CN113274306A - Preparation method of daily-use healthy and environment-friendly oral deodorant - Google Patents
Preparation method of daily-use healthy and environment-friendly oral deodorant Download PDFInfo
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- CN113274306A CN113274306A CN202110591413.1A CN202110591413A CN113274306A CN 113274306 A CN113274306 A CN 113274306A CN 202110591413 A CN202110591413 A CN 202110591413A CN 113274306 A CN113274306 A CN 113274306A
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- 239000002781 deodorant agent Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 50
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 40
- 210000000214 mouth Anatomy 0.000 claims abstract description 34
- 239000000463 material Substances 0.000 claims abstract description 31
- 229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000004376 Sucralose Substances 0.000 claims abstract description 21
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims abstract description 21
- BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 claims abstract description 21
- 235000019408 sucralose Nutrition 0.000 claims abstract description 21
- 239000011701 zinc Substances 0.000 claims abstract description 21
- 229910052725 zinc Inorganic materials 0.000 claims abstract description 21
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 20
- 239000011780 sodium chloride Substances 0.000 claims abstract description 20
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims abstract description 20
- 239000008367 deionised water Substances 0.000 claims abstract description 19
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 19
- CYDQOEWLBCCFJZ-UHFFFAOYSA-N 4-(4-fluorophenyl)oxane-4-carboxylic acid Chemical compound C=1C=C(F)C=CC=1C1(C(=O)O)CCOCC1 CYDQOEWLBCCFJZ-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000001509 sodium citrate Substances 0.000 claims abstract description 18
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims abstract description 18
- 239000001540 sodium lactate Substances 0.000 claims abstract description 18
- 229940005581 sodium lactate Drugs 0.000 claims abstract description 18
- 235000011088 sodium lactate Nutrition 0.000 claims abstract description 18
- 239000000706 filtrate Substances 0.000 claims abstract description 10
- 238000001914 filtration Methods 0.000 claims abstract description 10
- 235000003599 food sweetener Nutrition 0.000 claims abstract description 10
- 239000003765 sweetening agent Substances 0.000 claims abstract description 10
- 239000002562 thickening agent Substances 0.000 claims abstract description 10
- 238000002791 soaking Methods 0.000 claims abstract description 4
- 238000000034 method Methods 0.000 claims description 21
- 239000002994 raw material Substances 0.000 claims description 20
- 229940058349 sodium levulinate Drugs 0.000 claims description 15
- RDKYCKDVIYTSAJ-UHFFFAOYSA-M sodium;4-oxopentanoate Chemical compound [Na+].CC(=O)CCC([O-])=O RDKYCKDVIYTSAJ-UHFFFAOYSA-M 0.000 claims description 15
- 239000000230 xanthan gum Substances 0.000 claims description 14
- 229920001285 xanthan gum Polymers 0.000 claims description 14
- 229940082509 xanthan gum Drugs 0.000 claims description 14
- 235000010493 xanthan gum Nutrition 0.000 claims description 14
- 239000002245 particle Substances 0.000 claims description 3
- 229960001790 sodium citrate Drugs 0.000 claims description 2
- 229960002668 sodium chloride Drugs 0.000 claims 1
- 239000000126 substance Substances 0.000 abstract description 18
- 210000002200 mouth mucosa Anatomy 0.000 abstract description 9
- 230000007613 environmental effect Effects 0.000 abstract description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract description 3
- 239000000843 powder Substances 0.000 abstract description 3
- 238000010298 pulverizing process Methods 0.000 abstract description 3
- 239000011734 sodium Substances 0.000 abstract description 3
- 229910052708 sodium Inorganic materials 0.000 abstract description 3
- 230000009977 dual effect Effects 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 28
- 230000000694 effects Effects 0.000 description 23
- 238000012360 testing method Methods 0.000 description 21
- 230000003385 bacteriostatic effect Effects 0.000 description 14
- 239000002324 mouth wash Substances 0.000 description 11
- 238000005303 weighing Methods 0.000 description 11
- 229940051866 mouthwash Drugs 0.000 description 9
- 239000008399 tap water Substances 0.000 description 9
- 235000020679 tap water Nutrition 0.000 description 9
- 239000000523 sample Substances 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- 241000894006 Bacteria Species 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- 239000012456 homogeneous solution Substances 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 239000003242 anti bacterial agent Substances 0.000 description 4
- 229940088710 antibiotic agent Drugs 0.000 description 4
- 238000001514 detection method Methods 0.000 description 4
- 230000036039 immunity Effects 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- -1 organic acid sodium salts Chemical class 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 208000007117 Oral Ulcer Diseases 0.000 description 3
- 208000025865 Ulcer Diseases 0.000 description 3
