CN113559019A - Preparation method of wild chrysanthemum flower facial mask - Google Patents
Preparation method of wild chrysanthemum flower facial mask Download PDFInfo
- Publication number
- CN113559019A CN113559019A CN202110936290.0A CN202110936290A CN113559019A CN 113559019 A CN113559019 A CN 113559019A CN 202110936290 A CN202110936290 A CN 202110936290A CN 113559019 A CN113559019 A CN 113559019A
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- China
- Prior art keywords
- wild chrysanthemum
- solution
- volatile oil
- facial mask
- chrysanthemum flower
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Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8129—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers or esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers, e.g. polyvinylmethylether
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention discloses a preparation method of a wild chrysanthemum flower facial mask, which comprises the steps of preparing solution A, solution B and solution C, preparing a skin care facial mask through component analysis and prescription design, extracting volatile oil of wild chrysanthemum flowers by using a steam distillation method, analyzing the component composition of the volatile oil of the wild chrysanthemum flowers by using a gas chromatography-mass spectrometer, measuring the reducing power to evaluate the antioxidant performance of the volatile oil, optimizing the prescription composition and preparation process of the wild chrysanthemum flower facial mask, and primarily evaluating the sense and performance of the facial mask, wherein the facial mask has no layering phenomenon or oil floating phenomenon under the conditions of high temperature or low temperature, has good stability of the whole facial mask, and can effectively solve the problem that polyvinyl alcohol is difficult to dissolve.
Description
Technical Field
The invention relates to the technical field of wild chrysanthemum flower masks, and particularly relates to a preparation method of a wild chrysanthemum flower mask.
Background
Wild chrysanthemum (Dendranthemama indicum) belongs to a natural Chinese herbal medicine, belongs to a perennial herb of compositae, has a similar shape to that of wild chrysanthemum flower, is usually grown in wild zones such as hilly grassland, field edge and the like, and is produced in Yunnan, Hubei, Sichuan, Hebei and other areas, but is also very common in Huangshan areas of Anhui and is popular with common people because of higher medicinal and health-care functions.
Flos Chrysanthemi Indici has effects of clearing heat, removing pathogenic fire, removing summer-heat, removing toxic substance, lowering blood pressure, clearing heart fire, sterilizing, and relieving swelling. The volatile oil has certain antioxidation and bacteriostasis functions. The 3, 5-dicaffeoylquinic acid, 3, 4-dicaffeoylquinic acid and other phenolic acids in the wild chrysanthemum flower researched by Hanzhenza and the like have stronger anti-inflammatory activity, and luteolin and apigenin have various biological activities of anti-inflammation, antioxidation, antibiosis, antivirus and the like. Research shows that the wild chrysanthemum can resist external bacteria and viruses from entering the human body, has a certain effect on preventing certain diseases on the human body, and can also relieve eye fatigue, nourish eyes and protect eyesight.
The wild chrysanthemum has certain differences in biological and therapeutic effects, and the juxianjian research shows that the total content of flavonoids, phenolic acids, volatile oil and the like in the wild chrysanthemum are higher than those of the common wild chrysanthemum, the common wild chrysanthemum has the effects of reducing blood pressure and increasing capillary resistance, can be used for treating hyperlipidemia and arteriosclerosis, and the wild chrysanthemum has the effects of relieving swelling, removing toxicity, preventing mosquito bites and can be used for treating skin diseases.
The mask is a common carrier of beauty care products, is also a daily necessity, and is particularly popular among young women and women loving beauty. The types of the facial masks in the current market are nonwoven facial masks, silk facial masks, tencel facial masks, biological cellulose facial masks, wire drawing facial masks and the like. Zhang Chun has been found that Chinese medicinal materials can be used as facial mask additive for relieving and treating various diseases of human body, such as rhizoma Atractylodis, cortex Phellodendri, cortex moutan, etc. can be added into facial mask for treating acne; radix Angelicae sinensis, radix Angelicae Dahuricae, etc. are added into the facial mask for treating chloasma; the wild chrysanthemum is also a Chinese medicinal material and has the effects of diminishing inflammation and removing swelling.
