CN103891919A - Abelmoschus esculentus seed oil enriched in lipid-soluble vitamins and preparation method thereof - Google Patents
Abelmoschus esculentus seed oil enriched in lipid-soluble vitamins and preparation method thereof Download PDFInfo
- Publication number
- CN103891919A CN103891919A CN201410009352.3A CN201410009352A CN103891919A CN 103891919 A CN103891919 A CN 103891919A CN 201410009352 A CN201410009352 A CN 201410009352A CN 103891919 A CN103891919 A CN 103891919A
- Authority
- CN
- China
- Prior art keywords
- setose abelmoschus
- parts
- abelmoschus seed
- crude oil
- extraction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Landscapes
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention discloses abelmoschus esculentus seed oil enriched in lipid-soluble vitamins and a preparation method thereof. The abelmoschus esculentus seed oil is prepared by taking abelmoschus esculentus seeds as raw materials and matching with carrots, broccolis, kale borecoles, asparagus lettuces and hickory nuts. A preparation process comprises the following procedures: (1) weighing prepared materials; (2) preparing crude oil; (3) drying; (4) crushing; (5) extracting and enriching; (6) carrying out filter pressing; (7) de-coloring; (8) carrying out the filter pressing again and the like. The abelmoschus esculentus seed oil provided by the invention is enriched in the lipid-soluble vitamins including VA, VD, VE, VK and the like and unsaturated fatty acids, and is nutritional and healthy plant oil.
Description
Technical field
The invention belongs to food processing field, be specifically related to a kind of setose abelmoschus seed oil that is rich in liposoluble vitamin and preparation method thereof.
Technical background
Okra (
abelmoschusesculentus (L.) Moench) belong to Malvaceae (Malvaceae) Abelmoschus (AbelmoschusMedic), English name Okra, call foreign capsicum, swordweed, be described as " Green Ginseng ", " plant vigour " abroad, it is the annual herbaceous plant of Malvaceae, it originates in Africa, extensively cultivates in torrid areas, is mainly distributed in the areas such as Taiwan, Guangdong, Guangxi, Jiangxi, Hunan and Yunnan in China.Okra is precious from head to foot, and tender pod, flower, the equal edible of leaf are nutritious, there is the effects such as warming kidney to invigorate yang, antifatigue, enhancing immunity, after its tender pod is aging, produce seed abundant, the oil content of seed is higher, is rich in unrighted acid and balanced proportion, is a kind of potential good oil plant.
China is the consumption big country of edible oil, and the edible oil supply security problem of the whole nation 1,300,000,000 populations is the cardinal task of administering state affairs well and ensure national security all the time.At present, China's output of oil-bearing crop can not meet the demand of the whole nation to edible oil, and 2007, the degree of self-sufficiency of China's vegetable oil was only 39%, and 61% of imported petroleum product Yi Zhan China vegetable oil total quantity consumed makes China become maximum in the world oil plant importer.Meanwhile, the low yield of China oil crops not before, in domestic large oil crops in 2009, except rapeseed volume increase 7.4%, the equal underproduction of other oil crops such as soybean, peanut and cottonseed, China's edible oil Supply situation sternness as can be seen here.
Edible oil is that the mankind absorb fat and V
a, V
d, V
e, V
kdeng the important sources of liposoluble vitamin, investigation shows, the relatively single and unreasonable structure of the kind of China resident edible oil, if and taking setose abelmoschus seed as oil plant, Development and Production is rich in insatiable hunger fat and aliphatic acid and balanced proportion, the vegetable oil of liposoluble vitamin rich content simultaneously, the general level of the health of alleviating the supply of China's edible oil and promoting China resident edible oil being conducive to.
Summary of the invention
For the problems referred to above, the object of this invention is to provide a kind of setose abelmoschus seed oil that is rich in liposoluble vitamin and preparation method thereof.
Technical scheme of the present invention is as follows.
Be rich in a setose abelmoschus seed oil for liposoluble vitamin, it is taking okra seed as raw material, is equipped with the common fruits and vegetables such as carrot, broccoli, Brussels sprouts, asparagus lettuce, hickory nut and is prepared from; Wherein, carrot, broccoli are rich in vitamin A, and hickory nut is rich in vitamin E and vitamin D, and asparagus lettuce, Brussels sprouts are rich in vitamin K and vitamin E; Each raw material proportioning is by weight as follows above:
100 parts, okra seed;
2～8 parts, carrot;
2～6 parts of broccoli;
2～6 parts of Brussels sprouts;
2～10 parts of asparagus lettuces;
1～4 part of hickory nut.
As one of preferred version, the each raw material of the present invention proportioning is by weight as follows:
100 parts, okra seed;
3～6 parts, carrot;
3～5 parts of broccoli;
3～5 parts of Brussels sprouts;
4～8 parts of asparagus lettuces;
2～3 parts of hickory nuts.
