CN113615716A - Mite-removing and bacteriostatic spray composition and preparation process thereof - Google Patents

Mite-removing and bacteriostatic spray composition and preparation process thereof Download PDF

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Publication number
CN113615716A
CN113615716A CN202110731101.6A CN202110731101A CN113615716A CN 113615716 A CN113615716 A CN 113615716A CN 202110731101 A CN202110731101 A CN 202110731101A CN 113615716 A CN113615716 A CN 113615716A
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China
Prior art keywords
mite
veratrum
silver ion
extract
killing
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CN202110731101.6A
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Chinese (zh)
Inventor
侯俊行
刘智睿
林铱淳
周昊仁
王晓娟
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Foshan Fengqi Hongke Biotechnology Co ltd
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Foshan Fengqi Hongke Biotechnology Co ltd
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Priority to CN202110731101.6A priority Critical patent/CN113615716A/en
Publication of CN113615716A publication Critical patent/CN113615716A/en
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
    • A01N25/06—Aerosols
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16—Heavy metals; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives

Abstract

The invention discloses a mite-removing and bacteriostatic spray composition and a preparation process thereof, and relates to the technical field of household articles. The invention comprises the following components in percentage by mass: 10-20% of plant mite-repellent active group, 5-10% of organic lipid compound, 1-5% of chelated silver ion disinfectant and a proper amount of negative ion water, wherein the plant mite-repellent active group comprises a veratrum extract extracted from veratrum particles and a rosemary extract extracted from rosemary particles, and the weight ratio of the veratrum extract to the rosemary extract is 20-40: 60-80. The mite-removing and bacteriostatic spray disclosed by the invention is safe, stable and non-irritant, can be directly sprayed on a part needing removing bacteria and mites, has high-efficiency bacterium-inhibiting and mite-removing performances, can remove most of allergens of mites, has small irritation to skin, does not influence human health, can reduce pollution to environment, and is environment-friendly.

