CN113712831A - Breath-freshening toothpaste and preparation method thereof - Google Patents
Breath-freshening toothpaste and preparation method thereof Download PDFInfo
- Publication number
- CN113712831A CN113712831A CN202110995695.1A CN202110995695A CN113712831A CN 113712831 A CN113712831 A CN 113712831A CN 202110995695 A CN202110995695 A CN 202110995695A CN 113712831 A CN113712831 A CN 113712831A
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- CN
- China
- Prior art keywords
- toothpaste
- breath
- pca
- trehalose
- polyethylene glycol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229940034610 toothpaste Drugs 0.000 title claims abstract description 65
- 238000002360 preparation method Methods 0.000 title abstract description 17
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- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims abstract description 43
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 claims abstract description 32
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- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 claims abstract description 32
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- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims abstract description 30
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Abstract
The invention relates to the technical field of daily necessities, in particular to breath freshening toothpaste and a preparation method thereof, wherein the breath freshening toothpaste comprises toothpaste ingredients, a deodorant and deionized water, wherein the toothpaste ingredients comprise sorbitol, hydrated silica, polyethylene glycol, glycerol, edible essence, tetrasodium pyrophosphate, methylparaben, xanthan gum, sodium methyl cocoyl taurate, cocamidopropyl betaine, a plant flower extract and trichlorogalactose; the deodorant consists of trehalose, zinc citrate, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, and the breath-freshening toothpaste has the advantages of bacteriostasis, inflammation diminishing, periodontal maintenance, lasting aroma retention, bacteria elimination, long effective time and tartar removal; the method can prepare into paste and improve refreshing effect and antibacterial effect of toothpaste.
Description
Technical Field
The invention relates to the technical field of daily necessities, in particular to breath-refreshing toothpaste and a preparation method thereof.
Background
Experts show that halitosis is not uncommon and have been investigated to suggest that the incidence of halitosis in the population is about 30%. The halitosis is divided into halitosis of mouth origin and halitosis of non-mouth origin, wherein about 80% of halitosis belongs to halitosis of mouth origin. The halitosis brings social embarrassment to people.
Halitosis caused by oral problems, such as dental plaque, soft calculus, large accumulation of dental calculus, gingivitis, periodontitis, oral mucosa diseases and dental caries, is the most common cause of oral halitosis. In particular, halitosis caused by extensive caries and periodontitis is common. In addition, ulcerated wounds of the mucosa have blood exudation and also provide a source of odor for bacteria. Bacterial and viral infections on the oral mucosa often cause pathological changes of the tongue coating and cause halitosis. The lack of oral hygiene is also the most common cause of bad breath and is associated with non-brushing, non-rinsing, or incomplete brushing. Food residues in the mouth are accumulated for a long time and are fermented, decayed and decomposed under the action of bacteria to generate substances such as indole sulfhydryl, amine and the like, and a decayed stink is generated.
In the oral cavity of human beings, a plurality of bacteria capable of decomposing protein putrefaction are parasitized, mainly anaerobic bacteria, and can decompose protein substances, generate volatile sulfide and other peculiar smell substances, thereby causing the oral cavity to generate putrefactive odor.
In fact, for physiological or temporary bad breath, it can be removed quickly by good oral cleaning. In other words, if a healthy person has bad oral odor, it means that his oral hygiene does not perform much.
Antibacterial and anti-inflammatory toothpastes are also available on the market, but at present, the antibacterial and anti-inflammatory toothpastes cannot well care periodontal as long as the antibacterial and anti-inflammatory toothpastes are used for degerming, have short effective degerming time, have short aroma retention time and cannot play a breath freshening function for a long time.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide the breath freshening toothpaste which has the advantages of bacteriostasis, anti-inflammation, periodontal maintenance, lasting fragrance, long effective sterilization time and tartar removal.
The invention also aims to provide a preparation method of the breath-freshening toothpaste, which can prepare a formed paste and has the advantages of improving the freshening effect and the sterilizing effect of the toothpaste.
In order to achieve one of the above purposes, the invention provides the following technical scheme:
provides a breath-freshening toothpaste, which consists of toothpaste components and a deodorant,
the toothpaste ingredients comprise sorbitol, hydrated silica, polyethylene glycol, glycerol, edible essence, tetrasodium pyrophosphate, methylparaben, xanthan gum, sodium methyl cocoyl taurate, cocamidopropyl betaine, plant flower extract, trichlorogalactose and deionized water;
the deodorant consists of trehalose, zinc citrate, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer.
