CN106722771A - A kind of new garlic nutrient salt and preparation method thereof - Google Patents
A kind of new garlic nutrient salt and preparation method thereof Download PDFInfo
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- CN106722771A CN106722771A CN201611193034.2A CN201611193034A CN106722771A CN 106722771 A CN106722771 A CN 106722771A CN 201611193034 A CN201611193034 A CN 201611193034A CN 106722771 A CN106722771 A CN 106722771A
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- Prior art keywords
- salt
- garlic
- allicin
- iodine
- nutrient
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- 150000003839 salts Chemical class 0.000 title claims abstract description 608
- 235000004611 garlic Nutrition 0.000 title claims abstract description 415
- 238000002360 preparation method Methods 0.000 title claims abstract description 94
- 235000015097 nutrients Nutrition 0.000 title claims abstract description 88
- 244000245420 ail Species 0.000 title 1
- 240000002234 Allium sativum Species 0.000 claims abstract description 414
- 235000002639 sodium chloride Nutrition 0.000 claims description 691
- 235000010081 allicin Nutrition 0.000 claims description 221
- JDLKFOPOAOFWQN-VIFPVBQESA-N Allicin Natural products C=CCS[S@](=O)CC=C JDLKFOPOAOFWQN-VIFPVBQESA-N 0.000 claims description 220
- JDLKFOPOAOFWQN-UHFFFAOYSA-N allicin Chemical compound C=CCSS(=O)CC=C JDLKFOPOAOFWQN-UHFFFAOYSA-N 0.000 claims description 220
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 214
- 239000011630 iodine Substances 0.000 claims description 214
- 229910052740 iodine Inorganic materials 0.000 claims description 214
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 151
- 239000011780 sodium chloride Substances 0.000 claims description 87
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 81
- 239000007864 aqueous solution Substances 0.000 claims description 78
- 238000000034 method Methods 0.000 claims description 72
- 229920006395 saturated elastomer Polymers 0.000 claims description 68
- 239000002245 particle Substances 0.000 claims description 60
- 239000000284 extract Substances 0.000 claims description 52
- 238000009835 boiling Methods 0.000 claims description 50
- 239000013081 microcrystal Substances 0.000 claims description 49
- 238000010907 mechanical stirring Methods 0.000 claims description 47
- 235000011837 pasties Nutrition 0.000 claims description 43
- 238000003756 stirring Methods 0.000 claims description 41
- 230000008569 process Effects 0.000 claims description 32
- 239000000843 powder Substances 0.000 claims description 28
- 239000000243 solution Substances 0.000 claims description 27
- 239000003795 chemical substances by application Substances 0.000 claims description 24
- 238000002156 mixing Methods 0.000 claims description 22
- 229940029982 garlic powder Drugs 0.000 claims description 18
- 238000010298 pulverizing process Methods 0.000 claims description 14
- UOZDOLIXBYLRAC-UHFFFAOYSA-L [2-hydroxy-3-(trimethylazaniumyl)propyl]-trimethylazanium;diiodide Chemical compound [I-].[I-].C[N+](C)(C)CC(O)C[N+](C)(C)C UOZDOLIXBYLRAC-UHFFFAOYSA-L 0.000 claims description 11
- 239000000276 potassium ferrocyanide Substances 0.000 claims description 11
- XOGGUFAVLNCTRS-UHFFFAOYSA-N tetrapotassium;iron(2+);hexacyanide Chemical compound [K+].[K+].[K+].[K+].[Fe+2].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] XOGGUFAVLNCTRS-UHFFFAOYSA-N 0.000 claims description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 10
- 238000000605 extraction Methods 0.000 claims description 8
- 238000000855 fermentation Methods 0.000 claims description 6
- 230000004151 fermentation Effects 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 6
- 238000002425 crystallisation Methods 0.000 claims description 5
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 5
- 238000002386 leaching Methods 0.000 claims description 5
- 235000016709 nutrition Nutrition 0.000 claims description 5
- 230000035764 nutrition Effects 0.000 claims description 5
- 239000000377 silicon dioxide Substances 0.000 claims description 5
- KBPZVLXARDTGGD-UHFFFAOYSA-N 2,3-dihydroxybutanedioic acid;iron Chemical compound [Fe].OC(=O)C(O)C(O)C(O)=O KBPZVLXARDTGGD-UHFFFAOYSA-N 0.000 claims description 4
- 235000012241 calcium silicate Nutrition 0.000 claims description 4
- 229910001505 inorganic iodide Inorganic materials 0.000 claims description 4
- 238000000194 supercritical-fluid extraction Methods 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- 230000008025 crystallization Effects 0.000 claims description 3
- 229960002413 ferric citrate Drugs 0.000 claims description 3
- 239000000796 flavoring agent Substances 0.000 claims description 3
- 235000019634 flavors Nutrition 0.000 claims description 3
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 claims description 3
- NPFOYSMITVOQOS-UHFFFAOYSA-K iron(III) citrate Chemical group [Fe+3].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NPFOYSMITVOQOS-UHFFFAOYSA-K 0.000 claims description 3
- 238000000874 microwave-assisted extraction Methods 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 238000002137 ultrasound extraction Methods 0.000 claims description 3
- 239000011573 trace mineral Substances 0.000 claims description 2
- 235000013619 trace mineral Nutrition 0.000 claims description 2
- 239000002994 raw material Substances 0.000 abstract description 57
- 238000010411 cooking Methods 0.000 abstract description 4
- 206010012601 diabetes mellitus Diseases 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 4
- 235000013305 food Nutrition 0.000 abstract description 4
- 235000011194 food seasoning agent Nutrition 0.000 abstract description 4
- 230000003908 liver function Effects 0.000 abstract description 4
- 230000002265 prevention Effects 0.000 abstract description 4
- 239000002028 Biomass Substances 0.000 abstract description 2
- 231100000957 no side effect Toxicity 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 230000001737 promoting effect Effects 0.000 abstract description 2
- 238000005516 engineering process Methods 0.000 description 49
- 235000013339 cereals Nutrition 0.000 description 47
- 239000000047 product Substances 0.000 description 40
- 238000011084 recovery Methods 0.000 description 37
- 108090000790 Enzymes Proteins 0.000 description 30
- 102000004190 Enzymes Human genes 0.000 description 30
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 30
- 229940088598 enzyme Drugs 0.000 description 30
- 239000000706 filtrate Substances 0.000 description 30
- 238000001035 drying Methods 0.000 description 28
- XUHLIQGRKRUKPH-GCXOYZPQSA-N Alliin Natural products N[C@H](C[S@@](=O)CC=C)C(O)=O XUHLIQGRKRUKPH-GCXOYZPQSA-N 0.000 description 23
- XUHLIQGRKRUKPH-UHFFFAOYSA-N S-allyl-L-cysteine sulfoxide Natural products OC(=O)C(N)CS(=O)CC=C XUHLIQGRKRUKPH-UHFFFAOYSA-N 0.000 description 23
- XUHLIQGRKRUKPH-DYEAUMGKSA-N alliin Chemical compound OC(=O)[C@@H](N)C[S@@](=O)CC=C XUHLIQGRKRUKPH-DYEAUMGKSA-N 0.000 description 23
- 235000015295 alliin Nutrition 0.000 description 23
- 239000000320 mechanical mixture Substances 0.000 description 23
- 238000005303 weighing Methods 0.000 description 23
- 238000013019 agitation Methods 0.000 description 22
- 238000012856 packing Methods 0.000 description 22
- 238000001914 filtration Methods 0.000 description 12
- 239000006185 dispersion Substances 0.000 description 11
- 102000004196 processed proteins & peptides Human genes 0.000 description 11
- 108090000765 processed proteins & peptides Proteins 0.000 description 11
- 238000012216 screening Methods 0.000 description 11
- 238000007493 shaping process Methods 0.000 description 11
- 239000007788 liquid Substances 0.000 description 10
- 235000012249 potassium ferrocyanide Nutrition 0.000 description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 239000004744 fabric Substances 0.000 description 9
- 239000000203 mixture Substances 0.000 description 9
- 239000006228 supernatant Substances 0.000 description 8
- 238000005292 vacuum distillation Methods 0.000 description 7
- 239000012530 fluid Substances 0.000 description 6
- 238000004108 freeze drying Methods 0.000 description 6
- DWNBOPVKNPVNQG-LURJTMIESA-N (2s)-4-hydroxy-2-(propylamino)butanoic acid Chemical compound CCCN[C@H](C(O)=O)CCO DWNBOPVKNPVNQG-LURJTMIESA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 239000010647 garlic oil Substances 0.000 description 4
- 238000000227 grinding Methods 0.000 description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 3
- 108010059892 Cellulase Proteins 0.000 description 3
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 3
- 239000011575 calcium Substances 0.000 description 3
- 229910052791 calcium Inorganic materials 0.000 description 3
- 210000002318 cardia Anatomy 0.000 description 3
- 229940106157 cellulase Drugs 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 239000012467 final product Substances 0.000 description 3
- 235000013312 flour Nutrition 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000007789 sealing Methods 0.000 description 3
- 229910052711 selenium Inorganic materials 0.000 description 3
- 239000011669 selenium Substances 0.000 description 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 230000004060 metabolic process Effects 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 description 1
- 240000002900 Arthrospira platensis Species 0.000 description 1
- 235000016425 Arthrospira platensis Nutrition 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241001474374 Blennius Species 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- AUNGANRZJHBGPY-UHFFFAOYSA-N D-Lyxoflavin Natural products OCC(O)C(O)C(O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-UHFFFAOYSA-N 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 241000251511 Holothuroidea Species 0.000 description 1
- 241000237536 Mytilus edulis Species 0.000 description 1
- 241000237509 Patinopecten sp. Species 0.000 description 1
- 108091005804 Peptidases Proteins 0.000 description 1
- 239000004365 Protease Substances 0.000 description 1
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 1
- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 description 1
- 241001339782 Scapharca broughtonii Species 0.000 description 1
- 241000242583 Scyphozoa Species 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 241001125843 Trichiuridae Species 0.000 description 1
- 241001261505 Undaria Species 0.000 description 1
- 229930003471 Vitamin B2 Natural products 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 229960004424 carbon dioxide Drugs 0.000 description 1