- 230000000844 anti-bacterial effect Effects 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 201000010099 disease Diseases 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- 235000012054 meals Nutrition 0.000 description 3
- 230000002906 microbiologic effect Effects 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 231100000397 ulcer Toxicity 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 206010017533 Fungal infection Diseases 0.000 description 2
- 241000233866 Fungi Species 0.000 description 2
- 208000031888 Mycoses Diseases 0.000 description 2
- 241000191967 Staphylococcus aureus Species 0.000 description 2
- 208000002399 aphthous stomatitis Diseases 0.000 description 2
- 230000001580 bacterial effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 235000013361 beverage Nutrition 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 235000013373 food additive Nutrition 0.000 description 2
- 239000002778 food additive Substances 0.000 description 2
- 239000010794 food waste Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 206010006326 Breath odour Diseases 0.000 description 1
- 241000222122 Candida albicans Species 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- 206010018291 Gingival swelling Diseases 0.000 description 1
- 206010028034 Mouth ulceration Diseases 0.000 description 1
- 208000002193 Pain Diseases 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241000589517 Pseudomonas aeruginosa Species 0.000 description 1
- 241000194017 Streptococcus Species 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000003674 animal food additive Substances 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 239000007853 buffer solution Substances 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- 229940095731 candida albicans Drugs 0.000 description 1
- 208000002925 dental caries Diseases 0.000 description 1
- 230000001877 deodorizing effect Effects 0.000 description 1
- 239000000645 desinfectant Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000035876 healing Effects 0.000 description 1
- 230000002949 hemolytic effect Effects 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 238000009629 microbiological culture Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 210000003097 mucus Anatomy 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000012488 sample solution Substances 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 230000016776 visual perception Effects 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
- ZPEJZWGMHAKWNL-UHFFFAOYSA-L zinc;oxalate Chemical compound [Zn+2].[O-]C(=O)C([O-])=O ZPEJZWGMHAKWNL-UHFFFAOYSA-L 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Inorganic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Emergency Medicine (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a preparation method of a daily-use environment-friendly healthy oral deodorant, which comprises the following steps: step 1: pulverizing sodium chloride, sodium citrate, sodium lactate, sodium fruoate, sodium lauryl sulfate, zinc glycyrrhetate, and sodium carbonate to obtain powder; step 2: putting the powdery material obtained in the step 1 into a beaker, sequentially adding a thickening agent and a sucralose sweetening agent, soaking for at least 3 hours, and adding deionized water into the obtained solution; and step 3: and (3) collecting the filtrate obtained in the step (2), filtering and concentrating to obtain the daily oral cavity deodorant, wherein the daily oral cavity deodorant is comprehensively considered from three aspects of micro-chemical environment, health and environmental protection, and the dual purposes of repairing oral mucosa are realized while the micro-chemical environment of the oral cavity is changed.
Description
Technical Field
The invention belongs to the technical field of daily oral cavity antibacterial cleaning, and particularly relates to a preparation method of a daily healthy environment-friendly oral cavity deodorant.
Background
Usually, after people get up in the morning, because the oral cavity is closed when people sleep, air is not smooth, and a lot of oral cavity mucus and other secretions exist, a lot of bacteria can be bred, so that peculiar smell is easily generated in the oral cavity. Local diseases of the oral cavity can also cause bad breath due to ulcer, gum swelling and pain, dental caries, food residue, etc. Therefore, people have many researches on the method, and many products are continuously put into the market.
The ethanol-containing disinfectant mouthwash has good effect, but seriously stimulates oral mucosa due to high concentration, and simultaneously brings difficulty to alcohol testing of drunk driving, thereby troubling consumers; the traditional Chinese medicine extract can also eliminate the peculiar smell of the oral cavity by oral bacteriostasis, but the content of effective components is low, because each plant contains thousands of chemical components, the effective components are only one or more of the chemical components, and the specific risks of other chemical components are unpredictable; antibiotic antibacterial technology can also realize the removal of oral peculiar smell by having good targeted sterilization to different bacteria, but long-term use of various antibiotics can cause bacteria to generate antibodies and arouse the risk of fungal infection, and the environment pollution can be caused when the antibiotics are put into the environment.