The reaction principle of the raw materials is as follows: the toothpaste component contains polyethylene glycol, glycerol and sorbitol as humectant, and hydrated silica as abrasive; sodium methyl cocoyl taurate, cocamidopropyl betaine as surfactant; edible essence and plant flower extract as perfume; tetrasodium pyrophosphate as alkaline component can react with tartar formed by magnesium and calcium deposition on teeth to remove tartar; methyl hydroxybenzoate as antiseptic; xanthan gum is used as adhesive; trichlorogalactose is a sweetener.
Trehalose, zinc citrate, bamboo leaf flavone and PCA cocoyl arginine ethyl ester salt in the deodorant can play a role in bacteriostasis and inflammation diminishing, wherein the trehalose can provide nonspecific protection for periodontal, the zinc citrate can supplement zinc, the bamboo leaf flavone can supplement bioflavonoid for periodontal parts, and the PCA cocoyl arginine ethyl ester salt can provide a lubricating effect; the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer can prolong the retention time of effective components and fragrance in the oral cavity, prolong the effective duration of sterilization and play a role in lasting deodorization.
In some embodiments, the plant flower extract is a gardenia extract. The gardenia extract has lasting and refreshing flavor and is suitable for use as an oral freshener.
In some embodiments, the sodium methylcocoyltaurate is a natural amino acid type surfactant with good safety properties.
In some embodiments, the toothpaste ingredients comprise the following raw materials in weight percent:
sorbitol 15-70%, hydrated silica 10-25%, polyethylene glycol 0.5-7%, glycerin 1-8%, edible essence 0.02-1.5%, tetrasodium pyrophosphate 0.02-1.5%, methyl hydroxybenzoate 0.1-0.5%, xanthan gum 0.1-1.5%, sodium methyl cocoyl taurate 0.5-2%, cocamidopropyl betaine 0.05-2%, plant flower extract 0.01-1%, and trichlorogalactose 0.02-1%;
the deodorant comprises the following raw materials in percentage by weight:
trehalose 0.2-5%, zinc citrate 0.02-1.5%, bamboo leaf flavone 0.02-1.5%, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer 0.02-2%, PCA cocoyl arginine ethyl ester 0.001-0.1%;
the balance of water.
The raw materials with the formula amount can realize the best sterilization effect, stability, periodontal curing effect and refreshing effect.
The breath-freshening toothpaste has the beneficial effects that:
(1) the ingredients of the toothpaste of the invention include ethylene glycol, glycol and sorbitol as humectants, hydrated silica as abrasive; sodium methyl cocoyl taurate, cocamidopropyl betaine as surfactant; sorbitol, hydrated silica, polyethylene glycol, glycerin, flavoring essence and plant flower extract as perfume; tetrasodium pyrophosphate as alkaline component can react with tartar formed by magnesium and calcium deposition on teeth to remove tartar; methyl hydroxybenzoate as antiseptic; xanthan gum is used as adhesive; trichlorogalactose is a sweetener.
(2) Trehalose, zinc citrate, bamboo leaf flavone and PCA cocoyl arginine ethyl ester salt in the deodorant can play a role in bacteriostasis and inflammation diminishing, wherein the trehalose can provide nonspecific protection for periodontal, the zinc citrate can supplement zinc, the bamboo leaf flavone supplements bioflavonoid for periodontal parts, and the PCA cocoyl arginine ethyl ester salt provides a lubricating effect; the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer can prolong the retention time of effective components and fragrance in the oral cavity, prolong the effective duration of sterilization and play a role in lasting deodorization.
(3) The invention has the advantages of good deodorization effect from multiple dimensions of degerming and diminishing inflammation, maintaining periodontal, removing tartar, improving refreshing duration time, degerming duration time and the like.
