CN114606058A - Extraction method of agilawood aromatic liquid - Google Patents

Extraction method of agilawood aromatic liquid Download PDF

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Publication number
CN114606058A
CN114606058A CN202011421644.XA CN202011421644A CN114606058A CN 114606058 A CN114606058 A CN 114606058A CN 202011421644 A CN202011421644 A CN 202011421644A CN 114606058 A CN114606058 A CN 114606058A
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CN
China
Prior art keywords
agilawood
volatile oil
liquid
aromatic liquid
tincture
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202011421644.XA
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Chinese (zh)
Inventor
丁宗妙
林师宝
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hainan Island Aquilaria Scientific Research Institute
Hainan Xiangshu Chenxiang Industry Group Co ltd
Original Assignee
Hainan Island Aquilaria Scientific Research Institute
Hainan Xiangshu Chenxiang Industry Group Co ltd
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Filing date
Publication date
Application filed by Hainan Island Aquilaria Scientific Research Institute, Hainan Xiangshu Chenxiang Industry Group Co ltd filed Critical Hainan Island Aquilaria Scientific Research Institute
Priority to CN202011421644.XA priority Critical patent/CN114606058A/en
Publication of CN114606058A publication Critical patent/CN114606058A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/027Recovery of volatiles by distillation or stripping
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F3/00Tea; Tea substitutes; Preparations thereof
    • A23F3/06Treating tea before extraction; Preparations produced thereby
    • A23F3/14Tea preparations, e.g. using additives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F3/00Tea; Tea substitutes; Preparations thereof
    • A23F3/34Tea substitutes, e.g. matè; Extracts or infusions thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/022Refining
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/025Recovery by solvent extraction
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2209/00Aspects relating to disinfection, sterilisation or deodorisation of air
    • A61L2209/20Method-related aspects
    • A61L2209/21Use of chemical compounds for treating air or the like

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Food Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Botany (AREA)
  • Zoology (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses an extraction method of agilawood aromatic liquid, relating to the technical field of agilawood, and comprising the following steps: s1, selecting agilawood raw materials, selecting agilawood with the oil content of more than 12%, and crushing for later use; s2, extracting volatile oil, namely adding the agilawood powder into a volatile oil extraction tank, adding 6-10 times of water, soaking for 12-24 hours, distilling to extract the agilawood volatile oil, and collecting for later use; s3, extracting with a high alcohol solution, pouring out the poached liquid after the volatile oil is extracted, collecting the poached liquid for later use, and performing cooking extraction on the filter residue for 2-3 times by using edible alcohol with the temperature of 60-85 ℃, wherein the amount of the edible alcohol is 5-8 times of the mass of the materials; the invention provides the agilawood fragrant liquid with abundant agilawood fragrance and effective substances, so that agilawood volatile oil can be well suspended in the agilawood extracting solution, agilawood fragrant components can be sprayed more uniformly during aromatherapy, and the consistency of fragrance front and back is ensured.