- 229910002090 carbon oxide Inorganic materials 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012611 container material Substances 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000006253 efflorescence Methods 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- 150000008131 glucosides Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000002779 inactivation Effects 0.000 description 1
- 150000002496 iodine Chemical class 0.000 description 1
- 150000002497 iodine compounds Chemical class 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 241000238565 lobster Species 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 235000020638 mussel Nutrition 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 230000006911 nucleation Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 230000003204 osmotic effect Effects 0.000 description 1
- 238000005554 pickling Methods 0.000 description 1
- JLKDVMWYMMLWTI-UHFFFAOYSA-M potassium iodate Chemical compound [K+].[O-]I(=O)=O JLKDVMWYMMLWTI-UHFFFAOYSA-M 0.000 description 1
- 239000001230 potassium iodate Substances 0.000 description 1
- 235000006666 potassium iodate Nutrition 0.000 description 1
- 229940093930 potassium iodate Drugs 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 206010037844 rash Diseases 0.000 description 1
- 229960002477 riboflavin Drugs 0.000 description 1
- 229930182490 saponin Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 235000017709 saponins Nutrition 0.000 description 1
- 235000020637 scallop Nutrition 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 235000010413 sodium alginate Nutrition 0.000 description 1
- 229940005550 sodium alginate Drugs 0.000 description 1
- 239000000661 sodium alginate Substances 0.000 description 1
- GTSHREYGKSITGK-UHFFFAOYSA-N sodium ferrocyanide Chemical compound [Na+].[Na+].[Na+].[Na+].[Fe+2].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] GTSHREYGKSITGK-UHFFFAOYSA-N 0.000 description 1
- 239000000264 sodium ferrocyanide Substances 0.000 description 1
- 235000012247 sodium ferrocyanide Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 229940082787 spirulina Drugs 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- BUUPQKDIAURBJP-UHFFFAOYSA-N sulfinic acid Chemical compound OS=O BUUPQKDIAURBJP-UHFFFAOYSA-N 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 235000019640 taste Nutrition 0.000 description 1
- 239000011716 vitamin B2 Substances 0.000 description 1
- 235000019164 vitamin B2 Nutrition 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 150000003751 zinc Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses a kind of new garlic nutrient salt and preparation method thereof, the main body of this new garlic nutrient salt is edible salt, simultaneously the garlic nutrient thing containing 0.1 30 wt%.Retain original special odor and nutriment of garlic in new garlic nutrient salt, edible effect of garlic, anti-curing oncoma, prevention diabetes, liver function protecting, preventing cold etc. are played while Cooking Seasoning.Raw material sheet as food, by it is nontoxic, safely, the pure biomass preparation method that has no side effect, retain garlic nutrient thing.Preparation is simple, and promotional value is very strong.
Description
Technical field
The invention belongs to salt field, more particularly to edible salt field, and in particular to a kind of new garlic nutrient salt and its system
Preparation Method.
Background technology
Salt with " kings of hundred tastes " laudatory title, is one of most important material of human survival, and it is not merely flavouring,
Material even more indispensable in body.Salt maintains the balance of the osmotic pressure of human body, and other psychological needs.Therefore, at present
Almost often meal will take food salt in our diet.Because system is without, the edible product salt of foreign countries and its abundant, various functions and
Purposes has the product salt of correlation, but, country's edible salt product category is relatively deficient at present, only purified salt, iodizedsalt, plus
Zinc salt, snow salt etc..State's inner salt changes and gradually advances, and in January, 2017 changes policy by salt is implemented, and decontrols salt market, salt market urgency
The product salt of various novelties need to be developed, for different crowd and demand, market is enriched.
Modern medicine study confirms, garlic integrates that kind more than 100 is medicinal and health-care components, wherein sulfur-bearing volatile matter 43
Kind, vulcanize sulfinic acid（Such as allicin）13 kinds of esters, 8 kinds of peptides, 9 kinds of amino acid, 12 kinds of glucoside, 11 kinds of enzyme.Garlic can also
Enhance metabolism, anti-curing oncoma, prevention diabetes, liver function protecting, preventing cold etc..Garlic nutrient thing is added into edible salt
In, while Cooking Seasoning, retain original peat-reek and nutriment of garlic, play edible effect of garlic.
There are the Variety salt product such as spirulina salt, alga iodine salt at present, but these salt product effects are relatively simple in China market,
It is limited for crowd.There is within 2015 patent report directly to bakee garlic during grinding adds salt, it is big during this patent system is standby
The nutriment of garlic is likely to be broken.A class nutriment allicin in tool document report garlic is through broken in Garlic cell
Afterwards, substance reaction is just obtained, and this is not specifically contemplated that in current disclosed patent.This is correctly recognized in this patent
A bit, process garlic with the method for science and obtain garlic nutrient thing, not only remain the peat-reek of garlic, and retain garlic
In effectively nutriment.
The content of the invention
The invention provides a kind of new garlic nutrient salt and preparation method thereof, this new garlic nutrient salt is in Cooking Seasoning
While, retain original peat-reek and nutriment of garlic, enhance metabolism, anti-curing oncoma, prevention diabetes, protection
Liver function, preventing cold etc..
The technical scheme that patent of the present invention is used is：The main component of described new garlic nutrient salt is salt and garlic
Nutrients, the content of the garlic nutrient thing is 0.1-30wt%.
The garlic nutrient thing is garlic powder or garlic nutrient extract；Garlic powder is the powder that garlic crushed after being dried is made
End, garlic nutrient extract is selected from garlic and is extracted through extraction method of squeezing the juice, crystallisation, microwave extraction method, ultrasonic extraction, solution
One or more preparation method is carried in method, leaching centrifugal process, ferment treatment method, super critical extraction, fermentation method, freeze-drying etc.
The garlic nutrient extract for taking.
The garlic nutrient thing is allicin, and the content of allicin is 0.1-3 wt%.
Described new garlic nutrient salt also contains anticaking agent, and the content of anticaking agent is 0.0001-0.005wt%；Anticaking agent
Selected from one or more in ferric citrate, potassium ferrocyanide, sodium ferrocyanide, tartaric acid iron, silica, calcium silicates.
The salt is that the propiodal of the iodizedsalt is that edible inorganic iodide or rich iodine are organic without salt compounded of iodine or iodizedsalt
Propiodal.
One or more be chosen in sea salt, lake salt, well salt, rock salt or lake salt of the salt, chlorine in the salt
The purity for changing sodium is more than 98%, and particle diameter is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain.
Be chosen for crude salt, refined salt or the various micro- or nutrition of addition, the extraordinary of flavor substance of the salt are eaten
One or more in salt, the purity of the Sodium Chloride in Salt is more than 98%, and particle diameter is 0.07 ~ 1.0 mm, whiteness is 55% ~
95% microcrystal grain.
The preparation method of described new garlic nutrient salt is mechanical mixing or condensing crystallizing method.
Described mechanical mixing comprises the following steps：To addition garlic nutrient thing and anticaking agent in salt（Herein can be with
Selection is without anticaking agent）, 50-60 DEG C is heated to after being well mixed, keep 10-12h to obtain garlic salt.
Condensing crystallizing method comprises the following steps：
1）Appropriate pure water is measured, after being heated to micro-boiling, salt is slowly added to, be configured to saturated aqueous solution, stirred in machinery
Mixing down makes all salinities fully dissolve；
2）By garlic nutrient thing and anticaking agent（If being not added with anticaking agent, unification is not added with following step）, delay under mechanical stirring
It is slow to add step 1）Prepared salt saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that garlic nutrient
Thing and anticaking agent are uniformly dispersed in salt saturated aqueous solution；
3）After garlic nutrient thing and anticaking agent are uniformly dispersed in salt saturated aqueous solution, continuing churned mechanically condition
Under, by the temperature control of mixed liquor 60 ~ 100oC, slowly steams moisture, by the concentration of garlic nutrient thing, anticaking agent and salt
Crystallization, 60 are placed in during to pasty stateoC~100 oResidual moisture is steamed in the air dry oven of C, block garlic salt is obtained；
4）To step 5）In the block garlic salt that obtains carry out pulverization process, obtain powdered garlic salt.
Containing garlic oil, alliin, allicin, enzyme, peptides, saponins, allicin, big in garlic nutrient extract
One or more in garlic powder etc..
Preferably, the salt is selected from any salt kind that sea salt, lake salt, well salt, rock salt, lake salt etc. have found；Also may be used
Selected from one or more in crude salt, refined salt or the various trace elements of addition or nutrition, the extraordinary salt of flavor substance；Also may be used
Selected from salt compounded of iodine（Propiodal can be the edible such as Potassiumiodate, KI inorganic iodide and the organic propiodal of rich iodine：As sea-tangle, marine alga,
In the extracts containing iodine containing iodine food such as undaria pinnitafida, seaweed, fresh hairtail, blood clam are dry, clam is dry, dried scallop, mussel, sea cucumber, jellyfish, lobster
One or several, use preceding first efflorescence to 60-200 mesh）, also selected from without salt compounded of iodine or Cardia Salt.Wherein sodium chloride is pure
It is more than 98% to spend, and particle diameter is 0.07-1.0 mm, and whiteness is 55%-95% microcrystal grains.
