effect of the perfume is increased, and through the jasmine and the clove, the fragrance of the perfume is improved.

Description

Perfume containing plant natural components and preparation method thereof
Technical Field
The invention relates to the technical field of perfume preparation, in particular to perfume containing plant natural components and a preparation method thereof.
Background
The perfume is an alcohol solution of essence, and is added with a proper amount of fragrance fixing agent and the like, so that the perfume has aromatic and strong fragrance, has the main function of being sprayed on parts such as lappets, handkerchiefs, hairlines and the like to emit pleasant fragrance, and is one of important cosmetics;
however, in the existing preparation process, the plant essential oil cannot be effectively extracted from the plant, so that part of the plant essential oil is remained, and meanwhile, in the preparation process, the energy cannot be repeatedly utilized, so that the resource waste is caused, so that for the situations, in order to avoid the technical problems, the perfume containing the plant natural components and the preparation method thereof are necessary to overcome the defects in the prior art.
Disclosure of Invention
The invention provides perfume containing plant natural components and a preparation method thereof, which can effectively solve the problems that the plant essential oil cannot be effectively extracted from plants in the background art, so that part of the plant essential oil is remained, and simultaneously, energy cannot be repeatedly utilized in the preparation process, so that the resource is wasted.
In order to achieve the purpose, the invention provides the following technical scheme: a perfume containing plant natural components and its preparation method comprise the following steps;
s1, pouring the materials into a crusher at the top end of the placing rack for crushing, feeding the crushed materials into a distillation retort through a feeding pipe for distillation, and sealing the feeding pipe through a sealing ball to avoid hot gas leakage;
s2, heating water in the evaporation tank through the heating plate to generate steam, sending the steam into the distillation tank through the conveying pipe to distill the material, cooling and liquefying the material through the cooling tank, sending the liquefied material into the centrifuge to separate and discharge the material, sending the discharged waste liquid into the distillation cylinder through the return pipe to distill the waste liquid, and sending the waste liquid into the storage cylinder through the two condensation pipes;
s4, feeding water with high temperature in the cooling tank into the evaporation tank through the water outlet pipe, and feeding water in the water tank into the cooling pipe through the water feeding pipe to replace the water in the cooling tank, so as to ensure the heat exchange effect;
s5, the adjusting rod is driven to rotate by rotating the turntable, so that the bottom cover is conveniently driven to descend, and the materials on the grid plate are conveniently cleaned;
s6, mixing the prepared plant essential oil with essence and alcohol, stirring uniformly, aging, sterilizing, filtering the prepared perfume, mixing colors, inspecting and packaging.
Further, the perfume containing the plant natural ingredients comprises the following components:
15-55% of plant essential oil, 5-20% of essence and 30-60% of alcohol;
the plant essential oil comprises the following components:
5-7 parts of lavender, 3-4 parts of mint, 2-3 parts of wormwood, 2-3 parts of camphor, 4-6 parts of jasmine flower, 4-5 parts of clove and 4-7 parts of tea leaves.
Compared with the prior art, the invention has the beneficial effects that: the invention has scientific and reasonable structure and safe and convenient use:
1. the high-efficiency distillation and energy utilization mechanism is arranged, the water in the evaporation tank is heated by the heating plate to generate steam, then the steam is sent into the distillation retort to carry out steam distillation on the material on the grid plate by the matching of the fixed cylinder and the delivery pipe, the distillation effect is improved, the steam is sent into the upper leakage box and the condensation pipe through the connecting pipe, the steam in the condensing pipe is cooled and liquefied by the water in the cooling tank and is discharged into a centrifuge for oil-water separation, meanwhile, the vertical rod of the rotating motor rotates, and the rotating wheel is matched with the driving belt to drive the rotating rod and the stirring blade to rotate, materials in the distillation tank are stirred, so that the distillation effect is further improved, the rotary vane is pushed to rotate in the steam rising process, the rotating efficiency of the rotary rod and the rotary vane is further improved, and the energy consumption of a rotary motor is reduced;
in the heat exchange process, the water temperature in the cooling tank rises, and when the temperature rises to a set temperature, the electromagnetic valve is started through the temperature sensor, so that the water with the temperature in the cooling tank is sent into the evaporation tank for secondary utilization, the water temperature in the evaporation tank is improved, and the evaporation efficiency of the water is increased;
through back flow and water pump cooperation, send into the waste liquid inside the retort to at the in-process of evaporating pot evaporating water, heat the distillation to the inside waste liquid of retort, make the waste liquid evaporate, and through the liquefaction of second condenser pipe with steam discharge, then store inside the holding vessel, and then extract the crude oil from the waste liquid, improved the utilization effect to the resource.
