CN113701799A - Multifunctional in-situ characterization and test device - Google Patents

Multifunctional in-situ characterization and test device Download PDF

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Publication number
CN113701799A
CN113701799A CN202111010429.5A CN202111010429A CN113701799A CN 113701799 A CN113701799 A CN 113701799A CN 202111010429 A CN202111010429 A CN 202111010429A CN 113701799 A CN113701799 A CN 113701799A
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China
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heat preservation
mounting seat
probe
heat
multifunctional
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CN202111010429.5A
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Chinese (zh)
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钱显威
邹杰
简家文
李雪宾
涂建鑫
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Ningbo University
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Ningbo University
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Priority to CN202111010429.5A priority Critical patent/CN113701799A/en
Publication of CN113701799A publication Critical patent/CN113701799A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01DMEASURING NOT SPECIALLY ADAPTED FOR A SPECIFIC VARIABLE; ARRANGEMENTS FOR MEASURING TWO OR MORE VARIABLES NOT COVERED IN A SINGLE OTHER SUBCLASS; TARIFF METERING APPARATUS; MEASURING OR TESTING NOT OTHERWISE PROVIDED FOR
    • G01D18/00Testing or calibrating apparatus or arrangements provided for in groups G01D1/00 - G01D15/00

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  • General Physics & Mathematics (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)

Abstract

The invention discloses a multifunctional in-situ characterization and test device, which comprises a mounting seat and a sealing cover plate, wherein the upper end of the mounting seat is provided with an accommodating cavity, heat-insulating ceramic plates are arranged at the periphery and the bottom of the accommodating cavity, all the heat-insulating ceramic plates enclose a heat-insulating chamber, a heating table is arranged in the heat-insulating chamber, and a heating assembly and a temperature control assembly are arranged in the heating table; the side wall of the heat preservation chamber is provided with at least two probes, and when the sensor element to be detected is placed on the heating table, all the probes are pressed on the upper surface of the sensor element to be detected; the side wall of the mounting seat is provided with an air inlet and an air outlet which are communicated with the heat preservation chamber; the sealing cover plate is detachably connected to the upper end of the mounting seat, the accommodating cavity is located in the range sealed by the sealing cover plate, and a light-transmitting piece is arranged on the sealing cover plate in a position corresponding to the heat preservation chamber. The multifunctional in-situ testing device disclosed by the invention can realize the detection of the sensor under the environment with controllable temperature, humidity and gas parameters, and has the advantages of simple structure and convenience in operation.

Description

Multifunctional in-situ characterization and test device
Technical Field
The invention relates to the field of performance testing devices for electronic materials and sensors, in particular to a multifunctional in-situ characterization and testing device.
Background
In the research, development and production stages of electronic materials and sensors, in-situ characterization and testing are carried out on the electronic materials and the sensors, the sensitive mechanism is analyzed, and various test data of the sensors are required to be acquired, so that great promotion effects are provided for the development of the sensors and the optimization of the sensors in the next step. If a closed gas environment needs to be provided when the gas sensor is subjected to in-situ characterization and testing, higher requirements are made on an in-situ characterization and testing device.
At present, the existing gas sensor element testing device on the market has a complex structure and high cost, and cannot be well applied to the detection process of a laboratory; in addition, the existing detection device applied to the laboratory can not meet the test requirements of local high-temperature in-situ and quick response parameters, secondly, a large cavity caused by a complex structure easily causes the delay of a sensor response curve when atmosphere is switched, and the test performance is single, so that the more accurate test requirements can not be met.
Disclosure of Invention
The present invention is directed to solving at least one of the problems of the prior art. Therefore, the invention provides a multifunctional in-situ characterization and testing device, which can realize the sensor performance detection and in-situ observation characterization functions under various environments of temperature, humidity and gas, and has the advantages of simple structure, convenient atmosphere switching, stable temperature control, small cavity volume, convenient operation and good practical application effect.
