CN112931441A - Fish bait essential oil and using method thereof - Google Patents
Fish bait essential oil and using method thereof Download PDFInfo
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- CN112931441A CN112931441A CN202110393983.XA CN202110393983A CN112931441A CN 112931441 A CN112931441 A CN 112931441A CN 202110393983 A CN202110393983 A CN 202110393983A CN 112931441 A CN112931441 A CN 112931441A
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- 241000251468 Actinopterygii Species 0.000 claims abstract description 54
- 239000002994 raw material Substances 0.000 claims abstract description 46
- 239000000843 powder Substances 0.000 claims abstract description 42
- 239000000419 plant extract Substances 0.000 claims abstract description 29
- 239000003094 microcapsule Substances 0.000 claims abstract description 27
- 241000196324 Embryophyta Species 0.000 claims abstract description 24
- 238000002360 preparation method Methods 0.000 claims abstract description 22
- 244000223014 Syzygium aromaticum Species 0.000 claims abstract 2
- 235000016639 Syzygium aromaticum Nutrition 0.000 claims abstract 2
- 238000002156 mixing Methods 0.000 claims description 54
- 238000002791 soaking Methods 0.000 claims description 37
- 238000004821 distillation Methods 0.000 claims description 34
- 239000000463 material Substances 0.000 claims description 29
- 239000000203 mixture Substances 0.000 claims description 29
- 238000003756 stirring Methods 0.000 claims description 29
- 238000001914 filtration Methods 0.000 claims description 27
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 25
- 235000019476 oil-water mixture Nutrition 0.000 claims description 22
- 239000007788 liquid Substances 0.000 claims description 20
- 241000402754 Erythranthe moschata Species 0.000 claims description 19
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- 239000000706 filtrate Substances 0.000 claims description 15
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- 238000010992 reflux Methods 0.000 claims description 9
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- 235000014113 dietary fatty acids Nutrition 0.000 claims description 8
- 239000000194 fatty acid Substances 0.000 claims description 8
- 229930195729 fatty acid Natural products 0.000 claims description 8
- 108010064470 polyaspartate Proteins 0.000 claims description 8
- -1 sorbitan fatty acid ester Chemical class 0.000 claims description 8
- 241000195649 Chlorella <Chlorellales> Species 0.000 claims description 7
- 235000019733 Fish meal Nutrition 0.000 claims description 7
- 239000004467 fishmeal Substances 0.000 claims description 7
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- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 5
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- 241000607598 Vibrio Species 0.000 claims description 5
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- 239000011521 glass Substances 0.000 claims description 5
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- 235000013372 meat Nutrition 0.000 claims description 4
- 150000003839 salts Chemical class 0.000 claims description 4
- 235000008422 Schisandra chinensis Nutrition 0.000 claims description 3
- 241000219094 Vitaceae Species 0.000 claims description 3
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- 241000361919 Metaphire sieboldi Species 0.000 claims description 2
- 235000013312 flour Nutrition 0.000 claims description 2
- 238000004898 kneading Methods 0.000 claims description 2
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- 241000270959 Pelophylax nigromaculatus Species 0.000 claims 1
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- 235000009754 Vitis X bourquina Nutrition 0.000 description 6
- 235000012333 Vitis X labruscana Nutrition 0.000 description 6
- 235000014787 Vitis vinifera Nutrition 0.000 description 6
- 241000243686 Eisenia fetida Species 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 244000151018 Maranta arundinacea Species 0.000 description 4
- 235000010804 Maranta arundinacea Nutrition 0.000 description 4
- 241001336827 Rana chensinensis Species 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
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Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01K—ANIMAL HUSBANDRY; AVICULTURE; APICULTURE; PISCICULTURE; FISHING; REARING OR BREEDING ANIMALS, NOT OTHERWISE PROVIDED FOR; NEW BREEDS OF ANIMALS
- A01K97/00—Accessories for angling
- A01K97/04—Containers for bait; Preparation of bait
- A01K97/045—Preparation of bait; Ingredients
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Environmental Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Biodiversity & Conservation Biology (AREA)
- Animal Husbandry (AREA)
- General Chemical & Material Sciences (AREA)
- Fodder In General (AREA)
- Feed For Specific Animals (AREA)
Abstract
The invention provides fish bait essential oil which comprises the following raw materials, by weight, 500 parts of clove bud 300-; when the essential oil is extracted by the traditional method, the extraction rate of the essential oil is low, the purity is difficult to control, and the essential oil is always subject to fouling, and in the extraction and preparation process, the breaking of plant raw material cell walls can be rapidly promoted by using the essential oil accelerant, so that the oil yield and the purity of the essential oil are improved; the aquatic plant extract which is suitable for the hobby of fish shoal is added during the extraction of the essential oil, so that the essential oil has sufficient fragrance and can attract the fish shoal when in use; in addition, when the bait is powdery bait, the introduction of the environment-friendly microcapsule component increases the cohesive force among the powder, so that the bait can be agglomerated for a long time, and the embarrassing situation that the bait is frequently changed due to the dispersion of the bait in water is avoided.
Description
Technical Field
The invention belongs to the technical field of essential oil application, and particularly relates to bait essential oil and a using method thereof.
Background
The essential oil is extracted from leaves, flowers, seeds, fruits, roots, barks, resins, hearts and other parts of plants by steam distillation, cold pressing, fat absorption and solvent extraction, and has high-concentration fragrance and volatility. Besides essential oil extracted from a certain part of the plant, essential oil can be extracted from a plurality of parts of the plant, for example, bitter orange can extract essential oil from 3 parts of buds, leaves and fruits, the price of the essential oil is high, the main reason is low extraction rate, the purity is difficult to control, and the problem about extracting 1kg of essential oil is that a large amount of plant raw materials are required, which is always solved by the market.