2. The convenient water replenishing mechanism is arranged, when the water level in the cooling tank is lowered to the minimum, the floating ring is lowered to drive the movable rod, the connecting plate, the vertical plate and the inclined plate to slide, so that the push block and the push rod are pushed to move, the sealing plate is separated from the water adding pipe, water in the water tank conveniently enters the cooling tank through the water adding pipe, the water in the cooling tank is replaced, the subsequent cooling effect is ensured, when the water level in the cooling tank is raised to the maximum, the other movable rod, the connecting plate, the vertical plate and the inclined plate are pushed to reset, then the push rod, the lantern ring and the sealing plate are pushed to reset through the telescopic characteristic of the reset spring, the water adding pipe is sealed again, water supply is stopped, water overflow in the cooling tank is avoided, and resource waste is avoided;
in addition, at the in-process that the riser removed, through the flexible characteristic of tensioning spring, promote slide bar and fixture block and remove, make inside fixture block one end embedding fixed plate to spacing to carrying on the riser, avoiding the riser to slide, in addition at watered in-process, through the flexible characteristic of supporting spring, promote the gag lever post, make the gag lever post slide along the vertical section of thick bamboo, adjusted the position of clamp plate, increased the inside pressure of water tank, improved the effect of drainage.
3. The convenient feeding mechanism is arranged, the crushing roller is driven by the driving motor to rotate to crush the materials in the crusher, so that the materials fall into the feeding pipe, the distillation of the materials is facilitated, meanwhile, in the crushing process, the power is transmitted through the matching of the driving wheel and the belt to drive the rotating rod and the spiral material plate to rotate and convey the materials, in addition, in the rotating rod rotating and pushing process, the positioning ring is driven to rotate, the fixing ring, the transverse rod and the sealing ball are pushed to move through the matching of the arc-shaped plates, the sealing of the feeding pipe is relieved, the materials are conveniently fed into the distillation retort to be distilled, and the convenience of feeding is improved,
in addition, through the characteristic of stretch cord shrink, pulling horizontal pole and ball sealer reset, seal up the inlet pipe again, avoid the inside steam of retort to disperse outward, after the distillation is accomplished, through rotating the carousel, make the carousel drive the regulation pole rotatory, pulling bottom, bracing piece and grid plate descend, make grid plate roll-off retort inside, be convenient for clear up the material on the grid plate, improved the convenience of clearance, guaranteed the inside clean and tidy nature of retort.
4. The mixed processing through various plants is arranged, the health of the perfume is improved, harm to a human body is avoided, meanwhile, through the mutual matching of the lavender, the mint and the camphor, the mosquito repelling effect of the perfume is improved, the refreshing effect and the consciousness restoring effect can be achieved, the effect of the perfume is increased, and through the jasmine and the clove, the fragrance of the perfume is improved.
Synthesize, carry out reasonable utilization to the energy through high-efficient distillation and energy utilization mechanism, improve the distillation effect to the material, increased the oil yield, shortened the time of distillation preparation, can carry out recovery processing to the waste liquid simultaneously, prepare out crude oil, avoid the wasting of resources, conveniently change the inside water of cooling tank through convenient moisturizing mechanism in addition to guaranteed refrigerated effect, made things convenient for the steam liquefaction, improved the efficiency of preparation.
Drawings
The accompanying drawings, which are included to provide a further understanding of the invention and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the principles of the invention and not to limit the invention.
In the drawings:
FIG. 1 is a flow chart of the process for preparing the perfume of the present invention;
FIG. 2 is a schematic view of the mounting structure of the spacer of the present invention;
FIG. 3 is a schematic view of the installation structure of the water outlet pipe of the present invention;
FIG. 4 is a schematic structural diagram of the high efficiency distillation and energy utilization mechanism of the present invention;
FIG. 5 is a schematic view of the mounting structure of the turntable of the present invention;
FIG. 6 is a schematic view of the mounting structure of the platen of the present invention;
FIG. 7 is a schematic structural view of a convenient water replenishment mechanism of the present invention;
fig. 8 is a schematic structural view of the convenient feeding mechanism of the present invention.
Reference numbers in the figures: 1. placing a rack; 2. cushion blocks; 3. a breaker; 4. a water tank;
5. a high-efficiency distillation and energy utilization mechanism; 501. an evaporator tank; 502. heating plates; 503. a distillation tank; 504. a fixed cylinder; 505. a delivery pipe; 506. a rotating rod; 507. rotating leaves; 508. stirring blades; 509. a cooling tank; 510. an upper leakage box; 511. a connecting pipe; 512. a lower leakage box; 513. a condenser tube; 514. a centrifuge; 515. a rotating electric machine; 516. a vertical rod; 517. a rotating wheel; 518. a transmission belt; 519. a water outlet pipe; 520. an electromagnetic valve; 521. a temperature sensor; 522. a return pipe; 523. a water pump; 524. a distillation column; 525. a second condenser pipe; 526. a storage cylinder; 527. an oil outlet pipe;
6. a convenient water supplementing mechanism; 601. a limiting plate; 602. a floating ring; 603. a sleeve; 604. a movable rod; 605. a connecting plate; 606. a vertical plate; 607. a sloping plate; 608. a transverse plate; 609. a slide bar; 610. a clamping block; 611. tensioning the spring; 612. a fixing plate; 613. a limiting groove; 614. a water feeding pipe; 615. a collar; 616. an extension plate; 617. a push block; 618. a push rod; 619. a return spring; 620. a sealing plate; 621. pressing a plate; 622. fixing the rod; 623. a vertical cylinder; 624. a support spring;
7. a convenient feeding mechanism; 701. a feed pipe; 702. rotating the rod; 703. a spiral material plate; 704. a driving wheel; 705. a belt; 706. a drive motor; 707. a crushing roller; 708. a groove is embedded; 709. a cross bar; 710. a fixing ring; 711. a positioning ring; 712. an arc-shaped plate; 713. an elastic cord; 714. a sealing ball; 715. a bump; 716. a limiting rod; 717. a support; 718. adjusting a rod; 719. a turntable; 720. a bottom cover; 721. a support bar; 722. a grid plate.