The invention adopts a technical scheme that: the multifunctional in-situ characterization and test device comprises an installation seat and a sealing cover plate, wherein an inwards-concave containing cavity is formed in the upper end of the installation seat, heat-preservation ceramic plates are arranged on the periphery and the bottom of the containing cavity, all the heat-preservation ceramic plates form a heat preservation chamber in a surrounding mode, a heating table is arranged in the heat preservation chamber, and a heating assembly and a temperature control assembly are arranged in the heating table; the side wall of the heat preservation chamber is provided with at least two probes, and when the element to be detected is placed on the heating table, all the probes are pressed on the upper surface of the element to be detected; an air inlet hole and an air outlet hole which are communicated with the heat preservation chamber are arranged on the side wall of the mounting seat; the sealing cover plate is detachably connected to the upper end of the mounting seat, the accommodating cavity is located in the range sealed by the sealing cover plate, and a light-transmitting piece is arranged on the sealing cover plate in a position corresponding to the heat preservation chamber.
Compared with the prior art, the testing and characterizing device has the following advantages:
the testing device disclosed by the invention is a multi-purpose in-situ testing and characterization device, is used for detecting the performance of a sensor element, integrates temperature, humidity, gas control and sensor performance detection, and can realize in-situ characterization of a reaction kinetic process of the sensor element in a high-temperature environment; a light-transmitting piece is arranged in the center of the sealing cover plate of the in-situ test cavity and is used for transmitting light of different wave bands, so that the light-adding treatment is conveniently carried out by using infrared spectrums or Raman spectrums and the like in the experiment; the high temperature of the in-situ test cavity is realized by an internal heating table, and the heating table is matched with a temperature control device to realize PID closed-loop control of the temperature so as to realize continuous regulation of the temperature; the periphery of the heating table is coated by heat-insulating ceramics, so that local high temperature in the aluminum test cavity can be realized; in addition, the inner cavity structure of the mounting seat is more simplified, the cavity area is smaller, gas switching is quicker and more convenient during testing, and the response recovery time is shorter. On the other hand, the manufacturing cost is also reduced, more autonomy and convenience are provided for researchers, and the precious time on the research is saved.
As the improvement, the thermal-insulation ceramic plate is made for porous ceramic material, just one side of nearly heat preservation room is equipped with the mounting groove respectively on the thermal-insulation ceramic plate of the mount pad left and right sides, the embedded fixed ceramic plate that is equipped with fine and close ceramic material and makes of mounting groove, be equipped with the mounting hole along left right direction intercommunication on the fixed ceramic plate, the setting of probe symmetry is on the fixed ceramic plate of the left and right sides, just probe one end cartridge is in the mounting hole, and thermal-insulation ceramic plate, mount pad and external probe pin connection are worn out in proper order to the other end of probe. The heat-insulating ceramic plate in the improved structure is made of porous ceramic, so that the heat-insulating ceramic plate is light in weight and good in heat-insulating effect; in addition, since the installation of the probe needs to be perforated, in order to ensure the structural strength, a dense ceramic material with better mechanical property and processability is selected as the material for fixing the ceramic plate.
The fixed ceramic plate is provided with a plug hole and an adjusting hole which are communicated with each other along the direction from outside to inside, the probe can be assembled in the plug hole in a sliding way along the horizontal direction, and one end of the probe close to the heat preservation chamber can move downwards in the adjusting hole; the upper end of the fixed ceramic plate is respectively provided with a fastening screw which vertically extends to the inside of the inserting hole and the adjusting hole; and the lower end of the fastening screw is abutted against the side wall of the probe. In the above-mentioned improvement structure, the probe can horizontal sliding adjustment left and right sides position on fixed ceramic plate to the head position of probe can also carry out the fine setting of upper and lower position, thereby can guarantee like this that the probe can down move about and can withstand sensor element, carry on spacingly to it, prevent to wait to detect the component emergence offset of waiting under the high temperature.