Disclosure of Invention
The invention aims to provide a preparation method of a daily-use environment-friendly healthy oral deodorant, which aims to solve the problems that the existing mouthwash is easy to stimulate oral mucosa, and bacteria can generate antibodies and stimulate fungal infection risks when the gargle containing antibiotics is used for a long time.
The invention adopts the following technical scheme: a preparation method of a daily-use environment-friendly healthy oral deodorant comprises the following steps:
step 1: pulverizing sodium chloride, sodium citrate, sodium lactate, sodium fruoate, sodium lauryl sulfate, zinc glycyrrhetate, and sodium carbonate to obtain powder;
step 2: putting the powdery material obtained in the step 1 into a beaker, sequentially adding a thickening agent and a sucralose sweetening agent, soaking for at least 3 hours, and adding deionized water into the obtained solution;
and step 3: and (3) collecting the filtrate obtained in the step (2), filtering and concentrating to obtain the daily oral cavity deodorant.
The daily environment-friendly healthy oral deodorant is prepared from the following components in parts by weight:
the total content of the raw materials is 1000 parts.
Further, the feed additive is prepared from the following raw materials in parts by weight: 5 parts of sodium chloride, 15 parts of sodium citrate, 2 parts of sodium lactate, 1 part of sodium levulinate, 5 parts of sodium lauryl sulfate, 1.5 parts of zinc glycyrrhetate, 2 parts of sodium carbonate, 1 part of thickening agent, 0.1 part of sucralose sweetening agent and the balance of deionized water.
Further, the particle size of the sodium carbonate is 15-50 microns.
Further, the thickening agent is xanthan gum, and the sweetening agent is sucralose.
Further, the diameter of the powdery material in the step 1 is 380-830 mu m.
The invention adopts another technical scheme that the daily-use environment-friendly healthy oral deodorant is prepared from the following raw materials in parts by weight:
the total content of the raw materials is 1000 parts.
The invention has the beneficial effects that: the invention comprehensively considers the micro-chemical environment, the health and the environmental protection, realizes the double purposes of repairing the oral mucosa while changing the micro-chemical environment of the oral cavity, and solves the problems that the existing gargle is easy to stimulate the oral mucosa, and bacteria can generate antibodies and stimulate the infection risk of the fungi when the gargle containing antibiotics is used for a long time. The raw materials are put into the environment after being used and can be rapidly degraded without causing environmental pollution, the whole process from the production source to the putting environment can be realized, the production is carried out by a simple physical mixing method, the process is simple, and the industrialization prospect is wide.
Detailed Description
The present invention will be described in detail with reference to the following embodiments.
The invention provides a preparation method of a daily-use environment-friendly healthy oral deodorant, which comprises the following steps:
step 1: pulverizing sodium chloride, sodium citrate, sodium lactate, sodium fruoate, sodium lauryl sulfate, zinc glycyrrhetate, and sodium carbonate to obtain powder;
step 2: putting the powdery material obtained in the step 1 into a beaker, sequentially adding a thickening agent and a sucralose sweetening agent, soaking for at least 3 hours, and adding deionized water into the obtained solution;
and step 3: and (3) collecting the filtrate obtained in the step (2), filtering and concentrating to obtain the daily oral cavity deodorant.
The daily environment-friendly healthy oral deodorant is prepared from the following components in parts by weight:
the total content of the raw materials is 1000 parts.
The oral cavity deodorant is prepared from zinc glycyrrhetate, and the zinc glycyrrhetate is added to accelerate the healing speed of oral ulcer and improve the oral immunity. Sodium citrate, sodium lactate, sodium levulinate and other organic acid sodium salts are selected to improve the taste, assist sodium carbonate to increase the pH buffering capacity and increase the time for keeping the effect after removing the peculiar smell in the oral cavity. Sodium chloride is selected to assist oral bacteriostasis and regulate mouthfeel.
