CN115501140A - Toothpaste with lasting fragrance in oral cavity and preparation method thereof - Google Patents
Toothpaste with lasting fragrance in oral cavity and preparation method thereof Download PDFInfo
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- CN115501140A CN115501140A CN202211420122.7A CN202211420122A CN115501140A CN 115501140 A CN115501140 A CN 115501140A CN 202211420122 A CN202211420122 A CN 202211420122A CN 115501140 A CN115501140 A CN 115501140A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/24—Phosphorous; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Oral & Maxillofacial Surgery (AREA)
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Abstract
The invention belongs to the technical field of daily necessities, and particularly relates to an oral lasting fragrance toothpaste and a preparation method thereof. The invention relates to an oral lasting fragrance toothpaste, which comprises the following components in percentage by weight: 1.8 to 11 percent of bacteriostatic fragrance-retaining agent, 10 to 20 percent of rubbing agent, 15 to 70 percent of humectant, 0.5 to 4 percent of surfactant, 0.05 to 0.5 percent of sweetening agent, 0.3 to 0.8 percent of adhesive, 0.1 to 0.4 percent of preservative and the balance of water; the antibacterial fragrance-retaining agent comprises blueberry leaf essential oil and blueberry essence. The blueberry leaf essential oil and the blueberry essence are used as antibacterial fragrance retention agents, the blueberry leaf essential oil is diffused and dissolved in oral mucosa, the retention time is long, the release speed is slow, the fragrance is released durably, the taste is mild, discomfort cannot be caused, and the antibacterial and anti-inflammatory effects are achieved, so that the oral environment is healthy and the breath is fresh.
Description
Technical Field
The invention belongs to the technical field of daily necessities, and particularly relates to an oral lasting fragrance-retaining toothpaste and a preparation method thereof.
Background
Bad breath is not rare and it is considered by investigation that the incidence of bad breath in a population is about 30%. The halitosis is divided into halitosis of mouth origin and halitosis of non-mouth origin, wherein about 80% of halitosis belongs to halitosis of mouth origin. Bad breath can cause embarrassment in face-to-face socialization. For oral malodor and bad breath, in addition to good oral cleaning, it is necessary to cover the bad breath with a perfume.
Conventional perfumes have a temporary masking effect on oral malodor and bad breath but are short lasting and leave the fragrance for no more than 30 minutes, which is undesirable for users because the on-the-road time can be more than 30 minutes. This means that the social location is reached and the bad breath problem reappears.
Disclosure of Invention
Aiming at the problems in the prior art, the invention aims to provide an oral lasting fragrance toothpaste and a preparation method thereof.
In order to solve the problems, the technical scheme adopted by the invention is as follows:
an oral cavity lasting fragrance retaining toothpaste comprises the following components in percentage by weight: 1.8 to 11 percent of bacteriostatic fragrance-retaining agent, 10 to 20 percent of rubbing agent, 15 to 70 percent of humectant, 0.5 to 4 percent of surfactant, 0.05 to 0.5 percent of sweetening agent, 0.3 to 0.8 percent of adhesive, 0.1 to 0.4 percent of preservative and the balance of water;
the antibacterial fragrance-retaining agent comprises blueberry leaf essential oil and blueberry essence.
Optionally, the blueberry leaf essential oil is obtained by supercritical carbon dioxide extraction.
Optionally, the mass ratio of the blueberry leaf essential oil to the blueberry essence is (1.5-4): 1.
optionally, the abrasive is one or more of calcium carbonate, dibasic calcium phosphate, or hydrated silica.
Optionally, the humectant comprises sorbitol and polyethylene glycol, glycerin.
Optionally, the binder is one or more of sodium carboxymethylcellulose, xanthan gum, sodium alginate and carrageenan
Optionally, the preservative is paraben and the sweetener is trichlorogalactose.