Detailed Description
The preferred embodiments of the present invention will be described in conjunction with the accompanying drawings, and it will be understood that they are described herein for the purpose of illustration and explanation and not limitation.
Example (b): as shown in figure 1, the invention provides a technical scheme, a method for preparing perfume containing plant natural ingredients, which comprises the following steps;
s1, pouring the materials into the crusher 3 at the top end of the placing rack 1 for crushing, feeding the crushed materials into the distillation retort 503 through the feeding pipe 701 for distillation, and sealing the feeding pipe 701 through the sealing ball 714 to avoid hot gas leakage;
s2, heating the water in the evaporator 501 by the heating plate 502 to generate steam, sending the steam into the distillation tank 503 through the delivery pipe 505 to distill the material, cooling and liquefying by the cooling tank 509, sending into the centrifuge 514 to separate and discharge, sending the discharged waste liquid into the distillation cylinder 524 through the return pipe 522 to distill the waste liquid, and sending into the storage cylinder 526 through the secondary condenser 525;
s3, sending water with higher temperature in the cooling tank 509 into the evaporation tank 501 through the water outlet pipe 519, sending water in the water tank 4 into the cooling pipe 509 through the water feeding pipe 614, replacing the water in the cooling tank 509, and ensuring the heat exchange effect;
s4, the adjusting rod 718 is driven to rotate through the rotating turntable 719, so that the bottom cover 720 is conveniently driven to descend, and materials on the grid plate 722 are conveniently cleaned;
s5, mixing the prepared plant essential oil with essence and alcohol, stirring uniformly, aging, sterilizing, filtering the prepared perfume, mixing colors, inspecting and packaging.
A perfume containing plant natural components comprises the following components:
30% of plant essential oil, 15% of essence and 55% of alcohol;
the plant essential oil comprises the following components:
7 parts of lavender, 3 parts of mint, 3 parts of wormwood, 2 parts of camphor, 6 parts of jasmine flower, 4 parts of clove and 5 parts of tea leaves.
As shown in fig. 2-8, a cushion block 2 is fixedly connected to one side of the top end of a placing rack 1 through bolts, a crusher 3 is installed at the top end of the cushion block 2, a water tank 4 is connected to one end of the placing rack 1, a high-efficiency distillation and energy utilization mechanism 5 is arranged at the top end of the placing rack 1, and the high-efficiency distillation and energy utilization mechanism 5 comprises an evaporation tank 501, a heating plate 502, a distillation tank 503, a fixed cylinder 504, a delivery pipe 505, a rotating rod 506, a rotating blade 507, a stirring blade 508, a cooling tank 509, an upper leakage box 510, a connecting pipe 511, a lower leakage box 512, a condensing pipe 513, a centrifuge 514, a rotating motor 515, a vertical rod 516, a rotating wheel 517, a transmission belt 518, a water outlet pipe 519, an electromagnetic valve 520, a temperature sensor 521, a return pipe 522, a water pump 523, a distillation cylinder 524, a second condensing pipe 525, a storage cylinder 526 and an oil outlet pipe 527;
the top end of the placing frame 1 is connected with an evaporating pot 501 in a clamping manner, heating plates 502 are arranged in the evaporating pot 501 at equal intervals, a distillation pot 503 is connected to the position, corresponding to one side of the evaporating pot 501, of the top end of the placing frame 1 in a clamping manner, fixed cylinders 504 are respectively welded to the top ends of the evaporating pot 501 and the distillation pot 503, a conveying pipe 505 is welded to the outer side of the fixed cylinder 504 positioned at the top of the evaporating pot 501 in a welding manner, rotating rods 506 are respectively connected to the top ends of the two fixed cylinders 504 in a rotating manner, rotating blades 507 are welded to the outer sides of the two rotating rods 506 at equal intervals corresponding to the positions in the fixed cylinders 504, and stirring blades 508 are welded to the outer side of one rotating rod 506 at equal intervals corresponding to the position in the distillation pot 503;
a cooling tank 509 is clamped at the position, corresponding to one side of the distillation tank 503, of the top end of the placing frame 1, an upper leakage box 510 is clamped at the top end of the cooling tank 509, a connecting pipe 511 is connected at the position, corresponding to one side of the top end of the upper leakage box 510, the other end of the connecting pipe 511 is connected with the outer side of the fixed cylinder 504 at the top end of the distillation tank 503, a lower leakage box 512 is clamped at the bottom end of the cooling tank 509, condenser pipes 513 are welded between the upper leakage box 510 and the lower leakage box 512 at equal intervals, a centrifuge 514 is installed at the bottom end of the lower leakage box 512 corresponding to the bottom of the placing frame 1, the bottom end of the centrifuge 514 is fixedly connected with a rotating motor 515 through bolts, a vertical rod 516 is cast at the top end of an output shaft of the rotating motor 515, rotating wheels 517 with different sizes are fixedly connected at the top ends of the vertical rod 516 and the rotating rod 506, a driving belt 518 is sleeved outside the rotating wheels 517, for utilizing heat energy, the other end of the conveying pipe 505 is connected with one end of the distillation tank 503, the rotating directions of the two rotating blades 507 are the same, the diameter of the rotating wheel 517 positioned in the middle of the transmission belt 518 is larger than that of the other two rotating wheels 517, one end of the cooling tank 509 is welded with a water outlet pipe 519, the other end of the water outlet pipe 519 is connected with one end of the water tank 4, an electromagnetic valve 520 is installed on the outer side of the water outlet pipe 519, and a temperature sensor 521 is installed on the inner wall of the cooling tank 509;
