CN102653701A - Method for extracting suaeda salsa seed oil - Google Patents
Method for extracting suaeda salsa seed oil Download PDFInfo
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- CN102653701A CN102653701A CN2011100492182A CN201110049218A CN102653701A CN 102653701 A CN102653701 A CN 102653701A CN 2011100492182 A CN2011100492182 A CN 2011100492182A CN 201110049218 A CN201110049218 A CN 201110049218A CN 102653701 A CN102653701 A CN 102653701A
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- suaeda salsa
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Abstract
The invention relates to a method for extracting suaeda salsa seed oil. The method specifically comprises the following steps of: baking screened suaeda salsa seeds in a baking oven at 80-100 EDG C for 6-8 hours, cracking grains by using a grinder after cooling, wrapping the grains with filter paper, adding the grains in an extraction pipe, adding solvent in a siphon of a soxhlet extractor to the two-thirds of the height of the siphon by virtue of a funnel from a mouth of a condenser pipe, conducting heating extraction in a constant temperature water bath pot at 70-80 EDG C, distilling extract after extraction for 7-10 hours, recovering an organic solvent, and separating out an oil layer for later use. The method is wide in sources of raw materials, simple in process flow, and high in extraction efficiency and is very natural.
Description
Technical field
The present invention relates to a kind of method of from the halophytes Suaeda salsa, extracting seed oil.
Background technology
Suaeda salsa (Suaeda salsa (L.) Pall) has another name called that alkali is fluffy, salt wormwood artemisia, Suaeda salsa; Be the Chenopodiaceae Suaeda, China mainly be distributed in Soviet Union, Zhejiang, Shandong, Shanxi, Ji,, Shan, Inner Mongol 7 provinces and the Northeast, aboundresources; Gather easily; For a long time, Suaeda salsa runs its course, and never causes enough attention of people.Now, along with deepening continuously of development research, Suaeda salsa is a kind of quality vegetables, cash crop and the plant resources with value medical health care.
Nutritive ingredient is complete and abundant in seed that alkali is fluffy and the cauline leaf, and lipid content accounts for 36.5% of dry-matter in its seed, is higher than soybean, and wherein unsaturated fatty acids accounts for 90%, and linolic acid accounts for 70%, and linolenic acid accounts for 6.08%.The protein contnt of fresh and tender cauline leaf accounts for 40% of dry-matter, and contains abundant VITAMINs and trace element, and calcium, phosphorus, iron and vitamin G content all were higher than vegetables such as spinach, tomato and Radix Dauci Sativae during alkali was fluffy; Vitamin C content is higher than or is equivalent to general vegetables; Wei ShengsuB2 content is 5～8 times of general vegetables; It is high about 10 times to contain the general food of Se amount.The trace element that in the fluffy juice of alkali, contains 9 kinds of needed by human, wherein calcium, magnesium, zinc, iron, nickel content enrich.What deserves to be mentioned is; Essential amino acid content is high in the protein of fluffy seed of alkali and cauline leaf; And the present known good natural food of texture ratio is all more balanced; In its protein, the complete protein index that the essential amino acid content and the World Health Organization provide is quite approaching, is superior to the composition of indispensable amino acid in tenaculat Habenaria, soybean, the egg.Suaeda salsa is one of wild plant resource that has exploitation value; Be the oil crops good, that oleaginousness is high, a large amount of datas show that common seepweed seeds oil has high healthy nutritive value; Be a kind of table oil, can be used as new oil resource fully and develop.
Summary of the invention
The Suaeda salsa seed is a raw material to originate widely in the present invention, with a kind of method of instrument stripping oil from the Suaeda salsa seed of simple and regular.
The present invention realizes through following technical scheme.
A kind of method of extracting Suaeda salsa seed oil; Be specially and screen the good fluffy seed sample of alkali and in 80-100 ℃ of baking oven, toast 6-8 hour; After cooling with the kibbler seed that breaks; And wrap with filter paper and to put into extraction tube, add solvent to Soxhlet extractor U trap height 2/3, extracting in 70-80 ℃ of thermostat water bath then by funnel from the condensation mouth of pipe.After extracting 7-10 hour, the distillation extract reclaims organic solvent, and it is subsequent use to isolate oil reservoir.It is normal hexane, sherwood oil or ether that above-mentioned digestion agent can be.
Suaeda salsa seed oil colours pool dark yellow, acid value 1.84mgKOH/g, iodine value 176.4gl2/100g, saponification value 194.6mgKOH/g that the present invention extracts.Suaeda salsa seed oil ingredient and market high-quality edible oil commonly used is (table 1) quite.
Table 1 common seepweed seeds oil and edible oil component commonly used are relatively
Description of drawings
The oily total ion current figure of Suaeda salsa seed that Fig. 1 extracts for the present invention
Embodiment:
Embodiments of the invention have embodied this patent protection domain, but this patent protection domain does not limit to following examples.
Instance one: will screen the good fluffy seed 10g of alkali and in 100 ℃ baking oven, toast 5 hours; Pulverize with kibbler after cooling and wrap powder with filter paper; In the flask of Soxhlet extractor, adding ether, to reach volumetrical approximately half the, and 6 Soxhlet extractors series connection are inserted the filter paper packet branch in 6 extraction tubes; Add ether to U trap height 2/3 by funnel from the condensation mouth of pipe, heating in thermostat water bath then (bath temperature 75～80 degree) extracting.After the extracting 8 hours, stop heating, take off extractor and change water distilling apparatus into, reclaim ether, separate oil reservoir, oil yield 20.12% (g/g).