Bait, i.e. food eaten by fish. The bait is food for attracting fishes to hook during fishing, and is further all usable substances capable of gathering fishes or attracting fishes to hook during fishing. Is also the same thing that is essential. Common baits such as earthworms, rice balls and the like do not have special fragrance which accords with the preference of fish groups, the action is not obvious in the actual fishing process of gathering fish, and powder baits which are commonly sold in the market at present are generally polymerized and hooked on a fishhook by water or other liquid.
Therefore, in order to solve the problems, the invention provides the fish bait essential oil which has rich fragrance and very accords with the preference of fish schools, when the fish bait essential oil is mixed with powdered fish bait for use, the fish bait is hooked on a fish hook for a long time when the special viscosity of the essential oil can be effective, the fish bait is not easy to disperse and fall off, the using effect is good, and the fish bait essential oil is proved to be popular among a plurality of fishing enthusiasts through tests.
Disclosure of Invention
The invention aims to: the fish bait essential oil prepared by matching various functional components with the raw materials is fragrant when used, and is popular with fish schools when mixed with bait;
the second object of the present invention is to: provides a method for using the bait essential oil, the bait prepared by scientific raw material and auxiliary material proportion is suitable for a plurality of fish schools.
The invention is realized by the following technical scheme: the fish bait essential oil comprises the following raw materials, by weight, 300 parts of clove buds, 450 parts of musk, 650 parts of musk, 100 parts of aquatic plant extracts, 20-60 parts of environment-friendly microcapsule components and 3-7 parts of an essential oil accelerant; the specific process comprises the following steps:
(1) cleaning and mixing clove buds and musk with clean water, and mixing the cleaned and mixed materials with water at the temperature of 50-70 ℃ according to a mass ratio of 1: 5-12, soaking for 12-18h, heating to 85-100 deg.C, adding essential oil promoter, and soaking for 18-36 h; filtering to obtain a soaking solution A and filter residues; mixing the aquatic plant extract with the soaking solution A, and stirring for 1-3h at 300-700r/min to obtain a soaking solution B;
(2) transferring the filter residue into a distillation tank, flatly paving the filter residue on a middle sieve plate, placing the impregnation liquid B at the bottom of the distillation tank, heating the bottom of the distillation tank, and adopting a steam distillation mode, wherein the flow rate of steam is 20-30 m/s; collecting vapor liquid from the upper end of the distillation retort through a condenser, wherein the vapor liquid is an oil-water mixture primary material 1, and filter residues of the distillation retort are reserved for later use;
(3) mixing the distilled filter residue with water at the temperature of 60-70 ℃ according to the proportion of 1: 1-3, placing the mixture in a sealed glass tank, stirring uniformly, standing for 24-48h, transferring the mixture to a distillation tank again, distilling the mixture in water, and collecting distillate to obtain an oil-water mixture primary material 2;
(4) mixing the oil-water mixture primary material 1 and the oil-water mixture primary material 2, and separating by an oil-water separation membrane to obtain crude oil and water; extracting the crude oil by a supercritical carbon dioxide extraction device, filtering to remove impurities to obtain essential oil, mixing the environment-friendly microcapsule components in parts by weight with the essential oil, stirring at the rotating speed of 1000-2000r/min for 1-2h to obtain the bait essential oil, and subpackaging, sealing and storing.
The preparation method of the aquatic plant extract comprises the steps of cleaning and draining the aquatic plants, adding 3-5 times of 10% potassium hydroxide solution by mass concentration, adding 0.02-0.1 time of N-acetylmuramic polysaccharide hydrolase by weight of the aquatic plants, uniformly stirring, standing for 3-5h, heating, refluxing and extracting for 3 times, 1-2h each time, and decompressing, concentrating and drying to obtain a powdery aquatic plant extract;
the aquatic plants are mixed according to the mass ratio of 1: 1: 1: 1, mixture of Maranta arundinacea, Rana chensinensis, Hibiscus mutabilis and folium Phyllostachydis Henonis;
the raw materials of the environment-friendly microcapsule component and the preparation method are that the raw materials comprise 8 to 12 portions of seafood shell grinding powder, 5 to 9 portions of fish meal, 10 to 16 portions of water, 2 to 6 portions of chlorella and 1 to 3 portions of microbial flora by weight; mixing the raw materials uniformly according to a ratio, stirring and dispersing at a rotating speed of 500r/min for 3-5h under the condition of solar light irradiation, transferring to a concentration tank, concentrating until the water content is less than 5%, and drying and grinding to particles within 200um to obtain the nano-particles; wherein the microbial flora comprises alcaligenes, bacillus, vibrio desulfurizate, rhizobium and azotobacter chroococcum according to the mass ratio of 1: 1.5-2.5: 0.5-1: 1-2: 1.5-3.
The seafood shell grinding powder is prepared from the following components in percentage by mass of 1: 2: 2: 1: 3, the mixture of the waste abalone shell, the scallop shell, the conch shell, the flower shell and the green crab shell is ground to prepare the abalone shell, and the particle size of the abalone shell, the scallop shell, the flower shell and the green crab shell is less than 100 um.
The essential oil promoter is prepared as follows: the mass ratio of the components is 10-15: 5-8: 1-3 of polyaspartic acid salt, sorbitan fatty acid ester and compound natural organic acid extract, and the particle size is less than 50 um.
