CN113749279A - Coffee-flavored refreshing cigarette oil and preparation method thereof - Google Patents

Coffee-flavored refreshing cigarette oil and preparation method thereof Download PDF

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Publication number
CN113749279A
CN113749279A CN202111229375.1A CN202111229375A CN113749279A CN 113749279 A CN113749279 A CN 113749279A CN 202111229375 A CN202111229375 A CN 202111229375A CN 113749279 A CN113749279 A CN 113749279A
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parts
powder
coffee
refreshing
oil
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杨继广
杨占文
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Qihuang Treasure Beijing Technology Co ltd
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Qihuang Treasure Beijing Technology Co ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/10Devices using liquid inhalable precursors
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40Constructional details, e.g. connection of cartridges and battery parts
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/70Manufacture

Abstract

The invention belongs to the technical field of Chinese herbal medicine electronic cigarette oil, and discloses coffee-flavored refreshing cigarette oil and a preparation method thereof. The tobacco tar is prepared from pure plant Chinese herbal medicines and does not contain any chemical raw materials and components. It is mainly pungent, bitter and slightly cold in nature, and enters spleen and lung meridians as the channels of the herbs. The sea-buckthorn can promote blood circulation and remove blood stasis; the dried ginger returns yang to dredge vessels; herba Cephalanoploris has effects of cooling blood and stopping bleeding; yuzhu can nourish yin and moisten dryness; rhodiola rosea strengthens spleen and tonifies qi; the black pepper warms the middle and dissipates qi; the chrysanthemum has the effects of clearing liver and improving vision; the cogongrass rhizome is used for cooling blood and stopping bleeding; cape jasmine fruit clears heat and promotes diuresis. The prescription has effects of invigorating spleen, invigorating qi, promoting blood circulation, dredging collaterals, promoting qi circulation, dispelling pathogenic wind heat, removing liver fire, and improving eyesight. The preparation method reduces the loss of effective components, and the extract is easy to store. And the product is purified again by distillation, so that the quality of the product is ensured. The coffee extract not only improves the using taste and the fragrance, but also is beneficial to refreshing the mind of a user and achieving the anti-fatigue effect because the coffee contains various alkaloids, and has safety and no uncomfortable feeling because the content belongs to a low dosage range.

Description

Coffee-flavored refreshing cigarette oil and preparation method thereof
Technical Field
The invention belongs to the technical field of Chinese herbal medicine electronic cigarette oil, and particularly relates to coffee-flavored refreshing cigarette oil and a preparation method thereof.
Background
In the current situation of the current commercial society, social workers under a modern working mechanism are under high-intensity and overload mental pressure and living pressure, the working time is up to ten hours every day, the workers sit on the internet in front of a computer screen to work, in addition, the environment and the air are polluted, most of the diets in the working period are fast foods, and in addition, the fast-paced life of the workers in the long years leads to that many caregivers are in poor immune function at a light age, so that the working and living pressure of many workers is very high, and most people form a smoking habit to be decompressed.
However, cigarettes contain a large amount of harmful substances such as nicotine and tar, and electronic cigarettes have become a widely known product to reduce the intake of harmful substances by smokers. The electronic cigarette has the same appearance, smoke, taste and sensation as a cigarette. The tobacco tar is a product which is absorbed by a user after components in the tobacco tar are changed into steam by means of atomization and the like.
At present, most of raw materials of the electronic cigarette are extracted from tobacco plants or other substances, and some raw materials are prepared by adopting a chemical synthesis method, so that the tobacco tar avoids the harm of tar generated when a common cigarette is burnt to a great extent when the electronic cigarette is used, or selectively avoids other harms of the tobacco, such as the intake of nicotine. However, the electronic cigarettes on the market are poor in taste, have single functions, contain chemical raw materials and other ingredients, and have strong influence on the physical functions of smokers.
However, people need to properly regulate themselves in daily life, and many health care products or beverages can promote people to achieve the aim of refreshing, but the products can treat symptoms and do not treat the root causes. The problem of unrealistic regulation of the body by using Chinese herbal medicines in daily life exists, and moreover, the Chinese herbal medicines are difficult to take and the taking environment is seriously limited. However, it is a new trend to combine the taste of coffee that people like with the Chinese herbal medicine with the functions of regulating body and refreshing brain.
Disclosure of Invention
In order to solve the problems in the prior art, the invention aims to provide coffee-flavored refreshing cigarette smoke oil and a preparation method thereof.
The technical scheme adopted by the invention is as follows: the coffee-flavored refreshing cigarette oil is characterized by being prepared from the following raw materials in parts by mass:
60-100 parts of coffee extract, 3-9 parts of sea buckthorn, 3-10 parts of dried ginger, 5-10 parts of common cephalanoplos herb, 6-12 parts of fragrant solomonseal rhizome, 6-12 parts of rhodiola rosea, 1-3 parts of black pepper, 5-9 parts of chrysanthemum, 10-30 parts of lalang grass rhizome, 5-10 parts of cape jasmine fruit and 70-120 parts of oil agent.