The upper end surfaces of the left side and the right side of the mounting seat are provided with clamping grooves for containing probe leads, and the upper end of the mounting seat and the left side and the right side of the heat preservation chamber are respectively provided with a first avoiding groove for communicating the clamping grooves with the containing cavity; one end of the probe, which is far away from the heat preservation chamber, extends into the first avoiding groove. In the improved structure, because the requirement of checking the tightness of the device is met, when the device is installed, the lead wire of the probe and the clamping groove on the installation seat need to be sealed, when the subsequent left and right positions of the probe need to be finely adjusted, the lead wire in the clamping groove cannot be moved; the first recess of dodging just has played the effect of regulation this moment, promptly, when the installation, the first lead wire of can reserving a little bit of length in dodging the inslot, and the probe can not touch the lead wire in the draw-in groove like this when the level fine-tuning, guarantees the leakproofness.
Preferably, the heating assembly comprises a heating rod and a thermocouple which extend along the front-back direction of the heating table, and through holes for the wiring ends of the heating rod and the thermocouple to penetrate out are respectively formed in the heat preservation ceramic plate on the front side of the mounting seat; and the front side wall of the mounting seat is provided with a mounting hole for the heating rod and the lead of the thermocouple to penetrate out simultaneously. In the above-mentioned improvement structure, realize the mounting hole that two sets of signal lead wires of heating rod, thermocouple worn out simultaneously, reduce the mount pad trompil, retrench mount pad inner space to reduce inside cavity area.
In a further improvement, a second avoidance groove communicated with the heat preservation chamber is formed in the upper end of the mounting seat and located in front of the heat preservation chamber, and one ends of the heating rod and the thermocouple far away from the heating platform penetrate through the through hole and extend into the second avoidance groove; the mounting hole is communicated with the second avoiding groove. The arrangement of the second avoidance groove in the structure can facilitate the installation of the heating assembly on the installation seat, and the sealing performance in the heat preservation chamber can be better guaranteed.
In a further improvement, the air inlet hole and the air outlet hole are respectively formed in the front side wall and the rear side wall of the mounting seat, and the air inlet hole is communicated with the second avoiding groove; the upper end surfaces of the heat preservation ceramic plates on the front side and the rear side of the heat preservation chamber are flush with the upper end surface of the heating table. In the above-mentioned improved structure, the inlet port lets in and sends out the through-hole and can be quick and enter into detection area for wait to detect the component and can realize the detection of different environmental requirements fast, raise the efficiency.
And the bottom of the accommodating cavity is provided with a sunken concave cavity, so that a space is reserved between the heat-insulating ceramic plate and the bottom of the concave cavity after the heat-insulating ceramic plate is assembled at the bottom of the accommodating cavity. Make in the above-mentioned improved structure and leave an isolated space between bottom thermal insulation ceramic plate and the mount pad main part, have a certain amount of gas in the space, thereby have the performance heat preservation effect that makes thermal insulation ceramic plate can be better, the heat can not directly distribute away through the mount pad.
Preferably, the mounting seat and the sealing cover plate are made of aluminum materials; and a plurality of heat dissipation holes which are communicated up and down are arranged on the mounting seat and the sealing cover plate. The aluminum material has light weight, the heat dissipation block is convenient to carry; in addition, the heat dissipation holes are formed in the mounting seat and the sealing cover plate, and heat dissipation efficiency is further improved.
Preferably, the probe is made of gold-plated tungsten steel. The probe is made of gold-plated tungsten steel, the tungsten steel probe can ensure the testing sensitivity at high temperature, and the gold-plated layer can prevent tungsten steel from being oxidized by testing gas at high temperature to cause the probe to be non-conductive.
Drawings
Fig. 1 is an exploded view of the multifunctional in-situ test device of the present invention.
FIG. 2 is a schematic structural diagram of the multifunctional in-situ testing device of the present invention without a sealing cover plate.
Fig. 3 is a schematic structural view of the mount of the present invention.
Fig. 4 is a schematic view of the mounting base of fig. 3 after the insulating ceramic plate is mounted.
Fig. 5 is a schematic half-section of the structure of fig. 4.
Fig. 6 is a sectional view of a fixed ceramic plate in the present invention.
Fig. 7 is a partial sectional view of a sealing cover plate structure in the present invention.