The preparation method of the toothpaste with lasting fragrance for the oral cavity is characterized by comprising the following steps of:
s1, placing the humectant, the adhesive, the preservative and deionized water in a homogenizer for mixing for 12-15min to obtain a homogeneous mixture;
s2, placing the antibacterial fragrance-retaining agent, the friction agent, the surfactant, the sweetener and the homogeneous mixture into a vacuum paste making machine, grinding and mixing at a high speed for 20-30min, and degassing in vacuum to obtain the toothpaste.
Compared with the prior art, the invention has the beneficial effects that:
the blueberry essential oil and the blueberry essence are used as antibacterial fragrance retention agents, the blueberry leaf essential oil is diffused and dissolved in oral mucosa, the retention time is long, the release speed is slow, the fragrance is released for a long time, the taste is mild, discomfort cannot be caused, the antibacterial and anti-inflammatory effects are achieved, the oral environment is healthy, and the breath is fresh.
Detailed Description
The invention is further described with reference to specific examples.
The extraction method of the blueberry leaf essential oil comprises the following steps: putting the dried blueberry leaves into a crusher for crushing, and sieving by a 50-mesh sieve; weighing 100g of blueberry leaf powder, placing in an extraction kettle, sealing, and subjecting the instrument to CO extraction 2 Leak detection is carried out; setting the extraction temperature to be 30 ℃, the output temperature to be 75 ℃, pressurizing after the temperature is stable, and regulating the pressure to be 25MPa; and (4) after the pressure is stable, extracting for 1h, and collecting the blueberry leaf essential oil.
The blueberry essence extraction method comprises the following steps: mixing 200g of fresh blueberries, 150g of 75% ethanol and 300g of water, and soaking for 48 hours under the condition that the vacuum degree is-0.050 MPa; heating to 80 deg.C, decocting for 1h, and filtering to obtain filtrate and residue; decolorizing the filtrate with active carbon, and concentrating at 100 deg.C to 12g to obtain fructus Myrtilli extract; and adding 5g of ethyl acetate, 10g of vanillin and 2 parts of raspberry ketone into the blueberry extract, and stirring and mixing to obtain the blueberry essence.
Example 1
The toothpaste with lasting fragrance for the oral cavity comprises the following components in percentage by mass: 2% of bacteriostatic fragrance-retaining agent, 20% of rubbing agent, 69% of humectant, 4% of surfactant, 0.1% of sweetening agent, 0.3% of adhesive, 0.4% of preservative and the balance of water. Wherein the bacteriostatic fragrance-retaining agent comprises the following components: 1.5 parts of blueberry leaf essential oil and 0.5 part of blueberry essence; the friction agent comprises the following components: 10 parts of calcium hydrogen phosphate and 10 parts of hydrated silica; the humectant comprises the following components: 60 parts of sorbitol, 5 parts of polyethylene glycol and 4 parts of glycerol; the surfactant is sodium lauryl sulfate; the sweetener is trichlorogalactose; the adhesive is xanthan gum; the antiseptic is methyl hydroxybenzoate.
The preparation method of the toothpaste comprises the following steps:
s1, placing a humectant, an adhesive, a preservative and deionized water in a homogenizer, and mixing for 15min to obtain a homogeneous mixture;
and S2, putting the antibacterial fragrance-retaining agent, the friction agent, the surfactant, the sweetening agent and the homogeneous mixture into a vacuum paste making machine, grinding and mixing for 20min, and performing vacuum degassing to obtain the toothpaste.
Example 2
The toothpaste with lasting fragrance for the oral cavity comprises the following components in percentage by mass: 8% of bacteriostatic fragrance-retaining agent, 12% of friction agent, 47% of humectant, 1.5% of surfactant, 0.21% of sweetening agent, 0.45% of adhesive, 0.22% of preservative and the balance of water. The antibacterial fragrance-retaining agent comprises the following components: 3 parts of blueberry leaf essential oil and 1 part of blueberry essence; the abrasive is hydrated silica; the humectant comprises the following components: 40 parts of sorbitol, 2 parts of polyethylene glycol and 5 parts of glycerol; the surfactant is sodium lauryl sulfate; the sweetener is trichlorogalactose; the adhesive is xanthan gum; the antiseptic is methyl hydroxybenzoate.
