CN113214008A - Special foliar fertilizer for corn and preparation method thereof - Google Patents

Special foliar fertilizer for corn and preparation method thereof Download PDF

Info

Publication number
CN113214008A
CN113214008A CN202110539013.6A CN202110539013A CN113214008A CN 113214008 A CN113214008 A CN 113214008A CN 202110539013 A CN202110539013 A CN 202110539013A CN 113214008 A CN113214008 A CN 113214008A
Authority
CN
China
Prior art keywords
corn
parts
foliar fertilizer
special
weight
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN202110539013.6A
Other languages
Chinese (zh)
Other versions
CN113214008B (en
Inventor
邵长禄
夏婕
王丽娟
路海鹏
宋君
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zibo Xinnongji Crop Science Co ltd
Original Assignee
Zibo Xinnongji Crop Science Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zibo Xinnongji Crop Science Co ltd filed Critical Zibo Xinnongji Crop Science Co ltd
Priority to CN202110539013.6A priority Critical patent/CN113214008B/en
Publication of CN113214008A publication Critical patent/CN113214008A/en
Application granted granted Critical
Publication of CN113214008B publication Critical patent/CN113214008B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/20Liquid fertilisers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Fertilizers (AREA)

Abstract

The invention relates to the technical field of foliar fertilizers, and particularly relates to a foliar fertilizer special for corn and a preparation method thereof. The foliar fertilizer special for the corn is prepared from the following raw materials in parts by weight: 30-45 parts of corn germ residues, 30-55 parts of bean dregs, 15-25 parts of pig hair, 18-25 parts of duck lung, 35-90 parts of major elements, 5-20 parts of medium trace elements, 70-100 parts of nutritional ingredients and 1-10 parts of a spreader. The special foliar fertilizer for the corn is suitable for the whole growth period of corn crops, improves the absorption efficiency, increases the yield, is simple and quick to produce, is convenient to use and is environment-friendly. The invention also provides a preparation method of the composition.