Description

Mite-removing and bacteriostatic spray composition and preparation process thereof
Technical Field
The invention belongs to the technical field of household articles, and particularly relates to a mite-removing and bacteriostatic spray composition and a preparation process thereof.
Background
Mites belong to a class of small animals in the Guangdong subclass of the Arabidopis of the phyla Arthropoda, and the mites are found to be closely related to human health, such as spider mites, chiggers, scabies, Demodex mites, flour mites, dust mites, Typhae mites and the like which can bite people to suck blood and damage the skin, cause 'acne rosacea' or Demodex, anaphylaxis, urinary tract mites, pulmonary mites, intestinal mites and scabies and seriously harm the human health. In the living space of people, a plurality of bacteria and mite microorganisms can be contacted every day, the bacteriostatic mite-killing spraying agent can be generated by transportation in order to avoid the harm of the bacteria and mites to human bodies, and the bacteriostatic mite-killing spraying agent can be directly sprayed on the surface of fabrics, vessels or skin to kill bacteria or mites.
The patent application with the publication number of CN106350257A discloses a mite-removing laundry detergent which comprises essence, sulfur, orange oil, sodium sulfate, fatty alcohol-polyoxyethylene ether, a synergist and water, wherein the mass parts of the components are as follows: 2.6-3.5 parts of essence, 5-6.6 parts of sulfur, 3.4-4.5 parts of orange oil, 2-3 parts of sodium sulfate, 2-3.1 parts of fatty alcohol-polyoxyethylene ether, 4-6 parts of synergist and 20-30 parts of water. The mite-removing laundry detergent disclosed by the invention is strong in dirt-removing capacity, can effectively clean stubborn oil stains, yellow spots, rust stains, stains and the like of clothes, has good killing power for common mites, can remove most of mites in an incubation hotbed, does not damage the clothes, and is bright in color and luster. Insoluble substances do not remain on the surface of the cleaning object, and the quality of the cleaning object is not affected.
The sulfur disclosed in the application is corrosive, and the bactericide and the mite removing component belong to synthetic chemical raw materials, so that the components remained on the surface of the skin can irritate the skin in the using process, influence the health of the skin and cause certain pollution to the environment.
The patent application with the publication number of CN107418796A discloses a mite-killing soap solution which is prepared from the following raw materials in parts by weight: 2-6 parts of soap base, 2-6 parts of tea saponin, 1-3 parts of sodium perborate, 1-3 parts of sodium carbonate, 1-3 parts of tetrapotassium pyrophosphate, 4-12 parts of essence, 2-6 parts of wheat protein, 2-4 parts of sorbitol, 1-3 parts of palmitin, 2-6 parts of carboxymethyl cellulose, 2-6 parts of pyriminostrobin, 2-6 parts of pyridaben, 3-9 parts of whitening agent and 2-6 parts of bleaching agent. The mite-killing soap solution prepared by the invention has strong dirt-removing power, is easy to rinse and milder, and can effectively kill mites.
The mixed liquid disclosed in the application is added with a whitening agent and a bleaching agent, the main component of the bleaching agent is sodium hypochlorite, chlorine can be generated, and the chlorine belongs to a strong corrosive gas, damages the respiratory organs of a human body and is harmful to the skin.
Disclosure of Invention
The invention aims to provide a mite-killing bacteriostatic spray composition and a preparation process thereof, and solves the technical problems that components remained on the surface of skin in the using process of the existing mite-killing bacteriostatic spray can stimulate the skin, influence the health of the skin and cause certain pollution to the environment.
In order to achieve the purpose, the invention is realized by the following technical scheme:
the mite-removing bacteriostatic spray composition comprises the following components in percentage by mass: 10-20% of plant mite-repellent active group, 5-10% of organic lipid compound, 1-5% of chelated silver ion disinfectant and a proper amount of negative ion water, wherein the plant mite-repellent active group comprises a veratrum extract extracted from veratrum particles and a rosemary extract extracted from rosemary particles, and the weight ratio of the veratrum extract to the rosemary extract is 20-40: 60-80.
Optionally, veratrum: the plant of genus Veratrum of family Liliaceae is perennial herb, has short and thick rhizome, has leaves in stem, often has residual leaf sheath cracked into fibrous shape in the base, usually has broad leaves, has stem holding, has strong pulse and has fold, green white or dark purple, amphoteric or miscellaneous property, has short stem, and is arranged into tip-growing large cone inflorescence.
Optionally, rosemary: the shrubs of dicotyledons, Labiatae and Rosmarinus are favorable for warm climate, and the leaves of Rosmarinus officinalis are leathery and relatively drought-resistant, so that China is introduced in Europe and the coast of the Mediterranean coast in northern Africa far away in the Caowei period.
Alternatively, the organic lipid compound comprises glycerol, glycerol: has a chemical formula of C3H8O3Colorless, odorless, sweet in taste, clear, viscous and liquid in appearance, is an organic matter, and has a boiling point: 290 ℃ at760mmHg, melting point: 18.17 ℃ and relative density 25 ℃: 1.2551, solubility: can absorb moisture from the air, hydrogen sulfide, hydrogen cyanide and sulfur dioxide, and is insoluble in benzene, chloroform, carbon tetrachloride, carbon disulfide, petroleum ether and oils.
Optionally, the effective component of the silver ion in the chelated silver ion disinfectant is 35ppm, the chelated silver ion disinfectant comprises chelated silver ion water, silicone oil and a surfactant, the chelated silver ion water comprises chelated silver ions and deionized water, and the chelation refers to an effect that metal ions are connected with two or more coordination atoms in the same molecule through coordination bonds in a chemical reaction to form a heterocyclic structure containing the metal ions.
A preparation process of mite-killing and bacteriostatic spray comprises the following steps:
