CN113440439A - Rose essential oil hair conditioner - Google Patents
Rose essential oil hair conditioner Download PDFInfo
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- CN113440439A CN113440439A CN202110833825.1A CN202110833825A CN113440439A CN 113440439 A CN113440439 A CN 113440439A CN 202110833825 A CN202110833825 A CN 202110833825A CN 113440439 A CN113440439 A CN 113440439A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention relates to a rose essential oil hair conditioner which comprises rose essential oil, tamarind leavening, rosemary essential oil, niacin vitamin E ester, an emulsifier, a preservative, a humectant, a pH regulator and water. According to the invention, by adding the tamarind fermentation product and the rose essential oil, the combination of the tamarind fermentation product and the rose essential oil can lock hair moisture while decontaminating, and repair and nourish hair; the emulsifying property is better, and the dirt-removing power is stronger; has synergistic effect in protecting hair protein.
Description
Technical Field
The invention relates to the technical field of preparation of daily necessities, in particular to rose essential oil hair conditioner and a preparation method thereof.
Background
The main chemical component of hair is scleroprotein, which is composed of 18 amino acids such as cystine. Hair is natural polymer fibers formed by winding these amino acids through hydrogen chains, salt chains, and disulfide chains, and is tough and elastic, and has the characteristic of being able to return to its original shape immediately after being bent. Since the hydrogen chain has poor resistance to water and the salt chain has poor resistance to alkali, the recovery ability of the salt chain is lowered when the hydrogen chain is cleaved with water or alkali, and the salt chain loses its normal elasticity. Compared with hydrogen bonds and salt bonds, the disulfide bonds have strong tolerance and are generally not influenced by water and alkali at normal temperature. The perming is that the hydrogen bond and salt bond of the hair are cut off, then the disulfide bond is cut off, so that the hair is soft and waved, and then the three bonds are repaired. Hair contains water, fat, nitrogen, sulfur and melanin in addition to hard protein, and contains various metal elements such as calcium, sodium, potassium, zinc, copper, iron, manganese, etc.
The hair conditioner has the effects that after the head is washed by products such as shampoo and the like, the residual detergent on the head is neutralized and taken away, the scalp stimulated by the surfactant is relieved, the scalp is nourished, a certain film effect is formed to carry out moisture preservation and nursing on the scalp and the hair, the tangled hair is smooth and easy to comb, a certain sun-screening effect is provided, hair fiber damage is prevented, and certain brightness and elasticity are endowed. With the development of technology, people are demanding hair care products which, in addition to the above, also have the functions of repairing hair damage to some extent, as well as dressing and fixing hair style.
Based on the situation, the invention provides the rose essential oil hair conditioner and the preparation method thereof, and the problems can be effectively solved.
Disclosure of Invention
The invention aims to provide a rose essential oil hair conditioner and a preparation method thereof.
In order to achieve the purpose, the invention provides a rose essential oil hair conditioner which is prepared from the following raw materials in parts by weight: 15-25 parts of rose essential oil, 10-18 parts of tamarind leavening, 8-12 parts of rosemary essential oil, 1-3 parts of nicotinic acid vitamin E ester, 3-7 parts of sodium cetyl sulfate, 2-4 parts of potassium stearate, 6-10 parts of methyl hydroxybenzoate, 15-25 parts of simethicone, 5-9 parts of glycerol, 1-3 parts of citric acid and 90-110 parts of deionized water.
Preferably, the emulsifier comprises one or a combination of more than two of sodium dodecyl benzene sulfonate, sodium dodecyl sulfate, sodium hexadecyl benzene sulfonate, sodium hexadecyl sulfonate, sodium octadecyl benzene sulfonate, sodium octadecyl sulfate, sodium octadecyl sulfonate, sodium stearate and potassium stearate.
Preferably, the preservative comprises one or a combination of more than two of benzyl alcohol, sodium benzoate, nipagin ester, methylparaben and potassium sorbate.