Preparation method：By each component according to dense after the interval directly mechanical mixing of aforementioned proportion, spraying method and dissolving
The methods such as sheepshank crystalline substance mixing method uniformly mix.Garlic nutrient thing is obtained by corresponding preparation method, wherein, work is extracted in control
Condition in skill flow, nutriment is lost in during garlic is reduced as far as possible.
Described mechanical mixing comprises the following steps：To garlic nutrient thing and anticaking agent is added in salt, it is well mixed
After be heated to 50-60 DEG C, keep 10-12h to obtain garlic salt.
Described condensing crystallizing method comprises the following steps：
1）Appropriate pure water is measured, after being heated to micro-boiling, salt is slowly added to, be configured to saturated aqueous solution, stirred in machinery
Mixing down makes all salinities fully dissolve；
2）By garlic nutrient thing and anticaking agent, step 1 is slowly added under mechanical stirring）Prepared salt saturated aqueous solution,
And continue to stir 0.5 more than h in slight boiling condition, it is ensured that garlic nutrient thing and anticaking agent disperse in salt saturated aqueous solution
It is even；
3）After garlic nutrient thing and anticaking agent are uniformly dispersed in salt saturated aqueous solution, continuing churned mechanically condition
Under, by the temperature control of mixed liquor 60 ~ 100oC, slowly steams moisture, by the concentration of garlic nutrient thing, anticaking agent and salt
Crystallization, 60 are placed in during to pasty stateoC~100 oResidual moisture is steamed in the air dry oven of C, block garlic salt is obtained；
4）To step 5）In the block garlic salt that obtains carry out pulverization process, obtain powdered garlic salt.
It is of the invention compared with existing edible salt, with advantages below：
Retain original special odor and nutriment of garlic in new garlic nutrient salt, garlic is played while Cooking Seasoning
Edible effect, anti-curing oncoma, prevention diabetes, liver function protecting, preventing cold etc..Raw material sheet as food, by nontoxic
It is harmless, safely, the pure biomass preparation technology that has no side effect, retain garlic nutrient thing.Preparation is simple, promotional value
It is very strong.
Specific embodiment
Technical scheme, but protection domain not limited to this are illustrated with specific embodiment below：
Embodiment 1
Prepared without iodine garlic salt using mechanical mixing in the present embodiment, comprised the following steps successively：
By garlic nutrient extract 5wt%, refined salt 95wt%（The raw material of refined salt is lake salt）.It is equal according to aforementioned proportion stirring mixing
It is even, 50 DEG C are heated to afterwards keeps 12h to can obtain garlic salt.
Wherein garlic nutrient extract is as follows through the preparation method of solution extraction：
（1）The water that the fresh garlic of certain mass adds 2 times is soaked into 1 h, is crushed garlic using disintegrating machine, by pasty state garlic
After tiling, it is placed in 40 DEG C of baking ovens and processes 40 min；
（2）To water and the mixture of ethanol that 1 times is added in pasty state garlic（Water：Ethanol is 5:1）, stir 20 min；
（3）Above-mentioned liquid/paste is filtered using 3 layers of filter clothes, and the filter cloth squeezing of filter residue will be wrapped with；Multiple times of filtration is simultaneously pressed
Squeeze, be finally recovered filtrate and filter residue, collect filtrate；
（4）To the sodium alginate that filtrate quality 2% is added in filtrate, stirring and dissolving is uniform；The first of filtrate quality 2% is added afterwards
Shell amine, stirs 10 min, after uniform generation precipitation, then stands 20 min, and sediment is separated by filtration；
（5）Above-mentioned filtrate is fitted into clean container and is heated, carry out vacuum distillation, 5% to proper mass can stop；Will distillation
Thing takes out and dries at 60 DEG C in an oven, and to moisture less than 1%, grind into powder is to obtain garlic nutrient extract.
In this preparation method, the principle active components, wherein garlic such as alliin, enzyme, peptides, allicin are contained in extract
The recovery rate of propylhomoserin is 4.55g/kg garlics, the recovery rate of enzyme is 1.48g/kg garlics, the recovery rate of peptides is 0.89g/kg
Garlic, the recovery rate of allicin are 2.08g/kg garlics.
Embodiment 2
Prepared plus iodine garlic salt using mechanical mixing in the present embodiment, comprised the following steps successively：
By garlic nutrient extract 10wt%, ferric citrate 0.0015wt%, balance of iodizedsalt（Propiodal is edible inorganic iodine
Compound, the raw material of salt is selected from lake salt）, it is uniformly mixed according to aforementioned proportion, keep 11h at 55 DEG C afterwards.
Wherein garlic nutrient extract is as follows through the preparation method of enzymatic isolation method：
（1）Preliminary treatment garlic：Select high-quality garlic to be rinsed well with clear water, Li Xiashui is pulled out with screen cloth, smashing is used afterwards
Machine crushes garlic, is placed in 50 DEG C of baking ovens and processes 30 min；
（2）Ferment treatment garlic：To cellulase, pectase is added in above-mentioned treated garlic, the addition of enzyme is gross mass
2%, the min of stir process 60 at a temperature of 40 DEG C；
（3）Neutralisation treatment liquid：Take during NaOH that concentration is 1 mol/L adds above-mentioned pickling agent, it is stirring while adding, frequently
With the acid-base value of pH test paper test processes liquid, until for neutrality does not add NaOH；
（4）Dry：Above-mentioned treatment fluid is filtered in vacuum filter, filtered fluid is collected.Filtrate is placed in into cryogenic vacuum to do
Dried in dry machine, it is ensured that nutriment is not destroyed, and obtains final product garlic nutrient extract.
In this preparation method, the principle active components, wherein alliin such as alliin, enzyme, allicin are contained in extract
Recovery rate for 5.16g/kg garlics, enzyme recovery rate for 1.88g/kg garlics, allicin recovery rate for 2.21g/kg it is big
Garlic.
Embodiment 3
Prepared plus iodine garlic salt using mechanical mixing in the present embodiment, comprised the following steps successively：
By garlic nutrient extract 15wt%, tartaric acid iron 0.001wt%, balance of iodizedsalt（Propiodal is the organic propiodal of rich iodine, salt
Raw material be selected from rock salt）, it is well mixed according to aforementioned proportion sprinkling, keep 10h at 60 DEG C afterwards.
Wherein garlic nutrient extract is as follows through the preparation method of super critical extraction：
（1）Garlic is cleaned up, and is completely dried, make its moisture less than 5%, use pulverizer, bruisher or powder beater
Crush, grind garlic；
（2）In weighing the extractor in the garlic powder input means of supercritical extraction equipment of certain mass, while adding 4 times of volumes
80% ethanol entrainer, soaks 12 h at ambient temperature.When carrying out supercritical extract, extracting pressure is fixed as 30 M Pa, two
Carbonoxide flow velocity keeps 12 L/h constant, and separating still temperature is 75 DEG C, and pressure is 6.2 M Pa；
（3）Product in separator is taken out, that is, obtains garlic nutrient extract；
In this preparation method, containing principle active components such as alliin, allicins in extract, the recovery rate of wherein alliin is
6.22g/kg garlics, the recovery rate of allicin are 5.63g/kg garlics.
Embodiment 4
Using mixing method preparation is sprayed without iodine garlic salt in the present embodiment, comprise the following steps successively：
By garlic nutrient extract 12wt%, tartaric acid iron 0.0015wt%, balance of sea salt, sprayed according to aforementioned proportion and mixed,
Afterwards 10h is kept at 50 DEG C.
Wherein garlic nutrient extract is as follows through the preparation method of microwave extraction method：
（1）Certain mass is dried or fresh garlic is rinsed well with water, be ground into using pulverizer, bruisher or powder beater
Pasty state, is placed in 45 DEG C of baking ovens and processes 50 min；
（2）To water and the mixture of ethanol that 2 times are added in pasty liquid（Water：Ethanol is 5:1）, it is fitted into ceramic vessel（Container
Material can be used in micro-wave oven）, after 30 min of stirring, it is put into the min of microwave treatment 50 in micro-wave oven；
（3）Above-mentioned liquid/paste is filtered with 2 layers of filter clothes, and the filter cloth squeezing of filter residue will be wrapped with；Multiple times of filtration is simultaneously squeezed,
Filtrate and filter residue are finally recovered, filtrate is collected；
（4）Filtrate is fitted into clean container and is heated, carry out vacuum distillation, 5% to proper mass can stop；It is drawn off simultaneously
Grind into powder is to obtain garlic nutrient extract after drying at 70 DEG C in an oven.
In this preparation method, the principle active components, wherein garlic such as alliin, enzyme, peptides, allicin are contained in extract
The recovery rate of propylhomoserin is 4.18g/kg garlics, the recovery rate of enzyme is 0.84g/kg garlics, the recovery rate of peptides is 0.56g/kg
Garlic, the recovery rate of allicin are 5.26g/kg garlics.
Embodiment 5
Using mixing method preparation is sprayed without iodine garlic salt in the present embodiment, comprise the following steps successively：
By allicin 0.1wt%, silica 0.0015wt%, lake salt 50wt%, balance of well salt, mixed according to aforementioned proportion sprinkling
Close uniform, keep 11h at 55 DEG C afterwards.