In order to achieve the second purpose, the invention provides the following technical scheme:
the preparation method of the breath-freshening toothpaste comprises the following steps,
s1, weighing sorbitol, hydrated silica, polyethylene glycol, glycerol, edible essence, tetrasodium pyrophosphate, methylparaben, xanthan gum, cocamidopropyl betaine, plant flower fragrance extract, trichlorogalactose, trehalose, zinc citrate, bamboo leaf flavonoid, PCA (poly (lactic acid)) cocoyl arginine ethyl ester salt and acrylic acid/C10-30 alkanol acrylate cross-linked polymer according to formula amount for later use;
s2, adding the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer into polyethylene glycol and sorbitol for wetting, then adding part of deionized water, and homogenizing to obtain a suspension; adding xanthan gum into glycerol, and uniformly stirring and dispersing to obtain a first solution; adding the first solution into the suspension, and uniformly stirring to obtain a third solution; adding tetrasodium pyrophosphate, trehalose, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and sodium methyl cocoyl taurate into the other part of the ionized water, and stirring until the materials are completely dissolved to obtain a fourth solution; adding the fourth solution into the third solution, and stirring to obtain a uniform mucilage; dissolving methylparaben and plant flower extract in edible essence to obtain a fifth material;
and S3, adding the cocoamidopropyl betaine, the hydrated silica and the fifth material into the homogenized adhesive cement, and continuously grinding while stirring to obtain the toothpaste body.
In some embodiments, in S3, the grinding time is 10min to 20 min.
In some embodiments, in S3, the stirring time is 10min to 20 min.
In some embodiments, the toothpaste paste is also degassed in S3.
In the preparation method, the raw materials are mixed step by step, so that the raw materials can be correspondingly synergistic, for example, the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is added into the wetting agent, so that the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer can be well mixed in other components along with the wetting agent; the tetrasodium pyrophosphate, the trehalose, the bamboo leaf flavonoid and the PCA cocoyl arginine ethyl ester salt are fully mixed, so that the alkaline tetrasodium pyrophosphate, the abrasive hydrated silica, the trehalose, the bamboo leaf flavonoid and the PCA cocoyl arginine ethyl ester salt are fully mixed and generate a better coordination effect.
The preparation method of the breath-freshening toothpaste has the beneficial effects that:
(1) the preparation method of the invention mixes the raw materials step by step, thus leading the raw materials to have corresponding synergy, for example, the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is added into the wetting agent, leading the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer to be better mixed in other components along with the wetting agent; the tetrasodium pyrophosphate, the hydrated silica, the trehalose, the bamboo leaf flavonoid and the PCA cocoyl arginine ethyl ester salt are fully mixed, so that the alkaline tetrasodium pyrophosphate, the abrasive hydrated silica and the trehalose, the bamboo leaf flavonoid and the PCA cocoyl arginine ethyl ester salt are fully mixed and generate better coordination effect.
(2) The preparation method of the invention obtains corresponding synergistic function by step mixing, is easy to operate and is suitable for large-scale production and application.
Detailed Description
The present invention will be described in detail with reference to specific examples.
Example 1
The implementation discloses a breath-freshening toothpaste, which consists of toothpaste components, a deodorant and deionized water,
the toothpaste ingredients comprise sorbitol, hydrated silica, polyethylene glycol, glycerol, edible essence, tetrasodium pyrophosphate, methylparaben, xanthan gum, sodium methyl cocoyl taurate, cocamidopropyl betaine, plant flower extract and trichlorogalactose;
the deodorant consists of trehalose, zinc citrate, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer.
The functions and effects of the raw materials are as follows: trehalose, zinc citrate, bamboo leaf flavone and PCA cocoyl arginine ethyl ester salt with antibacterial and anti-inflammatory effects are added, so that the oral hygiene can be improved, and periodontal health can be realized; the addition of acrylic acid (ester)/C10-30 alkanol acrylate crosslinked polymer prolongs the retention time of effective components and fragrance in oral cavity.
In this embodiment, the plant flower extract is gardenia extract.
The toothpaste comprises the following raw materials in percentage by weight:
sorbitol 15%, hydrated silica 10%, polyethylene glycol 0.5%, glycerin 1%, edible essence 0.02%, tetrasodium pyrophosphate 0.02%, methylparaben 0.1%, xanthan gum 0.1%, sodium methyl cocoyl taurate 1.8%, cocamidopropyl betaine 0.05%, plant flower extract 0.01%, and trichlorogalactose 0.02%;
the deodorant comprises the following raw materials in percentage by weight:
trehalose 0.2%, zinc citrate 0.02%, bamboo leaf flavone 0.02%, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer 0.02%, PCA cocoyl arginine ethyl ester salt 0.001%;
the balance of water.