Preferably, the humectant comprises one or a combination of more than two of simethicone, glycerin, propylene glycol and butanediol.
Preferably, the pH regulator comprises one or a combination of two or more of citric acid, malic acid, sodium hydroxide, and triethanolamine.
Preferably, the tamarind ferment is prepared by the following method:
(1) crushing tamarind seeds, adding 1-2% phosphoric acid aqueous solution which is 10-15 times of tamarind seeds in weight, heating to 70-80 ℃, and extracting for 30-40 min; filtering for later use;
(2) inoculating mixed bacteria consisting of acetic acid bacteria and bifidobacteria according to the inoculation amount of 6-8% in any proportion, and continuously fermenting for 5-8 days at the temperature of 25-35 ℃;
(3) after the fermentation is finished, instantly sterilizing at high temperature, and filtering by a filter pressing method to obtain the tamarind fermented product.
Preferably, the hair conditioner consists of the following raw materials in parts by weight: 15 parts of rose essential oil, 10 parts of tamarind leavening, 8 parts of rosemary essential oil, 1 part of nicotinic acid vitamin E ester, 3 parts of sodium hexadecyl sulfate, 2 parts of potassium stearate, 6 parts of methyl hydroxybenzoate, 15 parts of simethicone, 5 parts of glycerol, 1 part of citric acid and 90 parts of deionized water.
Preferably, the hair conditioner consists of the following raw materials in parts by weight: 25 parts of rose essential oil, 18 parts of tamarind leavening, 12 parts of rosemary essential oil, 3 parts of nicotinic acid vitamin E ester, 7 parts of sodium cetyl sulfate, 4 parts of potassium stearate, 10 parts of methyl hydroxybenzoate, 25 parts of simethicone, 9 parts of glycerol, 3 parts of citric acid and 110 parts of deionized water.
The invention also provides a preparation method of the rose essential oil hair conditioner, which comprises the following steps:
(1) adding deionized water into a water phase pot, adding sodium hexadecyl sulfate and potassium stearate while stirring, uniformly stirring and dispersing, heating to 75-80 ℃, adding vitamin E nicotinate and tamarind leavening, preserving heat, and stirring for 5-10 min;
(2) putting rose essential oil into an oil phase pot, adding rosemary essential oil, simethicone and glycerol, and stirring for 5-10 min;
(3) filtering the water phase material, pumping into a vacuum emulsifying pot, adding the filtered oil phase material, homogenizing for 20-30 min, and keeping the temperature for 10-15 min; cooling to below 50 deg.C, adding methyl hydroxybenzoate and citric acid, stirring, and cooling to room temperature.
Compared with the prior art, the invention has the following beneficial effects:
1. according to the invention, by adding the tamarind fermentation product and the rose essential oil, the combination of the tamarind fermentation product and the rose essential oil can lock hair moisture while decontaminating, and repair and nourish hair; the emulsifying property is better, and the dirt-removing power is stronger; has synergistic effect in protecting hair protein.
2. The raw materials of the invention are sufficient in China and proper in price, so that the large-scale production of the invention is not limited by too high cost; meanwhile, the preparation method is simple, the total production cost is low, and the industrial large-scale production is facilitated.
Detailed Description
Example 1
The specific raw materials were weighed as in table 1, and the preparation steps were as follows:
(1) adding deionized water into water phase pot, adding sodium hexadecyl sulfate and potassium stearate while stirring, stirring and dispersing uniformly, heating to 75 deg.C, adding vitamin E nicotinate and tamarind fermented product, keeping the temperature, and stirring for 5 min;
(2) putting flos Rosae Rugosae essential oil into oil phase pan, adding herba Rosmarini officinalis essential oil, dimethyl silicone oil and glycerol, and stirring for 10 min;
(3) filtering the water phase material, pumping into a vacuum emulsifying pot, adding the filtered oil phase material, homogenizing for 20min, and keeping the temperature for 15 min; cooling to below 50 deg.C, adding methyl hydroxybenzoate and citric acid, stirring, and cooling to room temperature.