Based on the unique advantages and market prospects of the traditional Chinese medicine mask, the effect and effect difference of wild chrysanthemum and wild chrysanthemum is analyzed, and the wild chrysanthemum has better protection and repair effects on skin, so that the wild chrysanthemum is selected as a raw material, natural volatile oil is extracted to serve as an active part, the extracted wild chrysanthemum volatile oil is subjected to component analysis and antioxidant analysis of the volatile oil, the possibility that the volatile oil is used as a mask additive is analyzed, and high-molecular materials such as polyvinyl alcohol and sodium hydroxymethyl cellulose are selected for prescription optimization, so that the skin care mask with oxidation resistance, moisture preservation and repair capabilities is prepared.
Disclosure of Invention
The invention aims to provide a preparation method of a wild chrysanthemum flower facial mask, which has no layering phenomenon or oil floating phenomenon, has good stability of the facial mask as a whole and can solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
a preparation method of a wild chrysanthemum flower facial mask, which is used for preparing solution A, solution B and solution C, comprises the following steps:
step 1: preparing a solution A: weighing 15g of polyvinyl alcohol, adding water to 100g, placing the mixture into a 100mL beaker for one day, then placing the beaker into a constant-temperature water bath magnetic stirrer at the temperature of 85 ℃, and fully stirring the mixture until the solution is transparent without turbidity; adding 3g of sodium carboxymethylcellulose into a 100mL beaker, adding 15g of water, continuously stirring for 20 minutes, adding 35g of water, heating in a water bath until the sodium carboxymethylcellulose is completely dissolved, uniformly mixing the two solutions, and fully stirring in a constant-temperature water bath magnetic stirrer at the temperature of 85 ℃ to uniformly mix;
step 2: preparing a solution B: diluting the extracted wild chrysanthemum volatile oil into 10mL respectively according to the proportion;
and step 3: preparing a solution C: and when the temperature of the solution A is reduced to about 40 ℃, adding the solution B into the solution A, then putting the solution A into a constant-temperature magnetic stirrer for fully stirring, pouring the mask solution onto a clean glass plate for paving after the solution A is uniformly stirred, airing the glass plate at room temperature, and removing the film when the film is formed, thus finishing the manufacturing of the mask.
Further, the wild chrysanthemum flower is crushed as follows: bagging the prepared dried wild chrysanthemum flowers, cleaning the dried wild chrysanthemum flowers by using a high-speed grinder, putting the wild chrysanthemum flowers into the high-speed grinder, adjusting the rotating speed of the grinder to 3000 r/min-4500 r/min for 2-3 minutes, repeating the steps for 3-5 times, finally bagging the ground wild chrysanthemum flowers in a drying box, and drying for 2 hours.
Further, the extraction steps of the wild chrysanthemum volatile oil in the step 2 are as follows: weighing 50g of wild chrysanthemum sample, and mixing the flower and distilled water according to the weight ratio of 1: 20, putting the mixture into a distillation flask, and shaking the mixture evenly; installing a volatile oil extraction device from bottom to top; placing the prepared sample liquid on a heater, adding 10mL of distilled water into a device connected with a flask, adding about 8mL of anhydrous ether, placing a volatile oil extraction device on a heating sleeve, electrifying a heating knob, adjusting the voltage to 220V, heating for about 15-20 min, and adjusting the voltage to about 50V until the water drop rate is 7 seconds per drop, thus stabilizing; after continuous distillation is carried out for 6-7 h, the power supply of a heater is turned off, and the ether volatile oil mixture is collected in a test tube; and (3) purifying the extracted volatile oil, adding a small amount of sodium sulfate into the mixture, oscillating, and sealing and storing the sample solution.
Further, the dilution ratio of the wild chrysanthemum volatile oil is 1:10, or 1:100, or 1: 1000.
Further, after extracting the wild chrysanthemum flower volatile oil, carrying out GC-MS detection, wherein the detection solution is prepared as follows: diluting the extracted wild chrysanthemum volatile oil by using n-hexane, wherein the ratio of the wild chrysanthemum volatile oil to the n-hexane is 1: and 10, injecting the sample into a gas chromatograph.