As two of preferred version, the each raw material of the present invention proportioning is by weight as follows:
100 parts, okra seed;
5 parts, carrot;
4 parts of broccoli;
4 parts of Brussels sprouts;
5 parts of asparagus lettuces;
2.5 parts of hickory nuts.
The present invention also provides a kind of preparation method of the setose abelmoschus seed oil that is rich in liposoluble vitamin, comprises following operation:
(1) weigh and get the raw materials ready: take respectively okra seed, carrot, broccoli, Brussels sprouts, asparagus lettuce, hickory nut by above-mentioned weight proportion, for subsequent use;
(2) prepare crude oil: okra seed was pulverized to 40 mesh sieves, and extracting screen underflow, adopts supercritical CO
2extraction process extracts and obtains setose abelmoschus seed crude oil, for subsequent use as for dry place, cool place after sealing;
(3) dry: carrot, broccoli, Brussels sprouts, asparagus lettuce are cut into the bulk of 2～4cm, are placed in vacuum drying chamber, be dried to water content lower than 8% in 40～60 DEG C, obtain each dry material, for subsequent use;
(4) pulverize: above dry material is mixed with hickory nut, and being crushed to afterwards granularity is 20～40 orders, obtains compound;
(5) Extraction and enrichment: the method Extraction and enrichment liposoluble vitamin that adopts vacuum frying, be added in extractor together with setose abelmoschus seed crude oil by compound, be 0.09～0.15MPa in vacuum, temperature is 50～65 DEG C, mixing speed is under the condition of 30～60r/min, fried 10～60min;
(6) press filtration: adopt plate and frame filter press to filter the fuel mixture after Extraction and enrichment, repeat 1～3 time, collect filtrate, for subsequent use;
(7) decolouring: the filtrate that step (6) is collected is transferred to bleacher, add the carclazyte of setose abelmoschus seed crude quality 1%～6% or 0.5～6% active carbon, be 70～90 DEG C in temperature, under the condition that mixing speed is 30～60r/min, decolouring 30～60min;
(8) press filtration again: adopt plate and frame filter press to filter the fuel mixture after above-mentioned decolouring, repeat 3～5 times, bright to filtrate clarification, collect filtrate, obtain product of the present invention.
The setose abelmoschus seed crude oil of described step (5) Extraction and enrichment has been taked anti-oxidant pretreatment, prior to adding the antioxidant of 0.2～0.4g/kg (with setose abelmoschus seed crude oil weighing scale) in setose abelmoschus seed crude oil, then by setose abelmoschus seed heating crude oil to 50～60 DEG C, for subsequent use after stirring.
Described antioxidant is the one of Tea Polyphenols, Rosmarinus officinalis extract, tocopherol.
The Extraction and enrichment of described step (5) also comprises the method for ultrasonic wave assisted extraction, be added in extractor together with setose abelmoschus seed crude oil by compound, at ultrasonic power 40～100Hz, 40～70 DEG C of temperature, Extraction and enrichment 10～30min under the condition of mixing speed 20～40r/min.
The Extraction and enrichment of described step (5) also comprises the method that heating is extracted, is added in extractor together with setose abelmoschus seed crude oil by compound, and 60～90 DEG C of heating-up temperatures, Extraction and enrichment 30～60min under the condition of mixing speed 20～40r/min.
invention advantage
The liposoluble vitamin content of setose abelmoschus seed oil prepared by employing the present invention is shown in Figure of description 1.
Brief description of the drawings
As seen from Figure 1, product of the present invention is than setose abelmoschus seed crude oil, and its liposoluble vitamin content significantly improves.Therefore, by taking in this product setose abelmoschus seed oil, not only can reach and supplement the object of aliphatic acid, comprehensively the liposoluble vitamin such as replenishing vitamins A, vitamin D, vitamin E and vitamin K.
Fig. 1 is that the liposoluble vitamin of the setose abelmoschus seed oil prepared of the present invention is containing spirogram.
Fig. 2 is that the liposoluble vitamin of the setose abelmoschus seed oil prepared of embodiment 1 is containing spirogram.
Fig. 3 is that the liposoluble vitamin of the setose abelmoschus seed oil prepared of embodiment 2 is containing spirogram.
Fig. 4 is that the liposoluble vitamin of the setose abelmoschus seed oil prepared of embodiment 3 is containing spirogram.
Fig. 5 is that the liposoluble vitamin of the setose abelmoschus seed oil prepared of embodiment 4 is containing spirogram.
Fig. 6 is that the liposoluble vitamin of the setose abelmoschus seed oil prepared of embodiment 5 is containing spirogram.
Fig. 7 is that the liposoluble vitamin of the setose abelmoschus seed oil prepared of embodiment 6 is containing spirogram.
Fig. 8 is that the liposoluble vitamin of the setose abelmoschus seed oil prepared of embodiment 7 is containing spirogram.