Coffee, name of traditional Chinese medicine. Is seed of Coffea arabica L, Coffea canephora Pierre ex Froehn, and Coffea canephora Bull ex Hien of Coffea of Rubiaceae. Has effects of refreshing mind, promoting urination, and invigorating stomach. It is mainly used for treating listlessness and anorexia. Slightly bitter and astringent taste, mild in nature. Chemical components: 1. and (3) small fruit coffee: the fruit contains alkaloids: caffeine, theobromine, theophylline. The seed contains sterol component: beta-sitosterol, stigmasterol, campesterol, cholesterol, 5-avenantrenol, 7-stigmasterol; fatty acid component: myristic acid, palmitic acid, stearic acid, oleic acid, linoleic acid, arachidic acid. The root, stem, leaf and seedling contain caffeine, theobromine, theophylline, 1, 7-dimethyl xanthine, scopoletin, p-hydroxybenzoic acid, vanillic acid, p-coumaric acid, ferulic acid, chlorogenic acid and caffeic acid. The leaf also contains ursolic acid. 2. Chinese fruit coffee: the fruit contains alkaloids: caffeine, theobromine, theophylline. Sterol component: beta-sitosterol, 24-methylene cycloartanol, 5-avenanthral-enol, etc. The seed also contains caffeic acid, ferulic acid, 3-O-4-O and 5-O-caffeoylquinic acid. 3. Big fruit coffee: the fruit contains caffeic acid. The leaf also contains 1, 3, 7, 9-tetramethyl uric acid, chaenomeles speciosa and methyl chaenomeles speciosa. The pharmacological action is as follows: 1. effects on the central nervous system: caffeine and its structural analog theophylline, which are the main active ingredients of coffee, have strong central excitation. But theophylline has stronger action and longer maintenance time than caffeine. The methylxanthine compounds such as caffeine and theophylline can increase the CO content in respiratory center2The sensitivity of (2). It also has an excitatory effect on the respiratory center, and the compounds may still cause nausea and vomiting, which are partly related to their central effects. The caffeine 85-250mg can be administered by people to improve the work ability of long-time mental laborStrong, the reaction time is shortened, but the working capacity involving delicate muscle coordination and accurate timing or calculation is reduced. Additional data indicate that such compounds are specific against the effects of opioid preparations, including analgesia. Intrathecal injection of caffeine in mouse dose not producing hyperalgesia (hyperalgesia) can increase ED of morphine analgesia50. Studies have shown that long-term caffeine intake can lead to tolerance and drug dependence. 2. Effect on the cardiovascular system: the administration of 250-350mg caffeine to a person who has never used such a drug results in a slight increase in heart rate and an increase in systolic and diastolic blood pressure. However, the dosage has no effect on patients who take caffeine for a long time. At high doses, both caffeine and theophylline can cause tachycardia. Sensitive patients may develop arrhythmias such as extra systoles. Caffeic acid intravenous injection can reduce blood pressure rise of normal rat caused by endothelin (ET-1), caffeic acid oral administration for a long time can reduce blood pressure of DOCA hypertension model rat, has obvious inhibiting effect on cardiac and vascular tissue hyperplasia, can reduce ET-1 concentration in blood plasma, and can reduce increase of C-fos and Heat Shock Protein (HSP)70mRNA gene expression caused by ET-1. 3. Effect on smooth muscle: the methylxanthine compound can relax various smooth muscles, the most important of which is the relaxation of the tracheal smooth muscle, and the effect is particularly obvious in the condition that the tracheal smooth muscle is contracted by using medicaments in clinical asthma and experiments. In addition, the compounds can also specifically resist the action of opioid on the gastrointestinal tract. 4. Other functions are as follows: caffeine has the effect of enhancing the working capacity of human skeletal muscles and also increases the twitch tension of cats indirectly stimulating the quadriceps. Prolonged coffee consumption can increase plasma cholesterol levels, but this is not due to caffeine and is related to other components contained in the coffee. Glutamate induces apoptosis of cerebellar granule neurons, caffeine antagonizes the effects of glutamate, its IC50The concentration was 50 mmol/L.