The preparation method of the compound natural organic acid extract comprises the following steps: taking 10-15 parts of tamarind, 2-7 parts of schisandra chinensis, 3-6 parts of dark plum and 3-7 parts of grapes as raw materials, and carrying out the following steps:
(1) crushing tamarind and Chinese magnoliavine fruit into coarse powder, soaking the coarse powder in 5-8 times of hydrogen peroxide solution with the mass fraction of 0.1-0.3% by weight for 6-10h, filtering, washing filter residues with clear water for 3-5 times, adding 800 parts by weight of 10-15% ethanol solution for soaking for 15-20h, and filtering to obtain filtrate a;
(2) crushing mume fructus and fructus Vitis Viniferae with juicer, adding 10-15% ethanol solution 3-5 times of the total weight of mume fructus and fructus Vitis Viniferae, soaking at 30-40 deg.C for 1-3 hr, adding filtrate a, mixing, filtering to obtain filtrate b, condensing and refluxing until no alcohol smell exists, concentrating, and drying.
The invention also provides a use method of the fish bait essential oil, which comprises the following steps:
the method comprises the following steps: when the bait is earthworm, screwed meat, fresh meat or insect, the bait essential oil is sprayed on the surface of the bait in a spraying mode, wherein the spraying amount of the bait essential oil is 0.2-0.4ml, and the bait is immediately fished in water after being sprayed.
The method 2 comprises the following steps: when the bait is powdery bait and is used for nesting and gathering fishes, the fish bait essential oil and water are mixed according to the proportion of 1: after 100 volume ratio, spraying the bait essential oil on the bait in a spraying way, wherein the spraying amount is 0.1L/kg, then immediately spraying the bait essential oil into water, and fishing can be started after 20 min;
the method 3 comprises the following steps: the bait is powdered bait for fishing, and the fish bait essential oil and water are mixed according to the proportion of 1: mixing 100 parts by volume, and mixing with bait according to the volume mass ratio of 0.4-0.6L: stirring 1kg of the mixture evenly, kneading the mixture into a dough shape, attaching a round hook with the diameter of 0.5cm to a fishhook, and fishing in water;
the powdered bait comprises flour, milk powder, plant powder, insect dry powder and chemically synthesized bait powder.
The invention has the advantages that:
(1) when the essential oil is extracted by the traditional method, the extraction rate of the essential oil is low, the purity is difficult to control, and the essential oil is always subject to scaling, and in the extraction and preparation process, the essential oil accelerant is used, so that the breakage of plant raw material cell walls can be quickly promoted, and the oil yield of the essential oil is improved;
(2) the aquatic plant extract which is suitable for the hobby of the fish school is added during the extraction of the essential oil, so that the essential oil has sufficient fragrance and can attract the fish school better when being used;
(3) when the bait is powdery bait, the introduction of the environment-friendly microcapsule component increases the cohesive force among the powder, so that the bait can be agglomerated for a long time, and the embarrassing situation that the bait is frequently changed due to the dispersion of the bait in water is avoided.
In order to make the bait essential oil and the using method thereof more clear, the invention is further described with reference to the specific embodiments.
DETAILED DESCRIPTION OF EMBODIMENT (S) OF INVENTION
Example 1
An essential oil for fish bait comprises raw materials of 400 parts by weight of clove buds, 550 parts by weight of musk, 150 parts by weight of aquatic plant extract, 40 parts by weight of environment-friendly microcapsule component and 5 parts by weight of essential oil accelerant; the specific process comprises the following steps:
(1) cleaning and mixing clove buds and musk with clean water, and mixing the cleaned and mixed materials with water at the temperature of 60 ℃ according to a mass ratio of 1: 9, mixing and soaking for 15 hours, heating to 95 ℃, adding an essential oil accelerant, and continuing to soak for 27 hours; filtering to obtain a soaking solution A and filter residues; mixing the aquatic plant extract with the soaking solution A, and stirring at 500r/min for 1-3h to obtain soaking solution B;
(2) transferring the filter residue into a distillation tank, flatly paving the filter residue on a middle sieve plate, placing the impregnation liquid B at the bottom of the distillation tank, heating the bottom of the distillation tank, and adopting a steam distillation mode, wherein the flow rate of steam is 25 m/s; collecting vapor liquid from the upper end of the distillation retort through a condenser, wherein the vapor liquid is an oil-water mixture primary material 1, and filter residues of the distillation retort are reserved for later use;
(3) mixing the distilled filter residue with 65 ℃ water according to the proportion of 1: 2, placing the mixture in a closed glass tank, stirring uniformly, standing for 36 hours, transferring the mixture to a distillation tank again, distilling the mixture in water, and collecting distillate to obtain an oil-water mixture primary material 2;
(4) mixing the oil-water mixture primary material 1 and the oil-water mixture primary material 2, and separating by an oil-water separation membrane to obtain crude oil and water; extracting the crude oil by a supercritical carbon dioxide extraction device, filtering to remove impurities to obtain essential oil, mixing the environment-friendly microcapsule components in parts by weight with the essential oil, stirring at a rotating speed of 1500r/min for 1.5h to obtain fish bait essential oil, subpackaging, sealing and storing.