Fig. 9 is that the liposoluble vitamin of the setose abelmoschus seed oil prepared of embodiment 8 is containing spirogram.
detailed description of the invention
Below in conjunction with example, detailed explanation method of the present invention and effect, but the invention is not restricted to following examples.
embodiment 1
(1) weigh and get the raw materials ready: prepare okra seed 100kg, carrot 2kg, broccoli 2kg, Brussels sprouts 2kg, asparagus lettuce 2kg, hickory nut 1kg, for subsequent use;
(2) prepare crude oil: okra seed was pulverized to 40 mesh sieves, and extracting screen underflow, adopts supercritical CO
2extraction process extracts and obtains setose abelmoschus seed crude oil 18.8kg, for subsequent use as for dry place, cool place after sealing;
(3) dry: carrot, broccoli, Brussels sprouts, asparagus lettuce are cut into the bulk of 2～4cm, are placed in vacuum drying chamber, be dried to water content lower than 8% in 40 DEG C, obtain each dry material, for subsequent use;
(4) pulverize: above dry material is mixed with hickory nut, and being crushed to afterwards granularity is 20～40 orders, obtains compound;
(5) Extraction and enrichment: first setose abelmoschus seed crude oil is carried out to anti-oxidant pretreatment, in setose abelmoschus seed crude oil, add the Tea Polyphenols of 0.4g/kg (with setose abelmoschus seed crude oil weighing scale), then by setose abelmoschus seed heating crude oil to 50～60 DEG C, for subsequent use after stirring; Adopting afterwards the method Extraction and enrichment liposoluble vitamin of vacuum frying, be added in extractor together with anti-oxidant pretreated setose abelmoschus seed crude oil by compound, is 0.09MPa in vacuum, and temperature is under the condition of 65 DEG C, fried 10min;
(6) press filtration: adopt plate and frame filter press to filter the fuel mixture after Extraction and enrichment, repeat 1 time, collect filtrate, for subsequent use;
(7) decolouring: the filtrate that step (6) is collected is transferred to bleacher, adds the carclazyte of setose abelmoschus seed crude quality 1%, is 70 DEG C in temperature, under the condition that mixing speed is 30r/min, decolouring 30min;
(8) press filtration again: adopt plate and frame filter press to filter the fuel mixture after above-mentioned decolouring, repeat 3 times, make filtrate clarification bright, collect filtrate, obtain product of the present invention.
The liposoluble vitamin content of the setose abelmoschus seed oil that after testing, prepared by the present embodiment is shown in Figure of description 2.
embodiment 2
(1) weigh and get the raw materials ready: prepare okra seed 100kg, carrot 8kg, broccoli 6kg, Brussels sprouts 6kg, asparagus lettuce 10kg, hickory nut 4kg, for subsequent use;
(2) prepare crude oil: okra seed was pulverized to 40 mesh sieves, and extracting screen underflow, adopts supercritical CO
2extraction process extracts and obtains setose abelmoschus seed crude oil 19.1kg, for subsequent use as for dry place, cool place after sealing;
(3) dry: carrot, broccoli, Brussels sprouts, asparagus lettuce are cut into the bulk of 2～4cm, are placed in vacuum drying chamber, be dried to water content lower than 8% in 60 DEG C, obtain each dry material, for subsequent use;
(4) pulverize: above dry material is mixed with hickory nut, and being crushed to afterwards granularity is 20～40 orders, obtains compound;
(5) Extraction and enrichment: first setose abelmoschus seed crude oil is carried out to anti-oxidant pretreatment, in setose abelmoschus seed crude oil, add the Tea Polyphenols of 0.2g/kg (with setose abelmoschus seed crude oil weighing scale), then by setose abelmoschus seed heating crude oil to 50～60 DEG C, for subsequent use after stirring; Adopting afterwards the method Extraction and enrichment liposoluble vitamin of vacuum frying, be added in extractor together with anti-oxidant pretreated setose abelmoschus seed crude oil by compound, is 0.15MPa in vacuum, and temperature is under the condition of 65 DEG C, fried 60min;
(6) press filtration: adopt plate and frame filter press to filter the fuel mixture after Extraction and enrichment, repeat 3 times, collect filtrate, for subsequent use;
(7) decolouring: the filtrate that step (6) is collected is transferred to bleacher, adds the carclazyte of setose abelmoschus seed crude quality 6%, is 70 DEG C in temperature, under the condition that mixing speed is 40r/min, decolouring 60min;
(8) press filtration again: adopt plate and frame filter press to filter the fuel mixture after above-mentioned decolouring, repeat 5 times, make filtrate clarification bright, collect filtrate, obtain product of the present invention.