centrifuge 514 outside one end welding has the back flow 522, water pump 523 is installed to the back flow 522 outside, the back flow 522 other end corresponds the inside position department butt fusion of evaporating pot 501 and has a distillation column 524, distillation column 524 top welding has a second condenser pipe 525, the second condenser pipe 525 other end butt fusion has a storage cylinder 526, centrifuge 514 outside other end welding has an oil pipe 527, in order to discharge hot water, second condenser pipe 525 one end runs through evaporating pot 501 one end, the storage cylinder 526 outside welding has the discharge pipe, hot plate 502, rotating electrical machines 515, temperature sensor 521 and water pump 523 all supply power through external power supply, temperature sensor 521's signal output part is connected with solenoid valve 520 input;
a convenient water replenishing mechanism 6 is arranged between the cooling tank 509 and the water tank 4, and the convenient water replenishing mechanism 6 comprises a limiting plate 601, a floating ring 602, a sleeve 603, a movable rod 604, a connecting plate 605, a vertical plate 606, an inclined plate 607, a transverse plate 608, a sliding rod 609, a clamping block 610, a tensioning spring 611, a fixing plate 612, a limiting groove 613, a water replenishing pipe 614, a lantern ring 615, an extension plate 616, a push block 617, a push rod 618, a return spring 619, a sealing plate 620, a pressing plate 621, a fixing rod 622, a vertical cylinder 623 and a supporting spring 624;
the inner wall of the cooling tank 509 is symmetrically welded with limiting plates 601, a floating ring 602 is slidably connected between the two limiting plates 601 corresponding to the inner position of the cooling tank 509, sleeves 603 are respectively welded at the top and bottom positions of the inner wall of the cooling tank 509, movable rods 604 are respectively movably connected inside the two sleeves 603, connecting plates 605 are respectively welded at the opposite ends of the two movable rods 604, in order to facilitate the movement of the stacked movable rods 604, a groove is formed at the position corresponding to one side of the limiting plate 601 outside the floating ring 602, a cavity is formed inside the floating ring 602, a sealing ring is sleeved at the connection part of the movable rods 604 and the cooling tank 509, risers 606 are respectively and symmetrically welded at one end of the two connecting plates 605, inclined plates 607 are respectively welded at one ends of the two risers 606, transverse plates 608 are respectively clamped at the adjacent ends of the two risers 606, a slide bar 609 is symmetrically and movably connected at one end of the transverse plates 608, a clamping block 610 is welded at the position corresponding to one side of the transverse plates 608, a tensioning spring 611 is sleeved at the position, corresponding to the other side of the transverse plate 608, of the outer side of the sliding rod 609, a fixing plate 612 is fixedly connected at the position, corresponding to one side of the vertical plate 606, of the outer side of the cooling tank 509 through bolts, and limiting grooves 613 are formed at positions, corresponding to one side of the clamping block 610, of one end of the fixing plate 612 at equal intervals;
a water feeding pipe 614 is welded between the cooling tank 509 and the water tank 4, a sleeve ring 615 is movably sleeved on the outer side of the water feeding pipe 614, extension plates 616 are welded on the top end and the bottom end of the sleeve ring 615, push blocks 617 are symmetrically welded on one end of the extension plates 616, push rods 618 are equidistantly cast on the other end of the sleeve ring 615, a reset spring 619 is sleeved on the outer side of the push rod 618 in a position corresponding to the outer side of the water tank 4, a sealing plate 620 is cast on one end of the push rod 618 in a position corresponding to the inner part of the water tank 4, in order to limit the vertical plate 606, one end of a fixture block 610 is embedded into a limiting groove 613, the inclined angle of the inclined plane of the inclined plate 607 is equal to that of the push block 617, and the outer diameter of the sealing plate 620 is larger than the inner diameter of the water feeding pipe 614;
a pressing plate 621 is movably connected to the inner wall of the water tank 4, fixing rods 622 are respectively welded to the corners of the top end of the pressing plate 621, a vertical cylinder 623 is movably connected to the top end of each fixing rod 622, the top end of each vertical cylinder 623 is connected with the top end of the water tank 4, and a supporting spring 624 is welded to the middle of the top end of the pressing plate 621;