The preparation method of the breath-freshening toothpaste is characterized by comprising the following steps: comprises the following steps of (a) carrying out,
s1, weighing sorbitol, hydrated silica, polyethylene glycol, glycerol, edible essence, tetrasodium pyrophosphate, methylparaben, xanthan gum, sodium methyl cocoyl taurate, cocamidopropyl betaine, plant flower extract, trichlorogalactose, trehalose, zinc citrate, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer according to formula amount for later use;
s2, adding the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer into polyethylene glycol and sorbitol for wetting, then adding part of deionized water, and homogenizing to obtain a suspension; adding xanthan gum into glycerol, and uniformly stirring and dispersing to obtain a first solution; adding the first solution into the suspension, and uniformly stirring to obtain a third solution; adding tetrasodium pyrophosphate, trehalose, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and sodium methyl cocoyl taurate into the other part of the ionized water, and stirring until the materials are completely dissolved to obtain a fourth solution; adding the fourth solution into the third solution, and stirring to obtain a uniform mucilage; dissolving methylparaben and plant flower extract in edible essence to obtain a fifth material;
and S3, adding the cocoamidopropyl betaine, the hydrated silica and the fifth material into the homogenized adhesive cement, and continuously grinding while stirring to obtain the toothpaste body.
The preparation method has the following effects: through step-by-step mixing, the corresponding synergistic function is obtained, and the operation is easy.
In this embodiment, in S3, the grinding time is 10 min.
In this example, in S3, the stirring time was 10 min.
In this embodiment, in S3, the toothpaste body is also degassed.
Example 2
The implementation discloses a breath-freshening toothpaste, which consists of toothpaste components, a deodorant and deionized water,
the toothpaste component comprises sorbitol, hydrated silica, polyethylene glycol, glycerol, edible essence, tetrasodium pyrophosphate, methylparaben, xanthan gum, sodium methyl cocoyl taurate, cocamidopropyl betaine, plant flower extract, and trichlorogalactose
The deodorant consists of trehalose, zinc citrate, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer ethanol.
The functions and effects of the raw materials are as follows: trehalose, zinc citrate, bamboo leaf flavone and PCA cocoyl arginine ethyl ester salt with antibacterial and anti-inflammatory effects are added, so that the oral hygiene can be improved, and periodontal health can be realized; the addition of acrylic acid (ester)/C10-30 alkanol acrylate crosslinked polymer prolongs the retention time of effective components and fragrance in oral cavity.
In this example, the plant floral extract is gardenia extract.
The toothpaste comprises the following raw materials in percentage by weight:
sorbitol 40%, hydrated silica 25%, polyethylene glycol 7%, glycerin 8%, edible essence 1.5%, tetrasodium pyrophosphate 1.5%, methylparaben 0.5%, xanthan gum 1.5%, sodium methyl cocoyl taurate 0.8%, cocamidopropyl betaine 2%, plant flower extract 1%, and trichlorogalactose 1%;
the deodorant comprises the following raw materials in percentage by weight:
5% of trehalose, 1.5% of zinc citrate, 1.5% of bamboo leaf flavone, 2% of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and 0.1% of PCA cocoyl arginine ethyl ester salt;
the balance of water.
The preparation method of the breath-freshening toothpaste is characterized by comprising the following steps: comprises the following steps of (a) carrying out,
s1, weighing sorbitol, hydrated silica, polyethylene glycol, glycerol, edible essence, tetrasodium pyrophosphate, methylparaben, xanthan gum, sodium methyl cocoyl taurate, cocamidopropyl betaine, plant flower extract, trichlorogalactose, trehalose, zinc citrate, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer according to formula amount for later use;
s2, adding the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer into polyethylene glycol and sorbitol for wetting, then adding part of deionized water, and homogenizing to obtain a suspension; adding xanthan gum into glycerol, and uniformly stirring and dispersing to obtain a first solution; adding the first solution into the suspension, and uniformly stirring to obtain a third solution; adding tetrasodium pyrophosphate, trehalose, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and sodium methyl cocoyl taurate into the other part of the ionized water, and stirring until the materials are completely dissolved to obtain a fourth solution; adding the fourth solution into the third solution, and stirring to obtain a uniform mucilage; dissolving methylparaben and plant flower extract in edible essence to obtain a fifth material;
and S3, adding the cocoamidopropyl betaine, the hydrated silica and the fifth material into the homogenized adhesive cement, and continuously grinding while stirring to obtain the toothpaste body.