Compared with the prior art, the invention has the beneficial effects that: the wild chrysanthemum flower facial mask takes the wild chrysanthemum flower as a raw material, volatile oil in the wild chrysanthemum flower is extracted by a distillation method, polyvinyl alcohol and glycerol are added in the preparation process of the facial mask, the facial mask has no layering phenomenon or oil floating phenomenon under the condition of high temperature or low temperature, the stability of the facial mask is integrally good, and the problem that the polyvinyl alcohol is difficult to dissolve can be effectively solved.
Drawings
FIG. 1 is a line graph of the antioxidant capacity of the wild chrysanthemum flower volatile oil of the present invention;
fig. 2 is a data diagram of Vc reducing power according to the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
A preparation method of a wild chrysanthemum flower facial mask, which is used for preparing solution A, solution B and solution C, comprises the following steps:
step 1: preparing a solution A: weighing 15g of polyvinyl alcohol, adding water to 100g, placing the mixture into a 100mL beaker for one day, then placing the beaker into a constant-temperature water bath magnetic stirrer at the temperature of 85 ℃, and fully stirring the mixture until the solution is transparent without turbidity; adding 3g of sodium carboxymethylcellulose into a 100mL beaker, adding 15g of water, continuously stirring for 20 minutes, adding 35g of water, heating in a water bath until the sodium carboxymethylcellulose is completely dissolved, uniformly mixing the two solutions, and fully stirring in a constant-temperature water bath magnetic stirrer at the temperature of 85 ℃ to uniformly mix;
step 2: diluting the extracted wild chrysanthemum volatile oil into 10mL respectively according to the proportion of (1:10, 1:100, 1: 1000);
and step 3: preparing a solution C: and when the temperature of the solution A is reduced to about 40 ℃, adding the solution B into the solution A, then putting the solution A into a constant-temperature magnetic stirrer for fully stirring, pouring the mask solution onto a clean glass plate for paving after the solution A is uniformly stirred, airing the glass plate at room temperature, and removing the film when the film is formed, thus finishing the manufacturing of the mask.
The wild chrysanthemum flower is crushed as follows: bagging the prepared dried wild chrysanthemum flowers, cleaning the dried wild chrysanthemum flowers by using a high-speed grinder, putting the wild chrysanthemum flowers into the high-speed grinder, adjusting the rotating speed of the grinder to 3000 r/min-4500 r/min for 2-3 minutes, repeating the steps for 3-5 times, finally bagging the ground wild chrysanthemum flowers in a drying box, and drying for 2 hours.
The extraction steps of the wild chrysanthemum volatile oil are as follows: weighing 50g of wild chrysanthemum sample, and mixing the flower and distilled water according to the weight ratio of 1: 20, putting the mixture into a distillation flask, and shaking the mixture evenly; installing a volatile oil extraction device from bottom to top; placing the prepared sample liquid on a heater, adding 10mL of distilled water into a device connected with a flask, adding about 8mL of anhydrous ether, placing a volatile oil extraction device on a heating sleeve, electrifying a heating knob, adjusting the voltage to 220V, heating for about 15-20 min, and adjusting the voltage to about 50V until the water drop rate is 7 seconds per drop, thus stabilizing; after continuous distillation is carried out for 6-7 h, the power supply of a heater is turned off, and the ether volatile oil mixture is collected in a test tube; and (3) purifying the extracted volatile oil, adding a small amount of sodium sulfate into the mixture, oscillating, and sealing and storing the sample solution.
Extracting the wild chrysanthemum volatile oil, and then carrying out GC-MS detection, wherein the detection solution is prepared as follows: diluting the extracted wild chrysanthemum volatile oil by using n-hexane, wherein the ratio of the wild chrysanthemum volatile oil to the n-hexane is 1: and 10, injecting the sample into a gas chromatograph.