Wherein allicin is as follows through leaching the preparation method of centrifugal process：
（1）The fresh garlic of certain mass is rinsed well with water, pasty state is ground into using pulverizer, bruisher or powder beater,
It is placed in 40 DEG C of baking ovens and processes 50 min；
（2）To water and the mixture of ethanol that 15 times are added in pasty liquid（Water：Ethanol is 4:1）, load clean sealing with cover
In container, after 0.5 h of stirring, 1 h is stood, after 0.5 h is stirred for afterwards, stand 3 h；
（3）After the cover open of sealing container, container is heated, the liquid/paste heated while stirring in container boils 20
Stop heating after min；
（4）Above-mentioned liquid/paste is filtered with 4 layers of filter clothes, and the filter cloth squeezing of filter residue will be wrapped with；Multiple times of filtration is simultaneously squeezed,
Filtrate and filter residue are finally recovered, filtrate is collected；
（5）Filtrate is centrifuged 5 min under 5000 rpm/min, supernatant is taken, supernatant is fitted into clean container and is heated to
80 DEG C, vacuum distillation is carried out, 5% to proper mass can stop；It is drawn off and is pulverized after drying at 50 DEG C in an oven
End obtains garlic nutrient extract, and separating-purifying obtains allicin from garlic nutrient extract.
In this preparation method, the principle active components, wherein garlic such as alliin, enzyme, peptides, allicin are contained in extract
The recovery rate of propylhomoserin is 8.66g/kg garlics, the recovery rate of enzyme is 2.08g/kg garlics, the recovery rate of peptides is 1.06g/kg
Garlic, the recovery rate of allicin are 10.32g/kg garlics.
Embodiment 6
Using mixing method preparation is sprayed without iodine garlic salt in the present embodiment, comprise the following steps successively：
By allicin 3wt%, silica 0.0015wt%, the sea salt of 60 wt%, balance of lake salt, mixed according to aforementioned proportion sprinkling
Close uniform, keep 10h at 60 DEG C afterwards.
The preparation method of the wherein crystallized method of allicin is as follows：
（1）The garlic of certain mass is rinsed well with water, pasty state is ground into using pulverizer, bruisher or powder beater, be placed in
40 min are processed in 50 DEG C of baking ovens.The water of 2 times of volume and the mixture of ethanol are added thereto to again（Water：Ethanol is 2-4:1）, leaching
1 h is steeped, after being heated to 100 DEG C, continues to soak 3 h；
（2）Soak is with 4 layers of filter-cloth filtering；
（3）Filtrate is centrifuged 5 min under 5000 rpm/min, supernatant is taken, by supernatant at 90 DEG C, vacuum distillation is carried out,
To the 5% of proper mass；
（4）It is drawn off and drying crystalline at 55 DEG C in an oven, grind into powder is to obtain garlic nutrient extract.
In this preparation method, the principle active components, wherein garlic such as alliin, enzyme, peptides, allicin are contained in extract
The recovery rate of propylhomoserin is 6.52g/kg garlics, the recovery rate of enzyme is 2.58g/kg garlics, the recovery rate of enzyme is 0.97g/kg
Garlic, the recovery rate of allicin are 8.29g/kg garlics.
Embodiment 7
Prepared without iodine garlic salt using mechanical mixing in the present embodiment, comprised the following steps successively：
By allicin 2wt%, calcium silicates 0.0008wt%, balance of crude salt（Crude salt comes from well salt）, it is mixed according to aforementioned proportion stirring
Close uniform, keep 11h to obtain garlic salt at 55 DEG C.
Wherein the enzyme treated method of allicin, the preparation method of freeze-drying are as follows：
（1）The garlic of certain mass is rinsed well with water, after unnecessary water is leached, pulverizer, bruisher or powder beater is used
Pasty state is ground into, is placed in 55 DEG C of baking ovens and is processed 30 min；
（2）The garlic pastel of certain mass is weighed, 2 times of water is added, the compound protease of quality 1% is added（Cellulase and
The mass ratio of pectase is 1:2）, plus concentration adjusted to optimal pH for 1 mol/L hydrochloric acid, the h of stirring reaction 2 after being warming up to 40 DEG C,
100 DEG C are heated afterwards to seething with excitement, 25 more than min are kept, and inactivate enzyme；
（3）By sterilized filtering fermentation liquor, filtrate is collected, step-down distillation makes filtrate volume reduce to the 5% of original volume,
Collected and be put into dry, grinding in freeze drier, that is, obtained garlic nutrient extract, garlic nutrient extract separated and is carried
It is pure to obtain allicin；
In this preparation method, in extract containing the principle active component such as alliin, enzyme, allicin, wherein alliin is carried
Take rate for 5.86g/kg garlics, enzyme recovery rate for 2.98g/kg garlics, allicin recovery rate be 12.21g/kg garlics.
Embodiment 8
Prepared without iodine garlic salt using mechanical mixing in the present embodiment, comprised the following steps successively：
By garlic nutrient extract 5wt%, potassium ferrocyanide 0.0006wt%, balance of lake salt, stirred according to aforementioned proportion and mixed
It is uniform to keep 10h at 60 DEG C, obtain garlic salt.
Wherein allicin is as follows through the preparation method of solution extraction, leaching centrifugal process：
（1）The water that the fresh garlic of certain mass adds 1 times is soaked into 1 h, is crushed garlic using disintegrating machine, by pasty state garlic
After tiling, it is placed in 50 DEG C of baking ovens and processes 20 min；
（2）To water and the mixture of ethanol that 1 times is added in pasty state garlic（Water：Ethanol is 5:1）, stir 10 min.
（3）Above-mentioned liquid/paste is filtered using the filter cloth of layer 2-4, and the filter cloth squeezing of filter residue will be wrapped with；Multiple mistake
Filter and squeeze, be finally recovered filtrate and filter residue, collect filtrate；
（4）By the filtering of above-mentioned treatment fluid, filtrate is collected, filtrate is centrifuged 10 min under 5500 rpm/min, take supernatant, will
Supernatant is heated to 85 DEG C in being fitted into clean container, carries out vacuum distillation, and 5% to proper mass can stop；Be drawn off and
Grind into powder is to obtain garlic nutrient extract after being dried at 65 DEG C in baking oven；
In this preparation method, the principle active components, wherein alliin such as alliin, enzyme, peptides, allicin are contained in extract
Recovery rate for 9.11g/kg garlics, enzyme recovery rate for 2.68g/kg garlics, peptides recovery rate for 1.52g/kg garlics,
The recovery rate of allicin is 14.29g/kg garlics.
Embodiment 9
Prepared without iodine garlic salt using mechanical mixing in the present embodiment, comprised the following steps successively：
By garlic nutrient extract 7wt%, silica 0.0006wt%, balance of rock salt, mix equal according to aforementioned proportion stirring
It is even, 12h is kept at 50 DEG C, obtain garlic salt.
Wherein the enzyme treated method of garlic nutrient extract, the preparation method of fermentation method are as follows：
（1）The garlic of certain mass is rinsed well with water, after unnecessary water is leached, using pulverizer, bruisher, powder beater,
Sander etc. is crushed；
（2）The garlic pasty state of certain mass is weighed, 2 times of water is added, the cellulase of quality 0.02%, plus hydrochloric acid regulation is added
PH is 6-6.5, the h of stirring reaction 3 after being warming up to 35-55 DEG C, and 100 DEG C are heated afterwards to seething with excitement, and keeps 20 more than min, makes enzyme
Inactivation；
（3）After above-mentioned treatment fluid is down into room temperature, the glucose of gross mass 5% is added, add the bright beading of butterfat of quality 1.5%
Bacterium, after 10 h of fermentation, plus concentration is that 1 mol/L NaOH regulations pH is neutralized, and sterilize 25 more than min at 121 DEG C of HTHP；
（4）By sterilized filtering fermentation liquor, filtrate is collected, step-down distillation makes filtrate volume reduce to the 5% of original volume,
Collected and be put into dry, grinding in baking oven, that is, obtained garlic nutrient extract.
In this preparation method, the principle active components, wherein alliin such as alliin, enzyme, allicin are contained in extract
Recovery rate for 3.89g/kg garlics, enzyme recovery rate for 0.91g/kg garlics, allicin recovery rate for 9.18g/kg it is big
Garlic.
Embodiment 10
Prepared without iodine garlic salt using mechanical mixing in the present embodiment, comprised the following steps successively：
By garlic nutrient extract 22wt%, calcium silicates 0.0006wt%, balance of refined salt（Refined salt is with lake salt as raw material）, according to upper
The ratio of stating is uniformly mixed, and it is that can obtain garlic salt to keep 12h at 50 DEG C afterwards.
Wherein the freeze-dried method of garlic nutrient extract, the preparation method of ultrasonic extraction are as follows：
（1）The garlic peeling of certain mass is rinsed well with water, after unnecessary water is leached, using pulverizer, bruisher, powder is beaten
Machine, sander etc. are ground into pasty state；
（2）After pasty state freeze-drying, flour mill is made garlic powder；
（3）To water and the mixture of ethanol that 1.5 times are added in garlic powder（Water：Ethanol is 2:1）, load clean sealing with cover
In container, after 10 min of stirring, it is fitted into container, container is placed in ultrasonic 2 h in ultrasonic instrument；
（4）By the filtering of above-mentioned treatment fluid, filtrate is collected, filtrate is fitted into 70 DEG C are heated in clean container, carry out vacuum distillation,
To proper mass 5% can stop；It is drawn off and drying crystalline at 70 DEG C in an oven, grind into powder is to obtain garlic battalion
Support extract；
In this preparation method, in extract containing the principle active component such as alliin, enzyme, allicin, wherein alliin is carried
Take rate for 5.35g/kg garlics, enzyme recovery rate for 3.21g/kg garlics, allicin recovery rate be 1.86g/kg garlics.
Embodiment 11
Prepared without iodine garlic salt using mechanical mixing in the present embodiment, comprised the following steps successively：
By garlic nutrient extract 30wt%, potassium ferrocyanide 0.0006wt%, balance of addition selenium extraordinary salt（Extraordinary salt
Raw material be lake salt）, it is uniformly mixed according to aforementioned proportion, it is that can obtain garlic salt to keep 10h at 60 DEG C.