Wherein shown in the figure:
1-mounting seat, 1.1-holding cavity, 1.2-concave cavity, 1.3-air inlet hole, 1.4-air outlet hole, 1.5-mounting hole, 1.6-clamping groove, 1.7-first avoiding groove, 1.8-second avoiding groove, 1.9-limiting boss, 2-insulating ceramic plate, 2.1-mounting groove, 3-heating table, 4-probe, 5-sealing cover plate, 6-light-transmitting piece, 7-fixing ceramic plate, 7.1-plugging hole, 7.2-adjusting hole, 8-fastening screw, 9-heat-radiating hole, 10-sealing gasket, 11-sealing gasket, 12-glass fixing ring, 13-ceramic screw and 14-insulating chamber.
Detailed Description
The invention is further described with reference to the following figures and detailed description.
In the description of the present invention, it should be noted that the terms "left, right", "upper end", "front, rear", "middle", "inner and outer", "lower end", "inner", "both sides", etc., indicate orientations or positional relationships based on those shown in the drawings, and are only for convenience of description and simplicity of description, but do not indicate or imply that the device or element being referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus, should not be construed as limiting the present invention. It should also be noted that the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the term "connected" is to be interpreted broadly, e.g. as a fixed connection, a detachable connection, or an integral connection; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
As shown in fig. 1 and 2, the invention provides a multifunctional in-situ testing device, which comprises a rectangular mounting base 1, wherein an inward concave accommodating cavity 1.1 is arranged in the middle of the upper end of the mounting base 1, the accommodating cavity 1.1 is of a rectangular cavity structure, heat-insulating ceramic plates 2 are arranged around and at the bottom of the accommodating cavity 1.1, and all the heat-insulating ceramic plates 2 enclose a heat-insulating chamber 14 with an upper opening, as shown in fig. 4; a heating table 3 is arranged in the inner cavity of the heat preservation chamber 14, and after the arrangement, a heating detection area is formed between the upper end surface of the heating table 3 and the inner side walls of the four circumferential heat preservation ceramic plates 2; in addition, a heating assembly and a temperature control assembly are arranged in the heating table 3; at least two probes 4 are arranged on the side wall of the heat preservation chamber 14, and when the element to be detected is placed on the heating table 3, all the probes 4 are pressed against the upper surface of the element to be detected (sensor element), so that the performance detection of the sensor element is realized. In this embodiment, the sensor element concerned is a sensor chip.
Preferably, at least two probes 4 in the above structure are symmetrically arranged on any two opposite side walls of the mounting base 1, and the probes 4 on the two side walls are symmetrically arranged with each other, so that the probes 4 are more stable and accurate for the press-fit detection of the element to be detected. Specifically, four probes 4 are respectively arranged on the left side and the right side of the heat preservation chamber 14 shown in fig. 2, and the four probes 4 are symmetrically arranged in the left-right direction, so that four groups of probes 4 for detection are realized, the four sensor elements can be simultaneously detected, the probes 4 can also play a role in compressing and positioning when being used for detecting the performance of the sensor elements, and specific how to realize vertical compression positioning is specifically explained in the following text.
On the other hand, in the structure of the embodiment, an air inlet hole 1.3 and an air outlet hole 1.4 which are communicated with the heat preservation chamber 14 are arranged on the side wall of the mounting seat 1; therefore, various different gases can be introduced into the heat preservation chamber 14, and the performance detection of the sensor element under different gas environments can be realized; in addition, a trace amount of moisture can be added into the gas introduced into the heat preservation chamber 14, so that environment detection of different humidity is realized, namely, multifunctional testing of the sensor element in environments with different temperatures, gases and humidity can be realized through one detection device.
In the structure, because the whole test environment needs to be carried out under the sealed environment, the upper end of the mounting seat 1 is detachably connected with the sealing cover plate 5, the accommodating cavity 1.1 is located in the range sealed by the sealing cover plate 5, the heat preservation chamber 14 forms a sealed chamber, in addition, the light transmission piece 6 is detachably assembled in the middle of the sealing cover plate 5, namely, the position corresponding to the heat preservation chamber 14, and the preferable light transmission piece 6 is a light transmission glass sheet.