Sea buckthorn, the name of traditional Chinese medicine. Is dried mature fruit of Hippophae rhamnoides L. belonging to genus Hippophae of family Elaeagnaceae. Has the effects of invigorating spleen, promoting digestion, relieving cough, eliminating phlegm, promoting blood circulation and removing blood stasis. It is mainly indicated for spleen deficiency with poor appetite, cough with excessive phlegm and blood stasis. Sweet and sour in taste and warm in nature; it enters spleen, stomach and lung meridians. Chemical components: the product contains vitamins (C, VA, VE, VB1, VB2, VB12, VK) and folic acid; flavonoids and terpenoids; proteins and various amino acids; fats and fatty acids; a saccharide. In addition, the beverage also contains alkaloid, coumarin and acidic substances, and is rich in minerals and trace elements. The pharmacological action is as follows: the fructus Hippophae flavone has effects of improving myocardial microcirculation, reducing myocardial oxygen consumption, resisting angiosclerosis, and resisting inflammation; the oleum Hippophae and its fruit juice have antifatigue, blood lipid reducing, radioprotective, antiulcer, hepatoprotective, and immunity enhancing effects.
Dried ginger, named as traditional Chinese medicine. Is dried rhizome of Zingiber officinale Rosc. of Zingiberaceae. Has the effects of warming spleen and stomach for dispelling cold, restoring yang and dredging collaterals, and warming lung and resolving fluid retention. It can be used for treating abdominal psychroalgia, emesis, diarrhea, yang exhaustion, cough and asthma due to cold-fluid retention, and arthralgia due to cold-dampness. Pungent taste and hot property; it enters spleen, stomach, heart and lung meridians. Chemical components: contains volatile oil about 2%, and mainly contains zingiberene, phellandrene, camphene, zingiberone, gingerol, zingiberone, borneol, gingerol, citral, etc. It also contains resin, starch and amino acids. The pharmacological action is as follows: rhizoma Zingiberis has tranquilizing, analgesic, antiinflammatory, anticoagulant, anoxia resisting, and other effects, and has effects on cardiovascular function, adrenal cortex function, and digestive system. Toxicity of Zingiberis rhizoma is low, and its methanol extract is used as LD for subcutaneous injection in mice50It was 33.5g (crude drug)/kg. Zingiberis rhizoma ether extract mouse gavage LD50It was 16.3 ml/kg. Mouse intravenous injection LD extracted from ethanol of dried ginger50It was 2.08 g/kg. The book Jing: "controlling chest fullness, cough, adverse rising of qi, warming middle energizer, stopping bleeding, sweating, expelling wind-damp arthralgia, and diarrhea of intestine ". ".
Common cephalanoplos herb, named as traditional Chinese medicine. Is aerial part of MB. of Cirsium setosum (Wld.) belonging to genus Cirsium of family Compositae. Has effects of cooling blood, stopping bleeding, removing blood stasis, removing toxic substance, and resolving carbuncle. It can be used for treating hemorrhage due to blood heat, hematemesis, hematuria, metrorrhagia, and carbuncle, swelling, and sore due to excessive fire-heat toxin. Sweet and bitter taste and cool in nature; it enters heart and liver meridians. Chemical components: mainly contains alkaloid, flavone, triterpene and simple phenolic acid. Wherein the hemostatic active components include acacetin-7-rhamnoside, rutin, caffeic acid, chlorogenic acid, protocatechuic aldehyde, taraxasterol, etc. The pharmacological action is as follows: 1. effects on the blood system: herba Cephalanoploris has effects of contracting blood vessel, increasing platelet number, promoting platelet aggregation, increasing thrombin activity, and inhibiting fibrinolysis, thereby accelerating hemostasis. 2. Effects on the cardiovascular system: the herba Cirsii decoction has direct sympathomimetic effect. 3. Bacteriostasis: the herba Cephalanoploris decoction has certain inhibitory effect on white larynx bacillus, pneumococcus, hemolytic streptococcus, Staphylococcus aureus, Pseudomonas aeruginosa, proteus, Escherichia coli, typhoid bacillus, etc. 4. Anti-inflammatory action: animal experiments prove that the traditional Chinese medicine composition has a certain anti-inflammatory effect on the formaldehyde arthritis. 5. In addition, herba Cephalanoploris has certain effects of reducing blood lipid, promoting bile flow, promoting urination, tranquilizing, and inhibiting tumor.
Yuzhu, the name of Chinese medicine. Is rhizome of Dr uce (Polygonatum odoratum (Mill.) Dr uce) belonging to family Liliaceae, genus Polygonatum. Has effects in nourishing yin, moistening dryness, promoting salivation, and quenching thirst. It can be used for treating cough due to dryness-heat, thirst due to body fluid consumption, exogenous pathogenic factors due to yin deficiency, headache, and fever. Sweet in taste and neutral in nature; it enters lung and stomach meridians.