the convenient feeding mechanism 7 is arranged at the position, corresponding to the bottom of the crusher 3, outside the distillation tank 503, and comprises a feeding pipe 701, a rotating rod 702, a spiral material plate 703, a transmission wheel 704, a belt 705, a driving motor 706, a crushing roller 707, an embedded groove 708, a cross bar 709, a fixing ring 710, a positioning ring 711, an arc-shaped plate 712, an elastic rope 713, a sealing ball 714, a bump 715, a limiting rod 716, a support 717, an adjusting rod 718, a rotary disc 719, a bottom cover 720, a supporting rod 721 and a grating plate 722;
a feeding pipe 701 is welded at the position, corresponding to the bottom of the crusher 3, on the outer side of the distillation tank 503, a rotating rod 702 is rotatably connected inside the feeding pipe 701, a spiral material plate 703 is welded on the outer side of the rotating rod 702, driving wheels 704 are rotatably connected at one end of the crusher 3 and one end of the feeding pipe 701, belts 705 are sleeved on the outer sides of the two driving wheels 704, a driving motor 706 is fixedly connected at one end of the crusher 3 through bolts, and a crushing roller 707 is welded at the position, corresponding to the inner position of the crusher 3, of an output shaft of the driving motor 706;
an embedded groove 708 is formed in one end of the rotating rod 702, a cross rod 709 is movably connected to the inner wall of the embedded groove 708, a fixing ring 710 is fixedly sleeved on the outer side of the cross rod 709, a positioning ring 711 is welded to the inner wall of the embedded groove 708 corresponding to the inner side of the fixing ring 710, an arc plate 712 is welded to the adjacent end of the positioning ring 711 and the fixing ring 710 at equal distance, an elastic rope 713 is rotated to the end of the cross rod 709 corresponding to the inner position of the embedded groove 708, a sealing ball 714 is welded to the other end of the cross rod 709 corresponding to the inner position of the distillation retort 503, a bump 715 is symmetrically welded to the outer side of the sealing ball 714 corresponding to the inner position of the distillation retort 503, and a limiting rod 716 is symmetrically welded to one end of the bump 715;
the welding of the corresponding rack 1 bottom position department in the retort 503 outside has support 717, there is regulation pole 718 support 717 bottom through threaded connection, and it has carousel 719 to adjust pole 718 bottom melt, it is connected with bottom 720 to adjust the rotation of pole 718 top, the welding of bottom 720 top equidistance has bracing piece 721, the bracing piece 721 top corresponds the welding of retort 503 inside position department has grid plate 722, for the convenience carry the material, inlet pipe 701 one end is run through to dwang 702 one end and is connected with drive wheel 704 one end, crushing roller 707 one end is run through breaker 3 and is connected with drive wheel 704 one end, driving motor 706 supplies power through external power source, the stretch cord 713 other end is connected with embedded groove 708 inner wall.
The working principle and the using process of the invention are as follows: firstly, materials are put into a crusher 3, a driving motor 706 drives a crushing roller 707 to rotate to crush the materials in the crusher 3, so that the materials fall into a feeding pipe 701, meanwhile, in the process of crushing the materials, power is transmitted through the matching of a driving wheel 704 and a belt 705, a rotating rod 702 and a spiral material plate 703 are driven to rotate to convey the materials in the feeding pipe 701, in addition, in the process of rotating and pushing the materials through the rotating rod 702, a positioning ring 711 is driven to rotate, a fixing ring 710, a cross rod 709 and a sealing ball 714 are pushed to move through the matching of an arc-shaped plate 712, the sealing of the feeding pipe 701 is released, the materials are conveniently fed into a distillation tank 503 to be distilled, in addition, through the characteristic of contraction of an elastic rope 713, the cross rod 709 and the sealing ball 714 are pulled to reset, the feeding pipe 701 is sealed again, and the hot gas in the distillation tank 503 is prevented from being scattered outside, meanwhile, the matching of the bump 715 and the limiting rod 716 can limit the position of the sealing ball 714, so that the rotation of the sealing ball 714 is avoided, and the moving effect of the sealing ball 714 is ensured;
then, the water in the evaporation tank 501 is heated by the heating plate 502 to generate steam, then the steam is sent into the distillation tank 503 to distill the material on the grid plate 722 through the matching of the fixed cylinder 504 and the conveying pipe 505, the steam with the plant essential oil in the material is sent into the upper leakage box 510 and the condensation pipe 513 through the connecting pipe 511, meanwhile, the steam in the condensation pipe 513 is cooled through the water in the cooling tank 509 to improve the liquefaction efficiency, the liquefied liquid flows into the centrifuge 514 through the lower leakage box 512, the rotating motor 515 rotates with the liquid in the centrifuge 514 to centrifugally separate the liquid, and then the liquid is discharged through the oil outlet pipe 527;
in addition, the vertical rod 516, the rotating wheel 517 and the transmission belt 518 are matched to drive the rotating rod 506 and the stirring blade 508 to rotate, so that materials in the distillation tank 503 are stirred, the distillation effect is further improved, the rotating blade 507 is pushed to rotate in the steam rising process, the rotating efficiency of the rotating rod 506 and the stirring blade 508 is further improved, and the energy consumption of the rotating motor 515 is reduced;