Description

Extraction method of agilawood aromatic liquid
Technical Field
The invention relates to the technical field of agilawood, and particularly relates to an extraction method of agilawood aromatic liquid.
Background
At present, the agilawood hydrolat is mainly used as an aromatherapy liquid, mainly is a byproduct in the production process of the agilawood volatile oil, contains a small number of absorbable agilawood components, has light fragrance and weak aromatherapy effect, and meanwhile, after the agilawood volatile oil and the agilawood hydrolat are shaken, the agilawood volatile oil quickly floats on the surface of the agilawood hydrolat, cannot form a suspension oil liquid, is not suitable for being used together for aromatherapy, and needs to be improved.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides an extraction method of agilawood aromatic liquid, which solves the problems mentioned in the background technology.
In order to achieve the purpose, the invention is realized by the following technical scheme: the extraction method of the agilawood aromatic liquid comprises the following steps:
s1, selecting agilawood raw materials, selecting agilawood with the oil content of more than 12%, and crushing for later use;
s2, extracting volatile oil, namely adding the agilawood powder into a volatile oil extraction tank, adding 6-10 times of water, soaking for 12-24 hours, distilling to extract the agilawood volatile oil, and collecting for later use;
s3, extracting with a high alcohol solution, pouring out the poached liquid after the volatile oil is extracted, collecting the poached liquid for later use, and performing cooking extraction on the filter residue for 2-3 times by using edible alcohol with the temperature of 60-85 ℃, wherein the amount of the edible alcohol is 5-8 times of the mass of the materials;
s4, concentrating the mixed solution, mixing the extract and the boiled solution, concentrating the mixture to be 0.6-2.4 times of the mass of the materials, pouring out the concentrated solution from which the pasty precipitate is removed, and obtaining agilawood tincture;
s5, preparing agilawood aromatic liquid, wherein agilawood tincture in S4 is one agilawood aromatic liquid, the agilawood volatile oil obtained by extracting the batch of agilawood raw material is mixed with the agilawood tincture, and the agilawood volatile oil is impacted into countless tiny oily particles by forcibly shaking or stirring at high speed by using a stirrer, and the countless tiny oily particles are uniformly dispersed in the agilawood tincture to form turbid liquid, namely the other agilawood aromatic liquid;
s6, storing and using the agilawood aromatic liquid, wherein the agilawood aromatic liquid is preferably stored in an environment of 4-8 ℃, is directly added into an aromatherapy machine during aromatherapy, and can also be used as an additive of health-care food such as agilawood tea and the like.
In the above method for extracting agilawood fragrant liquid, preferably, the agilawood fragrant liquid comprises agilawood tincture, a mixed solution of agilawood tincture and agilawood volatile oil.
In the method for extracting agilawood fragrant liquid, preferably, after S1, the agilawood raw material can be directly cooked and extracted with 60-85 degrees of edible alcohol for 2-3 times, and after multiple times of mixing of extraction liquids, the mixture is concentrated to be 0.8-3 times of the mass of the material.
The method for extracting agilawood aroma liquid is characterized in that the agilawood aroma tincture is a clear transparent liquid or suspension.
Compared with the prior art, the invention has the following beneficial effects: the agilawood fragrant liquid is rich in agilawood fragrance and effective substances, agilawood volatile oil can be well suspended in the agilawood extracting solution, agilawood fragrant components can be sprayed more uniformly during aromatherapy, and the consistency of fragrance is ensured.
Detailed Description
All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides a technical scheme that: the extraction method of the agilawood aromatic liquid comprises the following steps:
s1, selecting agilawood with the oil content of more than 12%, and crushing for later use;
s2, extracting volatile oil, namely adding the agilawood powder into a volatile oil extraction tank, adding 6-10 times of water, soaking for 12-24 hours, distilling and extracting the agilawood volatile oil, and collecting for later use;
s3, extracting with a high alcohol solution, pouring out the poached liquid after the volatile oil is extracted, collecting the poached liquid for later use, and performing cooking extraction on the filter residue for 2-3 times by using edible alcohol with the temperature of 60-85 ℃, wherein the amount of the edible alcohol is 5-8 times of the mass of the materials;
s4, concentrating the mixed solution, mixing the extract and the boiled solution, concentrating the mixture to be 0.6-2.4 times of the mass of the materials, pouring out the concentrated solution from which the pasty precipitate is removed, and obtaining agilawood tincture;
s5, preparing agilawood aromatic liquid, wherein agilawood tincture in S4 is one agilawood aromatic liquid, the agilawood volatile oil obtained by extracting the batch of agilawood raw material is mixed with the agilawood tincture, and the agilawood volatile oil is impacted into countless tiny oily particles by forcibly shaking or stirring at high speed by using a stirrer, and the countless tiny oily particles are uniformly dispersed in the agilawood tincture to form turbid liquid, namely the other agilawood aromatic liquid;
s6, storing and using the agilawood aromatic liquid, wherein the agilawood aromatic liquid is preferably stored in an environment of 4-8 ℃, is directly added into an aromatherapy machine during aromatherapy, and can also be used as an additive of health-care food such as agilawood tea and the like.
The lignum Aquilariae Resinatum aromatic liquid comprises lignum Aquilariae Resinatum tincture, and mixed solution of lignum Aquilariae Resinatum volatile oil.
And (S1), directly cooking and extracting the agilawood raw material for 2-3 times by using edible alcohol with the temperature of 60-85 ℃, mixing the extraction solutions for many times, and concentrating until the mass of the extraction solutions is 0.8-3 times of that of the material.
The agilawood tincture is clear transparent liquid or suspension.
The aromatic liquid can be used as aromatherapy liquid, and also can be used as additive for health food such as lignum Aquilariae Resinatum tea.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (4)