The purpose of the sodium carbonate is to dominate the overall pH adjustment of the system, improving the oral pH environment. The addition of sodium lauryl sulfate can increase the oral cleaning effect during the gargling process and the comfort during the gargling process. The oral cavity micro-chemical environment is adjusted by taking sodium carbonate as a main factor, the maintaining time of the adjusted micro-chemical environment is prolonged by an organic acid sodium salt, the micro-chemical environment adjusting strength is enhanced by sodium chloride in an auxiliary mode, the zinc glycyrrhetate increases the oral cavity immunity, the sodium lauryl sulfate increases the comfort and the cleaning effect in the gargling process, and the aim of quickly removing the peculiar smell of the oral cavity is finally achieved by quickly improving the oral cavity micro-chemical environment on the basis of guaranteeing the oral cavity health through the combined action of the components. The system effectively removes nitrogen, phosphorus, potassium and other elements causing the water body to be rich in oxidation elements, the main components are easy to degrade, and the water body pollution is not caused after the water body is discharged into the environment after the water body is used.
In some embodiments, the composition is prepared from the following raw materials in parts by weight: 5 parts of sodium chloride, 15 parts of sodium citrate, 2 parts of sodium lactate, 1 part of sodium levulinate, 5 parts of sodium lauryl sulfate, 1.5 parts of zinc glycyrrhetate, 2 parts of sodium carbonate, 1 part of thickening agent, 0.1 part of sucralose sweetening agent and the balance of deionized water.
In some embodiments, the particle size of the sodium carbonate is 15 microns to 50 microns.
In some embodiments, the thickening agent is xanthan gum and the sweetener is sucralose.
In some embodiments, the diameter of the powdery material in step 1 is 380 to 830 μm.
The invention adopts another technical scheme that the daily-use environment-friendly healthy oral deodorant is prepared from the following raw materials in parts by weight:
the total content of the raw materials is 1000 parts.
The invention comprehensively considers the micro-chemical environment, the health and the environmental protection, realizes the double purposes of repairing the oral mucosa while changing the micro-chemical environment of the oral cavity, and solves the technical problems existing in the background technology. The raw materials can be rapidly degraded in the putting environment after being used, so that the environment pollution is avoided, the whole process from the production source to the putting environment is healthy and pollution-free, the production is realized by a simple physical mixing method, the process is simple, and the industrialization prospect is wide.
Example 1
Step 1: weighing 50g of sodium chloride, 10g of sodium citrate, 1g of sodium lactate, 15g of sodium levulinate, 10g of sodium lauryl sulfate, 1g of zinc glycyrrhetate and 1g of sodium carbonate, and crushing to obtain a powdery material; the diameter of the powdery material is 380-830 mu m;
step 2: putting the powdery material obtained in the step 1 into a beaker, sequentially adding 1g of xanthan gum and 0.15g of sucralose to soak for at least 3 hours, and adding deionized water into the obtained solution;
and step 3: and (3) collecting the filtrate obtained in the step (2), filtering and concentrating to obtain the daily oral cavity deodorant.
Example 2
Step 1: weighing 5g of sodium chloride, 15g of sodium citrate, 2g of sodium lactate, 1g of sodium levulinate, 5g of sodium lauryl sulfate, 1.5g of zinc glycyrrhetate and 2g of sodium carbonate, and crushing to obtain a powdery material; the diameter of the powdery material is 380-830 mu m;
step 2: putting the powdery material obtained in the step 1 into a beaker, sequentially adding 1g of xanthan gum and 0.1g of sucralose to soak for at least 3 hours, and adding deionized water into the obtained solution;
and step 3: and (3) collecting the filtrate obtained in the step (2), filtering and concentrating to obtain the daily oral cavity deodorant.
Example 3
Step 1: respectively weighing 20g of sodium chloride, 10g of sodium citrate, 2g of sodium lactate, 15g of sodium levulinate, 15g of sodium lauryl sulfate, 2.5g of zinc glycyrrhetate and 5g of sodium carbonate, and crushing to obtain powdery materials; the diameter of the powdery material is 380-830 mu m;
step 2: putting the powdery material obtained in the step 1 into a beaker, sequentially adding 2g of xanthan gum and 0.2g of sucralose to soak for at least 3 hours, and adding deionized water into the obtained solution;
and step 3: and (3) collecting the filtrate obtained in the step (2), filtering and concentrating to obtain the daily oral cavity deodorant.