Rhodiola root, name of Chinese medicine. Is rhizome of rhodiola rosea Rholioa rosea limn. or rhodiola crenulata R.euryphylla (Frod.) S.H.Fu. of Crassulaceae. Has the effects of invigorating spleen, invigorating qi, clearing lung-heat, relieving cough, promoting blood circulation, and removing blood stasis. It is used for treating spleen qi deficiency syndrome, lung yin deficiency syndrome, and cough due to lung heat. Sweet taste and cold nature; it enters spleen and lung meridians. Chemical components: the product contains salidroside, benzhydryl piperidine, beta-sitosterol, etc. The pharmacological action is as follows: rhodiola rosea or salidroside has the effects of resisting fatigue, anoxia, cold and microwave radiation, improving work efficiency and mental activity, enhancing excitability of brainstem reticular system, enhancing response to light and electrical stimulation, and regulating the content of central nervous system medium to be normal. The rhodiola rosea can enhance the secretion function of thyroid, adrenal gland and ovary, improve the total protein content of muscle and the level of RNA, increase the number of hemoglobin and erythrocyte in blood, promote the normalization of oxidative metabolism index of loaded muscle, and resist tetanus toxin. Rhodiola rosea pair S180The sarcoma cell has inhibitory effect.
Black pepper, the name of traditional Chinese medicine. Is dried near-ripe fruit of Piper nigrum L. of Piper genus of Piperaceae family. Has effects of warming middle-jiao, dispelling qi, relieving pain, relieving diarrhea, stimulating appetite, and removing toxic substance. Can be used for treating stomach cold pain, emesis, anorexia, and food toxicity of fish. Pungent taste and hot property; it enters stomach and large intestine meridians. Chemical components: contains volatile oil, black pepper 1.2-2.6%, piperine A, piperine B, piperine C, and neopiperine. The pharmacological action is as follows: piperine can prolong sleep time of rat with pentobarbital, and resist convulsion of pentaerythrite or pentaerythrite actuator; the oral administration of the product can promote secretion of bile of rat; and has anti-inflammatory effect.
Chrysanthemum flower, name of traditional Chinese medicine. Is a dried capitula of Chrysanthemum morifolium Ramat. Has the effects of dispelling wind and heat, suppressing liver yang, removing liver heat, improving eyesight, and clearing away heat and toxic materials. It can be used for treating wind-heat type common cold, early stage of epidemic febrile disease, vertigo due to liver-yang, excessive liver-wind, conjunctival congestion, blurred vision, sore, carbuncle, and toxic swelling. Pungent, sweet and bitter in flavor, slightly cold in nature; it enters lung meridian. The product contains volatile oil including Borneolum, Camphora, and chrysanthenone, and optionally chrysanthemin, adenine, choline, flavone, stachydrine, vitamin A, and vitamin B1Vitamin E, amino acid, acacetin and the like. The chrysanthemum water infusion or decoction has certain antibacterial effect on staphylococcus aureus, various pathogenic bacilli and dermatophytes. The product also has inhibitory effect on influenza virus PR3 and leptospira. The flos Chrysanthemi preparation has effects of dilating coronary artery, increasing coronary blood flow, increasing myocardial oxygen consumption, lowering blood pressure, shortening blood coagulation time, relieving fever, resisting inflammation, and tranquilizing mind.
Lalang grass rhizome, name of traditional Chinese medicine. Is the rhizome of Imperata cylindrica Beauv.var.major (Nees) C.E.Hubb. of Imperata genus of Gramineae. Has effects of cooling blood, stopping bleeding, clearing heat, promoting urination, clearing lung-heat and stomach-heat. It can be used for treating hemorrhage due to blood heat, epistaxis, hemoptysis, hematuria, and stranguria with blood, stranguria due to toxic heat, edema, jaundice due to damp-heat, emesis due to stomach heat, and cough and asthma due to lung heat. Sweet in nature and cold in nature; it enters lung, stomach and bladder meridians. A saccharide-containing compound: glucose, sucrose, fructose, xylose, etc., and starch; simple acids and potassium salts: citric acid, malic acid, oxalic acid, and the like; a triterpene: imperatorin, arundol, fernitol, etc.; 5-hydroxytryptamine, and the like; other groupsCarotene, chlorophyll, vitamins, radix Pulsatillae, etc. 1. Effects on the blood nervous system: the cogongrass rhizome can obviously shorten bleeding and blood coagulation time and has the function of stopping bleeding. 2. The antibacterial effect is as follows: has inhibitory effect on pneumococcus, catacoccus, influenzae, Staphylococcus aureus, and Shigella flexneri and Song's dysentery bacillus, and has certain HBV virus resistance. 3. The diuretic effect is: the rhizoma imperatae decoction has the diuretic effect on experimental animals. The rhizoma imperatae decoction of 25g/kg is used for feeding the stomach of the rabbits, and the rabbits have bradykinesia and accelerated respiration after 36 hours, but the rabbits are recovered to be normal soon. LD (traditional Chinese medicine) prepared by performing intragastric administration on mice by adopting rhizoma imperatae decoction50More than 160 g/kg; LD of mice injected with refined water solution of cogongrass rhizome50The concentration of the mixed solution is 21.42 +/-1.09 g/kg.