Specifically, as shown in fig. 1, a layer of sealing gasket 10 is further disposed between the mounting seat 1 and the sealing cover plate 5 to achieve sealing engagement between the mounting seat 1 and the sealing cover plate 5, and preferably, the sealing gasket 10 is made of a polytetrafluoroethylene material and has better high temperature resistance. And the four corners of the upper cover 5 are respectively detachably connected and fixed with the mounting base 1 through corresponding connecting screws. In addition, a circular window 5.1 is arranged in the middle of the upper end of the sealing cover plate 5, a circular first step groove 5.2 for installing the light-transmitting member 6 is arranged on the periphery of the window, a sealing gasket 11 made of polytetrafluoroethylene is arranged between the light-transmitting member 6 and the first step groove 5.2, a circular second step groove 5.3 with the diameter larger than that of the first step groove 5.2 is also arranged above the first step groove 5.2 on the sealing cover plate 5, a glass fixing ring 12 is arranged on the second step groove 5.3, the inner end of the glass fixing ring 12 is tightly pressed and positioned on the upper end face of the light-transmitting member 6, and the outer end of the glass fixing ring 12 is fixed on the second step groove 5.3 through corresponding screw connections, so that the light-transmitting member 6 and the sealing cover plate 5 can be detachably and hermetically connected and fixed, and after the arrangement, the light-transmitting member 6 can be replaced according to requirements, as shown in fig. 7. The window for mounting the glass sheet on the upper cover of the test cavity is in a circular design, so that the strength of the upper cover of the test cavity can be better ensured; in addition, the lower end of the light-transmitting piece 6 is limited by a sealing washer 11 made of polytetrafluoroethylene material, so that the air tightness of the cavity is ensured, and meanwhile, the light-transmitting piece 6 is prevented from being fractured; the light-transmitting piece 6 is fixed by the annular glass fixing ring 12 made of aluminum, can be tightly fixed on the sealing cover plate 5 by using a screw of M3, and the screw does not penetrate through the sealing cover plate 5 and does not contact with the light-transmitting piece 6, so that the stability is ensured, and meanwhile, the sealing performance of the connecting structure of the light-transmitting piece 6 and the sealing cover plate 5 is ensured.
In the embodiment, the insulating ceramic plates 2 are made of porous ceramic materials, vertically extending mounting grooves 2.1 are respectively arranged on the left and right sides of the mounting seat 1 on one sides of the insulating ceramic plates 2 close to the insulating chamber 14, and fixed ceramic plates 7 made of compact ceramic materials are embedded in the mounting grooves 2.1; one end of the probe 4 passes through the fixed ceramic plate 7 and extends to the heat preservation chamber 14, and the other end of the probe 4 sequentially passes through the heat preservation ceramic plate 2 and the mounting seat 1 to be connected with an external probe lead.
As shown in fig. 2 and 6, the fixed ceramic plate 7 is provided with a plug hole 7.1 and an adjusting hole 7.2 which are communicated with each other along the direction from outside to inside, the probe 4 is slidably assembled in the plug hole 7.1 along the horizontal direction, and one end of the probe 4 close to the heat preservation chamber 14 can move downwards in the adjusting hole 7.2; the upper end of the fixed ceramic plate 7 is respectively provided with a fastening screw 8 which vertically extends to the insertion hole 7.1 and the inside of the adjusting hole 7.2, and the lower end of the fastening screw 8 is propped against the side wall of the probe 4. Specifically, as shown in fig. 6, the cylindrical hole of the plug hole 7.1, the adjusting hole 7.2 are vertically arranged waist-shaped holes, and the upper end surface of the adjusting hole 7.2 is flush with the upper end of the plug hole 7.1; when the probe 4 is inserted to a set position from the inserting hole 7.1 to the heat preservation chamber 14, the positioning of the probe 4 can be realized through the fastening screw 8 above the inserting hole 7.1, when the height of the probe 4 needs to be adjusted, the fastening screw 8 above the adjusting hole 7.2 can be screwed to promote the part of the probe 4 in the adjusting hole 7.2 to generate micro elastic deformation downwards, so that the probe 4 can be vertically pressed and limited on the upper surface of the sensor element, the signal detection is realized, meanwhile, the limiting effect is realized through the fact that the probe 4 is pressed on the upper end surface of the sensor element, and the inaccurate detection result caused by the position deviation of the sensor element in a high-temperature environment is avoided. On the other hand, the fixed ceramic plate 7 arranged in the structure realizes the fixation of the probe 4, can ensure the insulation between the probe 4 and the accommodating cavity 1.1, can ensure no short circuit between the probe 4 and the accommodating cavity 1.1, and can ensure the stable output of detection signals.