Description

Special foliar fertilizer for corn and preparation method thereof
Technical Field
The invention relates to the technical field of foliar fertilizers, and particularly relates to a foliar fertilizer special for corn and a preparation method thereof.
Background
Corn is the third crop in China, and the perennial planting area is 3000 ten thousand hm2About, it accounts for more than 30% of the total grain production in China. The whole growth period of the corn is subjected to a seedling emergence period, a trefoil period, an elongation period, a large flare period, a heading period, a flowering period and a mature period. The nutrient requirement of the corn in the whole growth period is that nitrogen is maximumThe potassium is the third place, and the phosphorus is the third place. Generally, every 100 kg of grains need to absorb 2.5 kg of nitrogen (N), 0.5 kg of phosphorus (P) and 1.7 kg of potassium (K) from soil. In addition, the corn is sensitive to zinc, the zinc influences the synthesis of endogenous auxin such as indoleacetic acid in corn plants, the iron influences the content of chlorophyll in leaf surfaces, the corn is a moderate boron-resistant crop, and the demand for manganese and molybdenum elements is low. The foliar fertilizer is a fertilizer type in which nutrient elements are applied to the surfaces of crop leaves and the basic functions are exerted through the absorption of the leaves, so that under the condition of reasonably applying a base fertilizer, the proportion among major elements, secondary elements and trace elements can be effectively balanced by spraying the special foliar fertilizer for the corn in each key period of the corn, and the special foliar fertilizer plays a key role in promoting the normal and rapid growth of plants and increasing the yield and improving the quality. The existing foliar fertilizers mostly adopt different types of amino acids and a large amount of functional chemical fertilizers, but the produced corn foliar fertilizers have high cost, large fertilizer demand and high investment, but the yield and the quality are still not high and are not environment-friendly.
The CN109400275A patent discloses a novel corn leaf fertilizer and a preparation method thereof, which adopts raw materials of potassium oxalate, sodium nitrate, trichloroisocyanuric acid, serine, histidine, methionine, salicylic acid, malic acid and cellulose triacetate, directly mixes and stirs the raw materials, and uses after dilution, thereby improving the corn yield, reducing the soil damage, mainly using the salicylic acid to improve the utilization rate, but the utilization rate of the fertilizer still needs to be improved, and the cost is higher.
The CN110483157A patent discloses a corn foliar fertilizer which comprises boric acid, potassium carbonate, epsilon-polylysine, humic acid, methylene succinic acid, trace elements, diethyl aminoethyl hexanoate and a chelating agent.
The CN105439693A patent discloses an lodging-resistant disease-resistant growth-promoting corn foliar fertilizer, which comprises the following components: the fertilizer is added with potassium, calcium, zinc, silicon and other elements, has high nutrient utilization rate and sterilization effect, prevents various maize bacterial wilt, large leaf spot and small leaf spot diseases and the like, but has high cost and low yield and still cannot solve the problems.
Disclosure of Invention
The technical problem to be solved by the invention is to provide the special foliar fertilizer for the corn, which is suitable for the whole growth period of corn crops, improves the absorption efficiency, increases the yield, and is simple and quick in production, convenient to use and environment-friendly. The invention also provides a preparation method of the composition.
The foliar fertilizer special for the corn is prepared from the following raw materials in parts by weight:
Figure BDA0003070886590000021
the macroelements are urea and phosphorus-potassium compound fertilizer, and the macroelements are composed of the following components in parts by weight: 15-40 parts of phosphorus-potassium compound fertilizer and 20-50 parts of urea.
The phosphorus-potassium compound fertilizer is one or more of monopotassium phosphate, potassium phosphite, potassium pyrophosphate and potassium tripolyphosphate, and preferably one or more of potassium phosphite, potassium pyrophosphate and potassium tripolyphosphate.