Cape jasmine, the name of traditional Chinese medicine. Is dried mature fruit of Gardenia jasminoides Ellis of Gardenia genus of Rubiaceae family. Has the effects of purging fire, relieving restlessness, clearing heat, promoting diuresis, cooling blood and removing toxic substances. It can be used for treating vexation due to heat diseases, jaundice due to damp-heat, stranguria with blood, hematemesis, epistaxis, conjunctival congestion, swelling and pain, and pyocutaneous disease due to pathogenic fire. Bitter taste and cold nature; it enters heart, lung and triple energizer meridians. Chemical components: the product contains isogeniposide, geniposide, jasmone glycoside, fructus Gardeniae glycoside, geniposide, flavonoid genistein, triterpenes crocin, crocetin, ursolic acid, etc. The pharmacological action is as follows: 1. action on digestive system: fructus Gardeniae has effects in reducing serum bilirubin content, relieving liver injury caused by carbon tetrachloride, and promoting bile flow and eliminating jaundice. Gardenia and its extracts have obvious effects of benefiting pancreas, benefiting gallbladder and reducing pancreatic enzymes. Gardenia has the pharmacological effects of improving the disease resistance of the organism of a patient with pancreatitis, improving the functions of the liver and the gastrointestinal system, relieving pancreatitis and the like. The gardenia water extract and geniposide are orally or duodenally administered, and have obvious purgative effect on animals. 2. Effect on the cardiovascular system: the fructus Gardeniae extract has effects of reducing myocardial contraction force, lowering blood pressure, and resisting atherosclerosis. 3. The function of resisting pathogenic microorganisms: fructus Gardeniae has inhibitory effect on Staphylococcus aureus, Diplococcus meningitidis, and Catalpa. The fructus Gardeniae water extract has effect in inhibiting various dermatophytes in vitro. The decoction has effects of killing leptospira and adult schistosome. 4. Effects on the nervous system: the fructus Gardeniae alcohol extract has tranquilizing effect and no pain relieving effect. 5. In addition, the gardenia extract has certain anti-inflammatory and soft tissue injury treatment effects.
Preferably, the tobacco tar is mainly prepared from the following raw materials in parts by mass:
70-95 parts of coffee extract, 5-8 parts of sea buckthorn, 4-9 parts of dried ginger, 6-9 parts of common cephalanoplos herb, 8-11 parts of fragrant solomonseal rhizome, 8-11 parts of rhodiola root, 1.5-2.5 parts of black pepper, 6-8 parts of chrysanthemum, 11-25 parts of lalang grass rhizome, 6-9 parts of cape jasmine fruit and 80-110 parts of oil agent.
Preferably, the tobacco tar is mainly prepared from the following raw materials in parts by mass:
85 parts of coffee extract, 6 parts of sea buckthorn, 7 parts of dried ginger, 8 parts of common cephalanoplos herb, 10 parts of fragrant solomonseal rhizome, 10 parts of rhodiola rosea, 2 parts of black pepper, 7 parts of chrysanthemum, 15 parts of lalang grass rhizome, 8 parts of cape jasmine and 90 parts of oil agent.
Preferably, the oil agent comprises one or more of glycerol, 1, 2-propylene glycol, polyethylene glycol and tobacco leaf extract.
A preparation method of coffee flavor refreshing cigarette oil comprises the following steps:
selecting sea buckthorn, dried ginger, common cephalanoplos herb, fragrant solomonseal rhizome, rhodiola rosea, black pepper, chrysanthemum, lalang grass rhizome and gardenia according to corresponding proportion, drying, crushing and grinding to obtain standby substances of sea buckthorn powder, dried ginger powder, common cephalanoplos herb powder, fragrant solomonseal rhizome powder, rhodiola rosea powder, black pepper powder, chrysanthemum powder, cogongrass rhizome powder and gardenia powder, mixing uniformly, and adding a solvent to obtain an extract;
distilling the obtained extract, standing, and separating water and oil to obtain Chinese medicinal essential oil;
and (3) uniformly mixing the obtained traditional Chinese medicine essential oil, oil and coffee extract to obtain a finished product of the coffee-flavored refreshing cigarette smoke.
Preferably, the sea buckthorn, the dried ginger, the common cephalanoplos herb, the fragrant solomonseal rhizome, the rhodiola rosea, the black pepper, the chrysanthemum, the lalang grass rhizome and the gardenia are selected and dried at the temperature of 30-40 ℃.
Preferably, the drying time is 10 to 20 minutes.
Preferably, the particle sizes of the standby products of the obtained sea buckthorn powder, the dried ginger powder, the common cephalanoplos herb powder, the polygonatum powder, the rhodiola root powder, the black pepper powder, the chrysanthemum powder, the cogongrass rhizome powder and the gardenia powder are all 150-280-mesh sieve.
Preferably, the solvent comprises one or more of cyclohexane, alcohol and ethyl acetate.