Wherein the freeze-dried method of garlic nutrient extract, the preparation method of solution extraction are as follows：
（1）The garlic peeling of certain mass is rinsed well with water, after unnecessary water is leached, using pulverizer, bruisher, powder is beaten
Machine, sander etc. are ground into pasty state, after pasty state garlic is tiled, are placed in 55 DEG C of baking ovens and process 35min；
（2）After pasty state freeze-drying, flour mill is made garlic powder；
（3）To water and the mixture of ethanol that 1 times is added in garlic powder（Water：Ethanol is 4:1）, stir 20 min；
（4）Above-mentioned liquid/paste is filtered using the filter cloth of layer 2-4, and the filter cloth squeezing of filter residue will be wrapped with；Multiple times of filtration is simultaneously
Squeezing, is finally recovered filtrate and filter residue, collects filtrate；
（5）By the filtering of above-mentioned treatment fluid, filtrate is collected, filtrate is centrifuged 10 min under 5500 rpm/min, take supernatant, will
Supernatant is heated to 80 DEG C in being fitted into clean container, carries out vacuum distillation, and 5% to proper mass can stop；Be drawn off and
Grind into powder is to obtain garlic nutrient extract after being dried at 60 DEG C in baking oven.
In this preparation method, the principle active components, wherein alliin such as alliin, enzyme, allicin are contained in extract
Recovery rate for 4.21g/kg garlics, enzyme recovery rate for 2.08g/kg garlics, allicin recovery rate for 4.74g/kg it is big
Garlic.
Embodiment 12
By garlic powder 22wt%, potassium ferrocyanide 0.0008wt%, balance of addition zinc extraordinary salt（The raw material of extraordinary salt is
Lake salt）.It is uniformly mixed according to aforementioned proportion, it is that can obtain garlic salt to keep 12h at 50 DEG C.
The preparation method of the wherein freeze-dried method of garlic powder is as follows：
（1）The garlic peeling of certain mass is rinsed well with water, after unnecessary water is leached, using pulverizer, bruisher, powder is beaten
Machine, sander etc. are ground into pasty state；
（2）It is placed in 55 DEG C of baking ovens and processes 40 min, after pasty state freeze-drying, flour mill is made garlic powder；
（3）Certain mass is taken without iodine edible salt, will be laid in without iodine edible salt in drying pallet, by the garlic powder with certain
Speed is uniformly sprayed at without on iodine edible salt, being heated to 50 DEG C to pallet and being kept for 12 hours, and one kind is obtained after fully drying
Garlic salt.
Embodiment 13
By garlic nutrient extract 20wt%, potassium ferrocyanide 0.001wt%, balance of Cardia Salt（The raw material of Cardia Salt is lake
Salt）, it is uniformly mixed according to aforementioned proportion, it is that can obtain garlic salt to keep 12h at 60 DEG C.
Wherein garlic nutrient extract is as follows through the preparation method of extraction method of squeezing the juice：
（1）Fresh garlic peeling is cleaned up, the garlic juice in garlic is squeezed out by oil press, be placed in 50 DEG C of baking ovens and locate
Manage 50 min；
（2）By garlic juice obtained above filtering, solid residue is leached, reclaim filtrate；
（3）The filtrate for obtaining will be reclaimed and descend drying under proper condition, then spontaneous nucleation is ground to 20-2000 mesh, obtained final product big
Garlic nutrition extraction of substance；
In this preparation method, in extract containing the principle active component such as alliin, enzyme, allicin, wherein alliin is carried
Take rate for 2.16g/kg garlics, enzyme recovery rate for 1.08g/kg garlics, allicin recovery rate be 1.51g/kg garlics.
Embodiment 14
The raw material of garlic salt is prepared according to following percentage by weight：It is garlic oil 10wt%, potassium ferrocyanide 0.0005wt%, balance of
Lake salt.
Certain mass Exposure to Sunlight salt compounded of iodine is taken by above-mentioned formula, Exposure to Sunlight salt compounded of iodine is laid in drying pallet, by the garlic oil
Uniformly it is sprayed on Exposure to Sunlight salt compounded of iodine with certain speed, 50 DEG C is heated to pallet and is kept for 12 hours, is obtained final product after fully drying
To a kind of garlic salt.Wherein garlic oil preparation process reference implementation example 13.
Embodiment 15
The raw material of garlic salt is prepared according to following weight percentage：It is garlic powder 15wt%, potassium ferrocyanide 0.0005wt%, balance of
Refined salt（The raw material of refined salt is sea salt）.
The preparation method of the wherein freeze-dried method of garlic powder is as follows：
（1）The garlic peeling of certain mass is rinsed well with water, unnecessary water is leached；
（2）It is placed in 50 DEG C of baking ovens and processes 50 min, reuses freeze drier by garlic freeze-drying；
（3）Dried garlic crushes powdering using pulverizer, bruisher, powder beater, sander etc., that is, obtain garlic powder；
（4）By garlic powder and crushing washing salt compounded of iodine, direct mechanical mixture is uniform according to the above ratio, that is, obtain a kind of garlic salt.
Embodiment 16
It is uniformly mixed, allicin 3wt%, potassium ferrocyanide 0.0005wt%, balance of lake salt 60 according to aforementioned proportion
DEG C keep 12h be that can obtain garlic salt.
The preparation concrete technology flow process of wherein allicin is shown in embodiment 1.
Embodiment 17
By allicin 2wt%, potassium ferrocyanide 0.0005wt%, 40 wt% lake salt, balance of rock salt, stirred according to aforementioned proportion
Well mixed, it is that can obtain garlic salt that 12h is kept at 60 DEG C afterwards.
The preparation concrete technology flow process of wherein allicin is shown in embodiment 2.
Embodiment 18
It is uniformly mixed, alliin 4wt%, potassium ferrocyanide 0.0008wt%, balance of lake salt 60 according to aforementioned proportion
It is that can obtain garlic salt that 12h is kept at DEG C.
The preparation concrete technology flow process of wherein alliin is shown in embodiment 5.
Embodiment 19
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps.
1）By the allicin of content >=90% 60o12 hours are dried under C, then control moisture grind 2% ~ 20%
It is standby to 60 mesh；
2）Weigh 10000 parts of salt（It is made up as raw material of sea salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 0.01 part of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains
It is powdered without iodine garlic salt.
Embodiment 20
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 70o11 hours are dried under C, then control moisture be ground to 100 2% ~ 20%
Mesh, it is standby；
2）Weigh 10000 parts of salt（It is made up as raw material of lake salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 0.01 part of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains
It is powdered without iodine garlic salt；
4）To step 3）In obtain it is powdered be quantitatively molded without iodine garlic salt or sample packing, obtain surely gauged big without iodine
Garlic salt.
The calibration being prepared from the present embodiment is quantitative without iodine garlic salt, can be according to different crowd to allicin and salt
Demand quantitatively used, being capable of the daily usage amount of easy control.
Embodiment 21
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 80o10 hours are dried under C, then control moisture be ground to 120 2% ~ 20%
Mesh, it is standby；
2）Weigh 10000 parts of salt（It is made up as raw material of well salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 0.01 part of allicin, step 3 is slowly added under mechanical stirring）Prepared salt
Saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin disperses in salt saturated aqueous solution
It is even；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 60oC, slowly steams moisture, by allicin and salt condensing crystallizing, 60 is placed in during to pasty stateoThe air blast of C is done
Residual moisture is steamed in dry case, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk carry out pulverization process without iodine garlic salt, obtain powdered without iodine garlic salt.
The present embodiment is obtained to be obtained without iodine garlic salt using condensing crystallizing method so that allicin can be scattered in sodium chloride
Inside particle so that both are scattered more uniform, can greatly reduce because of the uneven usage amount error brought of dispersion.
Embodiment 22
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 90o9 hours are dried under C, then control moisture be ground to 150 2% ~ 20%
Mesh, it is standby；
2）Weigh 10000 parts of salt（It is made up as raw material of rock salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 0.01 part of allicin, step 3 is slowly added under mechanical stirring）Prepared salt
Saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin disperses in salt saturated aqueous solution
It is even；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 70oC, slowly steams moisture, by allicin and salt condensing crystallizing, 80 is placed in during to pasty stateoThe air blast of C is done
Residual moisture is steamed in dry case, block plus iodine garlic salt product are obtained, wherein propiodal is the extract containing iodine of sea-tangle；
6）To step 5）In the bulk that obtains plus iodine garlic salt, quantitative screening is carried out according to block size, obtain calibration it is quantitative plus
Iodine garlic salt.Or after crushing is for the powdery product of 60 ~ 200 mesh, according to the step 4 in embodiment 2）Carry out quantitative shaping
Or sample packing, obtain surely gauged plus iodine garlic salt.
Embodiment 23
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 100o8 hours are dried under C, then control moisture be ground to 200 2% ~ 20%
Mesh, it is standby；
2）Weigh 10000 parts of salt（It is made up as raw material of lake salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 0.05 part of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains
It is powdered without iodine garlic salt.
Embodiment 24
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 110o7 hours are dried under C, then control moisture be ground to 60 2% ~ 20%
Mesh, it is standby；
2）Weigh 10000 parts of salt（It is made up as raw material of crude salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 0.05 part of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains
It is powdered without iodine garlic salt；
4）To step 3）In obtain it is powdered be quantitatively molded without iodine garlic salt or sample packing, obtain surely gauged big without iodine
Garlic salt.
The calibration being prepared from the present embodiment is quantitative without iodine garlic salt, can be according to different crowd to allicin and salt
Demand quantitatively used, being capable of the daily usage amount of easy control.