then, the waste liquid is sent into the distillation cylinder 524 through the cooperation of the return pipe 522 and the water pump 523, so that in the process of evaporating water by the evaporation tank 501, the waste liquid in the distillation cylinder 524 is heated and distilled to evaporate the waste liquid, the steam is discharged and liquefied through the second condensation pipe 525 and then stored in the storage cylinder 526, and further crude oil is extracted from the waste liquid, and the utilization effect of resources is improved;
then, the water in the cooling tank 509 is subjected to heat exchange to raise the temperature in the cooling tank 509, when the water temperature rises to a set temperature, the electromagnetic valve 520 is started to send the water in the cooling tank 509 into the evaporation tank 501 through the water outlet pipe 519, so that the waste of resources is avoided, the water is secondarily utilized, the water temperature in the evaporation tank 501 is improved, and the evaporation efficiency of the water is improved;
then, when the water level inside the cooling tank 509 is lowered to the minimum, the floating ring 602 is lowered, thereby pushing the movable rod 604 to be lowered, the vertical plate 606 and the inclined plate 607 are driven to slide by the matching of the connecting plate 605, the pushing block 617 and the pushing rod 618 are pushed to move, the sealing plate 620 is separated from the water feeding pipe 614, the water in the water tank 4 conveniently enters the cooling tank 509 through the water feeding pipe 614, the water inside the cooling tank 509 is replaced to ensure the subsequent cooling effect, and when the water level inside the cooling tank 509 rises to the maximum, the other movable rod 604 is pushed to rise, and then the vertical plate 606 and the inclined plate 607 are driven to reset through the matching of the connecting plate 605, meanwhile, by the telescopic characteristic of the reset spring 619, the push rod 618, the lantern ring 615 and the sealing plate 620 are pushed to reset, the water adding pipe 614 is sealed again, water supply is stopped, water in the cooling tank 509 is prevented from overflowing, and resource waste is avoided;
then, in the process of moving the vertical plate 606, the sliding rod 609 and the clamping block 610 are pushed to move by the telescopic characteristic of the tension spring 611, so that one end of the clamping block 610 is embedded into the fixing plate 612, the vertical plate 606 is limited, the vertical plate 606 is prevented from sliding, in addition, in the process of adding water, the limiting rod 716 is pushed by the telescopic characteristic of the support spring 624, the limiting rod 716 slides along the vertical cylinder 623, the position of the pressing plate 621 is adjusted, the pressure in the water tank 4 is increased, and the effect of draining water is improved;
finally, through rotating carousel 719, make carousel 719 drive the rotation of regulation pole 718, pulling bottom 720 descends to cooperation through bracing piece 721, pulling grid plate 722 descends, makes grid plate 722 roll-off retort 503 inside, thereby conveniently clears up the material on the grid plate 722, has improved the convenience of clearance, has guaranteed the inside clean and tidy nature of retort 503.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (10)

1. A preparation method of perfume containing plant natural components is characterized in that: comprises the following steps;
s1, pouring the materials into a crusher (3) at the top end of the placing rack (1) for crushing, feeding the crushed materials into a distillation tank (503) through a feeding pipe (701) for distillation, and sealing the feeding pipe (701) through a sealing ball (714) to avoid hot gas leakage;
s2, heating water in an evaporation tank (501) through a heating plate (502) to generate steam, sending the steam into a distillation tank (503) through a conveying pipe (505) to distill materials, cooling and liquefying through a cooling tank (509), sending the cooled and liquefied steam into a centrifuge (514) to be separated and discharged, sending the discharged waste liquid into a distillation cylinder (524) through a return pipe (522), distilling the waste liquid, and sending the waste liquid into a storage cylinder (526) through a secondary condensation pipe (525);
s4, sending water with higher temperature in the cooling tank (509) into the evaporation tank (501) through the water outlet pipe (519), sending water in the water tank (4) into the cooling pipe (509) through the water feeding pipe (614), and replacing the water in the cooling tank (509) to ensure the heat exchange effect;
s5, the adjusting rod (718) is driven to rotate through the rotating turntable (719), so that the bottom cover (720) is conveniently driven to descend, and materials on the grid plate (722) are conveniently cleaned;
s6, mixing the prepared plant essential oil with essence and alcohol, stirring uniformly, aging, sterilizing, filtering the prepared perfume, mixing colors, inspecting and packaging.
2. A perfume containing plant natural components is characterized in that: comprises the following components:
15-55% of plant essential oil, 5-20% of essence and 30-60% of alcohol;
the plant essential oil comprises the following components:
5-7 parts of lavender, 3-4 parts of mint, 2-3 parts of wormwood, 2-3 parts of camphor, 4-6 parts of jasmine flower, 4-5 parts of clove and 4-7 parts of tea leaves.