Example 2
The specific raw materials were weighed as in table 1, and the preparation steps were as follows:
(1) adding deionized water into water phase pot, adding sodium hexadecyl sulfate and potassium stearate while stirring, stirring and dispersing uniformly, heating to 80 deg.C, adding vitamin E nicotinate and tamarind fermented product, keeping the temperature, and stirring for 10 min;
(2) putting flos Rosae Rugosae essential oil into oil phase pan, adding herba Rosmarini officinalis essential oil, dimethyl silicone oil and glycerol, and stirring for 5 min;
(3) filtering the water phase material, pumping into a vacuum emulsifying pot, adding the filtered oil phase material, homogenizing for 30min, and keeping the temperature for 10 min; cooling to below 50 deg.C, adding methyl hydroxybenzoate and citric acid, stirring, and cooling to room temperature.
Example 3
The specific raw materials were weighed as in table 1, and the preparation steps were as follows:
(1) adding deionized water into water phase pot, adding sodium hexadecyl sulfate and potassium stearate while stirring, stirring and dispersing uniformly, heating to 80 deg.C, adding vitamin E nicotinate and tamarind fermented product, keeping the temperature, and stirring for 10 min;
(2) putting flos Rosae Rugosae essential oil into oil phase pan, adding herba Rosmarini officinalis essential oil, dimethyl silicone oil and glycerol, and stirring for 5 min;
(3) filtering the water phase material, pumping into a vacuum emulsifying pot, adding the filtered oil phase material, homogenizing for 20min, and keeping the temperature for 15 min; cooling to below 50 deg.C, adding methyl hydroxybenzoate and citric acid, stirring, and cooling to room temperature.
Comparative example 1
(1) Adding deionized water into water phase pot, adding sodium hexadecyl sulfate and potassium stearate while stirring, stirring and dispersing uniformly, heating to 80 deg.C, adding vitamin E nicotinate, keeping the temperature, and stirring for 10 min;
(2) putting flos Rosae Rugosae essential oil into oil phase pan, adding herba Rosmarini officinalis essential oil, dimethyl silicone oil and glycerol, and stirring for 5 min;
(3) filtering the water phase material, pumping into a vacuum emulsifying pot, adding the filtered oil phase material, homogenizing for 20min, and keeping the temperature for 15 min; cooling to below 50 deg.C, adding methyl hydroxybenzoate and citric acid, stirring, and cooling to room temperature.
Comparative example 2
(1) Adding deionized water into water phase pot, adding sodium hexadecyl sulfate and potassium stearate while stirring, stirring and dispersing uniformly, heating to 80 deg.C, adding vitamin E nicotinate and tamarind fermented product, keeping the temperature, and stirring for 10 min;
(2) putting rosemary essential oil into an oil phase pot, adding simethicone and glycerol, and stirring for 5 min;
(3) filtering the water phase material, pumping into a vacuum emulsifying pot, adding the filtered oil phase material, homogenizing for 20min, and keeping the temperature for 15 min; cooling to below 50 deg.C, adding methyl hydroxybenzoate and citric acid, stirring, and cooling to room temperature.
TABLE 1
Example 4 moisturizing and emulsifying Properties testing
Accurately weighing M as 20g of each of examples 1-3, comparative examples 1 and 2 and glycerin reference0Preparing aqueous solution H with the mass fraction of 10 percent0Placing in a drying oven maintained at 40 deg.C and 43% relative humidity with saturated sodium carbonate solution, weighing M after 24 hrn(M) water loss rate according to the formula%0-Mn)/H0And calculating the water loss rate.