GC-MS chromatographic conditions: HP-5MS (30m is multiplied by 250 mu m is multiplied by 0.25 mu m) is selected; the carrier gas is high-purity helium; the flow rate of the carrier gas is 1.0 mL/min; the flow is not split, and the sample injection amount is 1 mu L; the injection port temperature is 265 ℃, the initial temperature of the chromatographic column is 60 ℃, and the temperature is kept for 3 min; raising the temperature to 260 ℃ at a speed of 5 ℃/min, and keeping the temperature for 10 min. Mass spectrum conditions: the ion source temperature is 230 ℃ and the maximum value is 250 ℃; the ionization mode is EI, the electron energy is 70eV, the temperature of a quadrupole is 150 ℃, and the maximum value is 200 ℃; the mass scanning range is 50-500 u; the solvent delay time is 3 min; the search was performed using the NIST08 standard spectral library.
And (3) detecting the reducing power of the wild chrysanthemum volatile oil: diluting 100 μ L of flos Chrysanthemi Indici volatile oil by volume ratio to concentration of 0.1%, 1.0%, 2.0%, 5.0%, mixing with 100 μ L of 6.6 phosphoric acid buffer solution and 100 μ L of 1% potassium ferricyanide solution, reacting in 50 deg.C water bath for 20min, cooling, adding 100 μ L of 10% trichloroacetic acid, centrifuging at 3000rpm for 15 min, collecting supernatant 90 μ L, adding 100 μ L of distilled water and 10 μ L of 0.1% ferric trichloride, standing for 10min, measuring light absorption value with spectrophotometer, and replacing 100 μ L of distilled water with potassium ferricyanide solution as blank control. Taking Vc as a positive control concentration, repeating the concentration for three times as same as the volatile oil, and taking an average value.
Designing a primary prescription of the wild chrysanthemum flower facial mask: firstly, crushing the wild chrysanthemum flower into fine powder by an ultra-high speed crusher, screening the crushed wild chrysanthemum flower fine powder by a sieve with 80 meshes, screening the screened wild chrysanthemum flower fine powder by a sieve with 100 meshes, finally pouring the screened wild chrysanthemum flower fine powder into a conical flask with a bottle plug, and placing the conical flask into a drying oven for later use.
The research experiment of the wild chrysanthemum flower facial mask formula comprises the following steps: referring to the preparation method of the mask which is small and bright in color, in the experimental process, as polyvinyl alcohol is difficult to dissolve and the dissolving time is long, air bubbles can be generated, and the following experiments are carried out to solve the problem:
respectively dissolving 10g, 15g and 20g of polyvinyl alcohol in 100mL of distilled water, heating in a water bath kettle at 85 ℃ for 30 minutes, adding 10g of glycerol, heating for dissolving for 30 minutes, adding 3g of sodium carboxymethylcellulose, and fully stirring until the sodium carboxymethylcellulose is completely dissolved. Standing and cooling to room temperature after the dissolved solution is dissolved, spreading the mask solution on a clean glass slide, and solidifying to form a film. The amounts of the above experimental glycerols were changed to 5g, 10g, and 15g, respectively, for comparison.
And (3) measuring the pH value of the mask: adopting a dilution method: firstly weighing 1.0g of wild chrysanthemum flower facial mask essence, adding 10mL of distilled water into a beaker, heating the beaker to about 50 ℃ in a digital display constant-temperature water bath kettle, stirring until the wild chrysanthemum flower facial mask is completely dissolved and uniformly dispersed, cooling the beaker to 25 ℃ at room temperature, measuring the temperature by using a precision acidimeter, repeating the steps for three times, and taking an average value.
The mask stability test determination comprises a heat resistance test and a cold resistance test, wherein the heat resistance test comprises the following steps: and (3) putting a small part of the prepared wild chrysanthemum flower facial mask in a beaker, covering the beaker, standing for one day in an environment with the temperature of 40 ℃, and observing whether the facial mask is layered or oil slick, whether the color is changed and the like. The cold resistance test procedure is as follows: and (3) taking a small part of the prepared wild chrysanthemum flower facial mask, placing the wild chrysanthemum flower facial mask in a beaker, covering the beaker, placing the beaker in an environment with the temperature of 5 ℃ in a refrigerator, standing for one day, and observing whether the facial mask is layered or oil slick, whether the color is changed or not and the like.