The preparation method has the following effects: through step-by-step mixing, the corresponding synergistic function is obtained, and the operation is easy.
In this embodiment, in S3, the grinding time is 15 min.
In this example, in S3, the stirring time was 15 min.
In this embodiment, in S3, the toothpaste body is also degassed.
Example 3
The implementation discloses a breath-freshening toothpaste, which consists of toothpaste components, a deodorant and deionized water,
the toothpaste ingredients comprise sorbitol, hydrated silica, polyethylene glycol, glycerol, edible essence, tetrasodium pyrophosphate, methylparaben, xanthan gum, sodium methyl cocoyl taurate, cocamidopropyl betaine, plant flower extract and trichlorogalactose;
the deodorant consists of trehalose, zinc citrate, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer.
The functions and effects of the raw materials are as follows: trehalose, zinc citrate, bamboo leaf flavone and PCA cocoyl arginine ethyl ester salt with antibacterial and anti-inflammatory effects are added, so that the oral hygiene can be improved, and periodontal health can be realized; the addition of acrylic acid (ester)/C10-30 alkanol acrylate crosslinked polymer prolongs the retention time of effective components and fragrance in oral cavity.
In this example, the plant floral extract is gardenia extract.
The toothpaste comprises the following raw materials in percentage by weight:
sorbitol 70%, hydrated silica 10%, polyethylene glycol 0.6%, glycerin 2%, edible essence 0.03%, tetrasodium pyrophosphate 0.5%, methylparaben 0.2%, xanthan gum 0.2%, sodium methyl cocoyl taurate 2%, cocamidopropyl betaine 0.06%, plant flower extract 0.03%, and trichlorogalactose 0.04%;
the deodorant comprises the following raw materials in percentage by weight:
2% of trehalose, 0.8% of zinc citrate, 1% of bamboo leaf flavone, 0.8% of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and 0.05% of PCA cocoyl arginine ethyl ester salt;
the balance of water.
The preparation method of the breath-freshening toothpaste is characterized by comprising the following steps: comprises the following steps of (a) carrying out,
s1, weighing sorbitol, hydrated silica, polyethylene glycol, glycerol, edible essence, tetrasodium pyrophosphate, methylparaben, xanthan gum, sodium methyl cocoyl taurate, cocamidopropyl betaine, plant flower extract, trichlorogalactose, trehalose, zinc citrate, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer according to formula amount for later use;
s2, adding the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer into polyethylene glycol and sorbitol for wetting, then adding part of deionized water, and homogenizing to obtain a suspension; adding xanthan gum into glycerol, and uniformly stirring and dispersing to obtain a first solution; adding the first solution into the suspension, and uniformly stirring to obtain a third solution; adding tetrasodium pyrophosphate, trehalose, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and sodium methyl cocoyl taurate into the other part of the ionized water, and stirring until the materials are completely dissolved to obtain a fourth solution; adding the fourth solution into the third solution, and stirring to obtain a uniform mucilage; dissolving methylparaben and plant flower extract in edible essence to obtain a fifth material;
and S3, adding the cocoamidopropyl betaine, the hydrated silica and the fifth material into the homogenized adhesive cement, and continuously grinding while stirring to obtain the toothpaste body.
The preparation method has the following effects: through step-by-step mixing, the corresponding synergistic function is obtained, and the operation is easy.
In this embodiment, in S3, the grinding time is 20 min.
In this example, in S3, the stirring time was 20 min.
In this embodiment, in S3, the toothpaste body is also degassed.
Comparative example 1
Comparative example 1 is different from example 1 in that the ingredients other than the deodorant, and the preparation method are the same as example 1, and thus detailed description thereof is omitted.
Comparison of effects
To verify the long-lasting effect of the breath freshening toothpaste of the present invention, the following tests were used:
10 subjects were selected and divided into 2 groups, one group was an experimental group, the other group was a control group, the experimental group brushed teeth with the toothpaste of example 1, the control group brushed teeth with the toothpaste of comparative example 1; the breath freshness was self-evaluated at 5min, 35min, 65min, 95min, 125min and 155min in the experimental group and the control group, respectively, and the evaluation results are shown in table 1.