40ml of each of examples 1 to 3 and comparative examples 1 and 2 was measured accurately, and the measured amount was charged into a triangular flask with a glass stopper, an equal amount of turpentine was added, the flask was allowed to stand for 1 minute with vigorous shaking from top to bottom for 5 times, and the emulsion was introduced into a 100ml volumetric flask, and the time was immediately recorded on a stopwatch, and when 10ml of the aqueous phase separated, the time separated was recorded as a relative comparison of the emulsifying power.
The test results are shown in Table 2.
TABLE 2 moisture retention and emulsification Property test results
| The water loss rate% | Emulsion residence time/s | |
| Example 1 | 7 | 125 |
| Example 2 | 9 | 120 |
| Example 3 | 7 | 123 |
| Comparative example 1 | 12 | 82 |
| Example 2 | 13 | 90 |
EXAMPLE 5 Hair conditioner photoprotection Effect test
Taking a hair bundle with the length of 15cm at the middle position of a natural healthy black hair bundle as a measurement object, soaking the hair bundle in anhydrous ether for 24h, washing with running water for 3 times, washing with distilled water for 1 time, coating the hair bundle with 3% of sodium dodecyl sulfate in a mass fraction of 0.5g/1g, rubbing and foaming for 2min, standing for 1min, soaking in warm water at 35 ℃ for 30s, washing with warm water at 35 ℃, and naturally drying. Dividing the treated hair bundles into 6 groups on average, namely, the groups of examples 1-3, the groups of comparative examples 1 and 2 and a blank group, smearing corresponding hair conditioner samples on the hair of each group except the blank group according to the proportion of 0.5g/1g of hair, continuously using for 15 days, waiting for 30min after each use, cleaning with warm water, and naturally airing in a dark room in a dark place. The hair treated by the hair conditioner adopts a xenon lamp (the radiation wavelength is 300-800 nm, the irradiation amplitude is 550W/m) simulating sunlight under the conditions of 40 ℃ and 50% of humidity2) Irradiating for 48h, and detecting protein loss (mg) per g hair 24h and 48h before and after irradiation. The test results are shown in Table 3.
TABLE 3 loss of protein content test results (mg)
| 24h | 48h | |
| Blank group | -1.58 | -2.25 |
| Example 1 | -0.32 | -0.65 |
| Example 2 | -0.28 | -0.58 |
| Example 3 | -0.31 | -0.60 |
| Comparative example 1 | -0.30 | -1.28 |
| Example 2 | -0.75 | -1.84 |
The foregoing descriptions of specific exemplary embodiments of the present invention have been presented for purposes of illustration and description. It is not intended to limit the invention to the precise form disclosed, and obviously many modifications and variations are possible in light of the above teaching. The exemplary embodiments were chosen and described in order to explain certain principles of the invention and its practical application to enable one skilled in the art to make and use various exemplary embodiments of the invention and various alternatives and modifications as are suited to the particular use contemplated. It is intended that the scope of the invention be defined by the claims and their equivalents.
Claims (9)
1. The rose essential oil hair conditioner is characterized by comprising the following raw materials in parts by weight: 15-25 parts of rose essential oil, 10-18 parts of tamarind leavening, 8-12 parts of rosemary essential oil, 1-3 parts of nicotinic acid vitamin E ester, 3-7 parts of sodium cetyl sulfate, 2-4 parts of potassium stearate, 6-10 parts of methyl hydroxybenzoate, 15-25 parts of simethicone, 5-9 parts of glycerol, 1-3 parts of citric acid and 90-110 parts of deionized water.
2. The rose essential oil hair conditioner of claim 1, wherein the emulsifier comprises one or a combination of two or more of sodium dodecyl benzene sulfonate, sodium dodecyl sulfate, sodium hexadecyl benzene sulfonate, sodium hexadecyl sulfate, sodium octadecyl benzene sulfonate, sodium octadecyl sulfate, sodium octadecyl sulfonate, sodium stearate, and potassium stearate.