the method comprises the following steps: preparing 5 parts of organic lipid compound, 1 part of chelated silver ion disinfectant and the balance of negative ion water;
step two: extraction: weighing veratrum particles and rosemary particles, mixing to obtain a mixed particle raw material, adding the mixed particle raw material into an absolute ethyl alcohol solution, and performing reflux extraction and filtration to obtain an extracting solution;
step three: preparation: mixing the solution of rhizoma et radix Veratri extract and herba Rosmarini officinalis extract with organic lipid compound and silver ion disinfectant, stirring, and making the extractive solution into microemulsion, soluble solution or aqua to obtain mite-removing and antibacterial spray.
Optionally, in the second step, the reflux temperature is 60-80 ℃, a precise temperature controller is used for monitoring temperature change, circulation of cooling water is ensured during reflux, and finally residual liquid in the reflux device is washed and recovered.
Optionally, in the second step, the feed-liquid ratio of the mixed particle raw material to the absolute ethyl alcohol solution is 1: 3, the ethanol solution with the concentration of 99.5 percent is absolute ethanol which is a mixture of ethanol and water, and the appearance and the properties are as follows: colorless liquid, having a special flavor, melting point: -114 ℃, density: 0.79g/cm3Boiling point: at 78 ℃.
Optionally, in the second step, the extraction is repeated for 15 times to obtain the required extract, and a soxhlet extractor is selected for extraction, wherein the soxhlet extractor comprises an extraction bottle, an extraction tube and a condenser.
Optionally, a stainless steel filter screen of 200 meshes is selected for filtering in the second step, and the diameter of the holes of the 200 meshes is 74.162 μm.
The embodiment of the invention has the following beneficial effects:
the mite-removing and bacteriostatic spray disclosed by the invention is safe, stable and non-irritant, can be directly sprayed on a part needing removing bacteria and mites, has high-efficiency bacterium-inhibiting and mite-removing performances, can remove most of allergens of mites, has small irritation to skin, does not influence human health, can reduce pollution to environment, and is environment-friendly.
Of course, it is not necessary for any product in which the invention is practiced to achieve all of the above-described advantages at the same time.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. The following description of at least one exemplary embodiment is merely illustrative in nature and is in no way intended to limit the invention, its application, or uses.
To maintain the following description of the embodiments of the present invention clear and concise, a detailed description of known functions and known components of the invention have been omitted.
In this embodiment, there is provided a mite-killing bacteriostatic spray composition comprising: the components with the following mass percentage content: 10-20% of plant acarid-expelling active groups, 5-10% of organic lipid compounds, 1-5% of chelated silver ion disinfectant and a proper amount of negative ion water, wherein the negative ion water has the effects of safety, zero stimulation, super-strong permeation, oxidation resistance and dirt stripping, the plant acarid-expelling active groups comprise a veratrum extract extracted from veratrum particles and a rosemary extract extracted from rosemary particles, and the weight ratio of the veratrum extract to the rosemary extract is 20-40: 60-80.
The application process of this embodiment is as follows: firstly, preparing 5 parts of organic lipid compounds, 1 part of chelated silver ion disinfectant and the balance of negative ion water, then extracting and filtering the veratrum particles and the rosemary particles, and uniformly stirring the veratrum extract and rosemary extract solution, the organic lipid compounds and the silver ion disinfectant to obtain the mite-removing and bacteriostatic spray. It should be noted that all the electric devices referred to in this application may be powered by a storage battery or an external power source.
The mite-removing and bacteriostatic spray disclosed by the invention is safe, stable and non-irritant, can be directly sprayed on a part needing removing bacteria and mites, has high-efficiency bacterium-inhibiting and mite-removing performances, can remove most of allergens of mites, has small irritation to skin, does not influence human health, can reduce pollution to environment, and is environment-friendly.
Veratrum of this embodiment: the plant of the genus veratrum of the family liliaceae is a Chinese medicinal material with extremely strong medicinal properties, and has the functions of resisting oxidation, resisting free radicals, preventing aging and killing pests.
Rosemary of this example: the leaves of rosemary are leather and relatively drought-resistant, and the rosemary has the effects of sterilizing, removing mites and expelling insects in native European regions and northern Mediterranean coasts of Africa when China is introduced in the Caowei period.
This implementationExemplary organic lipid compounds include glycerol, glycerol: has a chemical formula of C3H8O3Colorless, odorless, sweet in taste, clear, viscous and liquid in appearance, is an organic matter, and has a boiling point: 290 ℃ at760mmHg, melting point: 18.17 ℃ and relative density 25 ℃: 1.2551, solubility: can absorb moisture from the air, and also can absorb hydrogen sulfide, hydrogen cyanide and sulfur dioxide, is insoluble in benzene, chloroform, carbon tetrachloride, carbon disulfide, petroleum ether and oils, has little irritation to the skin, can protect the skin, reduces the sensitivity, and has no pollution to the environment.
The effective component of the silver ions in the chelated silver ion disinfectant of the embodiment is 35ppm, the chelated silver ion disinfectant comprises chelated silver ion water, silicone oil and a surfactant, the chelated silver ion water comprises chelated silver ions and deionized water, chelation refers to an effect that metal ions are connected with two or more coordination atoms in the same molecule through coordination bonds in a chemical reaction to form a heterocyclic structure containing the metal ions, and the chelated silver ion disinfectant does not contain elements harmful to human bodies and the environment and chemical residues, so that the environment cannot be polluted and the environmental friendliness is achieved.