The medium trace elements are one or more of calcium nitrate tetrahydrate, magnesium nitrate hexahydrate, magnesium sulfate monohydrate, copper sulfate pentahydrate, ferrous sulfate heptahydrate, ferrous sulfate monohydrate, manganese sulfate monohydrate, zinc sulfate heptahydrate, EDTA-Cu, EDTA-Fe, EDTA-Mn, EDTA-Zn, copper citrate, ferric citrate, manganese citrate, zinc citrate, ammonium heptamolybdate, boric acid, borax and sodium octaborate tetrahydrate.
The nutrient components are one or more of molasses fermentation liquor, fish protein, alginic acid, seaweed extract, chitosan oligosaccharide, gamma-polyglutamic acid, gamma-aminobutyric acid, bacillus thuringiensis and glycan polypeptide.
The spreader is one or more of tween 80, alkyl glycoside, triethanolamine ester, dodecylbenzene sulfonic acid, lauric acid and methyl silicone oil.
The preparation method of the foliar fertilizer special for corn comprises the following preparation steps:
(1) putting the treated duck lung, the pig hair, the corn germ residues and the bean dregs into a reaction kettle according to the formula amount, adding water for mixing, continuously adding a dilute hydrochloric acid solution, heating and preserving heat, and stirring for 10-12 hours to obtain a mixed solution;
(2) neutralizing the mixed solution obtained in the step (1) by using strong ammonia water, adjusting the pH to 3.0-4.5, and filtering to obtain clear liquid, namely the animal and plant source amino acid solution;
(3) adding medium trace elements into the animal and plant source amino acid solution obtained in the step (2) according to the formula amount, heating and stirring to obtain an amino acid chelated medium trace element solution;
(4) and (3) sequentially adding macroelements, nutrient components and a spreader into the amino acid chelated medium and trace element solution obtained in the step (3) according to the formula amount, and stirring for 0.5-1 h to obtain the special foliar fertilizer for corn.
The macroelement raw material adjusts the ratio of nitrogen, phosphorus and potassium to be within the range of (9-15): (1.5-5.5): 3-10.
In the step (1), firstly, the duck lungs are roughly cut into 1cm3And (3) processing the fragments, putting the fragments, the pig hair, the corn germ residues and the bean dregs into a reaction kettle, adding water with the same volume as the solid raw materials, uniformly mixing, continuously adding 18% dilute hydrochloric acid solution, heating to 105-110 ℃, preserving heat, and stirring for 10-12 hours at the rotating speed of 100-200 r/min to obtain a mixed solution.
The addition amount of the 18% dilute hydrochloric acid solution in the step (1) is 170-210 parts by weight of the raw material.
And (3) heating to 75-80 ℃, and stirring and reacting for 2 hours under the condition of 300-400 r/min to obtain the amino acid chelated medium and trace element solution.
Specifically, the preparation method of the foliar fertilizer special for corn comprises the following preparation steps:
(1) firstly, roughly cutting the lung of a duck into 1cm3Processing the fragments, namely putting 18-25 parts of duck lung, 15-25 parts of pig hair, 30-45 parts of corn germ residues and 30-55 parts of bean residues into a reaction kettle according to parts by weight, and adding the materials into the reaction kettleUniformly mixing the accumulated water, continuously adding 210 parts by weight of 18% dilute hydrochloric acid solution 170-25L/min, heating to 105-110 ℃, preserving heat, and stirring at a rotating speed of 100-200 r/min for 10-12 h to obtain a mixed solution.
(2) Neutralizing the mixed solution obtained in the step (1) by using strong ammonia water, adjusting the pH to 3.0-4.5, and filtering to obtain clear liquid, namely the animal and plant source amino acid solution;
(3) adding 5-20 parts by weight of medium and trace elements into the animal and plant source amino acid solution obtained in the step (2) according to the formula amount, heating to 75-80 ℃, and stirring and reacting for 2 hours under the condition of 300-400 r/min to completely chelate the amino acid and the medium and trace elements to obtain an amino acid chelated medium and trace element solution;
(4) and (3) sequentially adding 15-40 parts by weight of phosphorus-potassium compound fertilizer, 20-50 parts by weight of urea, 70-100 parts by weight of nutrient components and 1-10 parts by weight of spreader according to the formula amount into the amino acid chelated medium trace element solution in the step (3), and stirring for 0.5-1 h to obtain the special foliar fertilizer for corn.