Embodiment 25
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 120o6 hours are dried under C, then control moisture be ground to 70 2% ~ 20%
Mesh, it is standby；
2）Weigh 10000 parts of salt（It is made up as raw material of refined salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 0.05 part of allicin, step 3 is slowly added under mechanical stirring）Prepared salt
Saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin disperses in salt saturated aqueous solution
It is even；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 60oC, slowly steams moisture, by allicin and salt condensing crystallizing, 90 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk carry out pulverization process without iodine garlic salt, obtain powdered without iodine garlic salt.
The present embodiment is obtained to be obtained without iodine garlic salt using condensing crystallizing method so that allicin can be scattered in sodium chloride
Inside particle so that both are scattered more uniform, can greatly reduce because of the uneven usage amount error brought of dispersion.
Embodiment 26
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 130o5 hours are dried under C, then control moisture be ground to 60 2% ~ 20%
Mesh, it is standby；
2）Weigh 10000 parts of salt（The extraordinary salt of selenium is added, the raw material of extraordinary salt is lake salt）, wherein sodium chloride is pure
It is more than 98% to spend, and particle diameter is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 0.05 part of allicin, step 3 is slowly added under mechanical stirring）Prepared salt
Saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin disperses in salt saturated aqueous solution
It is even；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 100oC, slowly steams moisture, by allicin and salt condensing crystallizing, 60 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk without iodine garlic salt, quantitative screening is carried out according to block size, obtain calibrating quantitative nothing
Iodine garlic salt.Or after crushing is for the powdery product of 60 ~ 200 mesh, according to the step 4 in embodiment 2）Carry out quantitative shaping
Or sample packing, obtain surely gauged without iodine garlic salt.
Embodiment 27
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 150o4 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 10000 parts of salt（The extraordinary salt of zinc is added, the raw material of extraordinary salt is lake salt）, wherein sodium chloride is pure
It is more than 98% to spend, and particle diameter is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 0.1 part of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains
It is powdered without iodine garlic salt.
Embodiment 28
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 150o4 hours are dried under C, then control moisture be ground to 120 2% ~ 20%
Mesh, it is standby；
2）Weigh 10000 parts of salt（The extraordinary salt of iron is added, the raw material of extraordinary salt is well salt）, wherein sodium chloride is pure
It is more than 98% to spend, and particle diameter is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 0.1 part of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains
It is powdered without iodine garlic salt；
4）To step 3）In obtain it is powdered be quantitatively molded without iodine garlic salt or sample packing, obtain surely gauged big without iodine
Garlic salt.
The calibration being prepared from the present embodiment is quantitative without iodine garlic salt, can be according to different crowd to allicin and salt
Demand quantitatively used, being capable of the daily usage amount of easy control.
Embodiment 29
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 60o11 hours are dried under C, then control moisture be ground to 150 2% ~ 20%
Mesh, it is standby；
2）Weigh 10000 parts（The extraordinary salt of calcium is added, the raw material of extraordinary salt is lake salt）, the purity of wherein sodium chloride is
More than 98%, particle diameter is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 0.1 part of allicin, step 3 is slowly added under mechanical stirring）Prepared salt
Saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin disperses in salt saturated aqueous solution
It is even；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 70oC, slowly steams moisture, by allicin and salt condensing crystallizing, 90 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk carry out pulverization process without iodine garlic salt, obtain powdered without iodine garlic salt.
The present embodiment is obtained to be obtained without iodine garlic salt using condensing crystallizing method so that allicin can be scattered in sodium chloride
Inside particle so that both are scattered more uniform, can greatly reduce because of the uneven usage amount error brought of dispersion.
Embodiment 30
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 120o6 hours are dried under C, then control moisture be ground to 160 2% ~ 20%
Mesh, it is standby；
2）Weigh 10000 parts of salt（It is made up as raw material of 50% sea salt and 50% lake salt）, the wherein purity of sodium chloride
It is more than 98%, particle diameter is 0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 0.1 part of allicin, step 3 is slowly added under mechanical stirring）Prepared salt
Saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin disperses in salt saturated aqueous solution
It is even；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 60 ~ 100oC, slowly steams moisture, by allicin and salt condensing crystallizing, 60 is placed in during to pasty stateoC~
100 oResidual moisture is steamed in the air dry oven of C, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk without iodine garlic salt, quantitative screening is carried out according to block size, obtain calibrating quantitative nothing
Iodine garlic salt.Or after crushing is for the powdery product of 60 ~ 200 mesh, according to the step 4 in embodiment 2）Carry out quantitative shaping
Or sample packing, obtain surely gauged without iodine garlic salt.
Embodiment 31
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 110o8 hours are dried under C, then control moisture be ground to 60- 2% ~ 20%
80 mesh, it is standby；
2）Weigh 10000 parts of salt（It is made up as raw material of 60% well salt and 40% rock salt）, the wherein purity of sodium chloride
It is more than 98%, particle diameter is 0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 0.3 part of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains
It is powdered without iodine garlic salt.
Embodiment 32
The preparation technology of iodine garlic salt is added in turn include the following steps in the present embodiment.
1）By the allicin of content >=90% 70o12 hours are dried under C, then control moisture grind 2% ~ 10%
It is standby to 80 ~ 100 mesh；
2）Weigh 10000 parts of salt（It is made up as raw material of 30% sea salt, 50% lake salt and 20% rock salt）, wherein chlorine
The purity for changing sodium is more than 98%, and particle diameter is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 0.3 part of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains
Powdered plus iodine garlic salt, wherein propiodal is edible inorganic iodide；
4）To step 3）In obtain powdered plus iodine garlic salt be quantitatively molded or sample packing, obtain surely gauged plus iodine big
Garlic salt.
The calibration being prepared from the present embodiment quantitatively adds iodine garlic salt, can be according to different crowd to allicin and salt
Demand quantitatively used, being capable of the daily usage amount of easy control.
Embodiment 33
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 130o6 hours are dried under C, then control moisture be ground to 10% ~ 20%
150 mesh, it is standby；
2）Weigh 10000 parts of salt（60% crude salt and 40% plus calcium special type salt, the raw material of crude salt and extraordinary salt is pond
Salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 0.3 part of allicin, step 3 is slowly added under mechanical stirring）Prepared salt
Saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin disperses in salt saturated aqueous solution
It is even；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 100oC, slowly steams moisture, by allicin and salt condensing crystallizing, 60 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk carry out pulverization process without iodine garlic salt, obtain powdered without iodine garlic salt.
The present embodiment is obtained to be obtained without iodine garlic salt using condensing crystallizing method so that allicin can be scattered in sodium chloride
Inside particle so that both are scattered more uniform, can greatly reduce because of the uneven usage amount error brought of dispersion.
Embodiment 34
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 60o12 hours are dried under C, then control moisture be ground to 15% ~ 20%
150 ~ 200 mesh, it is standby；
2）Weigh 10000 parts of salt（It is with the raw material of extraordinary salt by 30% refined salt and 70% add selenium special type salt, crude salt
Lake salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 0.3 part of allicin, step 3 is slowly added under mechanical stirring）Prepared salt
Saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin disperses in salt saturated aqueous solution
It is even；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 70oC, slowly steams moisture, by allicin and salt condensing crystallizing, 90 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk without iodine garlic salt, quantitative screening is carried out according to block size, obtain calibrating quantitative nothing
Iodine garlic salt.Or after crushing is for the powdery product of 60 ~ 200 mesh, according to the step 4 in embodiment 2）Carry out quantitative shaping
Or sample packing, obtain surely gauged without iodine garlic salt.
Embodiment 35
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 70o11 hours are dried under C, control moisture 2% ~ 10%, be then ground to 60 ~
100 mesh, it is standby；
2）Weigh 10000 parts of salt（It is made up as raw material of 60% crude salt and 40% refined salt, the raw material of crude salt and refined salt is
Lake salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 0.7 part of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains
It is powdered without iodine garlic salt.
Embodiment 36
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 80o9 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 10000 parts of salt（By 70% plus calcium special type salt and 30% addition vitamin B2 extraordinary salt as original
Material is made, and the raw material of extraordinary salt is sea salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is 0.07 ~ 1.0 mm, whiteness
It is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 0.7 part of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains
It is powdered without iodine garlic salt；
4）To step 3）In obtain it is powdered be quantitatively molded without iodine garlic salt or sample packing, obtain surely gauged big without iodine
Garlic salt.
The calibration being prepared from the present embodiment is quantitative without iodine garlic salt, can be according to different crowd to allicin and salt
Demand quantitatively used, being capable of the daily usage amount of easy control.
Embodiment 37
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 135o8 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 10000 parts of salt（It is made up as raw material of sea salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 0.7 part of allicin, step 3 is slowly added under mechanical stirring）Prepared salt
Saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin disperses in salt saturated aqueous solution
It is even；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 60oC, slowly steams moisture, by allicin and salt condensing crystallizing, 90 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk carry out pulverization process without iodine garlic salt, obtain powdered without iodine garlic salt.
The present embodiment is obtained to be obtained without iodine garlic salt using condensing crystallizing method so that allicin can be scattered in sodium chloride
Inside particle so that both are scattered more uniform, can greatly reduce because of the uneven usage amount error brought of dispersion.
Embodiment 38
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 150o4 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 10000 parts of salt（It is made up as raw material of well salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 0.7 part of allicin, step 3 is slowly added under mechanical stirring）Prepared salt
Saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin disperses in salt saturated aqueous solution
It is even；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 85oC, slowly steams moisture, by allicin and salt condensing crystallizing, 95 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk without iodine garlic salt, quantitative screening is carried out according to block size, obtain calibrating quantitative nothing
Iodine garlic salt.Or after crushing is for the powdery product of 60 ~ 200 mesh, according to the step 4 in embodiment 2）Carry out quantitative shaping
Or sample packing, obtain surely gauged without iodine garlic salt.