Example 4
Step 1: respectively weighing 50g of sodium chloride, 1g of sodium citrate, 10g of sodium lactate, 10g of sodium levulinate, 10g of sodium lauryl sulfate, 0.5g of zinc glycyrrhetate and 0.5g of sodium carbonate, and crushing to obtain powdery materials; the diameter of the powdery material is 380-830 mu m;
step 2: putting the powdery material obtained in the step 1 into a beaker, sequentially adding 0.5g of xanthan gum and 0.25g of sucralose to soak for at least 3 hours, and adding deionized water into the obtained solution;
and step 3: and (3) collecting the filtrate obtained in the step (2), filtering and concentrating to obtain the daily oral cavity deodorant.
Example 5
Step 1: respectively weighing 10g of sodium chloride, 10g of sodium citrate, 2g of sodium lactate, 2g of sodium levulinate, 8g of sodium lauryl sulfate, 1g of zinc glycyrrhetate and 2g of sodium carbonate, and crushing to obtain powdery materials; the diameter of the powdery material is 380-830 mu m;
step 2: putting the powdery material obtained in the step 1 into a beaker, sequentially adding 1g of xanthan gum and 0.1g of sucralose to soak for at least 3 hours, and adding deionized water into the obtained solution;
and step 3: and (3) collecting the filtrate obtained in the step (2), filtering and concentrating to obtain the daily oral cavity deodorant.
Example 6
Step 1: respectively weighing 20g of sodium chloride, 12g of sodium citrate, 4g of sodium lactate, 8g of sodium levulinate, 12g of sodium lauryl sulfate, 2g of zinc glycyrrhetate and 3g of sodium carbonate, and crushing to obtain powdery materials; the diameter of the powdery material is 380-830 mu m;
step 2: putting the powdery material obtained in the step 1 into a beaker, sequentially adding 1.5g of xanthan gum and 0.2g of sucralose to soak for at least 3 hours, and adding deionized water into the obtained solution;
and step 3: and (3) collecting the filtrate obtained in the step (2), filtering and concentrating to obtain the daily oral cavity deodorant.
The invention comprehensively considers the micro-chemical environment, the health and the environmental protection, realizes the double purposes of repairing the oral mucosa while changing the micro-chemical environment of the oral cavity, and solves the technical problems existing in the background technology. The raw materials can be rapidly degraded in the putting environment after being used, so that the environment pollution is avoided, the whole process from the production source to the putting environment is healthy and pollution-free, the production is realized by a simple physical mixing method, the process is simple, and the industrialization prospect is wide.
Comparative example 1
Respectively weighing 20g of sodium chloride, 15g of sodium lauryl sulfate, 2.5g of zinc glycyrrhetate, 5g of sodium carbonate, 2g of xanthan gum and 0.2g of sucralose, respectively adding the materials into a 1000mL beaker, and adding deionized water until the total weight is 1000 g. Mechanically stirring at normal temperature to obtain homogeneous solution as the sample.
Comparative example 2
Respectively weighing 20g of sodium chloride, 10g of sodium citrate, 2g of sodium lactate, 15g of sodium levulinate, 15g of sodium lauryl sulfate, 2.5g of zinc glycyrrhetate, 2g of xanthan gum and 0.2g of sucralose, respectively adding the materials into a 1000mL beaker, and adding deionized water until the total weight is 1000 g. Mechanically stirring at normal temperature to obtain homogeneous solution as the sample.
Comparative example 3
5g of sodium carbonate are weighed and deionized water is added to a total weight of 1000 g. Mechanically stirring at normal temperature to obtain homogeneous solution as the sample.
Comparative example 4
Respectively weighing 10g of sodium citrate, 1g of sodium lactate, 15g of sodium levulinate, 10g of sodium lauryl sulfate, 1g of zinc glycyrrhetate, 1g of sodium carbonate, 1g of xanthan gum and 0.15g of sucralose, respectively adding the materials into a 1000mL beaker, and adding deionized water until the total weight is 1000 g. Mechanically stirring at normal temperature to obtain homogeneous solution as the sample.
Comparative example 5
Respectively weighing 50g of sodium chloride, 10g of sodium citrate, 1g of sodium lactate, 15g of sodium levulinate, 1g of zinc glycyrrhetate, 1g of sodium carbonate, 1g of xanthan gum and 0.15g of sucralose, respectively adding the materials into a 1000mL beaker, and adding deionized water until the total weight is 1000 g. Mechanically stirring at normal temperature to obtain homogeneous solution as the sample.