The yield of the wild chrysanthemum volatile oil is shown in Table 1
As can be seen from Table 1, the average oil yield of the volatile oil extracted from the wild chrysanthemum flower by steam distillation was 0.0504 mL-g-1. The yield of the wild chrysanthemum volatile oil researched by Zhang Fei et al is 0.55mL g-1Therefore, the possible reasons for the lower yield of the volatile oil in the experiment can be seen to be the crushing degree, the water adding amount, the soaking time and the distillation time of the dried wild chrysanthemum flowers. Orthogonal experiments can be carried out on the crushing degree, the water adding amount, the soaking time and the distillation time of the wild chrysanthemum in subsequent researches to obtain the optimal extraction condition.
GC-MS analysis of the volatile oil extracted from the wild chrysanthemum flowers is carried out to obtain the main components of the volatile oil shown in Table 2
It can be seen from table 2 that 25 compounds in the total amount of the wild chrysanthemum flower volatile oil account for 93.0512%, wherein the borneol accounts for 3.1745%, the eudesmol accounts for 11.699%, the caryophyllene oxide accounts for 25.969%, the alpha-bisabolol accounts for 11.902%, and the 1R-alpha-pinene accounts for 12.6548%, which account for more than half of the total amount (65.3993%) of the total amount of the whole wild chrysanthemum flower volatile oil, and are the main substances in the wild chrysanthemum flower volatile oil, while the compounds such as ethyl nonadecanoate, 8-hexylpentadecane, nonadecanoic acid, geraniol crotonate, isomyrcene epoxide, and curcumene account for the remaining 27.6519%.
From the detection data of GC-MS, the main components of the wild chrysanthemum volatile oil are terpenoids, alcohols and ketones. By referring to the analysis of the components of the wild chrysanthemum volatile oil by the Chenxiaohui and combining the analysis of the experimental result, the compound has obvious biological activity, is an important component of certain traditional Chinese medicines, and has the functions of pain relief, asthma relief, cough relief, antibiosis, antivirus, anticancer, anthelmintic and the like. Therefore, the wild chrysanthemum flower facial mask can kill fungi on the skin, remove bacteria in pores and skin and achieve the effect of cleaning the face.
The GC-MS analysis of the wild chrysanthemum volatile oil shows that the measured results are different from the existing documents, and the main components of the wild chrysanthemum volatile oil obtained by analyzing the components of the wild chrysanthemum volatile oil with reference to Haiping are 63.6 percent of 1R-alpha-pinene and 30.3 percent of caryophyllene oxide. The main reason is that different harvesting times in different producing areas have great influence on chemical components of the traditional Chinese medicine; in the Haiping paper, if the wild chrysanthemum volatile oil component is analyzed by using a solid phase extraction method, 70 ℃ is the optimal working temperature, and a 65-micron PDMS-DVB extraction head is the most appropriate extraction head, the invention uses steam distillation to extract GC-MS analysis, and different methods can also cause the difference of the main components of the volatile oil. In subsequent experiments, wild chrysanthemum flowers in different producing areas are selected, and the wild chrysanthemum flower volatile oil components are further researched by utilizing different experimental conditions.
The antioxidant capacity of the wild chrysanthemum volatile oil is shown in table 3, and is plotted as a line graph, which is shown in figure 1.
TABLE 3 data sheet of antioxidant capacity of volatile oil of wild chrysanthemum
As can be seen from the figure 1, the reducing power of the wild chrysanthemum volatile oil is increased along with the increase of the concentration, the reducing power of the wild chrysanthemum volatile oil is obvious, and the research on the reducing power of the premna microphylla volatile oil by referring to Wu Yongxiang is compared with a group of experiments. Therefore, Vc is selected as an antioxidant reference substance to measure the reducing power, and the measurement data is shown in figure 2. As can be seen from FIG. 2, the data of the reducing power of Vc is similar to that of the wild chrysanthemum flower volatile oil, and the Vc has been proved to have stronger antioxidant capacity, so that the antioxidant capacity of the wild chrysanthemum flower volatile oil is also weak.
In the formula, when the polyvinyl alcohol is prepared according to 10g, the dissolving time is short, no suspended particles exist, and the film forming effect is good; when 15g and 20g of polyvinyl alcohol were used, the dissolution time was long and the film formation effect was poor due to a large amount of suspended particle gum. It is inferred from this that the swelling and dissolution are likely to be caused by an excessively large amount of polyvinyl alcohol, and therefore it is most suitable to control the amount of polyvinyl alcohol to 10 g.