Preferably, as shown in fig. 2 and 4, the upper end surfaces of the left and right sides of the mounting base 1 are provided with a clamping groove 1.6 for accommodating a probe lead, and the upper end of the mounting base 1 and the left and right sides of the heat preservation chamber 14 are further provided with a first avoidance groove 1.7 for communicating the clamping groove 1.6 with the accommodating chamber 1.1; one end of the probe 4 far away from the insulation chamber 14 extends into the first avoiding groove 1.7.
In this embodiment, the heating assembly comprises a heating rod and a thermocouple (not shown in the figure) which are arranged along the front-back direction of the heating table 3 in an extending way, and through holes 2.1 for the connection terminal parts of the heating rod and the thermocouple to penetrate out are respectively arranged on the heat preservation ceramic plate 2 at the front side of the mounting seat 1; the front side wall of the mounting seat 1 is provided with a mounting hole 1.5 for leading wires of the heating rod and the thermocouple to simultaneously penetrate out. The mounting seat 1 is provided with a mounting hole 1.5 through which two groups of signal leads of the heating rod and the thermocouple can simultaneously penetrate, and specifically, the two groups of signal leads in the mounting hole 1.5 are led out through an aviation plug and are in butt joint with another aviation plug outside which is connected with the heating rod and the thermocouple signal lead.
More specifically, a second avoidance groove 1.8 communicated with the heat preservation chamber 14 is formed in the upper end of the mounting seat 1 and in front of the heat preservation chamber 14, and one ends of the heating rod and the thermocouple far away from the heating platform 3 penetrate through the through hole 2.1 and extend into the second avoidance groove 1.8; the mounting hole 1.3 is communicated with the second avoiding groove 1.8. As shown in fig. 4, an air inlet 1.3 and an air outlet 1.4 are respectively arranged on the front and rear side walls of the mounting seat 1, and the air inlet 1.3 is communicated with a second avoidance groove 1.8; the upper end surfaces of the heat preservation ceramic plates 2 at the front side and the rear side of the heat preservation chamber 14 are flush with the upper end surface of the heating table 3. Be provided with asymmetric inlet port 1.3 of fore-and-aft direction and venthole 1.4 on the lateral wall around mount pad 1, gaseous by inlet port 1.3 entering heat preservation room 14, discharge through venthole 1.4, and in this structure, 2 up end of the heat preservation ceramic plate that lie in heat preservation room 14 front and back both sides are less than the heat preservation ceramic plate 2 of the left and right sides, in order to form a low groove, the gas that lets in from inlet port 1.3 like this can dodge recess 1.8 through the second, then enter into heat preservation room 14 from the low groove, from the low groove of opposite side at last, discharge through venthole 1.4. Whole structure guarantees can be faster switch when letting in gas, reduces gaseous delay, reduces and switches the required reaction time of gas.
On the other hand, as shown in fig. 5, a sunken concave cavity 1.2 is formed at the bottom of the accommodating cavity 1.1, so that a space is reserved between the insulating ceramic plate 2 and the bottom of the concave cavity 1.2 after the insulating ceramic plate 2 is assembled at the bottom of the accommodating cavity 1.1. After setting up like this, the space that forms between insulating ceramic plate 2 and cavity 1.2 to have a certain amount of gas in the space, avoid insulating ceramic plate 2 and mount pad 1 direct contact, because in this embodiment, the better aluminum product of radiating effect that mount pad 1 adopted, but the local high temperature environment need be guaranteed again in insulating chamber 14 region, so interval setting in the above-mentioned structure has better heat preservation effect than direct contact.