The preparation method of the aquatic plant extract comprises the steps of cleaning and draining the aquatic plants, adding 4 times of 10% potassium hydroxide solution by weight and 0.06 times of N-acetylmuramic polysaccharide hydrolase by weight of the aquatic plants, uniformly stirring, standing for 4 hours, heating, refluxing and extracting for 3 times, 1.5 hours each time, concentrating and drying to obtain a powdery aquatic plant extract;
the aquatic plants are mixed according to the mass ratio of 1: 1: 1: 1, mixture of Maranta arundinacea, Rana chensinensis, Hibiscus mutabilis and folium Phyllostachydis Henonis;
the raw materials of the environment-friendly microcapsule component and the preparation method are that the raw materials comprise 10 parts of seafood shell grinding powder, 7 parts of fish meal, 13 parts of water, 4 parts of chlorella and 2 parts of microbial flora by weight; mixing the above raw materials uniformly according to a ratio, stirring and dispersing at a rotation speed of 400r/min for 4h under the condition of sunlight irradiation, transferring to a concentration tank, concentrating until the water content is less than 5%, and drying and grinding to obtain particles within 200 um; wherein the microbial flora comprises alcaligenes, bacillus, vibrio desulfurizate, rhizobium and azotobacter chroococcum according to the mass ratio of 1: 2: 0.8: 1.5: 2, and mixing the components in a ratio of 2.
The seafood shell grinding powder is prepared from the following components in percentage by mass of 1: 2: 2: 1: 3, the mixture of the waste abalone shell, the scallop shell, the conch shell, the flower shell and the green crab shell is ground to prepare the abalone shell, and the particle size of the abalone shell, the scallop shell, the flower shell and the green crab shell is less than 100 um.
The essential oil promoter is prepared as follows: the mass ratio of the components is 13: 7: 2, polyaspartate, sorbitan fatty acid ester and compound natural organic acid extract as raw materials, and the particle size of the product is less than 50 um.
The preparation method of the compound natural organic acid extract comprises the following steps: taking 13 parts of tamarind, 5 parts of Chinese magnoliavine fruit, 5 parts of dark plum fruit and 5 parts of grape as raw materials, and carrying out the following steps:
(1) crushing tamarind and Chinese magnoliavine fruit into coarse powder, soaking the coarse powder in hydrogen peroxide solution with the mass fraction of 0.2 percent, which is 6 times of the total weight of the coarse powder for 8 hours, filtering, washing filter residues for 4 times by using clear water, adding 650 parts by weight of ethanol solution with the volume fraction of 13 percent, soaking for 18 hours, and filtering to obtain filtrate a;
(2) crushing the dark plum and the grape by using a juicer, adding an ethanol solution with the volume fraction of 13 percent, the volume fraction of which is 4 times of the total weight of the dark plum and the grape, soaking for 2 hours at 35 ℃, adding the filtrate a, uniformly mixing, filtering to obtain a filtrate b, condensing and refluxing until no alcohol smell exists, and concentrating and drying.
Example 2
An essential oil for fish bait comprises, by weight, 300 parts of clove buds, 450 parts of musk, 100 parts of aquatic plant extract, 60 parts of environment-friendly microcapsule component and 7 parts of essential oil accelerator; the specific process comprises the following steps:
(1) cleaning and mixing clove buds and musk with clean water, and mixing the cleaned and mixed materials with water at 50 ℃ according to a mass ratio of 1: 5 for 18 hours, heating to 100 ℃, adding an essential oil accelerant, and continuing to soak for 36 hours; filtering to obtain a soaking solution A and filter residues; mixing the aquatic plant extract with the soaking solution A, and stirring for 1h at 700r/min to obtain soaking solution B;
(2) transferring the filter residue into a distillation tank, flatly paving the filter residue on a middle sieve plate, placing the impregnation liquid B at the bottom of the distillation tank, heating the bottom of the distillation tank, and adopting a steam distillation mode, wherein the flow rate of steam is 20 m/s; collecting vapor liquid from the upper end of the distillation retort through a condenser, wherein the vapor liquid is an oil-water mixture primary material 1, and filter residues of the distillation retort are reserved for later use;
(3) mixing the distilled filter residue with water at 60 ℃ according to the weight ratio of 1: 1, placing the mixture in a closed glass tank, stirring uniformly, standing for 24 hours, transferring the mixture to a distillation tank again, distilling the mixture in water, and collecting distillate to obtain an oil-water mixture primary material 2;
(4) mixing the oil-water mixture primary material 1 and the oil-water mixture primary material 2, and separating by an oil-water separation membrane to obtain crude oil and water; extracting the crude oil with supercritical carbon dioxide extraction device, filtering to remove impurities to obtain essential oil, mixing the above environmentally-friendly microcapsule components with the essential oil, stirring at 2000r/min for 2 hr to obtain fish bait essential oil, packaging, and sealing.
The preparation method of the aquatic plant extract comprises the steps of cleaning and draining the aquatic plants, adding a 10% potassium hydroxide solution with the mass concentration being 3 times of the weight of the aquatic plants, adding N-acetylmuramic polysaccharide hydrolase with the weight being 0.02 time of the weight of the aquatic plants, uniformly stirring, standing for 3 hours, heating and refluxing for extraction for 3 times, 1 hour each time, decompressing, concentrating and drying to obtain a powdery aquatic plant extract;
the aquatic plants are mixed according to the mass ratio of 1: 1: 1: 1, mixture of Maranta arundinacea, Rana chensinensis, Hibiscus mutabilis and folium Phyllostachydis Henonis;
the raw materials of the environment-friendly microcapsule component and the preparation method are that the raw materials comprise 8 parts of seafood shell grinding powder, 5 parts of fish meal, 10 parts of water, 6 parts of chlorella and 3 parts of microbial flora by weight; mixing the above raw materials uniformly according to a ratio, stirring and dispersing at a rotation speed of 500r/min for 3h under the condition of sunlight irradiation, transferring to a concentration tank, concentrating until the water content is less than 5%, and drying and grinding to obtain particles within 200 um; wherein the microbial flora comprises alcaligenes, bacillus, vibrio desulfurizate, rhizobium and azotobacter chroococcum according to the mass ratio of 1: 1.5: 0.5: 1: 1.5 in proportion.