Referring to the ratio of polyvinyl alcohol to glycerin obtained in the research of the sun womon yao 1:1, the moisturizing effect of the glycerin can be utilized to be well combined with water through hydrogen bonds, and the combining capacity of the skin and the water is improved. The experiment shows that: when 10g of glycerol is added, the solution becomes more transparent, no suspended matters exist, and the film forming effect is good; when 5g of the solution is added, the film forming effect is poor when the solution is diluted; when 15g of the solution is added, the solution is too viscous and has poor film forming effect; therefore, it is preferable to add 5g of glycerin. The optimal film-forming formula of the finally obtained wild chrysanthemum is as follows: 10g of polyoxyethylene, 3g of sodium carboxymethyl cellulose and 5g of glycerol.
The invention uses polyvinyl alcohol, hydroxymethyl cellulose sodium and other raw materials to make the facial mask. The polyvinyl alcohol is an organic high molecular compound, is white and flaky, is soluble in water, is low in cost and can be degraded[8]. The medical polyvinyl alcohol is safe and nontoxic to human bodies, has good biocompatibility, is commonly used in the aspects of eye medicine, eye drops, wound healing, skin repair and the like, and can also be used in cosmetics and skin moisturizing cream, so the polyvinyl alcohol is selected as a candidate auxiliary material of a membrane preparation raw material of the wild chrysanthemum flower facial mask. The method can improve the film forming property of the polyvinyl alcohol and can be applied in the subsequent research.
The relevant properties of the mask were tested in triplicate and the results are shown in Table 4
TABLE 4 measurement results of physical and chemical indexes of facial mask
As can be seen from table 4, the drying time of the mask was about 20 minutes, the pH of the mask was about 6.5, the stability of the mask was good, and neither delamination nor oil floating was observed in the heat and cold resistance test.
The invention takes wild chrysanthemum as raw material, volatile oil in the wild chrysanthemum is extracted by a distillation method, and the average oil yield of the volatile oil extracted from the wild chrysanthemum by a steam distillation method is measured to be 0.0504 mL-g-1And then the prescription design is carried out on the facial mask, and the result shows that the optimal film-forming formula of the wild chrysanthemum is as follows: 5.0 percent of polyvinyl alcohol, 1.5 percent of sodium carboxymethyl cellulose, 2.5 percent of glycerol and 2.5 percent of wild chrysanthemum flower volatile oil. And the reducing power of the wild chrysanthemum volatile oil is measured, the reducing power of the wild chrysanthemum volatile oil is found to be enhanced along with the increase of the concentration, the pH value of the mask is about 6.5, and then a stability test of the mask is carried out, so that the mask has no layering phenomenon or oil floating phenomenon under the conditions of high temperature or low temperature, and the stability of the mask is integrally shown to be good.
In the preparation process of the mask, the fact that polyvinyl alcohol is difficult to dissolve is found, the formula of the mask is researched through experiments, and when the polyvinyl alcohol is prepared according to 10g, the dissolving time is short, no suspended particles exist, and the film forming effect is good; the addition amount of the glycerol is researched, when 10g of the glycerol is added, the solution becomes more transparent, no suspended matters exist, and the film forming effect is good; therefore, the optimal formula of 10g of polyvinyl alcohol and 5g of glycerin is added in the preparation process of the mask, and the problem that the polyvinyl alcohol is difficult to dissolve can be effectively solved.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be able to cover the technical solutions and the inventive concepts of the present invention within the technical scope of the present invention.