As shown in fig. 3, the left side and the right side of the containing cavity 1.1 are further provided with limiting bosses 1.9, after the heat preservation ceramic plate 2 is assembled at the bottom of the containing cavity 1.1, the upper surface of the heat preservation ceramic plate 2 at the bottom is flush with the upper surface of the limiting bosses 1.9, after the arrangement, when the heat preservation ceramic plate 2 is assembled around the containing cavity 1.1, the heat preservation ceramic plates 2 at the left side and the right side of the containing cavity 1.1 are simultaneously pressed on the upper portions of the outer edges of the limiting bosses 1.9 and the heat preservation ceramic plate 2 at the bottom, as shown in fig. 5, the pressing positioning of the heat preservation ceramic plate 2 at the bottom of the containing cavity 1.1 can be realized, and the stability is improved.
In the structure, the mounting seat 1 and the sealing cover plate 5 are made of aluminum materials, so that a better heat dissipation effect is ensured; and a plurality of heat dissipation holes 9 which are communicated up and down are formed in the mounting seat 1 and the sealing cover plate 5, and corresponding through holes are also formed in a sealing gasket 10 between the sealing cover plate 5 and the mounting seat 1, so that the heat dissipation holes 9 in the mounting seat 1 and the sealing cover plate 5 are vertically communicated, and the heat dissipation effect is further improved.
In addition, the probe 4 is made of gold-plated tungsten steel. The material of the probe 4 in this embodiment is made of gold-plated tungsten steel because: the tungsten steel probe has very high strength below three thousand ℃, and can be ensured to be tightly propped against the sensor element; however, the tungsten steel probe is very easily oxidized in a high-temperature atmosphere environment, and the generated oxide layer can make the probe non-conductive. Noble metal gold is not easily oxidized at high temperature (below one thousand degrees centigrade), but is not suitable for being directly used as a probe material because of its soft texture and high price. The preferred gold-plated tungsten steel probe can solve the above problems, the tungsten steel can ensure the strength at high temperature, and the gold-plated layer can prevent the tungsten steel probe from being oxidized by the test gas at high temperature to be non-conductive.
In this embodiment, still be equipped with three ceramic screw support 13 in mount pad 1 bottom, as shown in fig. 5, three ceramic screw are triangle-shaped and distribute, and the triangle-shaped structure can make the support more firm, makes mount pad 1 of high temperature not direct contact desktop simultaneously, realizes that the physics is thermal-insulated, prevents to scald supporter such as desk.
The foregoing has described preferred embodiments of the present invention and is not to be construed as limiting the claims. The present invention is not limited to the above embodiments, and the specific structure thereof is allowed to vary, and various changes made within the scope of the claims of the present invention are within the scope of the present invention.

Claims (10)

1. A multi-functional normal position characterization and testing arrangement which characterized in that: the heat preservation device comprises a mounting seat (1) and a sealing cover plate (5), wherein an inwards concave containing cavity (1.1) is formed in the upper end of the mounting seat (1), heat preservation ceramic plates (2) are arranged on the periphery and the bottom of the containing cavity (1.1), all the heat preservation ceramic plates (2) are enclosed to form a heat preservation chamber (14), a heating table (3) is arranged in the heat preservation chamber (14), and a heating assembly and a temperature control assembly are arranged in the heating table (3); the side wall of the heat preservation chamber (14) is provided with at least two probes (4), and when the element to be detected is placed on the heating table (3), all the probes (4) are pressed against the upper surface of the sensor element to be detected; an air inlet hole (1.3) and an air outlet hole (1.4) which are communicated with the heat preservation chamber (14) are arranged on the side wall of the mounting seat (1); the sealing cover plate (5) is detachably connected to the upper end of the mounting seat (1), the accommodating cavity (1.1) is located in the range sealed by the sealing cover plate (5), and a light-transmitting piece (6) is arranged on the sealing cover plate (5) in a position corresponding to the heat preservation chamber (14).