Comparative example 6
Respectively weighing 50g of sodium chloride, 10g of sodium citrate, 1g of sodium lactate, 15g of sodium levulinate, 10g of sodium lauryl sulfate, 1g of sodium carbonate, 1g of xanthan gum and 0.15g of sucralose, respectively adding the materials into a 1000mL beaker, and adding deionized water until the total weight is 1000 g. Mechanically stirring at normal temperature to obtain homogeneous solution as the sample.
According to a microbiological detection method of a product B in appendix of GB15979-2002 hygienic Standard for Disposable sanitary articles, the oral bacteriostatic mouth wash provided in example 3 is subjected to microbiological index detection under the following detection conditions: the test environment temperature is 25 ℃ and the relative humidity is 65%. The test results are shown in Table 1 and meet the regulation of GB15979-2002 hygienic Standard for Disposable sanitary articles.
TABLE 1 EXAMPLE 3 data sheet of microbiological indicator test results
| Detecting the index | Unit of | Standard value | Measured value |
| Total number of bacterial colonies | cfu/mL | ≤200 | <10 |
| Fungi | cfu/mL | ≤100 | <10 |
| Coliform group bacteria | — | Cannot be detected | Not detected out |
| Pseudomonas aeruginosa | — | Cannot be detected | Not detected out |
| Staphylococcus aureus | — | Cannot be detected | Not detected out |
| Hemolytic streptococcus | — | Cannot be detected | Not detected out |
Bacteriostatic tests were carried out on the oral bacteriostatic mouthwashes provided in examples 1-6 and comparative examples 1-6 according to appendix C of GB 15979-2002.
Test strains: staphylococcus aureus ATCC6538, Escherichia coli 8099 and Candida albicans ATCC10231, provided by China general microbiological culture Collection center, with the strain generation number being 7, and TPS is used for preparing bacterial suspension.
And (3) testing the antibacterial performance: according to GB15979-2002 appendix C, each 5mL of example 3 sample solution is infected with 100. mu.L of the bacteria, the action time is 30s, 60s, 90s and 120s, and the temperature is 20 +/-1 ℃. The experiment was repeated 3 times.
The test results are given in the following table:
table 2 data table of average bacteriostatic rate test results of examples 1 to 4
Table 3: comparative example 1 average bacteriostasis rate test result data table
Table 4: comparative example 2 average bacteriostasis rate test result data table
Table 5: comparative example 3 average bacteriostasis rate test result data table
Table 6: comparative example 4 average bacteriostasis rate test result data table
Table 7: comparative example 5 average bacteriostasis rate test result data table
Table 8: comparative example 6 average bacteriostasis rate test result data table
As shown in the data tables of the detection results in tables 2 to 8, the bacteriostatic data of comparative examples 1 to 4, comparative example 2 and comparative example 3 are compared, and the sodium carbonate has obvious bacteriostatic action.
As can be seen from comparison of the bacteriostatic data of example 3 and comparative example 1, the addition of the organic acid sodium salt increases the pH value capacity, reduces the bacteriostatic effect at the initial stage, and increases the bacteriostatic effect with time.
As can be seen from the comparison of the bacteriostatic data of the example 1 and the comparative example 4, the addition of the sodium chloride increases the bacteriostatic rate and enhances the bacteriostatic effect.
As can be seen from comparison of the bacteriostatic data of the example 1 and the comparative examples 5 to 6, sodium lauryl sulfate and a small amount of zinc glycyrrhetate do not contribute to the bacteriostatic action.
The group test mainly aims at realizing the technology for quickly removing the oral odor on the basis of health and environmental protection, and aims at meeting the requirements of the masses, so the group test and the acquisition of the most visual experience of the tested group have important significance on whether the technology can be industrialized or commercialized.
50 volunteers (30 men and 20 women) are gathered to the society for visual perception test, 10mL of mouth wash is carried out for 60s (then tap water is used for mouth wash once again) for each person, the smell removal effect is judged by smelling the exhaled gas by other people before and after mouth wash, the mouth wash effect is compared with the tap water mouth wash effect, and the mouth feel in the mouth wash process is visually expressed.