The seafood shell grinding powder is prepared from the following components in percentage by mass of 1: 2: 2: 1: 3, the mixture of the waste abalone shell, the scallop shell, the conch shell, the flower shell and the green crab shell is ground to prepare the abalone shell, and the particle size of the abalone shell, the scallop shell, the flower shell and the green crab shell is less than 100 um.
The essential oil promoter is prepared as follows: the mass ratio of the components is 10: 5: 1, polyaspartate, sorbitan fatty acid ester and compound natural organic acid extract as raw materials, and the particle size of the product is less than 50 um.
The preparation method of the compound natural organic acid extract comprises the following steps: taking 10 parts of tamarind, 2 parts of Chinese magnoliavine fruit, 6 parts of dark plum fruit and 7 parts of grape as raw materials, and carrying out the following steps:
(1) crushing tamarind and Chinese magnoliavine fruit into coarse powder, soaking the coarse powder in a hydrogen peroxide solution with the mass fraction of 0.1 percent, which is 5 times of the total weight of the coarse powder for 6 hours, filtering, washing filter residues with clear water for 3 times, adding 500 parts by weight of an ethanol solution with the volume fraction of 10 percent, soaking the filter residues for 15 hours, and filtering to obtain a filtrate a;
(2) crushing the dark plum and the grape by using a juicer, adding an ethanol solution with the volume fraction of 10 percent, the volume fraction of which is 3 times of the total weight of the dark plum and the grape, soaking for 1 hour at 30 ℃, adding the filtrate a, uniformly mixing, filtering to obtain a filtrate b, condensing and refluxing until no alcohol smell exists, and concentrating and drying.
Example 3
An essential oil for fish bait comprises raw materials of 500 parts by weight of clove buds, 650 parts by weight of musk, 200 parts by weight of aquatic plant extract, 20 parts by weight of environment-friendly microcapsule component and 3 parts by weight of essential oil accelerant; the specific process comprises the following steps:
(1) cleaning and mixing clove buds and musk with clean water, and mixing the cleaned and mixed materials with water at 70 ℃ according to a mass ratio of 1: 12 for 12 hours, heating to 85 ℃, adding an essential oil accelerant, and continuing to soak for 18 hours; filtering to obtain a soaking solution A and filter residues; mixing the aquatic plant extract with the soaking solution A, and stirring for 3h at 300r/min to obtain soaking solution B;
(2) transferring the filter residue into a distillation tank, flatly paving the filter residue on a middle sieve plate, placing the impregnation liquid B at the bottom of the distillation tank, heating the bottom of the distillation tank, and adopting a steam distillation mode, wherein the flow rate of steam is 30 m/s; collecting vapor liquid from the upper end of the distillation retort through a condenser, wherein the vapor liquid is an oil-water mixture primary material 1, and filter residues of the distillation retort are reserved for later use;
(3) mixing the distilled filter residue with 70 ℃ water according to the proportion of 1: 3, mixing the materials in a sealed glass tank, stirring uniformly, standing for 48 hours, transferring the mixture to a distillation tank again, distilling the mixture in water, and collecting distillate to obtain an oil-water mixture primary material 2;
(4) mixing the oil-water mixture primary material 1 and the oil-water mixture primary material 2, and separating by an oil-water separation membrane to obtain crude oil and water; extracting the crude oil by a supercritical carbon dioxide extraction device, filtering to remove impurities to obtain essential oil, mixing the environment-friendly microcapsule components in parts by weight with the essential oil, stirring at the rotating speed of 1000r/min for 1h to obtain fish bait essential oil, and subpackaging, sealing and storing.
The preparation method of the aquatic plant extract comprises the steps of cleaning and draining the aquatic plants, adding 5 times of 10% potassium hydroxide solution by weight and 0.1 time of N-acetylmuramic polysaccharide hydrolase by weight of the aquatic plants, uniformly stirring, standing for 5 hours, heating and reflux-extracting for 3 times, 2 hours each time, decompressing, concentrating and drying to obtain a powdery aquatic plant extract;
the aquatic plants are mixed according to the mass ratio of 1: 1: 1: 1, mixture of Maranta arundinacea, Rana chensinensis, Hibiscus mutabilis and folium Phyllostachydis Henonis;
the raw materials of the environment-friendly microcapsule component and the preparation method are that the raw materials comprise 12 parts of seafood shell grinding powder, 9 parts of fish meal, 16 parts of water, 2 parts of chlorella and 1 part of microbial flora by weight; mixing the above raw materials uniformly according to a ratio, stirring and dispersing at a rotation speed of 300r/min for 5h under the condition of solar irradiation, transferring to a concentration tank, concentrating until the water content is less than 5%, and drying and grinding to obtain particles within 200 um; wherein the microbial flora comprises alcaligenes, bacillus, vibrio desulfurizate, rhizobium and azotobacter chroococcum according to the mass ratio of 1: 2.5: 1: 2: 3, and mixing the components in a ratio of 3.
The seafood shell grinding powder is prepared from the following components in percentage by mass of 1: 2: 2: 1: 3, the mixture of the waste abalone shell, the scallop shell, the conch shell, the flower shell and the green crab shell is ground to prepare the abalone shell, and the particle size of the abalone shell, the scallop shell, the flower shell and the green crab shell is less than 100 um.