Embodiment 39
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 60o11 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9999 parts of salt（Preventing decayed tooth salt, the raw material of preventing decayed tooth salt is rock salt）, the wherein purity of sodium chloride is more than 98%,
Particle diameter is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 1 part of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder
Last shape without iodine garlic salt.
Embodiment 40
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 80o10 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9999 parts of salt（It is made up as raw material of sea salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 1 part of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder
Last shape without iodine garlic salt；
4）To step 3）In obtain it is powdered be quantitatively molded without iodine garlic salt or sample packing, obtain surely gauged big without iodine
Garlic salt.
The calibration being prepared from the present embodiment is quantitative without iodine garlic salt, can be according to different crowd to allicin and salt
Demand quantitatively used, being capable of the daily usage amount of easy control.
Embodiment 41
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 120o8 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9999 parts of salt（It is made up as raw material of well salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 1 part of allicin, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied
And the aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin is uniformly dispersed in salt saturated aqueous solution；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 95oC, slowly steams moisture, by allicin and salt condensing crystallizing, 85 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk carry out pulverization process without iodine garlic salt, obtain powdered without iodine garlic salt.
The present embodiment is obtained to be obtained without iodine garlic salt using condensing crystallizing method so that allicin can be scattered in sodium chloride
Inside particle so that both are scattered more uniform, can greatly reduce because of the uneven usage amount error brought of dispersion.
Embodiment 42
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 85o12 hours are dried under C, control moisture 2% ~ 10%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9999 parts of salt（It is made up as raw material of lake salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 1 part of allicin, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied
And the aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin is uniformly dispersed in salt saturated aqueous solution；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 60oC, slowly steams moisture, by allicin and salt condensing crystallizing, 95 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk without iodine garlic salt, quantitative screening is carried out according to block size, obtain calibrating quantitative nothing
Iodine garlic salt.Or after crushing is for the powdery product of 60 ~ 200 mesh, according to the step 4 in embodiment 2）Carry out quantitative shaping
Or sample packing, obtain surely gauged without iodine garlic salt.
Embodiment 43
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 140oDried 5 hours under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9999 parts of salt（By adding iron special type salt, the raw material of extraordinary salt is well salt）, the wherein purity of sodium chloride
It is more than 98%, particle diameter is 0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 1.5 parts of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains
It is powdered without iodine garlic salt.
Embodiment 44
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 90o10 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9999 parts of salt（It is made up as raw material of rock salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 1.5 parts of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains
It is powdered without iodine garlic salt；
4）To step 3）In obtain it is powdered be quantitatively molded without iodine garlic salt or sample packing, obtain surely gauged big without iodine
Garlic salt.
The calibration being prepared from the present embodiment is quantitative without iodine garlic salt, can be according to different crowd to allicin and salt
Demand quantitatively used, being capable of the daily usage amount of easy control.
Embodiment 45
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 130o6 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9999 parts of salt（It is made up as raw material of crude salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 1.5 parts of allicin, step 3 is slowly added under mechanical stirring）Prepared salt
Saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin disperses in salt saturated aqueous solution
It is even；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 100oC, slowly steams moisture, by allicin and salt condensing crystallizing, 100 is placed in during to pasty stateoThe drum of C
Residual moisture is steamed in wind drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk carry out pulverization process without iodine garlic salt, obtain powdered without iodine garlic salt.
The present embodiment is obtained to be obtained without iodine garlic salt using condensing crystallizing method so that allicin can be scattered in sodium chloride
Inside particle so that both are scattered more uniform, can greatly reduce because of the uneven usage amount error brought of dispersion.
Embodiment 46
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 60o12 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9999 parts of salt（It is made up as raw material of refined salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 1.5 parts of allicin, step 3 is slowly added under mechanical stirring）Prepared salt
Saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin disperses in salt saturated aqueous solution
It is even；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 80oC, slowly steams moisture, by allicin and salt condensing crystallizing, 80 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk without iodine garlic salt, quantitative screening is carried out according to block size, obtain calibrating quantitative nothing
Iodine garlic salt.Or after crushing is for the powdery product of 60 ~ 200 mesh, according to the step 4 in embodiment 2）Carry out quantitative shaping
Or sample packing, obtain surely gauged without iodine garlic salt.
Embodiment 47
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 120o10 hours are dried under C, then control moisture be ground to 60 2% ~ 20%
~ 200 mesh, it is standby；
2）Weigh 9995 parts of salt（It is made up as raw material of lake salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 5 parts of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder
Last shape without iodine garlic salt.
Embodiment 48
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 80o12 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9995 parts of salt（It is made up as raw material of rock salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 5 parts of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder
Last shape without iodine garlic salt；
4）To step 3）In obtain it is powdered be quantitatively molded without iodine garlic salt or sample packing, obtain surely gauged big without iodine
Garlic salt.
The calibration being prepared from the present embodiment is quantitative without iodine garlic salt, can be according to different crowd to allicin and salt
Demand quantitatively used, being capable of the daily usage amount of easy control.
Embodiment 49
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 100o9 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9995 parts of salt（It is made up as raw material of lake salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 5 parts of allicin, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied
And the aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin is uniformly dispersed in salt saturated aqueous solution；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 80oC, slowly steams moisture, by allicin and salt condensing crystallizing, 70 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk carry out pulverization process without iodine garlic salt, obtain powdered without iodine garlic salt.
The present embodiment is obtained to be obtained without iodine garlic salt using condensing crystallizing method so that allicin can be scattered in sodium chloride
Inside particle so that both are scattered more uniform, can greatly reduce because of the uneven usage amount error brought of dispersion.
Embodiment 50
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 120o9 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9995 parts of salt（It is made up as raw material of lake salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 5 parts of allicin, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied
And the aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin is uniformly dispersed in salt saturated aqueous solution；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 90oC, slowly steams moisture, by allicin and salt condensing crystallizing, 80 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk without iodine garlic salt, quantitative screening is carried out according to block size, obtain calibrating quantitative nothing
Iodine garlic salt.Or after crushing is for the powdery product of 60 ~ 200 mesh, according to the step 4 in embodiment 2）Carry out quantitative shaping
Or sample packing, obtain surely gauged without iodine garlic salt.
Embodiment 51
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 90o10 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9990 parts of salt（It is made up as raw material of refined salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 10 parts of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder
Last shape without iodine garlic salt.
Embodiment 52
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 150o5 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9990 parts of salt（It is made up as raw material of sea salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 10 parts of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder
Last shape without iodine garlic salt；
4）To step 3）In obtain it is powdered be quantitatively molded without iodine garlic salt or sample packing, obtain surely gauged big without iodine
Garlic salt.
The calibration being prepared from the present embodiment is quantitative without iodine garlic salt, can be according to different crowd to allicin and salt
Demand quantitatively used, being capable of the daily usage amount of easy control.
Embodiment 53
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 110o6 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9990 parts of salt（It is made up as raw material of crude salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 10 parts of allicin, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied
And the aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin is uniformly dispersed in salt saturated aqueous solution；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 60oC, slowly steams moisture, by allicin and salt condensing crystallizing, 100 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk carry out pulverization process without iodine garlic salt, obtain powdered without iodine garlic salt.
The present embodiment is obtained to be obtained without iodine garlic salt using condensing crystallizing method so that allicin can be scattered in sodium chloride
Inside particle so that both are scattered more uniform, can greatly reduce because of the uneven usage amount error brought of dispersion.
Embodiment 54
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 80o8 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9990 parts of salt（It is made up as raw material of lake salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 10 parts of allicin, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied
And the aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin is uniformly dispersed in salt saturated aqueous solution；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 70oC, slowly steams moisture, by allicin and salt condensing crystallizing, 60 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk without iodine garlic salt, quantitative screening is carried out according to block size, obtain calibrating quantitative nothing
Iodine garlic salt.Or after crushing is for the powdery product of 60 ~ 200 mesh, according to the step 4 in embodiment 2）Carry out quantitative shaping
Or sample packing, obtain surely gauged without iodine garlic salt.
Embodiment 55
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 120o8 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9982 parts of salt（It is made up as raw material of rock salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 18 parts of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder
Last shape without iodine garlic salt.
Embodiment 56
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 100o10 hours are dried under C, then control moisture be ground to 60 2% ~ 20%
~ 200 mesh, it is standby；
2）Weigh 9982 parts of salt（It is made up as raw material of well salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 18 parts of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder
Last shape without iodine garlic salt；
4）To step 3）In obtain it is powdered be quantitatively molded without iodine garlic salt or sample packing, obtain surely gauged big without iodine
Garlic salt.
The calibration being prepared from the present embodiment is quantitative without iodine garlic salt, can be according to different crowd to allicin and salt
Demand quantitatively used, being capable of the daily usage amount of easy control.
Embodiment 57
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 80o9 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9982 parts of salt（It is made up as raw material of rock salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 18 parts of allicin, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied
And the aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin is uniformly dispersed in salt saturated aqueous solution；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 80oC, slowly steams moisture, by allicin and salt condensing crystallizing, 90 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk carry out pulverization process without iodine garlic salt, obtain powdered without iodine garlic salt.
The present embodiment is obtained to be obtained without iodine garlic salt using condensing crystallizing method so that allicin can be scattered in sodium chloride
Inside particle so that both are scattered more uniform, can greatly reduce because of the uneven usage amount error brought of dispersion.