The invention relates to a special foliar fertilizer for corn and a preparation method thereof, wherein an amino acid hydrolysis method is adopted as an acidolysis method, dilute hydrochloric acid solution is utilized to hydrolyze animal source and plant source leftovers to obtain crude amino acid solution, the crude amino acid solution is chelated with trace elements under certain conditions, macroelement raw materials are added to adjust the proportion of nitrogen to phosphorus to potassium within the range of (9-15) to (1.5-5.5) to (3-10), so as to prepare the special foliar fertilizer for corn, and finally, nutritional ingredients and active ingredients are supplemented to balance nutrition, so that the rapid growth of crops is stimulated, the spreadability of the fertilizer on leaf surfaces is increased, the absorption efficiency is greatly improved, and the special foliar fertilizer is suitable for the whole growth period of corn crops; the conversion rate of amino acid of different animal and plant leftovers and the hydrolysis difference of the dilute acid and the hydrolysis process with different concentrations on the amino acid have great influence on the special foliar fertilizer for the corn, the conversion rate of the amino acid of the duck lung and the pig hair in the animal source leftovers in the preparation method is high, and the conversion rate of the amino acid of the bean dregs in the plant source leftovers is high; from the aspect of controlling cost, the method adopts 18% hydrochloric acid to hydrolyze for 10-12 hours at 105-110 ℃ to achieve the optimal hydrolysis effect, the adopted raw materials are pig hair, duck lung, corn germ residue and bean dregs, the hydrolysate is rich in amino acid types, and the content of organic substances and active ingredients is higher than that of common amino acid liquid. The invention combines the spreader to effectively reduce the surface tension of the liquid fertilizer, improve the permeability, increase the contact surface of the fertilizer and the leaf epidermis, prolong the attachment time of the fertilizer on the leaf surface, promote the leaf surface absorption of active ingredients and the transportation on plants, and the formula of the invention is the regular preparation of the fertilizer requirement of crops.
Compared with the prior art, the invention has the following beneficial effects:
(1) the foliar fertilizer special for the corn, disclosed by the invention, has the advantages of absorption efficiency, suitability for the whole growth period of corn crops and high yield;
(2) the preparation method of the foliar fertilizer special for corn is simple and rapid and is convenient to use;
(3) the foliar fertilizer special for the corn adopts animal and plant leftovers of pig hair and duck lung, has high utilization rate, saves cost and is environment-friendly;
(4) the foliar fertilizer special for the corn has strong infiltration capacity, enables the foliar to be balanced in nutrition and improves the quality.
Detailed Description
The invention is further illustrated by the following examples.
Example 1
A preparation method of a foliar fertilizer special for corn comprises the following preparation steps:
(1) firstly, roughly cutting the lung of a duck into 1cm3Processing the fragments, namely putting 25 parts of processed duck lung, 20 parts of pig hair, 35 parts of corn germ residues and 30 parts of bean dregs into a reaction kettle according to parts by weight, adding water with the same volume as the solid raw material, uniformly mixing, continuously adding 200 parts of 18% dilute hydrochloric acid solution at the speed of 25L/min, heating to 110 ℃, preserving heat, and stirring for 12 hours at the rotating speed of 200r/min to obtain a mixed solution;
(2) neutralizing the mixed solution in the step (1) by using strong ammonia water, adjusting the pH to 4.0, and filtering to obtain clear liquid, namely the animal and plant source amino acid solution;
(3) adding 7 parts by weight of calcium nitrate tetrahydrate, 3 parts by weight of magnesium nitrate hexahydrate, 0.5 part by weight of copper sulfate pentahydrate, 2 parts by weight of EDTA-Fe, 5 parts by weight of zinc sulfate heptahydrate and 2.5 parts by weight of boric acid into the animal and plant source amino acid solution obtained in the step (2), heating to 80 ℃, stirring and reacting for 2 hours under the condition of 350r/min to completely chelate amino acid and medium and trace elements to obtain an amino acid chelated medium and trace element solution;