3. The rose essential oil hair conditioner of claim 1, wherein the preservative comprises one or a combination of two or more of benzyl alcohol, sodium benzoate, paraben, methylparaben, and potassium sorbate.
4. The rose essential oil hair conditioner of claim 1, wherein the moisturizer comprises one or a combination of two or more of dimethicone, glycerin, propylene glycol, butylene glycol.
5. The rose essential oil hair conditioner of claim 1, wherein the pH adjuster comprises one or a combination of two or more of citric acid, malic acid, sodium hydroxide, triethanolamine.
6. The rose essential oil hair conditioner according to claims 1 to 5, wherein the tamarind seed ferment is prepared by the following method:
(1) crushing tamarind seeds, adding 1-2% phosphoric acid aqueous solution which is 10-15 times of tamarind seeds in weight, heating to 70-80 ℃, and extracting for 30-40 min; filtering and reserving for later use.
(2) Inoculating acetic acid bacteria and bifidobacteria according to the inoculation amount of 6-8% and continuously fermenting for 5-8 days at the temperature of 25-35 ℃.
(3) After the fermentation is finished, instantly sterilizing at high temperature, and filtering by a filter pressing method to obtain the tamarind fermented product.
7. The rose essential oil hair conditioner of claim 1, wherein the hair conditioner is composed of the following raw materials in parts by weight: 15 parts of rose essential oil, 10 parts of tamarind leavening, 8 parts of rosemary essential oil, 1 part of nicotinic acid vitamin E ester, 3 parts of sodium hexadecyl sulfate, 2 parts of potassium stearate, 6 parts of methyl hydroxybenzoate, 15 parts of simethicone, 5 parts of glycerol, 1 part of citric acid and 90 parts of deionized water.
8. The rose essential oil hair conditioner of claim 1, wherein the hair conditioner is composed of the following raw materials in parts by weight: 25 parts of rose essential oil, 18 parts of tamarind leavening, 12 parts of rosemary essential oil, 3 parts of nicotinic acid vitamin E ester, 7 parts of sodium cetyl sulfate, 4 parts of potassium stearate, 10 parts of methyl hydroxybenzoate, 25 parts of simethicone, 9 parts of glycerol, 3 parts of citric acid and 110 parts of deionized water.
9. A method of preparing the rose essential oil hair conditioner of any one of claims 1 to 8, comprising the steps of:
(1) adding deionized water into a water phase pot, adding sodium hexadecyl sulfate and potassium stearate while stirring, uniformly stirring and dispersing, heating to 75-80 ℃, adding vitamin E nicotinate and tamarind leavening, preserving heat, and stirring for 5-10 min;
(2) putting rose essential oil into an oil phase pot, adding rosemary essential oil, simethicone and glycerol, and stirring for 5-10 min;
(3) filtering the water phase material, pumping into a vacuum emulsifying pot, adding the filtered oil phase material, homogenizing for 20-30 min, and keeping the temperature for 10-15 min; cooling to below 50 deg.C, adding methyl hydroxybenzoate and citric acid, stirring, and cooling to room temperature.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110833825.1A CN113440439A (en) | 2021-07-23 | 2021-07-23 | Rose essential oil hair conditioner |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202110833825.1A CN113440439A (en) | 2021-07-23 | 2021-07-23 | Rose essential oil hair conditioner |
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| CN113440439A true CN113440439A (en) | 2021-09-28 |
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| CN202110833825.1A Pending CN113440439A (en) | 2021-07-23 | 2021-07-23 | Rose essential oil hair conditioner |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113827525A (en) * | 2021-10-29 | 2021-12-24 | 扬州市永春旅游用品厂 | Hair-moistening shampoo and preparation method thereof |
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2021
- 2021-07-23 CN CN202110833825.1A patent/CN113440439A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113827525A (en) * | 2021-10-29 | 2021-12-24 | 扬州市永春旅游用品厂 | Hair-moistening shampoo and preparation method thereof |
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