2. The multifunctional in-situ characterization and testing device of claim 1, wherein: the heat-insulating ceramic plate (2) is made of porous ceramic materials, mounting grooves (2.1) are respectively formed in the sides, close to the heat-insulating chamber (14), of the heat-insulating ceramic plates (2) on the left side and the right side of the mounting seat (1), and fixed ceramic plates (7) made of compact ceramic materials are embedded in the mounting grooves (2.1); the probe (4) is symmetrically arranged on the fixed ceramic plates (7) on the left side and the right side, one end of the probe (4) penetrates through the fixed ceramic plates (7) to extend to the heat preservation chamber (14), and the other end of the probe (4) penetrates out of the heat preservation ceramic plates (2) and the mounting seat (1) in sequence to be connected with an external probe lead.
3. The multifunctional in-situ characterization and testing device of claim 2, wherein: the fixed ceramic plate (7) is provided with an inserting hole (7.1) and an adjusting hole (7.2) which are communicated with each other along the direction from outside to inside, the probe (4) can be assembled in the inserting hole (7.1) in a sliding way along the horizontal direction, and one end of the probe (4) close to the heat preservation chamber (14) can move downwards in the adjusting hole (7.2); the upper end of the fixed ceramic plate (7) is respectively provided with a fastening screw (8) which vertically extends to the inside of the inserting hole (7.1) and the adjusting hole (7.2), and the lower end of the fastening screw (8) is abutted against the side wall of the probe (4).
4. The multifunctional in-situ characterization and testing device of claim 3, characterized by: the upper end surfaces of the left side and the right side of the mounting seat (1) are provided with clamping grooves (1.6) for containing probe leads, and the upper end of the mounting seat (1) and the left side and the right side of the heat preservation chamber (14) are respectively provided with first avoiding grooves (1.7) for communicating the clamping grooves (1.6) with the containing cavities (1.1); one end of the probe (4) far away from the heat preservation chamber (14) extends into the first avoiding groove (1.7).
5. The multifunctional in-situ characterization and testing device according to any one of claims 1 to 4, characterized in that: the heating assembly comprises a heating rod and a thermocouple which extend along the front-back direction of the heating table (3), and through holes (2.1) for the wiring ends of the heating rod and the thermocouple to penetrate out are respectively formed in the heat-insulating ceramic plate (2) on the front side of the mounting seat (1); and the front side wall of the mounting seat (1) is provided with a mounting hole (1.5) for leading wires of the heating rod and the thermocouple to penetrate out simultaneously.
6. The multifunctional in-situ characterization and testing device of claim 5, wherein: a second avoidance groove (1.8) communicated with the heat preservation chamber (14) is formed in the upper end of the mounting seat (1) and located in front of the heat preservation chamber (14), and one ends, far away from the heating table (3), of the heating rod and the thermocouple penetrate through the through hole (2.1) and extend into the second avoidance groove (1.8); the mounting hole (1.5) is communicated with the second avoiding groove (1.8).
7. The multifunctional in-situ characterization and testing device of claim 6, wherein: the air inlet hole (1.3) and the air outlet hole (1.4) are respectively formed in the front side wall and the rear side wall of the mounting seat (1), and the air inlet hole (1.3) is communicated with the second avoiding groove (1.8); the upper end surfaces of the heat preservation ceramic plates (2) on the front side and the rear side of the heat preservation chamber (14) are lower than the heat preservation ceramic plates (2) on the left side and the right side, so that gas introduced from the gas inlet holes (1.3) can enter the heat preservation chamber (14) and is discharged from the gas outlet holes (1.4).
8. The multifunctional in-situ characterization and testing device of claim 1, wherein: the bottom of the accommodating cavity (1.1) is provided with a sunken concave cavity (1.2), so that a space is reserved between the bottom of the accommodating cavity (1.1) and the bottom of the concave cavity (1.2) after the heat-insulating ceramic plate (2) is assembled at the bottom of the accommodating cavity (1.1).
9. The multifunctional in-situ characterization and testing device of claim 1, wherein: the mounting seat (1) and the sealing cover plate (5) are made of aluminum materials; and a plurality of heat dissipation holes (9) which are communicated up and down are arranged on the mounting seat (1) and the sealing cover plate (5).
10. The multifunctional in-situ characterization and testing device of claim 1, wherein: the probe (4) is made of gold-plated tungsten steel.
CN202111010429.5A 2021-08-31 2021-08-31 Multifunctional in-situ characterization and test device Pending CN113701799A (en)

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