Preferably, the mass ratio of the total mass of the standby sea-buckthorn powder, the dried ginger powder, the common cephalanoplos herb powder, the fragrant solomonseal rhizome powder, the rhodiola root powder, the black pepper powder, the chrysanthemum flower powder, the cogongrass rhizome powder and the gardenia powder to the solvent is 1: 0.3-0.5 wt%.
The invention has the beneficial effects that:
the invention provides coffee-flavored refreshing cigarette oil, which is prepared from pure plant Chinese herbal medicines and does not contain any chemical raw materials and components.
The tobacco tar is mainly pungent, bitter and slightly cold in nature, and enters spleen and lung meridians as the medicine channels. The sea buckthorn has the effects of strengthening spleen to promote digestion, relieving cough and eliminating phlegm, and activating blood circulation to dissipate blood stasis; the dried ginger has the effects of warming the middle-jiao to dispel cold, restoring yang to promote blood circulation and warming the lung to eliminate retained fluid; herba Cephalanoploris has effects of cooling blood, stopping bleeding, removing blood stasis, removing toxic substance, and resolving carbuncle; rhizoma Polygonati Odorati has effects of nourishing yin, moistening dryness, promoting fluid production, and quenching thirst; rhodiola rosea has the effects of strengthening spleen and replenishing qi, clearing lung and relieving cough, and activating blood and dissolving stasis; black pepper, have warm middle energizer and dispel qi, lower qi and relieve pain, stop diarrhea, stimulate appetite, efficacy of detoxication; the chrysanthemum has the effects of dispelling wind and heat, suppressing liver yang, clearing liver, improving eyesight, and clearing away heat and toxic materials; the cogongrass rhizome has the effects of cooling blood, stopping bleeding, clearing heat, promoting urination and clearing away lung-heat and stomach-heat; gardenia has the effects of purging fire, relieving restlessness, clearing heat, promoting diuresis, cooling blood and removing toxicity. The above formula is an integral formula, and the compatibility of the formula is helpful for invigorating spleen and replenishing qi, promoting blood circulation and dredging collaterals, promoting qi circulation and dispelling wind and heat, clearing liver and improving eyesight, and cooling blood and warming middle warmer.
In the preparation process of the tobacco tar, the raw materials are dried, ground and crushed, and then the solvent is purified to obtain the extract, so that the loss of effective components in the raw materials is reduced, the influence on the effective components in the raw material treatment process in the initial stage is avoided, and the extract is easy to store. And then, the effective components in the extract are further purified again in a distillation mode, so that the quality of the final product is effectively ensured, and a certain sterilization effect is achieved in the purification process. After the coffee extract is added, the using taste and the fragrance of the tobacco tar are improved, the coffee contains caffeine and various alkaloids, so that the tobacco tar is helpful for refreshing the mind of a user and achieves the anti-fatigue effect, and meanwhile, the content of the coffee extract is maximized within the low-dose edible range, so that the tobacco tar is safe and does not cause discomfort.
Detailed Description
The present invention is further illustrated below with reference to specific examples. It will be appreciated by those skilled in the art that the following examples, which are set forth to illustrate the present invention, are intended to be part of the present invention, but not to be construed as limiting the scope of the present invention. The reagents used are all conventional products which are commercially available.
Example 1:
a preparation method of coffee flavor refreshing cigarette oil comprises the following steps:
selecting 30 g of sea buckthorn, 30 g of dried ginger, 50 g of common cephalanoplos herb, 60g of fragrant solomonseal rhizome, 60g of rhodiola rosea, 10 g of black pepper, 50 g of chrysanthemum, 10 g of lalang grass rhizome and 50 g of cape jasmine fruit according to corresponding proportion, drying at 30 ℃ for 10 minutes, crushing, grinding, and screening by a 150-mesh screen sieve to obtain standby substances of sea buckthorn powder, dried ginger powder, common cephalanoplos herb powder, fragrant solomonseal rhizome powder, rhodiola rosea powder, black pepper powder, chrysanthemum powder, cogongrass rhizome powder and cape jasmine fruit powder, mixing uniformly, and adding 105 g of cyclohexane to obtain an extract;
distilling the obtained extract, standing, and separating water and oil to obtain Chinese medicinal essential oil;
and uniformly mixing the obtained traditional Chinese medicine essential oil, 70 g of glycerol and 60g of coffee extract to obtain a finished product of the coffee-flavored refreshing cigarette smoke.
The selected cyclohexane is used for dissolving active ingredients of medicines, the using amount of the cyclohexane meets the use standard required by the country, and the content of the final product is lower than the minimum using amount of LD50 of big and small mice.