A preparation process of mite-killing and bacteriostatic spray comprises the following steps:
the method comprises the following steps: preparing 5 parts of organic lipid compound, 1 part of chelated silver ion disinfectant and the balance of negative ion water;
step two: extraction: weighing veratrum particles and rosemary particles, mixing to obtain a mixed particle raw material, weighing the veratrum particles and the rosemary particles by using an electronic balance, adding the mixed particle raw material into an absolute ethyl alcohol solution, and performing reflux extraction and filtration to obtain an extracting solution, wherein the electronic balance has the characteristics of high precision and sensitivity and high reaction speed;
step three: preparation: the veratrum extract and rosemary extract solution, organic lipid compounds and silver ion disinfectant are uniformly stirred, the extracting solution is prepared into microemulsion, soluble solution or aqueous solution, the microemulsion is safe to store and transport, the environmental pollution is less, a large amount of organic solvent can be saved, the soluble solution or aqueous solution has the characteristics of low phytotoxicity, small toxicity, easy dilution and safe and convenient use, the active ingredients are in a molecular or ionic state, and the prepared solvent is subpackaged into a spray bottle to obtain the mite-removing and bacteriostatic spray.
The reflux temperature is 60 ~ 80 ℃ in the step two of this embodiment, utilizes the change of accurate temperature control appearance monitoring temperature, improves backward flow efficiency, and the circulation of cooling water is guaranteed during the backward flow for the first time, and it is exactly that the utilization ratio of the improvement raw materials is convenient for to wash the recovery to the remaining liquid in the reflux unit at last.
In the second step of this example, the ratio of the mixed particle raw material to the absolute ethyl alcohol solution is 1: 3, the ethanol solution with the concentration of 99.5 percent is absolute ethanol which is a mixture of ethanol and water, and the appearance and the properties are as follows: colorless liquid, having a special flavor, melting point: -114 ℃, density: 0.79g/cm3Boiling point: and at 78 ℃, the ethanol is used as a solvent to separate and purify the mixed particle raw material by utilizing the solubility of the ethanol, so that the extracting solution has low viscosity, is easy to filter and is convenient to concentrate.
In the second step of this embodiment, the extraction is repeated 15 times to obtain the desired extract, and a soxhlet extractor is selected for extraction, which comprises an extraction bottle, an extraction tube and a condenser, and the solid substance is continuously extracted by the pure solvent by using the solvent reflux and siphon principles, thus saving the solvent, achieving high extraction efficiency, good selectivity, low energy consumption, simple equipment and simple operation.
In the second step of this embodiment, a stainless steel filter screen of 200 meshes is selected for filtration, the diameter of the holes of the 200 meshes is 74.162 μm, and the stainless steel filter screen has the following properties: the stainless steel filter screen with the mesh number is favorable for improving the filtering effect of the extracting solution.
Most of the existing bacteriostatic mite-removing spray takes 4-chloro-3, 5-dimethylphenol (PCMX) or cationic quaternary ammonium salt bactericides as bactericidal components and amides or acylureas substances as mite-removing components, the bactericides and mite-removing components belong to synthetic chemical raw materials, and components remained on the surface of the skin can irritate the skin in the using process, influence the health of the skin and cause certain pollution to the environment.
The organic lipid compound includes glycerol.
The mite-removing bacteriostatic spray composition comprises the following components in parts by weight: 5 parts of organic lipid compounds, 1 part of chelated silver ion disinfectant and the balance of negative ion water.
The preparation method of the veratrum extract and the rosemary extract comprises the following steps:
a, extracting: weighing veratrum particles and rosemary particles, mixing, and mixing according to a material-liquid ratio of 1: 3 adding 75% ethanol solution, reflux extracting at 60-80 deg.C, filtering to obtain extractive solution, and repeating the extraction process for 15 times.
b, preparation: the extractive solution can be made into microemulsion, soluble agent or aqua.
And uniformly stirring the veratrum extract and rosemary extract solution with an organic lipid compound and a silver ion disinfectant to obtain the mite-removing and bacteriostatic spray.
The above embodiments may be combined with each other.
It is noted that the terms first, second and the like in the description and in the claims of the present application are used for distinguishing between similar elements and not necessarily for describing a particular sequential or chronological order. It should be understood that the data so used may be interchanged under appropriate circumstances such that the embodiments of the application described herein may be practiced in sequences other than those described herein.
In the description of the present invention, it is to be understood that the orientation or positional relationship indicated by the orientation words such as "front, rear, upper, lower, left, right", "lateral, vertical, horizontal" and "top, bottom", etc., are usually based on orientation or positional relationship, and are for convenience only to facilitate description of the invention and to simplify description, and in the case of not making a contrary explanation, these orientation words do not indicate and imply that the device or element being referred to must have a specific orientation or be constructed and operated in a specific orientation, and therefore, should not be considered as limiting the scope of the invention; the terms "inner and outer" refer to the inner and outer relative to the profile of the respective component itself.