(4) and (3) sequentially adding 5 parts by weight of monopotassium phosphate, 20 parts by weight of potassium pyrophosphate, 50 parts by weight of urea, 20 parts by weight of chitosan oligosaccharide, 80 parts by weight of molasses fermentation liquor and 2 parts by weight of tween 80 into the amino acid chelated medium trace element solution obtained in the step (3), and stirring for 1h to obtain the special foliar fertilizer for corn.
Example 2
(1) Firstly, roughly cutting the lung of a duck into 1cm3Processing the fragments, namely putting 18 parts of processed duck lung, 25 parts of pig hair, 40 parts of corn germ residues and 40 parts of bean dregs into a reaction kettle according to parts by weight, adding water with the same volume as the solid raw material, uniformly mixing, continuously adding 180 parts of 18% dilute hydrochloric acid solution at the speed of 20L/min, heating to 105 ℃, preserving heat, and stirring for 12 hours at the rotating speed of 150r/min to obtain a mixed solution;
(2) neutralizing the mixed solution in the step (1) by using strong ammonia water, adjusting the pH to 4.5, and filtering to obtain clear liquid, namely the animal and plant source amino acid solution;
(3) adding 7 parts by weight of calcium nitrate tetrahydrate, 2 parts by weight of magnesium sulfate monohydrate, 0.5 part by weight of EDTA-Cu, 3 parts by weight of ferrous sulfate heptahydrate, 3 parts by weight of zinc sulfate heptahydrate, 1 part by weight of zinc citrate and 2.5 parts by weight of boric acid into the animal and plant source amino acid solution obtained in the step (2), heating to 80 ℃, and stirring and reacting for 2 hours under the condition of 400r/min to completely chelate amino acid and medium and trace elements to obtain an amino acid chelated medium and trace element solution;
(4) and (3) sequentially adding 10 parts by weight of potassium tripolyphosphate, 10 parts by weight of potassium pyrophosphate, 40 parts by weight of urea, 20 parts by weight of polysaccharide polypeptide, 60 parts by weight of molasses fermentation liquor, 2 parts by weight of Tween 80 and 3 parts by weight of dodecylbenzene sulfonic acid into the amino acid chelated medium trace element solution obtained in the step (3), and stirring for 0.5h to obtain the special foliar fertilizer for corn.
Example 3
(1) Firstly, roughly cutting the lung of a duck into 1cm3And (3) processing the fragments, namely putting 20 parts of processed duck lung, 15 parts of pig hair, 45 parts of corn germ residues and 55 parts of bean dregs in a reaction kettle according to parts by weight, adding water with the same volume as the solid raw material, uniformly mixing, continuously adding 210 parts of 18% dilute hydrochloric acid solution at the speed of 25L/min, heating to 110 ℃, preserving heat, and stirring for 12 hours at the rotating speed of 200r/min to obtain a mixed solution.
(2) Neutralizing the mixed solution in the step (1) by using strong ammonia water, adjusting the pH to 4.0, and filtering to obtain clear liquid, namely the animal and plant source amino acid solution;
(3) adding 7 parts by weight of calcium nitrate tetrahydrate, 3 parts by weight of magnesium nitrate hexahydrate, 1 part by weight of copper sulfate pentahydrate, 2 parts by weight of ferrous sulfate monohydrate, 4 parts by weight of EDTA-Zn, 1 part by weight of manganese citrate and 2.0 parts by weight of sodium octaborate tetrahydrate into the animal and plant source amino acid solution obtained in the step (2), heating to 80 ℃, stirring and reacting for 2 hours under the condition of 400r/min to completely chelate amino acid and medium and trace elements to obtain an amino acid chelated medium and trace element solution;
(4) and (3) sequentially adding 30 parts by weight of monopotassium phosphate, 40 parts by weight of urea, 15 parts by weight of chitosan oligosaccharide, 15 parts by weight of fish protein, 60 parts by weight of molasses fermentation liquor and 6 parts by weight of methyl silicone oil into the amino acid chelated medium trace element solution obtained in the step (3), and stirring for 1h to obtain the special foliar fertilizer for corn.
Example 4
The special foliar fertilizer for corns prepared in the examples 1 to 3 is applied to Zhao Xinzhuang village in the Guangxi county, the 12-mu corn field of Zhao Xinzhuang village in the Guangxi county is divided into 4 groups, each group has 3 mu, and the special foliar fertilizer for corns prepared in the examples 1, 2 and 3 is diluted by 600 times by 40ml of dosage per mu in three periods (large flare period, heading period and flowering period) of the corn in the 3 groups, and then is uniformly sprayed on the front and back surfaces of the corn leaves; spraying clear water on the leaf surfaces of the other group of the corn leaves to serve as a control group; the insecticidal, fungicidal and herbicidal agents and other nutritional fertilizers applied to the 4 fields were consistent throughout the test period.