The liposoluble vitamin content of the setose abelmoschus seed oil that after testing, prepared by the present embodiment is shown in Figure of description 3.
embodiment 3
(1) weigh and get the raw materials ready: prepare okra seed 100kg, carrot 8kg, broccoli 6kg, Brussels sprouts 6kg, asparagus lettuce 10kg, hickory nut 4kg, for subsequent use;
(2) prepare crude oil: okra seed was pulverized to 40 mesh sieves, and extracting screen underflow, adopts supercritical CO
2extraction process extracts and obtains setose abelmoschus seed crude oil 18.5kg, for subsequent use as for dry place, cool place after sealing;
(3) dry: carrot, broccoli, Brussels sprouts, asparagus lettuce are cut into the bulk of 2～4cm, are placed in vacuum drying chamber, be dried to water content lower than 8% in 60 DEG C, obtain each dry material, for subsequent use;
(4) pulverize: above dry material is mixed with hickory nut, and being crushed to afterwards granularity is 20～40 orders, obtains compound;
(5) Extraction and enrichment: first setose abelmoschus seed crude oil is carried out to anti-oxidant pretreatment, in setose abelmoschus seed crude oil, add the tocopherol of 0.2g/kg (with setose abelmoschus seed crude oil weighing scale), then by setose abelmoschus seed heating crude oil to 50～60 DEG C, for subsequent use after stirring; Adopting afterwards the method Extraction and enrichment liposoluble vitamin of vacuum frying, be added in extractor together with anti-oxidant pretreated setose abelmoschus seed crude oil by compound, is 0.12MPa in vacuum, and temperature is under the condition of 60 DEG C, fried 40min;
(6) press filtration: adopt plate and frame filter press to filter the fuel mixture after Extraction and enrichment, repeat 3 times, collect filtrate, for subsequent use;
(7) decolouring: the filtrate that step (6) is collected is transferred to bleacher, adds the active carbon of setose abelmoschus seed crude quality 6%, is 90 DEG C in temperature, under the condition that mixing speed is 50r/min, decolouring 30min;
(8) press filtration again: adopt plate and frame filter press to filter the fuel mixture after above-mentioned decolouring, repeat 5 times, make filtrate clarification bright, collect filtrate, obtain product of the present invention.
The liposoluble vitamin content of the setose abelmoschus seed oil that after testing, prepared by the present embodiment is shown in Figure of description 4.
embodiment 4
(1) weigh and get the raw materials ready: prepare okra seed 100kg, carrot 6kg, broccoli 3kg, Brussels sprouts 3kg, asparagus lettuce 5kg, hickory nut 2.5kg, for subsequent use;
(2) prepare crude oil: okra seed was pulverized to 40 mesh sieves, and extracting screen underflow, adopts supercritical CO
2extraction process extracts and obtains setose abelmoschus seed crude oil 18.1kg, for subsequent use as for dry place, cool place after sealing;
(3) dry: carrot, broccoli, Brussels sprouts, asparagus lettuce are cut into the bulk of 2～4cm, are placed in vacuum drying chamber, be dried to water content lower than 8% in 60 DEG C, obtain each dry material, for subsequent use;
(4) pulverize: above dry material is mixed with hickory nut, and being crushed to afterwards granularity is 20～40 orders, obtains compound;
(5) Extraction and enrichment: first setose abelmoschus seed crude oil is carried out to anti-oxidant pretreatment, in setose abelmoschus seed crude oil, add the Rosmarinus officinalis extract of 0.3g/kg (with setose abelmoschus seed crude oil weighing scale), then by setose abelmoschus seed heating crude oil to 50～60 DEG C, for subsequent use after stirring; Adopting afterwards the method Extraction and enrichment liposoluble vitamin of vacuum frying, be added in extractor together with anti-oxidant pretreated setose abelmoschus seed crude oil by compound, is 0.10MPa in vacuum, and temperature is under the condition of 60 DEG C, fried 50min;
(6) press filtration: adopt plate and frame filter press to filter the fuel mixture after Extraction and enrichment, repeat 3 times, collect filtrate, for subsequent use;
(7) decolouring: the filtrate that step (6) is collected is transferred to bleacher, adds the active carbon of setose abelmoschus seed crude quality 6%, is 80 DEG C in temperature, under the condition that mixing speed is 50r/min, decolouring 50min;
(8) press filtration again: adopt plate and frame filter press to filter the fuel mixture after above-mentioned decolouring, repeat 4 times, make filtrate clarification bright, collect filtrate, obtain product of the present invention.
The liposoluble vitamin content of the setose abelmoschus seed oil that after testing, prepared by the present embodiment is shown in Figure of description 5.