3. The method for preparing a perfume containing plant natural ingredients according to claim 1, wherein: rack (1) top one side position department is through bolt fixedly connected with cushion (2), breaker (3) are installed on cushion (2) top, rack (1) one end is connected with water tank (4), rack (1) top is provided with high-efficient distillation and energy utilization mechanism (5), high-efficient distillation and energy utilization mechanism (5) are including evaporating pot (501), hot plate (502), retort (503), solid fixed cylinder (504), conveyer pipe (505), bull stick (506), vane (507), stirring leaf (508), cooling tank (509), go up hourglass box (510), connecting pipe (511), leak box (512) down, condenser pipe (513), centrifuge (514), rotating electrical machines (515), montant (516), runner (517), drive belt (518), outlet pipe (519), solenoid valve (520), temperature sensor (521), A return pipe (522), a water pump (523), a distillation cylinder (524), a second condensation pipe (525), a storage cylinder (526) and an oil outlet pipe (527);
the top end of the placing frame (1) is connected with an evaporating pot (501) in a clamping mode, heating plates (502) are installed in the evaporating pot (501) at equal intervals, a distillation pot (503) is connected to the position, corresponding to one side of the evaporating pot (501), of the top end of the placing frame (1), fixing cylinders (504) are welded to the top ends of the evaporating pot (501) and the distillation pot (503), conveying pipes (505) are welded to the outer sides of the fixing cylinders (504) located at the top of the evaporating pot (501), rotating rods (506) are connected to the top ends of the two fixing cylinders (504) in a rotating mode, rotating blades (507) are welded to the positions, corresponding to the inner positions of the distillation pot (503), of the outer sides of the two rotating rods (506) at equal intervals, and stirring blades (508) are welded to the positions, corresponding to the inner positions of the distillation pot (503), of the outer sides of the rotating rods (506) at equal intervals;
the top end of the placing frame (1) is connected with a cooling tank (509) in a clamping manner corresponding to one side position of a distillation tank (503), the top end of the cooling tank (509) is connected with an upper leakage box (510), one side position of the top end of the upper leakage box (510) is connected with a connecting pipe (511), the other end of the connecting pipe (511) is connected with the outer side of a fixed cylinder (504) at the top end of the distillation tank (503), a lower leakage box (512) is connected with the bottom end of the cooling tank (509) in a clamping manner, a condensing pipe (513) is welded between the upper leakage box (510) and the lower leakage box (512) at equal distance, a centrifuge (514) is installed at the bottom end of the lower leakage box (512) corresponding to the bottom position of the placing frame (1), the bottom end of the centrifuge (514) is fixedly connected with a rotating motor (515) through bolts, the top end of the rotating motor (515) is provided with a vertical rod (516), the top ends of the vertical rod (516) and the rotating rod (506) are fixedly connected with rotating wheels (517) with different sizes, a transmission belt (518) is sleeved on the outer side of the rotating wheel (517), a water outlet pipe (519) is welded at one end of the cooling tank (509), the other end of the water outlet pipe (519) is connected with one end of the water tank (4), an electromagnetic valve (520) is installed on the outer side of the water outlet pipe (519), and a temperature sensor (521) is installed on the inner wall of the cooling tank (509);
centrifuge (514) outside one end welding has back flow (522), water pump (523) are installed in back flow (522) outside, the back flow (522) other end corresponds evaporating pot (501) inside position department butt fusion and has distillation column (524), distillation column (524) top welding has second condenser pipe (525), second condenser pipe (525) other end fusion has storage cylinder (526), centrifuge (514) outside other end welding has oil outlet pipe (527).
4. The method for preparing a perfume containing plant natural ingredients according to claim 3, wherein: the other end of the conveying pipe (505) is connected with one end of the distillation tank (503), the rotating directions of the two rotary vanes (507) are the same, and the diameter of the rotary wheel (517) positioned at the middle position of the transmission belt (518) is larger than the diameter of the other two rotary wheels (517).
5. The method for preparing a perfume containing plant natural ingredients according to claim 3, wherein: evaporating pot (501) one end is run through to second condenser pipe (525) one end, the welding of storage cylinder (526) outside has the discharge pipe, hot plate (502), rotating electrical machines (515), temperature sensor (521) and water pump (523) all supply power through external power source, the signal output part of temperature sensor (521) is connected with solenoid valve (520) input.
6. The method for preparing a perfume containing plant natural ingredients according to claim 3, wherein: a convenient water supplementing mechanism (6) is arranged between the cooling tank (509) and the water tank (4), and the convenient water supplementing mechanism (6) comprises a limiting plate (601), a floating ring (602), a sleeve (603), a movable rod (604), a connecting plate (605), a vertical plate (606), an inclined plate (607), a transverse plate (608), a sliding rod (609), a clamping block (610), a tensioning spring (611), a fixing plate (612), a limiting groove (613), a water adding pipe (614), a lantern ring (615), an extension plate (616), a push block (617), a push rod (618), a return spring (619), a sealing plate (620), a pressure plate (621), a fixing rod (622), a vertical cylinder (623) and a supporting spring (624);
limiting plates (601) are symmetrically welded on the inner wall of the cooling tank (509), floating rings (602) are connected between the two limiting plates (601) in a sliding manner and correspond to the inner position of the cooling tank (509), sleeves (603) are respectively welded at the top and the bottom of the inner wall of the cooling tank (509), movable rods (604) are respectively movably connected inside the two sleeves (603), connecting plates (605) are respectively welded at the opposite ends of the two movable rods (604), vertical plates (606) are respectively and symmetrically welded at one ends of the two connecting plates (605), inclined plates (607) are respectively welded at one ends of the two vertical plates (606), transverse plates (608) are respectively and fixedly connected at the adjacent ends of the two vertical plates (606), sliding rods (609) are symmetrically and movably connected at one end of the transverse plates (608), clamping blocks (610) are respectively welded at the positions of the transverse plates (609) corresponding to one side of the transverse plates (608), and tensioning springs (611) are sleeved at the outer sides of the sliding rods (609) and correspond to the positions of the other sides of the transverse plates (608), a fixing plate (612) is fixedly connected to the position, corresponding to one side of the vertical plate (606), of the outer side of the cooling tank (509) through bolts, and limiting grooves (613) are formed in the position, corresponding to one side of the clamping block (610), of one end of the fixing plate (612) at equal intervals;
a water adding pipe (614) is welded between the cooling tank (509) and the water tank (4), a sleeve ring (615) is movably sleeved on the outer side of the water adding pipe (614), extension plates (616) are respectively welded at the top end and the bottom end of the sleeve ring (615), push blocks (617) are symmetrically welded at one end of each extension plate (616), push rods (618) are equidistantly cast at the other end of the sleeve ring (615), a reset spring (619) is sleeved at the position, corresponding to the outer side of the water tank (4), on the outer side of each push rod (618), and a sealing plate (620) is cast at the position, corresponding to the inner position of the water tank (4), at one end of each push rod (618);
water tank (4) inner wall swing joint has clamp plate (621), each corner position department on clamp plate (621) top all welds has dead lever (622), dead lever (622) top swing joint has a vertical cylinder (623), and vertical cylinder (623) top is connected with water tank (4) top, clamp plate (621) top middle part position department butt fusion has supporting spring (624).