Claims (5)
1. The preparation method of the wild chrysanthemum flower mask is characterized by preparing solution A, solution B and solution C, and comprises the following steps:
step 1: preparing a solution A: weighing 15g of polyvinyl alcohol, adding water to 100g, placing the mixture into a 100mL beaker for one day, then placing the beaker into a constant-temperature water bath magnetic stirrer at the temperature of 85 ℃, and fully stirring the mixture until the solution is transparent without turbidity; adding 3g of sodium carboxymethylcellulose into a 100mL beaker, adding 15g of water, continuously stirring for 20 minutes, adding 35g of water, heating in a water bath until the sodium carboxymethylcellulose is completely dissolved, uniformly mixing the two solutions, and fully stirring in a constant-temperature water bath magnetic stirrer at the temperature of 85 ℃ to uniformly mix;
step 2: preparing a solution B: diluting the extracted wild chrysanthemum volatile oil into 10mL respectively according to the proportion;
and step 3: preparing a solution C: and when the temperature of the solution A is reduced to about 40 ℃, adding the solution B into the solution A, then putting the solution A into a constant-temperature magnetic stirrer for fully stirring, pouring the mask solution onto a clean glass plate for paving after the solution A is uniformly stirred, airing the glass plate at room temperature, and removing the film when the film is formed, thus finishing the manufacturing of the mask.
2. The preparation method of the wild chrysanthemum flower facial mask as claimed in claim 1, wherein the wild chrysanthemum flower is pulverized as follows: bagging the prepared dried wild chrysanthemum flowers, cleaning the dried wild chrysanthemum flowers by using a high-speed grinder, putting the wild chrysanthemum flowers into the high-speed grinder, adjusting the rotating speed of the grinder to 3000 r/min-4500 r/min for 2-3 minutes, repeating the steps for 3-5 times, finally bagging the ground wild chrysanthemum flowers in a drying box, and drying for 2 hours.
3. The preparation method of the wild chrysanthemum flower facial mask as claimed in claim 1, wherein the extraction step of the wild chrysanthemum flower volatile oil in the step 2 is as follows: weighing 50g of wild chrysanthemum sample, and mixing the flower and distilled water according to the weight ratio of 1: 20, putting the mixture into a distillation flask, and shaking the mixture evenly; installing a volatile oil extraction device from bottom to top; placing the prepared sample liquid on a heater, adding 10mL of distilled water into a device connected with a flask, adding about 8mL of anhydrous ether, placing a volatile oil extraction device on a heating sleeve, electrifying a heating knob, adjusting the voltage to 220V, heating for about 15-20 min, and adjusting the voltage to about 50V until the water drop rate is 7 seconds per drop, thus stabilizing; after continuous distillation is carried out for 6-7 h, the power supply of a heater is turned off, and the ether volatile oil mixture is collected in a test tube; and (3) purifying the extracted volatile oil, adding a small amount of sodium sulfate into the mixture, oscillating, and sealing and storing the sample solution.
4. The preparation method of the wild chrysanthemum flower facial mask as claimed in claim 1, wherein the dilution ratio of the wild chrysanthemum flower volatile oil is 1:10, or 1:100, or 1: 1000.
5. The preparation method of the wild chrysanthemum flower facial mask as claimed in claim 3, wherein the extraction of the wild chrysanthemum flower volatile oil is followed by GC-MS detection, and the preparation of the detection solution is as follows: diluting the extracted wild chrysanthemum volatile oil by using n-hexane, wherein the ratio of the wild chrysanthemum volatile oil to the n-hexane is 1: and 10, injecting the sample into a gas chromatograph.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105802738A (en) * | 2016-06-06 | 2016-07-27 | 重庆大学 | Extraction method of Flos chrysanthemi indici volatile oil |
| CN108619023A (en) * | 2018-06-21 | 2018-10-09 | 佛山市三水区嘉信农业技术研究院（普通合伙） | A kind of pseudo-ginseng anti-oxidant face mask and preparation method thereof |
| CN111728918A (en) * | 2020-08-13 | 2020-10-02 | 黄山学院 | Preparation method of wild chrysanthemum flower facial mask |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105802738A (en) * | 2016-06-06 | 2016-07-27 | 重庆大学 | Extraction method of Flos chrysanthemi indici volatile oil |
| CN108619023A (en) * | 2018-06-21 | 2018-10-09 | 佛山市三水区嘉信农业技术研究院（普通合伙） | A kind of pseudo-ginseng anti-oxidant face mask and preparation method thereof |
| CN111728918A (en) * | 2020-08-13 | 2020-10-02 | 黄山学院 | Preparation method of wild chrysanthemum flower facial mask |
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Application publication date: 20211029 |