Claims (10)

1. An acarus killing and bacteriostatic spray composition, which is characterized by comprising: the components with the following mass percentage content: 10-20% of plant mite-repellent active group, 5-10% of organic lipid compound, 1-5% of chelated silver ion disinfectant and a proper amount of negative ion water, wherein the plant mite-repellent active group comprises a veratrum extract extracted from veratrum particles and a rosemary extract extracted from rosemary particles, and the weight ratio of the veratrum extract to the rosemary extract is 20-40: 60-80.
2. The acarus-killing bacteriostatic spray composition of claim 1, wherein the weight ratio of veratrum: the plant of genus Veratrum of family Liliaceae is perennial herb, has short and thick rhizome, has leaves in stem, often has residual leaf sheath cracked into fibrous shape in the base, usually has broad leaves, has stem holding, has strong pulse and has fold, green white or dark purple, amphoteric or miscellaneous property, has short stem, and is arranged into tip-growing large cone inflorescence.
3. The acarus-killing bacteriostatic spray composition of claim 1, wherein rosemary: the shrubs of dicotyledons, Labiatae and Rosmarinus are favorable for warm climate, and the leaves of Rosmarinus officinalis are leathery and relatively drought-resistant, so that China is introduced in Europe and the coast of the Mediterranean coast in northern Africa far away in the Caowei period.
4. The acarus-killing bacteriostatic spray composition of claim 1 wherein the organic lipid compound comprises glycerol, glycerin: has a chemical formula of C3H8O3Colorless, odorless, sweet in taste, clear, viscous and liquid in appearance, is an organic matter, and has a boiling point: 290 ℃ at760mmHg, melting point: 18.17 ℃ and relative density 25 ℃: 1.2551, solubility: can absorb moisture from the air, hydrogen sulfide, hydrogen cyanide and sulfur dioxide, and is insoluble in benzene, chloroform, carbon tetrachloride, carbon disulfide, petroleum ether and oils.
5. The spray composition as claimed in claim 1, wherein the effective component of silver ion in the silver ion-chelated disinfectant is 35ppm, the silver ion-chelated disinfectant comprises silver ion-chelated water, silicone oil and surfactant, the silver ion-chelated water comprises silver ion-chelated ions and deionized water, and chelation refers to an action of metal ions in chemical reaction being connected with two or more coordination atoms in the same molecule by coordination bonds to form a heterocyclic structure containing metal ions.
6. A preparation process of mite-killing and bacteriostatic spray is characterized by comprising the following steps:
the method comprises the following steps: preparing 5 parts of organic lipid compound, 1 part of chelated silver ion disinfectant and the balance of negative ion water;
step two: extraction: weighing veratrum particles and rosemary particles, mixing to obtain a mixed particle raw material, adding the mixed particle raw material into an absolute ethyl alcohol solution, and performing reflux extraction and filtration to obtain an extracting solution;
step three: preparation: mixing the solution of rhizoma et radix Veratri extract and herba Rosmarini officinalis extract with organic lipid compound and silver ion disinfectant, stirring, and making the extractive solution into microemulsion, soluble solution or aqua to obtain mite-removing and antibacterial spray.
7. The preparation process of the spray for killing and inhibiting bacteria of claim 6, wherein the reflux temperature in the second step is 60-80 ℃, a precise temperature controller is used for monitoring the temperature change, the circulation of cooling water is ensured during reflux, and finally the residual liquid in the reflux device is washed and recovered.
8. The preparation process of the spray for killing mites and inhibiting bacteria as claimed in claim 6, wherein the feed-liquid ratio of the mixed particle raw material and the absolute ethyl alcohol solution in the second step is 1: 3, the ethanol solution with the concentration of 99.5 percent is absolute ethanol which is a mixture of ethanol and water, and the appearance and the properties are as follows: colorless liquid, having a special flavor, melting point: -114 ℃, density: 0.79g/cm3Boiling point: at 78 ℃.
9. The spray preparation process of claim 6, wherein in step two, the extraction is repeated 15 times to obtain the required extract, and a Soxhlet extractor is selected for extraction, wherein the Soxhlet extractor comprises an extraction bottle, an extraction tube and a condenser.
10. The preparation process of a spray for killing and inhibiting bacteria of claim 6, wherein the filtering in step two is performed by a stainless steel screen of 200 meshes, and the diameter of the holes of 200 meshes is 74.162 μm.
CN202110731101.6A 2021-06-29 2021-06-29 Mite-removing and bacteriostatic spray composition and preparation process thereof Pending CN113615716A (en)

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Application publication date: 20211109