The essential oil promoter is prepared as follows: the mass ratio of the components is 15: 8: 3, polyaspartic acid salt, sorbitan fatty acid ester and compound natural organic acid extract are used as raw materials and are mixed and ground to prepare the product, and the particle size of the product is less than 50 um.
The preparation method of the compound natural organic acid extract comprises the following steps: taking 15 parts of tamarind, 7 parts of schisandra chinensis, 3 parts of dark plum and 3 parts of grapes as raw materials, and carrying out the following steps:
(1) crushing tamarind and Chinese magnoliavine fruit into coarse powder, soaking the coarse powder in hydrogen peroxide solution with the mass fraction of 0.3 percent, which is 8 times of the total weight of the coarse powder for 10 hours, filtering, washing filter residues for 5 times by using clear water, adding 800 parts by weight of ethanol solution with the volume fraction of 15 percent, soaking for 15-20 hours, and filtering to obtain filtrate a;
(2) crushing mume fructus and fructus Vitis Viniferae with juicer, adding 15% ethanol solution 3-5 times of the total weight, soaking at 40 deg.C for 3 hr, adding filtrate a, mixing, filtering to obtain filtrate b, condensing and refluxing until no alcohol smell exists, concentrating and drying.
Example 4
An essential oil for fish bait comprises raw materials of 400 parts by weight of clove buds, 550 parts by weight of musk, 99 parts by weight of aquatic plant extract, 40 parts by weight of environment-friendly microcapsule component and 5 parts by weight of essential oil accelerant;
the rest is the same as example 1.
Example 5
An essential oil for fish bait comprises, by weight, 400 parts of clove buds, 550 parts of musk, 201 parts of aquatic plant extract, 40 parts of environment-friendly microcapsule component and 5 parts of essential oil accelerant;
the rest is the same as example 1.
Example 6
An essential oil for fish bait comprises raw materials of 400 parts by weight of clove buds, 550 parts by weight of musk, 150 parts by weight of aquatic plant extract, 39 parts by weight of environment-friendly microcapsule component and 5 parts by weight of essential oil accelerant;
the rest is the same as example 1.
Example 7
An essential oil for fish bait comprises raw materials of 400 parts by weight of clove buds, 550 parts by weight of musk, 150 parts by weight of aquatic plant extract, 61 parts by weight of environment-friendly microcapsule component and 5 parts by weight of essential oil accelerant;
the rest is the same as example 1.
Example 8
An essential oil of fish bait, wherein the raw materials of the environmentally friendly microcapsule component and the preparation method are that the raw materials comprise 7 portions of ground seafood shell powder, 4 portions of fish meal, 13 portions of water, 1 portion of chlorella and 2 portions of microbial flora by weight;
the rest is the same as example 1.
Example 9
The fish bait essential oil comprises 13 parts of seafood shell grinding powder, 10 parts of fish meal, 13 parts of water, 1 part of chlorella and 2 parts of microbial flora;
the rest is the same as example 1.
Example 10
An essential oil for fish bait comprises raw materials of 400 parts by weight of clove buds, 550 parts by weight of musk, 150 parts by weight of aquatic plant extract, 40 parts by weight of environment-friendly microcapsule component and 2 parts by weight of essential oil accelerant;
the rest is the same as example 1.
Example 11
An essential oil for fish bait comprises raw materials of 400 parts by weight of clove buds, 550 parts by weight of musk, 150 parts by weight of aquatic plant extract, 40 parts by weight of environment-friendly microcapsule component and 8 parts by weight of essential oil accelerant;
the rest is the same as example 1.
Example 12
The fish bait essential oil comprises an essential oil accelerator, a compound of a formula I, a compound of a formula II, a compound of a: 6, the polyaspartate and the sorbitan fatty acid ester are used as raw materials and are mixed and ground to prepare the water-soluble organic acid modified polyaspartate and the sorbitan fatty acid ester, and the raw materials are not added with a compound natural organic acid extract.
The rest is the same as example 1.
Example 13
The fish bait essential oil comprises an essential oil accelerator, a compound of a formula I, a compound of a formula II, a compound of a: 6: 4 polyaspartic acid salt, sorbitan fatty acid ester and composite natural organic acid extract as raw materials are mixed and ground to prepare the dispersing agent.
The rest is the same as example 1.
Example 14
A fish bait essential oil is prepared by the following specific preparation process:
(1) cleaning clove buds and musk with clean water, mixing the cleaned clove buds and the musk with the aquatic plant extract, and then mixing the mixture with water at the temperature of 60 ℃ according to a mass ratio of 1: 9, mixing and soaking for 15 hours, heating to 95 ℃, adding an essential oil accelerant, and continuing to soak for 27 hours; filtering to obtain a soaking solution and filter residues; (ii) a
(2) Transferring the filter residue into a distillation tank, flatly paving the filter residue on a middle sieve plate, placing the immersion liquid at the bottom of the distillation tank, heating the bottom of the distillation tank, and adopting a steam distillation mode, wherein the flow rate of steam is 25 m/s; collecting vapor liquid from the upper end of the distillation retort through a condenser, wherein the vapor liquid is an oil-water mixture primary material;
(3) separating the primary material of the oil-water mixture by an oil-water separation membrane to obtain crude oil and water; extracting the crude oil by a supercritical carbon dioxide extraction device, filtering to remove impurities to obtain essential oil, mixing the environment-friendly microcapsule component, the essential oil accelerant and the essential oil in parts by weight, stirring at the rotating speed of 1500r/min for 1.5h to obtain fish bait essential oil, subpackaging, sealing and storing.