TABLE 1
| Evaluation item | 5min | 35min | 65min | 95min | 125min | 155min |
| Example 1 | Has fresh degree | Has fresh degree | Has fresh degree | Has fresh degree | Has fresh degree | Has fresh degree |
| Comparative example 1 | Has fresh degree | Has fresh degree | Has fresh degree | Without freshness | Without freshness | Without freshness |
As can be seen from table 1 above: the breath freshening toothpaste disclosed by the invention has longer lasting time, and the breath freshening toothpaste has better refreshing lasting time.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention, and not for limiting the protection scope of the present invention, although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (11)
1. A breath-freshening toothpaste is characterized in that: consists of toothpaste components, deodorant and deionized water,
the toothpaste ingredients comprise sorbitol, hydrated silica, polyethylene glycol, glycerol, edible essence, tetrasodium pyrophosphate, methylparaben, xanthan gum, sodium methyl cocoyl taurate, cocamidopropyl betaine, plant flower extract and trichlorogalactose;
the deodorant consists of trehalose, zinc citrate, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer.
2. The breath freshening toothpaste as recited in claim 1 wherein: the plant flower extract is gardenia extract.
3. The breath freshening toothpaste as recited in claim 1 wherein: also included are abrasives including dibasic calcium phosphate and hydrated silica.
4. The breath freshening toothpaste as recited in claim 1 wherein: also comprises humectant including sorbitol and polyethylene glycol, and glycerol.
5. The breath freshening toothpaste as recited in claim 1 wherein: also included are surfactants including sodium methyl cocoyl taurate, cocamidopropyl betaine.
6. The toothpaste according to claim 1, wherein: also included are adhesives comprising xanthan gum and acrylic/C10-30 alkanol acrylate crosspolymer.
7. The toothpaste according to claim 1, wherein: the preservative is methyl hydroxybenzoate;
the toothpaste comprises the following raw materials in percentage by weight:
sorbitol 15-70%, hydrated silica 10-25%, polyethylene glycol 0.5-7%, glycerin 1-8%, edible essence 0.02-1.5%, tetrasodium pyrophosphate 0.02-1.5%, methyl hydroxybenzoate 0.1-0.3%, xanthan gum 0.02-1.5%, sodium methyl cocoyl taurate 0.05-2%, cocamidopropyl betaine 0.05-2%, plant flower extract 0.01-1%, and trichlorogalactose 0.02-1%;
the deodorant comprises the following raw materials in percentage by weight:
trehalose 0.2-5%, zinc citrate 0.02-1.5%, bamboo leaf flavone 0.02-1.5%, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer 0.02-2%, PCA cocoyl arginine ethyl ester 0.001-0.2%;
the balance of water.
8. A method of preparing a breath freshening toothpaste as claimed in any one of claims 1 to 7 which is characterized by: comprises the following steps of (a) carrying out,
s1, weighing sorbitol, hydrated silica, polyethylene glycol, glycerol, edible essence, tetrasodium pyrophosphate, methylparaben, xanthan gum, sodium methyl cocoyl taurate, cocamidopropyl betaine, plant flower extract, trichlorogalactose, trehalose, zinc citrate, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer according to formula amount for later use;
s2, adding the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer into polyethylene glycol and sorbitol for wetting, then adding part of deionized water, and homogenizing to obtain a suspension; adding xanthan gum into glycerol, and uniformly stirring and dispersing to obtain a first solution; adding the first solution into the suspension, and uniformly stirring to obtain a third solution; adding tetrasodium pyrophosphate, trehalose, bamboo leaf flavone, PCA cocoyl arginine ethyl ester salt and sodium methyl cocoyl taurate into the other part of the ionized water, and stirring until the materials are completely dissolved to obtain a fourth solution; adding the fourth solution into the third solution, and stirring to obtain a uniform mucilage; dissolving methylparaben and plant flower extract in edible essence to obtain a fifth material;
and S3, adding the cocoamidopropyl betaine, the hydrated silica and the fifth material into the homogenized adhesive cement, and continuously grinding while stirring to obtain the toothpaste body.
9. The method of preparing a breath freshening toothpaste as claimed in claim 8 wherein: in the step S3, the grinding time is 10-20 min.
10. The method of preparing a breath freshening toothpaste as claimed in claim 8 wherein: in the step S3, the stirring time is 10-20 min.
11. The method of preparing a breath freshening toothpaste as claimed in claim 8 wherein: in S3, the toothpaste is also degassed.
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