embodiment 5
(1) weigh and get the raw materials ready: prepare okra seed 100kg, carrot 6kg, broccoli 3kg, Brussels sprouts 3kg, asparagus lettuce 5kg, hickory nut 2.5kg, for subsequent use;
(2) prepare crude oil: okra seed was pulverized to 40 mesh sieves, and extracting screen underflow, adopts supercritical CO
2extraction process extracts and obtains setose abelmoschus seed crude oil 18.1kg, for subsequent use as for dry place, cool place after sealing;
(3) dry: carrot, broccoli, Brussels sprouts, asparagus lettuce are cut into the bulk of 2～4cm, are placed in vacuum drying chamber, be dried to water content lower than 8% in 60 DEG C, obtain each dry material, for subsequent use;
(4) pulverize: above dry material is mixed with hickory nut, and being crushed to afterwards granularity is 20～40 orders, obtains compound;
(5) Extraction and enrichment: first setose abelmoschus seed crude oil is carried out to anti-oxidant pretreatment, in setose abelmoschus seed crude oil, add the tocopherol of 0.3g/kg (with setose abelmoschus seed crude oil weighing scale), then by setose abelmoschus seed heating crude oil to 50～60 DEG C, for subsequent use after stirring; Adopt afterwards the method for ultrasonic wave assisted extraction, be added in extractor together with anti-oxidant pretreated setose abelmoschus seed crude oil by compound, at ultrasonic power 40Hz, temperature 70 C, Extraction and enrichment 30min under the condition of mixing speed 20r/min;
(6) press filtration: adopt plate and frame filter press to filter the fuel mixture after Extraction and enrichment, repeat 3 times, collect filtrate, for subsequent use;
(7) decolouring: the filtrate that step (6) is collected is transferred to bleacher, adds the active carbon of setose abelmoschus seed crude quality 1%, is 80 DEG C in temperature, under the condition that mixing speed is 50r/min, decolouring 50min;
(8) press filtration again: adopt plate and frame filter press to filter the fuel mixture after above-mentioned decolouring, repeat 4 times, make filtrate clarification bright, collect filtrate, obtain product of the present invention.
The liposoluble vitamin content of the setose abelmoschus seed oil that after testing, prepared by the present embodiment is shown in Figure of description 6.
embodiment 6
(1) weigh and get the raw materials ready: prepare okra seed 100kg, carrot 6kg, broccoli 4kg, Brussels sprouts 4kg, asparagus lettuce 5kg, hickory nut 4kg, for subsequent use;
(2) prepare crude oil: okra seed was pulverized to 40 mesh sieves, and extracting screen underflow, adopts supercritical CO
2extraction process extracts and obtains setose abelmoschus seed crude oil 18.2kg, for subsequent use as for dry place, cool place after sealing;
(3) dry: carrot, broccoli, Brussels sprouts, asparagus lettuce are cut into the bulk of 2～4cm, are placed in vacuum drying chamber, be dried to water content lower than 8% in 60 DEG C, obtain each dry material, for subsequent use;
(4) pulverize: above dry material is mixed with hickory nut, and being crushed to afterwards granularity is 20～40 orders, obtains compound;
(5) Extraction and enrichment, decolouring: first setose abelmoschus seed crude oil is carried out to anti-oxidant pretreatment, in setose abelmoschus seed crude oil, add the Tea Polyphenols of 0.2g/kg (with setose abelmoschus seed crude oil weighing scale), then by setose abelmoschus seed heating crude oil to 50～60 DEG C, for subsequent use after stirring; Adopt afterwards the method Extraction and enrichment liposoluble vitamin of ultrasonic wave assisted extraction, be added in extractor together with anti-oxidant pretreated setose abelmoschus seed crude oil by compound, at ultrasonic power 100Hz, 40 DEG C of temperature, Extraction and enrichment 10min under the condition of mixing speed 40r/min;
(6) press filtration: adopt plate and frame filter press to filter the fuel mixture after Extraction and enrichment, repeat 2 times, collect filtrate, for subsequent use;
(7) decolouring: the filtrate that step (6) is collected is transferred to bleacher, adds the active carbon of setose abelmoschus seed crude quality 3%, is 80 DEG C in temperature, under the condition that mixing speed is 50r/min, decolouring 40min;
(8) press filtration again: adopt plate and frame filter press to filter the fuel mixture after above-mentioned decolouring, repeat 5 times, make filtrate clarification bright, collect filtrate, obtain product of the present invention.
The liposoluble vitamin content of the setose abelmoschus seed oil that after testing, prepared by the present embodiment is shown in Figure of description 7.
embodiment 7
(1) weigh and get the raw materials ready: prepare okra seed 100kg, carrot 6kg, broccoli 4kg, Brussels sprouts 4kg, asparagus lettuce 5kg, hickory nut 4kg, for subsequent use;
(2) prepare crude oil: okra seed was pulverized to 40 mesh sieves, and extracting screen underflow, adopts supercritical CO
2extraction process extracts and obtains setose abelmoschus seed crude oil 18.2kg, for subsequent use as for dry place, cool place after sealing;
(3) dry: carrot, broccoli, Brussels sprouts, asparagus lettuce are cut into the bulk of 2～4cm, are placed in vacuum drying chamber, be dried to water content lower than 8% in 60 DEG C, obtain each dry material, for subsequent use;
(4) pulverize: above dry material is mixed with hickory nut, and being crushed to afterwards granularity is 20～40 orders, obtains compound;
(5) Extraction and enrichment, decolouring: first setose abelmoschus seed crude oil is carried out to anti-oxidant pretreatment, in setose abelmoschus seed crude oil, add the Tea Polyphenols of 0.4g/kg (with setose abelmoschus seed crude oil weighing scale), then by setose abelmoschus seed heating crude oil to 50～60 DEG C, for subsequent use after stirring; The method Extraction and enrichment liposoluble vitamin that adopts heating to extract afterwards, is added in extractor together with anti-oxidant pretreated setose abelmoschus seed crude oil by compound, 90 DEG C of heating-up temperatures, and Extraction and enrichment 30min under the condition of mixing speed 40r/min;
(6) press filtration: adopt plate and frame filter press to filter the fuel mixture after Extraction and enrichment, repeat 2 times, collect filtrate, for subsequent use;
(7) decolouring: the filtrate that step (6) is collected is transferred to bleacher, adds the active carbon of setose abelmoschus seed crude quality 3%, is 80 DEG C in temperature, under the condition that mixing speed is 50r/min, decolouring 40min;
(8) press filtration again: adopt plate and frame filter press to filter the fuel mixture after above-mentioned decolouring, repeat 5 times, make filtrate clarification bright, collect filtrate, obtain product of the present invention.
