CN106085588A - A kind of extract the method for capsaicin in chilli seed - Google Patents

A kind of extract the method for capsaicin in chilli seed Download PDF

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Publication number
CN106085588A
CN106085588A CN201610524308.5A CN201610524308A CN106085588A CN 106085588 A CN106085588 A CN 106085588A CN 201610524308 A CN201610524308 A CN 201610524308A CN 106085588 A CN106085588 A CN 106085588A
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CN
China
Prior art keywords
chilli seed
seed
capsaicin
chilli
capsicum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610524308.5A
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Chinese (zh)
Inventor
韦勇
范明达
李世源
刘玉申
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WENSHAN YONGRUN CAPSAICIN CO Ltd
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WENSHAN YONGRUN CAPSAICIN CO Ltd
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Publication date
Application filed by WENSHAN YONGRUN CAPSAICIN CO Ltd filed Critical WENSHAN YONGRUN CAPSAICIN CO Ltd
Priority to CN201610524308.5A priority Critical patent/CN106085588A/en
Publication of CN106085588A publication Critical patent/CN106085588A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/06Production of fats or fatty oils from raw materials by pressing
    • C11B1/08Production of fats or fatty oils from raw materials by pressing by hot pressing
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Edible Oils And Fats (AREA)

Abstract

The invention discloses and a kind of extract the method for capsaicin in chilli seed, choose the chilli seed that high-quality is full, remove Fructus Capsici skin and impurity, join in material frying machine after screening and stir-fry, join in spiral multistage oil press and squeeze, the granulated slag of squeezing removes solid impurity by multiple filtration sieve, then removes residual impurity with centrifuge;By adding heat abstraction abnormal flavour therein and moisture, refilter after it is cooled to room temperature,.Extraction process route of the present invention is short, energy resource consumption is few, extraction efficiency is high, capsaicin extraction rate reached more than 90%, capsicum seed oil extraction rate reached more than 95%, expressing process farthest remains the giving off a strong fragrance taste of capsicum seed oil and various nutrient substance, capsicum seed oil is limpid bright, aromatic flavor, also rich in unsaturated fatty acid, vitamin E and several mineral materials in addition to containing capsaicin, no solvent residue, meets modern's requirement to green health.