The preparation method of the toothpaste comprises the following steps:
s1, placing a humectant, an adhesive, a preservative and deionized water into a homogenizer and mixing for 12min to obtain a homogeneous mixture;
and S2, putting the antibacterial fragrance-retaining agent, the friction agent, the surfactant, the sweetening agent and the homogeneous mixture into a vacuum paste making machine, grinding and mixing for 30min, and performing vacuum degassing to obtain the toothpaste.
Example 3
The toothpaste with lasting fragrance for the oral cavity comprises the following components in percentage by mass: 10% of bacteriostatic fragrance-retaining agent, 10% of rubbing agent, 35% of humectant, 2% of surfactant, 0.5% of sweetening agent, 0.8% of adhesive, 0.15% of preservative and the balance of water. The antibacterial fragrance-retaining agent comprises the following components: 6 parts of blueberry leaf essential oil and 4 parts of blueberry essence; the abrasive is calcium carbonate; the humectant comprises the following components: 30 parts of sorbitol and 5 parts of glycerol; the surfactant is sodium lauryl sulfate; the sweetener is trichlorogalactose; the adhesive is xanthan gum; the antiseptic is methyl hydroxybenzoate.
The preparation method of the toothpaste comprises the following steps:
s1, placing a humectant, an adhesive, a preservative and deionized water into a homogenizer and mixing for 10min to obtain a homogeneous mixture;
and S2, placing the antibacterial flavor retention agent, the rubbing agent, the surfactant, the sweetening agent and the homogeneous mixture into a vacuum paste making machine, grinding and mixing for 25min, and performing vacuum degassing to obtain the toothpaste.
Comparative example 1
The comparative example differs from example 1 in that: the blueberry essence is used for replacing the same amount of blueberry leaf essential oil.
50 subjects were selected, and the average lasting fragrance of the breath was evaluated by sniffing at 10min,20min,30min,1 hour, 1.5 hours, and 2 hours on the morning of the first day using the toothpaste obtained in comparative example 1; the following morning, using the toothpaste obtained in example 1, the average lasting fragrance of breath was evaluated by sniffing at 10min,20min,30min,1 hour, 1.5 hours, and 2 hours, respectively. The evaluation results are shown in table 1. Smelling the scent component value: 1-basically no fragrance, 2-fragrance intensity is general, 3-fragrance is obvious, 4-fragrance is strong, and 5-fragrance is strong.
As can be seen from the data in Table 1, the oral cavity lasting fragrance toothpaste of the invention has a fragrance after 2 hours which is significantly stronger than the fragrance of the blank sample. Calculated by the same fragrance level, the average fragrance retention value of the toothpaste obtained in the comparative example 1 after 20min is close to the fragrance retention value of the toothpaste obtained in the example 1 in 2 hours, so that the fragrance retention duration of the toothpaste disclosed by the invention is more than 6 times that of the toothpaste obtained in the comparative example, the fragrance retention effect of the toothpaste added with the blueberry leaf essential oil is very good, and an excellent scheme is provided for removing halitosis and halitosis for consumers.
TABLE 1 toothpaste Performance test results
Claims (8)
1. The toothpaste with lasting fragrance for the oral cavity is characterized by comprising the following components in percentage by weight: 1.8 to 11 percent of bacteriostatic fragrance-retaining agent, 10 to 20 percent of friction agent, 15 to 70 percent of humectant, 0.5 to 4 percent of surfactant, 0.05 to 0.5 percent of sweetening agent, 0.3 to 0.8 percent of adhesive, 0.1 to 0.4 percent of preservative and the balance of water;
the antibacterial fragrance-retaining agent comprises blueberry leaf essential oil and blueberry essence.
2. The oral long-lasting fragrance-retaining toothpaste according to claim 1, wherein the blueberry leaf essential oil is obtained by supercritical carbon dioxide extraction.
3. The oral cavity lasting fragrance toothpaste according to claim 1, wherein the mass ratio of the blueberry leaf essential oil to the blueberry essence is (1.5-4): 1.