Instance two: will screen the good fluffy seed of alkali and in 80 ℃ of baking ovens, dry, and pulverize, and cross 40 mesh sieves with micromill.Take by weighing dry powder 10g; And wrap powder with filter paper; In the flask of Soxhlet extractor, adding sherwood oil, to reach volumetrical approximately half the, and 4 Soxhlet extractors series connection are inserted the filter paper packet branch in 4 extraction tubes; Add ether to U trap height 2/3 by funnel from the condensation mouth of pipe, heating in thermostat water bath then (bath temperature 75～80 degree) extracting.After the extracting 10 hours, stop heating, take off extractor and change water distilling apparatus into, reclaim sherwood oil, separate oil reservoir, oil yield 22.51% (g/g).
Claims (8)
1. a method of extracting Suaeda salsa seed oil is characterized in that the fluffy seed of alkali screens, cleans, toasts, breaks, and with the extracting of Soxhlet extractor constant temperature, distills extract afterwards, reclaims organic solvent, isolates Suaeda salsa seed oil.
2. according to the method for claim 1, it is characterized in that: described screening method is that Suaeda salsa seed cutting is crossed the 20-40 mesh sieve, obtained the fluffy seed of purified alkali.
3. according to the method for claim 1, it is characterized in that: described Suaeda salsa seed storing temperature continues 6-8 hour at 80-100 ℃.
4. according to the method for claim 1, it is characterized in that: described Suaeda salsa seed disruptive method is to use common kibbler.
5. according to the method for claim 1, it is characterized in that: described Soxhlet extractor can singly be used, and also can 2-8 series connection use.
6. according to the method for claim 1, it is characterized in that: described organic solvent can be normal hexane, sherwood oil or ether.
7. according to the method for claim 1, it is characterized in that: 70-80 ℃ of described water bath with thermostatic control temperature.
8. according to the method for claim 1, it is characterized in that: the described extracting time is 7-10 hour.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100492182A CN102653701A (en) | 2011-03-02 | 2011-03-02 | Method for extracting suaeda salsa seed oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100492182A CN102653701A (en) | 2011-03-02 | 2011-03-02 | Method for extracting suaeda salsa seed oil |
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| CN102653701A true CN102653701A (en) | 2012-09-05 |
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| CN2011100492182A Pending CN102653701A (en) | 2011-03-02 | 2011-03-02 | Method for extracting suaeda salsa seed oil |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103271171A (en) * | 2013-06-13 | 2013-09-04 | 山东三星玉米产业科技有限公司 | Edible blending oil comprising rapeseed oil and saline land suaeda salsa seed oil and preparation method thereof |
| CN109042488A (en) * | 2018-06-12 | 2018-12-21 | 山东胜伟旅游发展有限公司 | The method of the fluffy feeding dorking of saline-alkali land |
| CN109042486A (en) * | 2018-06-12 | 2018-12-21 | 山东胜伟旅游发展有限公司 | A method of utilizing the fluffy feeding cow of saline-alkali land |
| CN109042487A (en) * | 2018-06-12 | 2018-12-21 | 山东胜伟旅游发展有限公司 | Utilize the method for the fluffy feeding mutton sheep of saline-alkali land |
| CN109090021A (en) * | 2018-06-12 | 2018-12-28 | 山东胜伟旅游发展有限公司 | The method of the fluffy feeding milch goat of saline-alkali land |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101074405A (en) * | 2007-07-13 | 2007-11-21 | 杨庆利 | Extraction of common seepweed seeds oil by supercritical CO2 fluid |
-
2011
- 2011-03-02 CN CN2011100492182A patent/CN102653701A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101074405A (en) * | 2007-07-13 | 2007-11-21 | 杨庆利 | Extraction of common seepweed seeds oil by supercritical CO2 fluid |
Non-Patent Citations (1)
| Title |
|---|
| 李洪山，等: "盐地碱蓬籽油的提取及特性", 《中国油脂》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103271171A (en) * | 2013-06-13 | 2013-09-04 | 山东三星玉米产业科技有限公司 | Edible blending oil comprising rapeseed oil and saline land suaeda salsa seed oil and preparation method thereof |
| CN109042488A (en) * | 2018-06-12 | 2018-12-21 | 山东胜伟旅游发展有限公司 | The method of the fluffy feeding dorking of saline-alkali land |
| CN109042486A (en) * | 2018-06-12 | 2018-12-21 | 山东胜伟旅游发展有限公司 | A method of utilizing the fluffy feeding cow of saline-alkali land |
| CN109042487A (en) * | 2018-06-12 | 2018-12-21 | 山东胜伟旅游发展有限公司 | Utilize the method for the fluffy feeding mutton sheep of saline-alkali land |
| CN109090021A (en) * | 2018-06-12 | 2018-12-28 | 山东胜伟旅游发展有限公司 | The method of the fluffy feeding milch goat of saline-alkali land |
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Application publication date: 20120905 |