The liposoluble vitamin content of the setose abelmoschus seed oil that after testing, prepared by the present embodiment is shown in Figure of description 8.
embodiment 8
(1) weigh and get the raw materials ready: prepare okra seed 100kg, carrot 6kg, broccoli 4kg, Brussels sprouts 4kg, asparagus lettuce 5kg, hickory nut 4kg, for subsequent use;
(2) prepare crude oil: okra seed was pulverized to 40 mesh sieves, and extracting screen underflow, adopts supercritical CO
2extraction process extracts and obtains setose abelmoschus seed crude oil 18.2kg, for subsequent use as for dry place, cool place after sealing;
(3) dry: carrot, broccoli, Brussels sprouts, asparagus lettuce are cut into the bulk of 2～4cm, are placed in vacuum drying chamber, be dried to water content lower than 8% in 60 DEG C, obtain each dry material, for subsequent use;
(4) pulverize: above dry material is mixed with hickory nut, and being crushed to afterwards granularity is 20～40 orders, obtains compound;
(5) Extraction and enrichment, decolouring: first setose abelmoschus seed crude oil is carried out to anti-oxidant pretreatment, in setose abelmoschus seed crude oil, add the Tea Polyphenols of 0.4g/kg (with setose abelmoschus seed crude oil weighing scale), then by setose abelmoschus seed heating crude oil to 50～60 DEG C, for subsequent use after stirring; The method Extraction and enrichment liposoluble vitamin that adopts heating to extract afterwards, is added in extractor together with anti-oxidant pretreated setose abelmoschus seed crude oil by compound, 60 DEG C of heating-up temperatures, and Extraction and enrichment 60min under the condition of mixing speed 20r/min;
(6) press filtration: adopt plate and frame filter press to filter the fuel mixture after Extraction and enrichment, repeat 2 times, collect filtrate, for subsequent use;
(7) decolouring: the filtrate that step (6) is collected is transferred to bleacher, adds the active carbon of setose abelmoschus seed crude quality 3%, is 80 DEG C in temperature, under the condition that mixing speed is 50r/min, decolouring 40min;
(8) press filtration again: adopt plate and frame filter press to filter the fuel mixture after above-mentioned decolouring, repeat 5 times, make filtrate clarification bright, collect filtrate, obtain product of the present invention.
The liposoluble vitamin content of the setose abelmoschus seed oil that after testing, prepared by the present embodiment is shown in Figure of description 9.
Claims (8)
1. be rich in a setose abelmoschus seed oil for liposoluble vitamin, it is characterized in that it is taking okra seed as raw material, be equipped with carrot, broccoli, Brussels sprouts, asparagus lettuce, hickory nut and be prepared from, each raw material proportioning is by weight as follows:
100 parts, okra seed;
2～8 parts, carrot;
2～6 parts of broccoli;
2～6 parts of Brussels sprouts;
2～10 parts of asparagus lettuces;
1～4 part of hickory nut.
2. a kind of setose abelmoschus seed oil that is rich in liposoluble vitamin as claimed in claim 1, is characterized in that each raw material proportioning is by weight as follows:
100 parts, okra seed;
3～6 parts, carrot;
3～5 parts of broccoli;
3～5 parts of Brussels sprouts;
4～8 parts of asparagus lettuces;
2～3 parts of hickory nuts.
3. a kind of setose abelmoschus seed oil that is rich in liposoluble vitamin as claimed in claim 1, is characterized in that each raw material proportioning is by weight as follows:
100 parts, okra seed;
5 parts, carrot;
4 parts of broccoli;
4 parts of Brussels sprouts;
5 parts of asparagus lettuces;
2.5 parts of hickory nuts.