The rest is the same as example 1.
Example 15
Taking 1 part of each of the fish bait essential oil prepared by the methods of example 1 and examples 4 and 5, selecting 4 parts of market-sold red worm powder, wherein one part is a blank group, and mixing the fish bait essential oil and water according to a ratio of 1: 100, spraying the bait essential oil on the red worm powder in a spraying mode, uniformly stirring, immediately spraying the mixture into water, controlling the bait spraying area of each batch of samples within a range of 1 square meter, and observing the fish gathering condition through underwater photography after 20 min.
Test of
Test 1
Comparative examples methods 1-3 and examples methods 10-14 the extraction rates and purities of the bait essential oils prepared are summarized in table 1 below:
TABLE 1 essential oil extraction conditions TABLE
Test 2
1 part of each bait essential oil prepared by the following method in the embodiment is selected, 9 parts of market-sold red worm powder are selected, and the bait essential oil and water are mixed according to the proportion of 1: mixing the powder with the red worm powder according to the volume mass ratio of 0.5L: 1kg of the raw materials are uniformly stirred and kneaded into a dough, a round hook with the diameter of 0.5cm is attached to a fishhook, the round bait is tested in water and the dispersion condition of the round bait in water is recorded in the following table 2, wherein one part of the round hook is a blank group, and the water of the blank group replaces the mixed liquid of the fish bait essential oil and the water:
TABLE 2 bait dispersion situation table
From the comparison of the above experimental contents, it can be known that:
(1) the fish bait essential oil prepared by the methods in the embodiments has better using effect in the embodiments 1, 2 and 3, and is especially best in the embodiment 1;
(2) from table 1, comparative example 1, the addition amount of the essential oil accelerator or the compounding ratio of the raw materials for preparation of examples 10 to 13 are out of the technical range of the present invention, the preparation process of example 14 is out of the technical range of the present invention, and the extraction rate and purity of the essential oil are greatly reduced;
(3) as can be seen from the data in table 2, the addition amount or the preparation raw material ratio of the environmentally friendly microcapsule components in comparative example 1 and examples 6 to 9 is out of the technical range of the present invention, and the viscosity of the finished product fish bait essential oil is correspondingly affected, such as the environmentally friendly microcapsule component in example 6 has less addition amount and low viscosity, which causes the bait to be easily dispersed and fall off in water;
(4) as can be seen from Table 2, when comparing the blank group with other examples, the effect of using the single powder of red worms is obviously inferior to that of other examples.
Claims (8)
1. A bait essential oil is characterized in that: the raw materials comprise, by weight, 300-500 parts of clove bud, 450-650 parts of musk, 100-200 parts of aquatic plant extract, 20-60 parts of environment-friendly microcapsule component and 3-7 parts of essential oil accelerant; the specific process comprises the following steps:
(1) cleaning and mixing clove buds and musk with clean water, and mixing the cleaned and mixed materials with water at the temperature of 50-70 ℃ according to a mass ratio of 1: 5-12, soaking for 12-18h, heating to 85-100 deg.C, adding essential oil promoter, and soaking at constant temperature for 18-36 h; filtering to obtain a soaking solution A and filter residues; mixing the aquatic plant extract with the soaking solution A, and stirring for 1-3h at 300-700r/min to obtain a soaking solution B;
(2) transferring the filter residue into a distillation tank, flatly paving the filter residue on a middle sieve plate, placing the impregnation liquid B at the bottom of the distillation tank, heating the bottom of the distillation tank, and adopting a steam distillation mode, wherein the flow rate of steam is 20-30 m/s; collecting vapor liquid from the upper end of the distillation retort through a condenser, wherein the vapor liquid is an oil-water mixture primary material 1, and filter residues of the distillation retort are reserved for later use;
(3) mixing the distilled filter residue with water at the temperature of 60-70 ℃ according to the proportion of 1: 1-3, placing the mixture in a sealed glass tank, stirring uniformly, standing for 24-48h, transferring the mixture to a distillation tank again, distilling the mixture in water, and collecting distillate to obtain an oil-water mixture primary material 2;
(4) mixing the oil-water mixture primary material 1 and the oil-water mixture primary material 2, and separating by an oil-water separation membrane to obtain crude oil and water; extracting the crude oil by a supercritical carbon dioxide extraction device, filtering to remove impurities to obtain essential oil, mixing the environment-friendly microcapsule components in parts by weight with the essential oil, stirring at the rotating speed of 1000-2000r/min for 1-2h to obtain the bait essential oil, and subpackaging, sealing and storing.
2. The bait essential oil as claimed in claim 1, wherein: the preparation method of the aquatic plant extract comprises the steps of cleaning and draining the aquatic plants, adding 3-5 times of 10% potassium hydroxide solution by mass concentration, adding 0.02-0.1 time of N-acetylmuramic polysaccharide hydrolase by weight of the aquatic plants, uniformly stirring, standing for 3-5h, heating, refluxing and extracting for 3 times, 1-2h each time, and decompressing, concentrating and drying to obtain a powdery aquatic plant extract; the aquatic plants are mixed according to the mass ratio of 1: 1: 1: 1 mixture of Maranta, Rana Nigromaculata, Hibiscus Mutabilis, and folium Bambusae.