Description

A kind of extract the method for capsaicin in chilli seed
Technical field
The present invention relates to the making field of capsaicin, a kind of extract the method for capsaicin in chilli seed.
Background technology
Fructus Capsici (Capsicum annuum L.) is Solanaceae capsicum plants, originates in central and south america, existing plantation Spreading all over the world, China is the famous Fructus Capsici place of production.Fructus Capsici whole body is all precious, current research focus primarily upon Capsaicinoids, Pigment (including capsorubin, capsorubin, beta-carotene etc.), other also include the vitamin that in fruit and vegerable, content is the highest C, abundant vitamin E, folic acid, potassium, calcium, magnesium, phosphorus etc..Chilli seed is the important component part of Fructus Capsici, and chilli seed accounts for full dried fruits The 20%~40% of quality, but Chinese scholars is less to the research of chilli seed in the past.
In chilli seed, oil content enriches, and reaches about 20%, and in capsicum seed oil, unsaturated fatty acid content is up to more than 70%, Unsaturated fatty acid is a kind of fatty acid constituting body fat, is the fatty acid of needed by human.It addition, in chilli seed possibly together with Capsaicin, capsaicin is the pungency component in Fructus Capsici, can be widely used for field of food.
Summary of the invention
It is an object of the invention to provide and a kind of extract the method for capsaicin in chilli seed, to solve in above-mentioned background technology The problem proposed.
For achieving the above object, the present invention provides following technical scheme:
A kind of extract the method for capsaicin in chilli seed, specifically comprise the following steps that
(1) pretreatment
Choose the chilli seed rich in Capsaicin, remove the Fructus Capsici skin and impurity contained in chilli seed by vibrosieve, then through wind Optional equipment, removes shrivelled and mouldy chilli seed, obtains the chilli seed that high-quality is full;
(2) roasting is fried
Chilli seed after screening is joined in material frying machine, under the conditions of 100~180 DEG C, stir-fries 30~80min, until peppery Till green pepper seed turns yellow and gives out chilli seed distinctive giving off a strong fragrance taste;
(3) squeezing
Chilli seed after frying roasting joins in spiral multistage oil press, regulates inlet amount, and adjusting lock nut is controlled The grouts thickness that system is got rid of, regulation temperature control makes press chamber and pressing screw squeeze within the temperature range of being maintained at setting;
(4) refine
The capsicum seed oil that squeezing obtains contains substantial amounts of granulated slag, removes solid impurity by multiple filtration sieve;Again with centrifugal Residual impurity removed by machine;Finally, by adding heat abstraction abnormal flavour therein and moisture, refilter after it is cooled to room temperature Capsicum seed oil after refine.
As the further scheme of the present invention: in described (3), spiral multistage oil press Pressing Number is 4~6 grades, row The grouts thickness gone out is 0.5~3mm, and the temperature of press chamber and pressing screw is 120~180 DEG C.
As the present invention further scheme: in described (4), multiple filtration is 2~4 layers, centrifuge is high speed centrifugation Machine, heating-up temperature is 120~80 DEG C.
Compared with prior art, the invention has the beneficial effects as follows:
The present invention obtains, by vibrosieve and pneumatic separator, the chilli seed that high-quality is full, fries roasting chilli seed with material frying machine, uses Press apparatus squeezing chilli seed, the chilli seed crude oil that squeezing obtains capsicum seed oil after refine obtains refine.The present invention carries Taking technique route is short, and energy resource consumption is few, and extraction efficiency is high, capsaicin extraction rate reached more than 90%, capsicum seed oil extraction rate reached More than 95%, expressing process farthest remains the local flavor of product and various nutrient substance, and product is limpid bright, thick flavor Strongly fragrant, also rich in unsaturated fatty acid, vitamin E and several mineral materials, no solvent residue in addition to containing capsaicin, meet existing For people's requirement to green health.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, Obviously, described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based in the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, all Belong to the scope of protection of the invention.
Embodiment 1
Capsaicin extraction step in chilli seed:
(1) pretreatment
Choose Capsicum frutescens var chilli seed 100kg, remove the Fructus Capsici skin and other impurity contained in chilli seed, then warp by vibrosieve Crossing pneumatic separator, remove shrivelled and mouldy chilli seed, obtain the chilli seed 72kg that high-quality is full, the chilli seed after screening is through surveying Determining capsaicin content is 0.22% average oil content 19.7%;
(2) roasting is fried
Joining in material frying machine by the Capsicum frutescens var chilli seed after screening, stir-fry under the conditions of 130 DEG C 80min, until Fructus Capsici Till seed turns yellow and gives out chilli seed distinctive giving off a strong fragrance taste, now have penetrating odor and produce, smoke abatement need to be done and process;
(3) squeezing
After stir-fry being roasted, Capsicum frutescens var chilli seed joins in spiral 4 grades of oil presses, regulates inlet amount, adjusting lock nut The grouts thickness making discharge is 1mm, and regulation temperature control makes press chamber and pressing screw be maintained at 120~180 DEG C, obtains 15.3kg peppery after squeezing Green pepper seed crude oil;
(4) refine
Chilli seed crude oil squeezing obtained removes major part solid impurity by 2~4 layers of sieves, then uses high speed centrifugation Machine centrifugal segregation residual impurity, then be heated to 150 DEG C and go to eliminate the unusual smell and a small amount of moisture, filter i.e. after it is cooled to room temperature Capsicum seed oil after available 13.6kg refine, this capsicum seed oil capsaicin content 1.05% after measured, capsaicin extraction ratio is 90.15%, capsicum seed oil extraction ratio is 95.9%.
Embodiment 2
Capsaicin extraction step in chilli seed:
(1) pretreatment
Choose Capsicum frutescens var chilli seed 200kg, remove the Fructus Capsici skin and other impurity contained in chilli seed, then warp by vibrosieve Cross pneumatic separator, remove shrivelled and mouldy chilli seed, obtain the chilli seed 151kg that high-quality is full, the chilli seed warp after screening Measuring capsaicin content is 0.21% average oil content 19.5%;
(2) roasting is fried
Joining in material frying machine by the Capsicum frutescens var chilli seed after screening, stir-fry under the conditions of 150 DEG C 60min, until Fructus Capsici Till seed turns yellow and gives out chilli seed distinctive giving off a strong fragrance taste, now have penetrating odor and produce, smoke abatement need to be done and process;
(3) squeezing
After stir-fry being roasted, Capsicum frutescens var chilli seed joins in spiral 5 grades of oil presses, regulates inlet amount, adjusting lock nut The grouts thickness making discharge is 2mm, and regulation temperature control makes press chamber and pressing screw be maintained at 120~180 DEG C, obtains 30.2kg peppery after squeezing Green pepper seed crude oil;
(4) refine
Chilli seed crude oil squeezing obtained removes major part solid impurity by 3 layers of sieves, then uses high speed centrifuge Centrifugal segregation residual impurity, then be heated to 160 DEG C and go to eliminate the unusual smell and a small amount of moisture, filter after it is cooled to room temperature Obtaining the capsicum seed oil after 28.3kg refine, this chilli seed has the capsaicin content 1.01%, capsaicin extraction ratio to be after measured 90.2%, capsicum seed oil extraction ratio is 96.1%.
Embodiment 3
Capsaicin extraction step in chilli seed:
(1) pretreatment
Choose Capsicum frutescens var chilli seed 500kg, remove the Fructus Capsici skin and other impurity contained in chilli seed, then warp by vibrosieve Cross pneumatic separator, remove shrivelled and mouldy chilli seed, obtain the chilli seed 365kg that high-quality is full, the chilli seed warp after screening Measuring capsaicin content is 0.21% average oil content 19.56%;
(2) roasting is fried
Being joined in batches in material frying machine by Capsicum frutescens var chilli seed after screening, stir-fry under the conditions of 160 DEG C 55min, directly Turning yellow to chilli seed and giving out chilli seed distinctive giving off a strong fragrance taste, now have penetrating odor and produce, need to do at smoke abatement Reason;
(3) squeezing
After stir-fry being roasted, Capsicum frutescens var chilli seed joins in spiral 6 grades of oil presses, regulates inlet amount, adjusting lock nut The grouts thickness making discharge is 2.5mm, and regulation temperature control makes press chamber and pressing screw be maintained at 120~180 DEG C, obtains 75.3kg after squeezing Chilli seed crude oil;
(4) refine
Chilli seed crude oil squeezing obtained removes major part solid impurity by 3 layers of sieves, then uses high speed centrifuge Centrifugal segregation residual impurity, then be heated to 170 DEG C and go to eliminate the unusual smell and a small amount of moisture, filter after it is cooled to room temperature Obtaining the capsicum seed oil after 71.4kg refine, this chilli seed has the capsaicin content 0.97%, capsaicin extraction ratio to be after measured 90.3%, capsicum seed oil extraction ratio is 96.3%.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie In the case of the spirit or essential attributes of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter From the point of view of which point, all should regard embodiment as exemplary, and be nonrestrictive, the scope of the present invention is by appended power Profit requires rather than described above limits, it is intended that all by fall in the implication of equivalency and scope of claim Change is included in the present invention.