Embodiment 58
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 80o11 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9982 parts of salt（It is made up as raw material of lake salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 18 parts of allicin, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied
And the aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin is uniformly dispersed in salt saturated aqueous solution；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 90oC, slowly steams moisture, by allicin and salt condensing crystallizing, 85 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk without iodine garlic salt, quantitative screening is carried out according to block size, obtain calibrating quantitative nothing
Iodine garlic salt.Or after crushing is for the powdery product of 60 ~ 200 mesh, according to the step 4 in embodiment 2）Carry out quantitative shaping
Or sample packing, obtain surely gauged without iodine garlic salt.
Embodiment 59
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 120o10 hours are dried under C, then control moisture be ground to 60 2% ~ 20%
~ 200 mesh, it is standby；
2）Weigh 9975 parts of salt（It is made up as raw material of sea salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 25 parts of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder
Last shape without iodine garlic salt.
Embodiment 60
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 100o5 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9975 parts of salt（It is made up as raw material of lake salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Weigh step 1）In treat 25 parts of allicin, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder
Last shape without iodine garlic salt；
4）To step 3）In obtain it is powdered be quantitatively molded without iodine garlic salt or sample packing, obtain surely gauged big without iodine
Garlic salt.
The calibration being prepared from the present embodiment is quantitative without iodine garlic salt, can be according to different crowd to allicin and salt
Demand quantitatively used, being capable of the daily usage amount of easy control.
Embodiment 61
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps：
1）By the allicin of content >=90% 130o6 hours are dried under C, control moisture 2% ~ 20%, be then ground to 60 ~
200 mesh, it is standby；
2）Weigh 9975 parts of salt（It is made up as raw material of rock salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 25 parts of allicin, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied
And the aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin is uniformly dispersed in salt saturated aqueous solution；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 60oC, slowly steams moisture, by allicin and salt condensing crystallizing, 100 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk carry out pulverization process without iodine garlic salt, obtain powdered without iodine garlic salt.
The present embodiment is obtained to be obtained without iodine garlic salt using condensing crystallizing method so that allicin can be scattered in sodium chloride
Inside particle so that both are scattered more uniform, can greatly reduce because of the uneven usage amount error brought of dispersion.
Embodiment 62
Preparation technology without iodine garlic salt in the present embodiment in turn includes the following steps.
1）By the allicin of content >=90% 95o6.5 hours are dried under C, then control moisture grind 2% ~ 20%
It is standby to 60 ~ 200 mesh；
2）Weigh 9975 parts of salt（It is made up as raw material of sea salt）, the wherein purity of sodium chloride is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain；
3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water
Solution, makes all salinities fully dissolve under mechanical stirring；
4）Weigh step 1）In treat 25 parts of allicin, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied
And the aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that allicin is uniformly dispersed in salt saturated aqueous solution；
5）After allicin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor
Temperature control is 85oC, slowly steams moisture, by allicin and salt condensing crystallizing, 75 is placed in during to pasty stateoThe air blast of C
Residual moisture is steamed in drying box, bulk is obtained without iodine garlic salt product；
6）To step 5）In obtain bulk without iodine garlic salt, quantitative screening is carried out according to block size, obtain calibrating quantitative nothing
Iodine garlic salt.Or after crushing is for the powdery product of 60 ~ 200 mesh, according to the step 4 in embodiment 2）Carry out quantitative shaping
Or sample packing, obtain surely gauged without iodine garlic salt.
Claims (10)
1. a kind of new garlic nutrient salt, it is characterised in that：The main component of described new garlic nutrient salt is for salt and greatly
Garlic nutrients, the content of the garlic nutrient thing is 0.1-30wt%.
2. new garlic nutrient salt according to claim 1, it is characterised in that：The garlic nutrient thing is garlic powder or big
Garlic nutrition extract；Garlic powder is the powder that garlic crushed after being dried is made, and garlic nutrient extract is carried selected from garlic through squeezing the juice
Follow the example of, crystallisation, microwave extraction method, ultrasonic extraction, solution extraction, leaching centrifugal process, ferment treatment method, means of supercritical extraction
One or more garlic nutrient extract of extraction in the methods such as method, fermentation method.
3. new garlic nutrient salt according to claim 2, it is characterised in that：The garlic nutrient thing is allicin, greatly
The content of allicin is 0.1-3 wt%.
4. new garlic nutrient salt according to claim 1, it is characterised in that：Described new garlic nutrient salt also contains
Anticaking agent, the content of anticaking agent is 0.0001-0.005wt%；Anticaking agent is selected from ferric citrate, potassium ferrocyanide, ferrocyanide
One or more in sodium, tartaric acid iron, silica, calcium silicates.
5. the new garlic nutrient salt according to claim 1 or 2 or 3, it is characterised in that：The salt is without salt compounded of iodine or adds
Salt compounded of iodine, the propiodal of the iodizedsalt is edible inorganic iodide or the organic propiodal of rich iodine.
6. the new garlic nutrient salt according to claim 1 or 2 or 3, it is characterised in that：The salt is chosen for sea
One or more in salt, lake salt, well salt, rock salt or lake salt, the purity of the Sodium Chloride in Salt is more than 98%, and particle diameter is
0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain.
7. the new garlic nutrient salt according to claim 1 or 2 or 3, it is characterised in that：The salt is chosen for original
Salt, refined salt or add it is various trace element or nutrition, the extraordinary salt of flavor substance in one or more, in the salt
The purity of sodium chloride is more than 98%, and particle diameter is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain.
8. the preparation method of the new garlic nutrient salt described in claim 1 or 2 or 3 or 4, it is characterised in that：Described preparation
Method is mechanical mixing or condensing crystallizing method.
9. the preparation method of new garlic nutrient salt according to claim 8, it is characterised in that described mechanical mixing
Comprise the following steps：To garlic nutrient thing and anticaking agent is added in salt, 50-60 DEG C is heated to after being well mixed, keeps 10-
12h obtains garlic salt.
10. the preparation method of new garlic nutrient salt according to claim 8, it is characterised in that described condensing crystallizing
Method comprises the following steps：
1）Appropriate pure water is measured, after being heated to micro-boiling, salt is slowly added to, be configured to saturated aqueous solution, stirred in machinery
Mixing down makes all salinities fully dissolve；
2）By garlic nutrient thing and anticaking agent, step 1 is slowly added under mechanical stirring）Prepared salt saturated aqueous solution,
And continue to stir 0.5 more than h in slight boiling condition, it is ensured that garlic nutrient thing and anticaking agent disperse in salt saturated aqueous solution
It is even；
3）After garlic nutrient thing and anticaking agent are uniformly dispersed in salt saturated aqueous solution, continuing churned mechanically condition
Under, by the temperature control of mixed liquor 60 ~ 100oC, slowly steams moisture, by the concentration of garlic nutrient thing, anticaking agent and salt
Crystallization, 60 are placed in during to pasty stateoC~100 oResidual moisture is steamed in the air dry oven of C, block garlic salt is obtained；
4）To step 3）In the block garlic salt that obtains carry out pulverization process, obtain powdered garlic salt.
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| CN201610985590 | 2016-11-09 | ||
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| CN107252078A (en) * | 2017-06-27 | 2017-10-17 | 益盐堂（应城）健康盐制盐有限公司 | A kind of special-purpose salt with anti-oxidation function and preparation method thereof |
| CN108850985A (en) * | 2018-06-25 | 2018-11-23 | 南昌大学 | A kind of garlic powder, preparation method thereof |
| CN108850995A (en) * | 2018-06-25 | 2018-11-23 | 南昌大学 | A kind of chive powder, preparation method thereof |
| CN108850979A (en) * | 2018-06-25 | 2018-11-23 | 南昌大学 | A kind of spice salt production process inhibiting cured fish oxidation |
| CN109619528A (en) * | 2018-12-11 | 2019-04-16 | 中原工学院 | A kind of natto salt and preparation method thereof |
| CN109645433A (en) * | 2017-10-10 | 2019-04-19 | 江苏苏盐井神股份有限公司 | A kind of potassium iodide salt compounded of iodine and its production method |
| CN110169561A (en) * | 2019-06-25 | 2019-08-27 | 中原工学院 | A kind of green onion salt and preparation method thereof |
| CN111685304A (en) * | 2020-05-18 | 2020-09-22 | 云南省盐业有限公司 | Sodium chloride nutritive salt and preparation method thereof |
| CN113080428A (en) * | 2021-04-19 | 2021-07-09 | 云南省盐业有限公司 | Edible health-care salt and preparation method thereof |
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| CN107252078A (en) * | 2017-06-27 | 2017-10-17 | 益盐堂（应城）健康盐制盐有限公司 | A kind of special-purpose salt with anti-oxidation function and preparation method thereof |
| CN109645433A (en) * | 2017-10-10 | 2019-04-19 | 江苏苏盐井神股份有限公司 | A kind of potassium iodide salt compounded of iodine and its production method |
| CN108850985A (en) * | 2018-06-25 | 2018-11-23 | 南昌大学 | A kind of garlic powder, preparation method thereof |
| CN108850995A (en) * | 2018-06-25 | 2018-11-23 | 南昌大学 | A kind of chive powder, preparation method thereof |
| CN108850979A (en) * | 2018-06-25 | 2018-11-23 | 南昌大学 | A kind of spice salt production process inhibiting cured fish oxidation |
| CN109619528A (en) * | 2018-12-11 | 2019-04-16 | 中原工学院 | A kind of natto salt and preparation method thereof |
| CN110169561A (en) * | 2019-06-25 | 2019-08-27 | 中原工学院 | A kind of green onion salt and preparation method thereof |
| CN111685304A (en) * | 2020-05-18 | 2020-09-22 | 云南省盐业有限公司 | Sodium chloride nutritive salt and preparation method thereof |
| CN113080428A (en) * | 2021-04-19 | 2021-07-09 | 云南省盐业有限公司 | Edible health-care salt and preparation method thereof |
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