4. the oral permanent aroma-retaining toothpaste according to claim 1, wherein said abrasive is one or more of calcium carbonate, calcium hydrogen phosphate or hydrated silica.
5. The toothpaste with lasting fragrance of the oral cavity according to claim 1, wherein the humectant is one or more of sorbitol, polyethylene glycol, glycerol.
6. The toothpaste with lasting fragrance for the oral cavity according to claim 1, wherein the binder is one or more of sodium carboxymethylcellulose, xanthan gum, sodium alginate and carrageenan.
7. The toothpaste according to claim 1, wherein the preservative is methylparaben and the sweetener is trichlorogalactose.
8. A method of making an oral permanent flavor-retaining toothpaste as claimed in any one of claims 1 to 7 comprising the steps of:
s1, placing the humectant, the adhesive, the preservative and deionized water into a homogenizer to mix for 10-15min to obtain a homogeneous mixture;
and S2, placing the antibacterial flavor retention agent, the friction agent, the surfactant, the sweetening agent and the homogeneous mixture into a vacuum paste making machine, grinding and mixing at a high speed for 20-30min, and degassing in vacuum to obtain the toothpaste.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211420122.7A CN115501140A (en) | 2022-11-14 | 2022-11-14 | Toothpaste with lasting fragrance in oral cavity and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211420122.7A CN115501140A (en) | 2022-11-14 | 2022-11-14 | Toothpaste with lasting fragrance in oral cavity and preparation method thereof |
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| CN115501140A true CN115501140A (en) | 2022-12-23 |
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| CN202211420122.7A Pending CN115501140A (en) | 2022-11-14 | 2022-11-14 | Toothpaste with lasting fragrance in oral cavity and preparation method thereof |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1593377A (en) * | 2004-06-21 | 2005-03-16 | 钟朝锋 | Cactus toothpaste for reducing fever, diminishing the inflammation and reducing the pain |
| CN102961278A (en) * | 2012-11-13 | 2013-03-13 | 广西奥奇丽股份有限公司 | Hypoallergenic toothpaste |
| CN105018234A (en) * | 2015-07-07 | 2015-11-04 | 吉林大学 | Method for supercritical carbon dioxide extraction of essential oil of blueberry leaves |
| CN105560134A (en) * | 2014-10-09 | 2016-05-11 | 重庆能凯科技有限公司 | Cucumber-aroma toothpaste and preparation method thereof |
| CN113559012A (en) * | 2021-08-18 | 2021-10-29 | 南京上元堂沉香生物科技有限公司 | Agilawood toothpaste with function of inhibiting oral helicobacter pylori |
| CN113712831A (en) * | 2021-08-27 | 2021-11-30 | 广东南方洁灵科技实业有限公司 | Breath-freshening toothpaste and preparation method thereof |
-
2022
- 2022-11-14 CN CN202211420122.7A patent/CN115501140A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1593377A (en) * | 2004-06-21 | 2005-03-16 | 钟朝锋 | Cactus toothpaste for reducing fever, diminishing the inflammation and reducing the pain |
| CN102961278A (en) * | 2012-11-13 | 2013-03-13 | 广西奥奇丽股份有限公司 | Hypoallergenic toothpaste |
| CN105560134A (en) * | 2014-10-09 | 2016-05-11 | 重庆能凯科技有限公司 | Cucumber-aroma toothpaste and preparation method thereof |
| CN105018234A (en) * | 2015-07-07 | 2015-11-04 | 吉林大学 | Method for supercritical carbon dioxide extraction of essential oil of blueberry leaves |
| CN113559012A (en) * | 2021-08-18 | 2021-10-29 | 南京上元堂沉香生物科技有限公司 | Agilawood toothpaste with function of inhibiting oral helicobacter pylori |
| CN113712831A (en) * | 2021-08-27 | 2021-11-30 | 广东南方洁灵科技实业有限公司 | Breath-freshening toothpaste and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 易美华: "《生物资源开发利用》", 中国轻工业出版社, pages: 150 * |
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