Example 2:
a preparation method of coffee flavor refreshing cigarette oil comprises the following steps:
respectively selecting 90 g of sea buckthorn, 100 g of dried ginger, 100 g of common cephalanoplos herb, 120 g of fragrant solomonseal rhizome, 120 g of rhodiola rosea, 30 g of black pepper, 90 g of chrysanthemum, 30 g of lalang grass rhizome and 100 g of cape jasmine fruit according to corresponding proportion, drying at 40 ℃ for 20 minutes, crushing, grinding, and screening by a 280-mesh screen to obtain standby substances of sea buckthorn powder, dried ginger powder, common cephalanoplos herb powder, fragrant solomonseal rhizome powder, rhodiola rosea powder, black pepper powder, chrysanthemum powder, cogongrass rhizome powder and cape jasmine fruit powder, uniformly mixing, and adding 390 g of alcohol to obtain an extract;
distilling the obtained extract, standing, and separating water and oil to obtain Chinese medicinal essential oil;
and (3) uniformly mixing the obtained traditional Chinese medicine essential oil, 120 g of 1, 2-propylene glycol and 100 g of coffee extract to obtain a finished product of the coffee-flavored refreshing cigarette oil.
The above alcohol is 75-90% alcohol solution.
Example 3:
a preparation method of coffee flavor refreshing cigarette oil comprises the following steps:
selecting 50 g of sea buckthorn, 40 g of dried ginger, 60g of common cephalanoplos herb, 80 g of fragrant solomonseal rhizome, 80 g of rhodiola rosea, 15 g of black pepper, 60g of chrysanthemum, 110 g of lalang grass rhizome and 60g of cape jasmine fruit according to corresponding proportion, drying at 40 ℃ for 10 minutes, crushing, grinding, and screening by a 150-mesh screen to obtain standby substances of sea buckthorn powder, dried ginger powder, common cephalanoplos herb powder, fragrant solomonseal rhizome powder, rhodiola rosea powder, black pepper powder, chrysanthemum powder, cogongrass rhizome powder and cape jasmine fruit powder, mixing uniformly, and adding 166.5 g of ethyl acetate to obtain an extract;
distilling the obtained extract, standing, and separating water and oil to obtain Chinese medicinal essential oil;
and uniformly mixing the obtained traditional Chinese medicine essential oil, 80 g of polyethylene glycol and 70 g of coffee extract to obtain a finished product of the coffee flavor refreshing cigarette oil.
The above selected ethyl acetate is used for dissolving active ingredients of medicines, and the above ethyl acetateThe using amount meets the use standard required by the state, and the content of the final product is lower than the LD of rats and mice50The minimum amount of use of.
Example 4:
a preparation method of coffee flavor refreshing cigarette oil comprises the following steps:
selecting 80 g of sea buckthorn, 90 g of dried ginger, 90 g of herba cepbalanoplosis segeti, 110 g of polygonatum odoratum, 110 g of rhodiola rosea, 25g of black pepper, 80 g of chrysanthemum, 250 g of lalang grass rhizome and 90 g of gardenia according to corresponding proportions, drying at 30 ℃ for 20 minutes, crushing, grinding, and screening by a 280-mesh screen to obtain standby substances of sea buckthorn powder, dried ginger powder, herba cepbalanoplosis segeti powder, polygonatum odoratum powder, rhodiola rosea powder, black pepper powder, chrysanthemum powder, cogongrass rhizome powder and gardenia powder, mixing uniformly, and adding 277.5 g of alcohol to obtain an extract;
distilling the obtained extract, standing, and separating water and oil to obtain Chinese medicinal essential oil;
and uniformly mixing the obtained traditional Chinese medicine essential oil, 110 g of tobacco leaf extracting solution and 95 g of coffee extract to obtain a finished product of coffee-flavored refreshing cigarette oil.
Example 5:
a preparation method of coffee flavor refreshing cigarette oil comprises the following steps:
selecting 60g of sea buckthorn, 70 g of dried ginger, 80 g of herba cepbalae segeti, 100 g of polygonatum odoratum, 100 g of rhodiola rosea, 20 g of black pepper, 70 g of chrysanthemum, 150 g of lalang grass rhizome and 80 g of gardenia according to corresponding proportion, drying at 40 ℃ for 10 minutes, crushing, grinding, and screening by a 280-mesh screen to obtain standby substances of sea buckthorn powder, dried ginger powder, herba cepbalanoplosis segeti powder, polygonatum odoratum powder, rhodiola rosea powder, black pepper powder, chrysanthemum powder, cogongrass rhizome powder and gardenia powder, mixing uniformly, and adding 365 g of alcohol to obtain an extract;
distilling the obtained extract, standing, and separating water and oil to obtain Chinese medicinal essential oil;
and uniformly mixing the obtained traditional Chinese medicine essential oil, 90 g of glycerol and 85 g of coffee extract to obtain a finished product of the coffee-flavored refreshing cigarette smoke.
The using method comprises the following steps: can be applied by adding into cigarette case.