Table 9: experimental and comparative example population test data sheet
| Deodorizing effect | Taste of the product | |
| Example 1 | Good effect | Good effect |
| Example 2 | Good effect | Good effect |
| Example 3 | Good effect | Good effect |
| Example 4 | Good effect | Good effect |
| Comparative example 1 | Good effect | Slight irritation of throat |
| Comparative example 2 | Difference (D) | Good effect |
| Comparative example 3 | Good effect | Poor sensation of vomiting |
| Comparative example 4 | Good effect | Slight irritation of throat |
| Comparative example 5 | Good effect | Good but poor food residue removal. |
| Comparative example 6 | Good effect | Good effect |
Ulcer elimination test, 30 ordinary mouth ulcer patients (without basic disease) were tested in 3 groups, 10 tap water mouthwashes (rinse with tap water after meal, 3 times daily), 10 samples of example 1 (rinse with tap water for 60s after 10mL of example 1 sample after meal, rinse with tap water for 3 times daily), 10 samples of comparative example 6 (rinse with tap water for 60s after 10mL of comparative example 6 sample after meal, rinse with tap water for 3 times daily)
According to the medical knowledge, the ordinary oral ulcer patient (without basic disease) usually heals automatically in about 7 days, which is basically consistent with the situation of tap water gargling in the test process. As can be seen from the following table, the zinc oxalate has obvious effect on eliminating dental ulcer and can effectively enhance the oral immunity.
The invention takes food additives, beverage raw materials and the like as raw materials, guarantees the health and safety of the body from the source, neutralizes common acidic peculiar smell gas by temporarily changing the micro chemical environment of the oral cavity, realizes the rapid removal of the oral peculiar smell, and prolongs the time for removing the oral peculiar smell by the buffer solution technology. Meanwhile, the micromolecular organic acid salt which is beneficial to the restoration of oral mucosa is added, the source of the peculiar smell generated in the oral cavity is improved, the oral immunity is increased, the oral health is cared, and the aim of gradually realizing no peculiar smell generated in the oral cavity by long-term use is fulfilled. The invention comprehensively considers from three aspects of micro-chemical environment, health and environmental protection, realizes the dual purposes of repairing oral mucosa while changing the oral micro-chemical environment, the throwing environment of the raw materials can be quickly degraded after use without causing environmental pollution, the whole process from the production source to the throwing environment is healthy and pollution-free, the raw materials selected by the technology are food additives, beverage raw materials and the like, are easy to degrade, do not pollute the environment after use, are produced by a simple physical mixing method, have simple process and wide industrial prospect.
Claims (6)
1. The preparation method of the daily-use environment-friendly healthy oral deodorant is characterized by comprising the following steps of:
step 1, taking sodium chloride, sodium citrate, sodium lactate, sodium levulinate, sodium lauryl sulfate, zinc glycyrrhetate and sodium carbonate, and crushing to obtain a powdery material;
2, putting the powdery material obtained in the step 1 into a beaker, sequentially adding a thickening agent and a sucralose sweetening agent, soaking for at least 3 hours, and adding deionized water into the obtained solution;
and 3, collecting the filtrate obtained in the step 2, filtering and concentrating to obtain the daily oral cavity deodorant.
The daily environment-friendly healthy oral deodorant is prepared from the following components in parts by weight:
the total content of the raw materials is 1000 parts.
2. The preparation method of the daily use environment-friendly healthy oral deodorant according to claim 1, wherein the daily use environment-friendly healthy oral deodorant is prepared from the following raw materials in parts by weight: 5 parts of sodium chloride, 15 parts of sodium citrate, 2 parts of sodium lactate, 1 part of sodium levulinate, 5 parts of sodium lauryl sulfate, 1.5 parts of zinc glycyrrhetate, 2 parts of sodium carbonate, 1 part of thickening agent, 0.1 part of sucralose sweetening agent and the balance of deionized water.
3. The method for preparing a daily use environment-friendly healthy oral deodorant according to claim 2, wherein the particle size of the sodium carbonate is 15-50 microns.
4. The method for preparing a daily use environment-friendly healthy oral cavity deodorant according to claim 1 or 2, wherein the thickener is xanthan gum, and the sweetener is sucralose.
5. The method for preparing a daily use environment-friendly healthy oral deodorant according to claim 4, wherein the diameter of the powdery material in the step 1 is 380-830 μm.
6. The daily-use environment-friendly healthy oral deodorant is characterized by being prepared from the following raw materials in parts by weight:
the total content of the raw materials is 1000 parts.
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