The monitoring of the growth state of maize and yield calculations in the experimental and control groups of examples 1-3 are described separately and the results are shown in table 1:
TABLE 1 comparison of results
Grouping Growth vigor of plants Average mu yield (kilogram)
Example 1 Strong straw, strong root system, wide coverage, wide and thick leaf, dark green leaf color 643.6
Example 2 Strong straw, developed root system, wide and thick leaves and dark green leaf color 636
Example 3 Strong straw, strong root system, wide coverage, wide and thick leaf, and dark green color 603
Control group The straw is thin, the root system is small, and the leaf surface is narrow 537
Example 5
The foliar fertilizer special for corn prepared in the embodiments 1 to 3 is applied to 16 mu of corn field of the temple of Yucheng houses in Texas, and is divided into 4 groups, wherein each group has 4 mu, and 3 groups respectively dilute the foliar fertilizer special for corn prepared in the embodiments 1, 2 and 3 by 600 times in the dosage of 40ml per mu in three periods (large trumpet mouth period, heading period and flowering period) of corn and then uniformly spray the foliar fertilizer on the front and back surfaces of corn leaves; spraying clear water on the leaf surfaces of the other group of the corn leaves to serve as a control group; the insecticidal, fungicidal and herbicidal agents and other nutritional fertilizers applied to the 4 fields were consistent throughout the test period.
The monitoring of the growth state of maize and yield calculations in the experimental and control groups of examples 1-3 are described separately and the results are shown in table 2:
TABLE 2 comparison of results
Grouping Growth vigor of plants Average mu yield (kilogram)
Example 1 Short straw stout internodes, stout root system, wide and thick leaves and dark green leaf color 624
Example 2 Short straw stout internodes, stout root system, wide and thick leaves and dark green leaf color 627
Example 3 Short straw stout internodes, stout root system, wide and thick leaves and dark green leaf color 619
Control group The straws are thin, the root systems are small, and the leaves are thin 505
Example 6
The special foliar fertilizer for corn prepared in the examples 1 to 3 is applied to the green lotus stone village in the city cao county, 12 mu of the green lotus stone village in the city cao county is divided into 4 groups, each group has 3 mu, wherein the 3 groups respectively dilute the special foliar fertilizer for corn prepared in the examples 1, 2 and 3 by 600 times in the dosage of 40ml per mu in three periods (large flare period, heading period and flowering period) of the corn, and then uniformly spray the diluted foliar fertilizer on the front and back surfaces of the corn leaves; spraying clear water on the leaf surfaces of the other group of the corn leaves to serve as a control group; the insecticidal, fungicidal and herbicidal agents and other nutritional fertilizers applied to the 4 fields were consistent throughout the test period.
The monitoring of the growth state of maize and yield calculations in the experimental and control groups of examples 1-3 are described separately and the results are shown in table 3:
TABLE 3 comparison of results
Grouping Growth vigor of plants Average mu yield (kilogram)
Example 1 Strong straw, strong root system, wide and thick leaf and dark green leaf color 637
Example 2 The straw is stout,Thick root system, wide and thick leaf and dark green leaf color 642
Example 3 Strong straw, strong root system, wide and thick leaf and dark green leaf color 623
Control group The straws are thin, the root systems are small, and the blades are narrow 542
After the foliar fertilizer special for corn prepared in the embodiments 1 to 3 is applied in the embodiments 4 to 6, and a corresponding control group is provided, it can be seen from the experimental group and the control group that the foliar fertilizer special for corn disclosed by the invention is used in the key period of corn to improve the growth vigor and the yield increase effect of corn, and the corn sprayed with the foliar fertilizer disclosed by the invention has the advantages of strong straw, short internode, strong and wide root system, thick and green leaves, and more than 10% of yield increase, and the fertilizing effect is remarkable.