3. The bait essential oil as claimed in claim 1, wherein: the raw materials of the environment-friendly microcapsule component and the preparation method are that the raw materials comprise 8 to 12 portions of seafood shell grinding powder, 5 to 9 portions of fish meal, 10 to 16 portions of water, 2 to 6 portions of chlorella and 1 to 3 portions of microbial flora by weight; mixing the raw materials uniformly according to a ratio, stirring and dispersing at a rotating speed of 500r/min for 3-5h under the condition of solar light irradiation, transferring to a concentration tank, concentrating until the water content is less than 5%, and drying and grinding to particles within 200um to obtain the nano-particles; wherein the microbial flora comprises alcaligenes, bacillus, vibrio desulfurizate, rhizobium and azotobacter chroococcum according to the mass ratio of 1: 1.5-2.5: 0.5-1: 1-2: 1.5-3.
4. The bait essential oil as claimed in claim 3, wherein: the seafood shell grinding powder is prepared from the following components in percentage by mass of 1: 2: 2: 1: 3, grinding the mixture of the waste abalone shells, scallop shells, conch shells, flower carapace and green crab shells, wherein the particle size of the mixture is less than 100 um.
5. The bait essential oil as claimed in claim 1, wherein: the essential oil promoter is prepared as follows: the mass ratio of the components is 10-15: 5-8: 1-3 of polyaspartic acid salt, sorbitan fatty acid ester and compound natural organic acid extract, and the particle size is less than 50 um.
6. The bait essential oil as claimed in claim 5, wherein: the preparation method of the compound natural organic acid extract comprises the following steps: taking 10-15 parts of tamarind, 2-7 parts of schisandra chinensis, 3-6 parts of dark plum and 3-7 parts of grapes as raw materials, and carrying out the following steps:
(1) crushing tamarind and Chinese magnoliavine fruit into coarse powder, soaking the coarse powder in 5-8 times of hydrogen peroxide solution with the mass fraction of 0.1-0.3% by weight for 6-10h, filtering, washing filter residues with clear water for 3-5 times, adding 800 parts by weight of 10-15% ethanol solution for soaking for 15-20h, and filtering to obtain filtrate a;
(2) crushing mume fructus and fructus Vitis Viniferae with juicer, adding 10-15% ethanol solution 3-5 times of the total weight of mume fructus and fructus Vitis Viniferae, soaking at 30-40 deg.C for 1-3 hr, adding filtrate a, mixing, filtering to obtain filtrate b, condensing and refluxing until no alcohol smell exists, concentrating, and drying.
7. The use method of the bait essential oil as claimed in any of claims 1 to 6, which comprises the following steps:
the method comprises the following steps: when the bait is earthworm, screwed meat, fresh meat and insect, the bait essential oil is sprayed on the surface of the bait in a spraying way, wherein the spraying amount of the bait essential oil is 0.2-0.4ml, and the bait is immediately fished in water after being sprayed;
the method 2 comprises the following steps: when the bait is powdery bait and is used for nesting and gathering fishes, the fish bait essential oil and water are mixed according to the proportion of 1: after 100 volume ratio, spraying the bait essential oil on the bait in a spraying way, wherein the spraying amount is 0.1L/kg, then immediately spraying the bait essential oil into water, and fishing can be started after 20 min;
the method 3 comprises the following steps: the bait is powdered bait for fishing, and the fish bait essential oil and water are mixed according to the proportion of 1: mixing 100 parts by volume, and mixing with bait according to the volume mass ratio of 0.4-0.6L: stirring 1kg, kneading into dough, attaching round hook with diameter of 0.5cm to fishhook, and fishing in water.
8. The bait essential oil as claimed in claim 7, wherein: the powdered bait comprises flour, milk powder, plant powder, insect dry powder and chemically synthesized bait powder.
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH03228651A (en) * | 1989-11-22 | 1991-10-09 | Shiono Koryo Kk | Feeding and attractant active substance for fisheries animal |
| US5415862A (en) * | 1991-08-06 | 1995-05-16 | Flow-Rite Of Tennessee, Inc. | Effervescent liquid fish attractant composition with audible, visual, scent and taste enhancements and method of manufacturing the fish attractant |
| US5733539A (en) * | 1995-09-01 | 1998-03-31 | Research Institute For Production Development | Bait for fishes and shellfishes |
| CN1820626A (en) * | 2006-03-15 | 2006-08-23 | 吴孝顺 | Fishing bait |
| CN108402002A (en) * | 2018-05-18 | 2018-08-17 | 吕莉 | A kind of preparation method of fish bait |
| CN112400825A (en) * | 2020-11-25 | 2021-02-26 | 界首市兴隆渔具有限公司 | Environment-friendly freshwater fish bait and preparation method thereof |
-
2021
- 2021-04-13 CN CN202110393983.XA patent/CN112931441A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH03228651A (en) * | 1989-11-22 | 1991-10-09 | Shiono Koryo Kk | Feeding and attractant active substance for fisheries animal |
| US5415862A (en) * | 1991-08-06 | 1995-05-16 | Flow-Rite Of Tennessee, Inc. | Effervescent liquid fish attractant composition with audible, visual, scent and taste enhancements and method of manufacturing the fish attractant |
| US5733539A (en) * | 1995-09-01 | 1998-03-31 | Research Institute For Production Development | Bait for fishes and shellfishes |
| CN1820626A (en) * | 2006-03-15 | 2006-08-23 | 吴孝顺 | Fishing bait |
| CN108402002A (en) * | 2018-05-18 | 2018-08-17 | 吕莉 | A kind of preparation method of fish bait |
| CN112400825A (en) * | 2020-11-25 | 2021-02-26 | 界首市兴隆渔具有限公司 | Environment-friendly freshwater fish bait and preparation method thereof |
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Application publication date: 20210611 |