4. the method for preparation a kind of setose abelmoschus seed oil that is rich in liposoluble vitamin as claimed in claim 1, is characterized in that comprising following operation:
(1) weigh and get the raw materials ready: take respectively okra seed, carrot, broccoli, Brussels sprouts, asparagus lettuce, hickory nut by above-mentioned weight proportion, for subsequent use;
(2) prepare crude oil: okra seed was pulverized to 40 mesh sieves, and extracting screen underflow, adopts supercritical CO
2extraction process extracts and obtains setose abelmoschus seed crude oil, for subsequent use as for dry place, cool place after sealing;
(3) dry: carrot, broccoli, Brussels sprouts, asparagus lettuce are cut into the bulk of 2～4cm, are placed in vacuum drying chamber, be dried to water content lower than 8% in 40～60 DEG C, obtain each dry material, for subsequent use;
(4) pulverize: above dry material is mixed with hickory nut, and being crushed to afterwards granularity is 20～40 orders, obtains compound;
(5) Extraction and enrichment: the method Extraction and enrichment liposoluble vitamin that adopts vacuum frying, be added in extractor together with setose abelmoschus seed crude oil by compound, be 0.09～0.15MPa in vacuum, temperature is 50～65 DEG C, mixing speed is under the condition of 30～60r/min, fried 10～60min;
(6) press filtration: adopt plate and frame filter press to filter the fuel mixture after Extraction and enrichment, repeat 1～3 time, collect filtrate, for subsequent use;
(7) decolouring: the filtrate that step (6) is collected is transferred to bleacher, add the carclazyte of setose abelmoschus seed crude quality 1%～6% or 0.5～6% active carbon, be 70～90 DEG C in temperature, under the condition that mixing speed is 30～60r/min, decolouring 30～60min;
(8) press filtration again: adopt plate and frame filter press to filter the fuel mixture after above-mentioned decolouring, repeat 3～5 times, bright to filtrate clarification, collect filtrate, obtain product of the present invention.
5. a kind of preparation method who is rich in liposoluble vitamin setose abelmoschus seed oil as claimed in claim 4, the setose abelmoschus seed crude oil that it is characterized in that described step (5) Extraction and enrichment has been taked anti-oxidant pretreatment, prior to adding the antioxidant of 0.2～0.4g/kg (with setose abelmoschus seed crude oil weighing scale) in setose abelmoschus seed crude oil, then by setose abelmoschus seed heating crude oil to 50～60 DEG C, for subsequent use after stirring.
6. a kind of preparation method who is rich in liposoluble vitamin setose abelmoschus seed oil as claimed in claim 5, is characterized in that described antioxidant is the one of Tea Polyphenols, Rosmarinus officinalis extract, tocopherol.
7. a kind of preparation method who is rich in liposoluble vitamin setose abelmoschus seed oil as claimed in claim 4, it is characterized in that the Extraction and enrichment of described step (5) also comprises the method for ultrasonic wave assisted extraction, be added in extractor together with setose abelmoschus seed crude oil by compound, at ultrasonic power 40～100Hz, 40～70 DEG C of temperature, Extraction and enrichment 10～30min under the condition of mixing speed 20～40r/min.
8. a kind of preparation method who is rich in liposoluble vitamin setose abelmoschus seed oil as claimed in claim 4, the Extraction and enrichment that it is characterized in that described step (5) also comprises the method that heating is extracted, be added in extractor together with setose abelmoschus seed crude oil by compound, 60～90 DEG C of heating-up temperatures, Extraction and enrichment 30～60min under the condition of mixing speed 20～40r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410009352.3A CN103891919A (en) | 2014-01-09 | 2014-01-09 | Abelmoschus esculentus seed oil enriched in lipid-soluble vitamins and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410009352.3A CN103891919A (en) | 2014-01-09 | 2014-01-09 | Abelmoschus esculentus seed oil enriched in lipid-soluble vitamins and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103891919A true CN103891919A (en) | 2014-07-02 |
Family
ID=50983752
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410009352.3A Pending CN103891919A (en) | 2014-01-09 | 2014-01-09 | Abelmoschus esculentus seed oil enriched in lipid-soluble vitamins and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103891919A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104498179A (en) * | 2014-12-18 | 2015-04-08 | 贵州航天乌江机电设备有限责任公司 | Method for extracting okra seed oil |
| CN105495515A (en) * | 2015-12-09 | 2016-04-20 | 上海大学 | Preparation method of edible flavor enhancer with fried aromatic lettuce fragrance |
| CN104046511B (en) * | 2014-07-09 | 2016-05-25 | 宁夏六盘珍坊生态农业科技有限公司 | Improve the linseed oil preparation method of linseed oil quality |
| CN109287420A (en) * | 2018-09-06 | 2019-02-01 | 青岛农业大学 | A kind of method of quick predict peanut oil content |