Claims (10)

1. The special foliar fertilizer for the corn is characterized by comprising the following components in parts by weight: the feed is prepared from the following raw materials in parts by weight:
Figure FDA0003070886580000011
2. the foliar fertilizer special for corn according to claim 1, which is characterized in that: the macroelements are urea and phosphorus-potassium compound fertilizer, and the macroelements are composed of the following components in parts by weight: 15-40 parts of phosphorus-potassium compound fertilizer and 20-50 parts of urea.
3. The foliar fertilizer special for corn according to claim 2, characterized in that: the phosphorus-potassium compound fertilizer is one or more of potassium dihydrogen phosphate, potassium phosphite, potassium pyrophosphate and potassium tripolyphosphate.
4. The foliar fertilizer special for corn according to claim 1, which is characterized in that: the medium trace elements are one or more of calcium nitrate tetrahydrate, magnesium nitrate hexahydrate, magnesium sulfate monohydrate, copper sulfate pentahydrate, ferrous sulfate heptahydrate, ferrous sulfate monohydrate, manganese sulfate monohydrate, zinc sulfate heptahydrate, EDTA-Cu, EDTA-Fe, EDTA-Mn, EDTA-Zn, copper citrate, ferric citrate, manganese citrate, zinc citrate, ammonium heptamolybdate, boric acid, borax and sodium octaborate tetrahydrate.
5. The foliar fertilizer special for corn according to claim 1, which is characterized in that: the nutrient components are one or more of molasses fermentation liquor, fish protein, alginic acid, seaweed extract, chitosan oligosaccharide, gamma-polyglutamic acid, gamma-aminobutyric acid, bacillus thuringiensis and glycan polypeptide.
6. The foliar fertilizer special for corn according to claim 1, which is characterized in that: the spreader is one or more of tween 80, alkyl glycoside, triethanolamine ester, dodecylbenzene sulfonic acid, lauric acid and methyl silicone oil.
7. The preparation method of the special foliar fertilizer for corn of any one of claims 1 to 6, characterized by comprising the following steps: the preparation method comprises the following preparation steps:
(1) putting the treated duck lung, the pig hair, the corn germ residues and the bean dregs into a reaction kettle according to the formula amount, adding water for mixing, continuously adding a dilute hydrochloric acid solution, heating and preserving heat, and stirring for 10-12 hours to obtain a mixed solution;
(2) neutralizing the mixed solution obtained in the step (1) by using strong ammonia water, adjusting the pH to 3.0-4.5, and filtering to obtain clear liquid, namely the animal and plant source amino acid solution;
(3) adding medium trace elements into the animal and plant source amino acid solution obtained in the step (2) according to the formula amount, heating and stirring to obtain an amino acid chelated medium trace element solution;
(4) and (3) sequentially adding macroelements, nutrient components and a spreader into the amino acid chelated medium and trace element solution obtained in the step (3) according to the formula amount, and stirring for 0.5-1 h to obtain the special foliar fertilizer for corn.
8. The preparation method of the foliar fertilizer special for corn according to claim 7, characterized in that: in the step (1), firstly, the duck lungs are roughly cut into 1cm3And (3) processing the fragments, putting the fragments, the pig hair, the corn germ residues and the bean dregs into a reaction kettle, adding water with the same volume as the solid raw materials, uniformly mixing, continuously adding 18% dilute hydrochloric acid solution, heating to 105-110 ℃, preserving heat, and stirring for 10-12 hours at the rotating speed of 100-200 r/min to obtain a mixed solution.
9. The preparation method of the foliar fertilizer special for corn according to claim 7, characterized in that: the addition amount of the 18% dilute hydrochloric acid solution in the step (1) is 170-210 parts by weight of the raw material.
10. The preparation method of the foliar fertilizer special for corn according to claim 7, characterized in that: and (3) heating to 75-80 ℃, and stirring and reacting for 2 hours under the condition of 300-400 r/min to obtain the amino acid chelated medium and trace element solution.
CN202110539013.6A 2021-05-18 2021-05-18 Special foliar fertilizer for corn and preparation method thereof Active CN113214008B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110539013.6A CN113214008B (en) 2021-05-18 2021-05-18 Special foliar fertilizer for corn and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110539013.6A CN113214008B (en) 2021-05-18 2021-05-18 Special foliar fertilizer for corn and preparation method thereof