7. The method for preparing a perfume containing plant natural ingredients according to claim 5, wherein: the position department that corresponds limiting plate (601) one side in the floating ring (602) outside sets up flutedly, the cavity has been seted up to floating ring (602) inside, the sealing washer has been cup jointed with the junction of cooling tank (509) in movable rod (604).
8. The method for preparing a perfume containing plant natural ingredients according to claim 5, wherein: one end of the clamping block (610) is embedded into the limiting groove (613), the inclined angle of the inclined plane of the inclined plate (607) is equal to that of the inclined plane of the push block (617), and the outer diameter of the sealing plate (620) is larger than the inner diameter of the water adding pipe (614).
9. The method for preparing a perfume containing plant natural ingredients according to claim 3, wherein: a convenient feeding mechanism (7) is arranged at the position, corresponding to the bottom of the crusher (3), on the outer side of the distillation tank (503), and the convenient feeding mechanism (7) comprises a feeding pipe (701), a rotating rod (702), a spiral material plate (703), a transmission wheel (704), a belt (705), a driving motor (706), a crushing roller (707), an embedded groove (708), a cross rod (709), a fixing ring (710), a positioning ring (711), an arc-shaped plate (712), an elastic rope (713), a sealing ball (714), a convex block (715), a limiting rod (716), a support (717), an adjusting rod (718), a turntable (719), a bottom cover (720), a supporting rod (721) and a grating plate (722);
the feeding pipe (701) is welded on the outer side of the distillation tank (503) corresponding to the bottom of the crusher (3), a rotating rod (702) is rotatably connected inside the feeding pipe (701), a spiral material plate (703) is welded on the outer side of the rotating rod (702), one end of the crusher (3) and one end of the feeding pipe (701) are rotatably connected with driving wheels (704), belts (705) are sleeved on the outer sides of the two driving wheels (704), one end of the crusher (3) is fixedly connected with a driving motor (706) through bolts, and a crushing roller (707) is welded on the output shaft of the driving motor (706) corresponding to the inner position of the crusher (3);
an embedded groove (708) is formed in one end of the rotating rod (702), a cross rod (709) is movably connected to the inner wall of the embedded groove (708), a fixing ring (710) is fixedly sleeved on the outer side of the cross rod (709), a positioning ring (711) is welded to the position, corresponding to the inner side of the fixing ring (710), of the inner wall of the embedded groove (708), an arc-shaped plate (712) is welded to the adjacent end of the positioning ring (711) and the fixing ring (710) at equal distance, an elastic rope (713) is rotated to the position, corresponding to the inner position of the embedded groove (708), of one end of the cross rod (709), a sealing ball (714) is welded to the position, corresponding to the inner position of the distillation tank (503), of the other end of the cross rod (709), a bump (715) is symmetrically welded to the position, corresponding to the inner position of the distillation tank (503), and one end of the bump (715) is symmetrically welded to the positioning rod (716);
the welding of retort (503) outside corresponding rack (1) bottom position department has support (717), there is regulation pole (718) support (717) bottom through threaded connection, and adjusts pole (718) bottom founding and have carousel (719), it is connected with bottom (720) to adjust pole (718) top rotation, bottom (720) top equidistance welding has bracing piece (721), bracing piece (721) top corresponds retort (503) internal position department butt fusion and has grid plate (722).
10. The method for preparing a perfume containing plant natural ingredients according to claim 9, wherein: dwang (802) one end is run through inlet pipe (801) one end and is connected with drive wheel (804) one end, crushing roller (806) one end is run through breaker (3) and is connected with drive wheel (804) one end, driving motor (805) are supplied power through external power source, stretch cord (813) other end is connected with embedded groove (808) inner wall.
CN202111109303.3A 2021-09-22 2021-09-22 Perfume containing natural plant components and preparation method thereof Active CN113786359B (en)

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