| CN109580804A (en) * | 2018-10-25 | 2019-04-05 | 杭州邦沃森生物科技有限公司 | A kind of preparation method and detection method of high stability Turtle Oil |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1134230A (en) * | 1996-04-03 | 1996-10-30 | 临川市油酯化工厂 | Nutrient intensified oil and its producing process |
| CN1739369A (en) * | 2005-09-26 | 2006-03-01 | 吴水林 | Edible oil with rich nutrients and its prepn process |
| CN101568345A (en) * | 2006-10-19 | 2009-10-28 | 邦格阿里门特斯有限公司 | Triglyceridic nature oil with improved nutritional properties and process for the preparation thereof |
| CN102763737A (en) * | 2012-08-07 | 2012-11-07 | 饶雨农 | Production method of oil rich in natural vitamins |
| CN103013654A (en) * | 2013-01-05 | 2013-04-03 | 湖南奇异生物科技有限公司 | Okra seed oil and extraction method thereof |
-
2014
- 2014-01-09 CN CN201410009352.3A patent/CN103891919A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1134230A (en) * | 1996-04-03 | 1996-10-30 | 临川市油酯化工厂 | Nutrient intensified oil and its producing process |
| CN1739369A (en) * | 2005-09-26 | 2006-03-01 | 吴水林 | Edible oil with rich nutrients and its prepn process |
| CN101568345A (en) * | 2006-10-19 | 2009-10-28 | 邦格阿里门特斯有限公司 | Triglyceridic nature oil with improved nutritional properties and process for the preparation thereof |
| CN102763737A (en) * | 2012-08-07 | 2012-11-07 | 饶雨农 | Production method of oil rich in natural vitamins |
| CN103013654A (en) * | 2013-01-05 | 2013-04-03 | 湖南奇异生物科技有限公司 | Okra seed oil and extraction method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 华景清等: "《粮油加工技术》", 31 August 2010, 中国计量出版社 * |
| 张国治: "《油炸食品生产技术》", 30 June 2010, 化学工业出版社 * |
| 田科巍: "黄秋葵油脂及多糖提取工艺优化和组分分析", 《中国优秀硕士学位论文全文数据库 工程科技Ⅰ辑》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104046511B (en) * | 2014-07-09 | 2016-05-25 | 宁夏六盘珍坊生态农业科技有限公司 | Improve the linseed oil preparation method of linseed oil quality |
| CN104498179A (en) * | 2014-12-18 | 2015-04-08 | 贵州航天乌江机电设备有限责任公司 | Method for extracting okra seed oil |
| CN105495515A (en) * | 2015-12-09 | 2016-04-20 | 上海大学 | Preparation method of edible flavor enhancer with fried aromatic lettuce fragrance |
| CN109287420A (en) * | 2018-09-06 | 2019-02-01 | 青岛农业大学 | A kind of method of quick predict peanut oil content |
| CN109580804A (en) * | 2018-10-25 | 2019-04-05 | 杭州邦沃森生物科技有限公司 | A kind of preparation method and detection method of high stability Turtle Oil |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101617787B (en) | Process for continuously extracting a plurality of products from highland barley | |
| CN103891919A (en) | Abelmoschus esculentus seed oil enriched in lipid-soluble vitamins and preparation method thereof | |
| CN103087818A (en) | Method for ultrasonic wave assisted supercritical CO2 extraction of sunflower seed oil | |
| CN106496176A (en) | A kind of method from extracting proanthocyanidin from grape seeds | |
| CN103351968A (en) | Pitaya rice wine and preparation method thereof | |
| CN107629870A (en) | Method that is a kind of while extracting peanut oil and peanut protein | |
| CN102229857A (en) | Method for extracting wax gourd seed oil | |
| CN103045430A (en) | Anthocyanin-rich fructus rhodomyrti fermented fruit wine and preparation method thereof | |
| CN105054178A (en) | Choerospondias axillaris and mulberry beverage and preparation method thereof | |
| CN102885375B (en) | Solid beverage and preparation method thereof | |
| CN103330103A (en) | Pumpkin and lily rice dumplings for reducing blood sugar level | |
| CN104126678A (en) | Good-flavored plant blend oil rich in omega-3 polyunsaturated fatty acids and production method thereof | |
| CN103651964A (en) | Health oil with efficacy of reducing blood lipid | |
| CN103478639A (en) | Maca rice and application thereof | |
| CN111109511A (en) | Rapid peeling method for food-grade walnut kernels | |
| CN110373262A (en) | A kind of Lai wood fruit oil refinement method of low-cost and high-quality | |
| CN102106457A (en) | Method for detoxifying de-oiled jatropha curcas kernels | |
| CN101773265A (en) | Method for preparing jujube juice by enzymolysis and extraction of jujube powder | |
| CN105670767A (en) | Method using camellia oleifera seed cake for oil expression | |
| CN102948496B (en) | Method for pollen wall breaking by enzyme and extraction of pollen grease composition by supercritical CO2 | |
| CN104745425A (en) | Yellow wine lees beverage and preparation method thereof | |
| CN104322998A (en) | Piglet feed and preparation method thereof | |
| CN103734342A (en) | Five-cereal tartaric acid soybean milk and preparation method thereof | |
| CN107432341A (en) | The preparation method of the compound jasmine tea of the root of gansui | |
| CN105994793A (en) | Processing method of Chinese wampee fruit, frangipani and tea nutritive powder |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C12 | Rejection of a patent application after its publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20140702 |