Publications (2)

Publication Number Publication Date
CN113214008A true CN113214008A (en) 2021-08-06
CN113214008B CN113214008B (en) 2023-04-11

Family

ID=77092606

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202110539013.6A Active CN113214008B (en) 2021-05-18 2021-05-18 Special foliar fertilizer for corn and preparation method thereof

Country Status (1)

Country Link
CN (1) CN113214008B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113880639A (en) * 2021-10-26 2022-01-04 淄博新农基作物科学有限公司 Humic acid fertilizer and preparation method thereof
CN117902942A (en) * 2024-03-15 2024-04-19 黑龙江农垦乾源肥业有限公司 Corn yield-increasing functional fertilizer

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102718605A (en) * 2012-07-19 2012-10-10 湖南省烟草公司郴州市公司 Method for producing amino acid tobacco-specific foliar fertilizer by using abandoned fur
CN105060975A (en) * 2015-07-23 2015-11-18 安徽合一生态农业有限公司 Efficient foliar fertilizer with amino acid and preparation method for efficient foliar fertilizer with amino acid
CN105237093A (en) * 2015-09-06 2016-01-13 定远县绿森苑农林开发有限公司 High-effective foliar fertilizer specially used for soya beans and preparation method thereof
CN106478206A (en) * 2015-08-24 2017-03-08 安徽亚环生物科技有限公司 A kind of high-activity humic acid fertilizer based on chicken barnyard manure and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102718605A (en) * 2012-07-19 2012-10-10 湖南省烟草公司郴州市公司 Method for producing amino acid tobacco-specific foliar fertilizer by using abandoned fur
CN105060975A (en) * 2015-07-23 2015-11-18 安徽合一生态农业有限公司 Efficient foliar fertilizer with amino acid and preparation method for efficient foliar fertilizer with amino acid
CN106478206A (en) * 2015-08-24 2017-03-08 安徽亚环生物科技有限公司 A kind of high-activity humic acid fertilizer based on chicken barnyard manure and preparation method thereof
CN105237093A (en) * 2015-09-06 2016-01-13 定远县绿森苑农林开发有限公司 High-effective foliar fertilizer specially used for soya beans and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113880639A (en) * 2021-10-26 2022-01-04 淄博新农基作物科学有限公司 Humic acid fertilizer and preparation method thereof
CN117902942A (en) * 2024-03-15 2024-04-19 黑龙江农垦乾源肥业有限公司 Corn yield-increasing functional fertilizer
CN117902942B (en) * 2024-03-15 2024-05-31 黑龙江农垦乾源肥业有限公司 Corn yield-increasing functional fertilizer

Also Published As

Publication number Publication date
CN113214008B (en) 2023-04-11

Similar Documents

Publication Publication Date Title
CN100546948C (en) Plant source disease-resistant foliage fertilizer and preparation method thereof
CN102910980B (en) Foliar fertilizer for controlling various physiological diseases of crops
CN103396232A (en) Biological fertilizer
CN102311289A (en) Organic water soluble fertilizer
CN113214008B (en) Special foliar fertilizer for corn and preparation method thereof
CN103333018B (en) A kind of long-acting slow-releasing and controlled-releasing corn fertilizer
CN102659456A (en) Amino-acid organic compound fertilizer and production method thereof
CN108947633A (en) A kind of growth-promoting root liquid fertilizer and the preparation method and application thereof
CN110382448A (en) Dissolved fertilizer preparaton and its application method
CN110590464A (en) Four-in-one total-nutrient composite microbial fertilizer
CN104072250A (en) Method for preparing fertilizers by comprehensively utilizing oil residue
CN104557294A (en) Special water-soluble fertilizer for roses and preparation method
CN108456061A (en) A kind of disease resistance promotees absorption safety and stablizes foliar fertilizer and preparation method thereof
CN111548217A (en) Organic high-potassium water-soluble fertilizer and preparation method thereof
CN102503650A (en) Amino acid chelated fertilizer and preparation method thereof
CN102101809B (en) Preparation process and using method for amino acid rare-earth zinc micro-fertilizer
Jamilah Mowing rice crop as ratoon and applying Chromolaena odorata compost to support food security
CN115124376A (en) Compound biological fertilizer and preparation method thereof
CN115108865A (en) Green composite biological stimulator and preparation method thereof
CN108164340A (en) A kind of preparation method of the organic fertilizer containing microbial inoculum
CN107445738A (en) A kind of water-soluble fertilizer containing amino acid for adding furfural acid
CN113896595A (en) Multi-element water-soluble compound microbial fertilizer and preparation method thereof
CN112661562A (en) Water soluble foliage water flush fertilizer and its production method
KR102607263B1 (en) Synergistic agricultural formulations comprising diacyl or diaryl urea and at least one nutrient mixture
CN105237133A (en) Amino acid organic/inorganic mixed fertilizer

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: Corn specific foliar fertilizer and its preparation method

Effective date of registration: 20230524

Granted publication date: 20230411

Pledgee: Zibo Branch of China Post Savings Bank Co.,Ltd.

Pledgor: ZIBO XINNONGJI CROP SCIENCE CO.,LTD.

Registration number: Y2023980041511

PE01 Entry into force of the registration of the contract for pledge of patent right