1. The extraction method of the agilawood aromatic liquid is characterized by comprising the following steps: the method comprises the following steps:
s1, selecting agilawood raw materials, selecting agilawood with the oil content of more than 12%, and crushing for later use;
s2, extracting volatile oil, namely adding the agilawood powder into a volatile oil extraction tank, adding 6-10 times of water, soaking for 12-24 hours, distilling to extract the agilawood volatile oil, and collecting for later use;
s3, extracting with a high alcohol solution, pouring out the poached liquid after the volatile oil is extracted, collecting the poached liquid for later use, and performing cooking extraction on the filter residue for 2-3 times by using edible alcohol with the temperature of 60-85 ℃, wherein the amount of the edible alcohol is 5-8 times of the mass of the materials;
s4, concentrating the mixed solution, mixing the extract and the boiled solution, concentrating the mixture to be 0.6-2.4 times of the mass of the materials, pouring out the concentrated solution from which the pasty precipitate is removed, and obtaining agilawood tincture;
s5, preparing agilawood aromatic liquid, wherein agilawood tincture in S4 is one agilawood aromatic liquid, the agilawood volatile oil obtained by extracting the batch of agilawood raw material is mixed with the agilawood tincture, and the agilawood volatile oil is impacted into countless tiny oily particles by forcibly shaking or stirring at high speed by using a stirrer, and the countless tiny oily particles are uniformly dispersed in the agilawood tincture to form turbid liquid, namely the other agilawood aromatic liquid;
s6, storing and using the agilawood aromatic liquid, wherein the agilawood aromatic liquid is preferably stored in an environment of 4-8 ℃, is directly added into an aromatherapy machine during aromatherapy, and can also be used as an additive of health-care food such as agilawood tea and the like.
2. The extraction method of agilawood aromatic liquid according to claim 1, which is characterized in that: the lignum Aquilariae Resinatum aromatic liquid comprises lignum Aquilariae Resinatum tincture, and mixed solution of lignum Aquilariae Resinatum tincture and lignum Aquilariae Resinatum volatile oil.
3. The extraction method of agilawood aromatic liquid according to claim 2, characterized by comprising the following steps: and (8) after S1, directly cooking and extracting the agilawood raw material for 2-3 times by using edible alcohol with the temperature of 60-85 ℃, mixing the extraction solutions for many times, and concentrating until the mass of the extraction solutions is 0.8-3 times that of the material.
4. The extraction method of agilawood aromatic liquid according to claim 3, characterized by comprising the following steps: the agilawood tincture is a clear transparent liquid or suspension.
CN202011421644.XA 2020-12-08 2020-12-08 Extraction method of agilawood aromatic liquid Pending CN114606058A (en)

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Application Number Priority Date Filing Date Title
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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI243686B (en) * 2000-05-31 2005-11-21 Shiseido Co Ltd Method for collecting fragrance ingredient and perfume composition and cosmetic containing the fragrance ingredient
CN101057820A (en) * 2007-05-16 2007-10-24 徐海波 Rose pure dew added rose essential and its manufacturing technology
CN101280243A (en) * 2008-06-04 2008-10-08 杨利民 Method for extracting rose essence oil and rose absolute by water vapor water distillation technology
CN101691522A (en) * 2009-09-30 2010-04-07 云南省农业科学院药用植物研究所 Method for extracting rose damascana and rose flower water from roses
CN103789094A (en) * 2014-01-21 2014-05-14 广州大学 Method for extracting agilawood essential oil from agilawood chips
CN107746749A (en) * 2017-09-28 2018-03-02 江永百润福天然植物科技发展有限公司 A kind of preparation method and Lignum Aquilariae Resinatum extract from agalloch eaglewood residue production Lignum Aquilariae Resinatum extract
CN110151822A (en) * 2019-05-23 2019-08-23 湖南宏蒂康生命科技有限公司 A kind of preparation method of natural plant health-care massage champignon essence oil and champignon hydrosol

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI243686B (en) * 2000-05-31 2005-11-21 Shiseido Co Ltd Method for collecting fragrance ingredient and perfume composition and cosmetic containing the fragrance ingredient
CN101057820A (en) * 2007-05-16 2007-10-24 徐海波 Rose pure dew added rose essential and its manufacturing technology
CN101280243A (en) * 2008-06-04 2008-10-08 杨利民 Method for extracting rose essence oil and rose absolute by water vapor water distillation technology
CN101691522A (en) * 2009-09-30 2010-04-07 云南省农业科学院药用植物研究所 Method for extracting rose damascana and rose flower water from roses
CN103789094A (en) * 2014-01-21 2014-05-14 广州大学 Method for extracting agilawood essential oil from agilawood chips
CN107746749A (en) * 2017-09-28 2018-03-02 江永百润福天然植物科技发展有限公司 A kind of preparation method and Lignum Aquilariae Resinatum extract from agalloch eaglewood residue production Lignum Aquilariae Resinatum extract
CN110151822A (en) * 2019-05-23 2019-08-23 湖南宏蒂康生命科技有限公司 A kind of preparation method of natural plant health-care massage champignon essence oil and champignon hydrosol

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
张洪广;张晓斌;胡勇;石星星;王杰;: "玫瑰纯露的制备及其在化妆品中的应用", 广东化工, no. 18, pages 24 - 25 *
黎贵卿;杨素华;宋业昌;邱米;陆顺忠;: "减压水蒸气蒸馏提取茉莉花精油和纯露的工艺", 香料香精化妆品, no. 03 *

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Application publication date: 20220610