Claims (3)

1. one kind is extracted the method for capsaicin in chilli seed, it is characterised in that specifically comprise the following steps that
(1) pretreatment
Choose the chilli seed rich in Capsaicin, remove the Fructus Capsici skin and impurity contained in chilli seed by vibrosieve, then set through selecting crude drugs with winnower Standby, remove shrivelled and mouldy chilli seed, obtain the chilli seed that high-quality is full;
(2) roasting is fried
Chilli seed after screening is joined in material frying machine, under the conditions of 100~180 DEG C, stir-fries 30~80min, until chilli seed Till turning yellow and giving out chilli seed distinctive giving off a strong fragrance taste;
(3) squeezing
Chilli seed after frying roasting joins in spiral multistage oil press, regulates inlet amount, and adjusting lock nut controls row The grouts thickness removed, regulation temperature control makes press chamber and pressing screw squeeze within the temperature range of being maintained at setting;
(4) refine
The capsicum seed oil that squeezing obtains contains substantial amounts of granulated slag, removes solid impurity by multiple filtration sieve;Go with centrifuge again Except residual impurity;Finally, by adding heat abstraction abnormal flavour therein and moisture, after it is cooled to room temperature, refilter i.e. available essence Capsicum seed oil after refining.
Capsaicin new method for extracting in chilli seed the most according to claim 1, it is characterised in that in described (3), spirally Multistage oil press Pressing Number is 4~6 grades, and the grouts thickness of discharge is 0.5~3mm, the temperature of press chamber and pressing screw be 120~ 180℃。
Capsaicin new method for extracting in chilli seed the most according to claim 1, it is characterised in that multilamellar mistake in described (4) Filter is 2~4 layers, and centrifuge is high speed centrifuge, and heating-up temperature is 120~80 DEG C.
CN201610524308.5A 2016-07-06 2016-07-06 A kind of extract the method for capsaicin in chilli seed Pending CN106085588A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107177414A (en) * 2017-07-14 2017-09-19 云南宏绿辣素有限公司 A kind of method that spiral oil press produces Zanthoxylum essential oil
CN107307248A (en) * 2017-06-08 2017-11-03 中北大学 A kind of purple perilla albumen nanometer beverage and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1107508A (en) * 1994-10-08 1995-08-30 周兆彦 Pure red pepper oil and its preparing process
CN102342332A (en) * 2011-09-23 2012-02-08 天津市天联调味制品有限公司 Method for preparing fragrant and hot essential oil
CN103525539A (en) * 2013-10-11 2014-01-22 天津市天联调味制品有限公司 Method for preparing chili seed oil with stable spicy fragrance
CN103881806A (en) * 2014-04-16 2014-06-25 襄汾县晋润食品有限公司 Method for extruding oil from chilli seeds
CN104804860A (en) * 2015-04-02 2015-07-29 新疆冠农果茸集团股份有限公司 Manufacturing method for capsicum seed oil

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1107508A (en) * 1994-10-08 1995-08-30 周兆彦 Pure red pepper oil and its preparing process
CN102342332A (en) * 2011-09-23 2012-02-08 天津市天联调味制品有限公司 Method for preparing fragrant and hot essential oil
CN103525539A (en) * 2013-10-11 2014-01-22 天津市天联调味制品有限公司 Method for preparing chili seed oil with stable spicy fragrance
CN103881806A (en) * 2014-04-16 2014-06-25 襄汾县晋润食品有限公司 Method for extruding oil from chilli seeds
CN104804860A (en) * 2015-04-02 2015-07-29 新疆冠农果茸集团股份有限公司 Manufacturing method for capsicum seed oil

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107307248A (en) * 2017-06-08 2017-11-03 中北大学 A kind of purple perilla albumen nanometer beverage and preparation method thereof
CN107177414A (en) * 2017-07-14 2017-09-19 云南宏绿辣素有限公司 A kind of method that spiral oil press produces Zanthoxylum essential oil

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Application publication date: 20161109