The present invention is not limited to the above alternative embodiments, and any other products in various forms can be obtained by the present invention, and the present invention is within the protection scope of the present invention. The above embodiments should not be construed as limiting the scope of the present invention, and it will be understood by those skilled in the art that modifications may be made to the technical solutions described in the above embodiments, or equivalent substitutions may be made to some or all of the technical features thereof, without departing from the scope of the present invention, and at the same time, such modifications or substitutions may not make the essence of the corresponding technical solutions depart from the scope of the embodiments of the present invention.

Claims (10)

1. The coffee-flavored refreshing cigarette oil is characterized by being prepared from the following raw materials in parts by mass:
60-100 parts of coffee extract, 3-9 parts of sea buckthorn, 3-10 parts of dried ginger, 5-10 parts of common cephalanoplos herb, 6-12 parts of fragrant solomonseal rhizome, 6-12 parts of rhodiola rosea, 1-3 parts of black pepper, 5-9 parts of chrysanthemum, 10-30 parts of lalang grass rhizome, 5-10 parts of cape jasmine fruit and 70-120 parts of oil agent.
2. The coffee flavor refreshing cigarette pack tobacco tar is characterized by being prepared from the following raw materials in parts by mass:
70-95 parts of coffee extract, 5-8 parts of sea buckthorn, 4-9 parts of dried ginger, 6-9 parts of common cephalanoplos herb, 8-11 parts of fragrant solomonseal rhizome, 8-11 parts of rhodiola root, 1.5-2.5 parts of black pepper, 6-8 parts of chrysanthemum, 11-25 parts of lalang grass rhizome, 6-9 parts of cape jasmine fruit and 80-110 parts of oil agent.
3. The coffee flavor refreshing cigarette pack tobacco tar is characterized by being prepared from the following raw materials in parts by mass:
85 parts of coffee extract, 6 parts of sea buckthorn, 7 parts of dried ginger, 8 parts of common cephalanoplos herb, 10 parts of fragrant solomonseal rhizome, 10 parts of rhodiola rosea, 2 parts of black pepper, 7 parts of chrysanthemum, 15 parts of lalang grass rhizome, 8 parts of cape jasmine and 90 parts of oil agent.
4. The coffee flavor refreshing cigarette pack according to any one of claims 1 to 3, wherein the oil comprises one or more of glycerol, 1, 2-propylene glycol, polyethylene glycol and tobacco leaf extract.
5. A process for the preparation of a coffee flavoured refreshing cigarette smoke as claimed in any of claims 1 to 3, said process comprising the steps of:
selecting sea buckthorn, dried ginger, common cephalanoplos herb, fragrant solomonseal rhizome, rhodiola rosea, black pepper, chrysanthemum, lalang grass rhizome and gardenia according to corresponding proportion, drying, crushing and grinding to obtain standby substances of sea buckthorn powder, dried ginger powder, common cephalanoplos herb powder, fragrant solomonseal rhizome powder, rhodiola rosea powder, black pepper powder, chrysanthemum powder, cogongrass rhizome powder and gardenia powder, mixing uniformly, and adding a solvent to obtain an extract;
distilling the obtained extract, standing, and separating water and oil to obtain Chinese medicinal essential oil;
and (3) uniformly mixing the obtained traditional Chinese medicine essential oil, oil and coffee extract to obtain a finished product of the coffee-flavored refreshing cigarette smoke.
6. The method for preparing the coffee-flavored refreshing cigarette pack oil according to claim 5, wherein the sea buckthorn, the dried ginger, the common cephalanoplos herb, the fragrant solomonseal rhizome, the rhodiola rosea, the black pepper, the chrysanthemum, the lalang grass rhizome and the gardenia are selected, and the drying temperature is 30-40 ℃.
7. The method for preparing the coffee flavor refreshing cigarette pack according to claim 6, wherein the drying time is 10-20 minutes.
8. The method for preparing coffee flavor refreshing cigarette oil as claimed in claim 5, wherein the particle sizes of the standby materials of sea buckthorn powder, dried ginger powder, common cephalanoplos herb powder, rhizoma polygonati powder, rhodiola rosea powder, black pepper powder, chrysanthemum powder, cogongrass rhizome powder and gardenia powder are all 150-280 mesh sieve.
9. The method of claim 5, wherein the solvent comprises one or more of cyclohexane, alcohol and ethyl acetate.
10. The preparation method of the coffee-flavored refreshing cigarette oil according to claim 5, wherein the mass ratio of the total mass of the standby sea buckthorn powder, the dried ginger powder, the common cephalanoplos herb powder, the polygonatum powder, the rhodiola root powder, the black pepper powder, the chrysanthemum powder, the cogongrass rhizome powder and the gardenia powder to the solvent is 1: 0.3-0.5 wt%.
CN202111229375.1A 2021-10-21 2021-10-21 Coffee-flavored refreshing cigarette oil and preparation method thereof Withdrawn CN113749279A (en)

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Application publication date: 20211207