CN110169561A

CN110169561A - A kind of green onion salt and preparation method thereof

Info

Publication number: CN110169561A
Application number: CN201910555883.5A
Authority: CN
Inventors: 米立伟; 卫武涛; 周松峰; 陈卫华; 崔世忠
Original assignee: Zhongyuan University of Technology
Current assignee: Zhongyuan University of Technology
Priority date: 2019-06-25
Filing date: 2019-06-25
Publication date: 2019-08-27

Abstract

The present invention provides a kind of green onion salt and preparation method thereof, belong to food seasoning field.The present invention cleverly selects salt as carrier using green onion and salt as primary raw material, and suitable green onion and its extract are added by different modes, is uniformly mixed, series green onion product salt is made.According to the optimization of formulation condition, which can be used as edible salt and seasoning salt.The green onion salt prepared using technology path of the invention is had salt itself and rendered palatable the function of seasoning, and has the distinctive healthcare function of green onion.Easy to operate, raw material sources are extensive, at low cost and environmentally friendly, and product stability is good, are convenient for large-scale industrial production.The method can control the content of green onion nutriment in product, suitable for the preparation containing the natural drugs active ingredients salt such as other green onions and its derivative by the ratio of control green onion and salt.

Description

A kind of green onion salt and preparation method thereof

Technical field

The present invention relates to food dressing fields, and in particular to a kind of green onion salt and preparation method thereof.

Background technique

With the development of economy, people's nutrition consciousness step up, requirement of the people to food start pursue taste good, mouth Feel, multielement nutrition, and requires the multiple actions such as prevention disease, conditioning body.Green onion is commonly to eat in daily life One of material has the function of rendering palatable, whet the appetite.In addition, in green onion be rich in multivitamin, acrid flavour, it is warm-natured and, have removing toxic substances seasoning, Raising immunity, sweating is antibacterial, vasodilator, prevents the effects of senile dementia.

Salt be all from ancient times to the present people life it is essential, be to one of most important substance of human survival, and The daily salinity of general population is 5 ~ 8 grams.Thus it is guaranteed that, as the carrier of edible health care product, increasing while salt seasons Its health-care efficacy is added to have become the research hotspot of food seasoning field.There are spirulina salt, mushroom salt etc. in China market at present Plant salt product, but these product salts can only play seasoning and promote fragrant effect, be unable to satisfy the needs for improving human health.Certainly, Also there is patent report that green tea powder is added in commodity salt and prepare health-care salt, but the health-care salt haves the defects that poor taste.

This patent is by simple method uniformly mixed green onion and its extract with salt according to a certain percentage, preparation Healthy green onion salt out, which, which has to deliver, activates yang, seasoning of detoxifying, the content of nitrite in reduction gastric juice, improves immunity, promotees It into blood circulation, prevention senile dementia, reduces bad cholesterol, the health-care efficacies such as relieve fatigue, and the preparation method has work The advantages that sequence is simple, low energy consumption, environmentally protective, production life cycle is short, cheap, is easy to be received by customers.

According to the inventors knowledge, report is had no at present green onion is added in salt, or prepared mouthfeel and health-care effect is equal Good vegetalitas eats the related patents and document of green onion salt.

Summary of the invention

The invention proposes a kind of green onion salt and preparation method thereof, it is therefore an objective to be directed to current hypertension, cardiovascular disease, old age The high-incidence disease such as dementia researches and develops a kind of green onion salt.This method is with easy to operate, with short production cycle, product quality is good, green ring It protects, the advantages that low energy consumption, cheap, it is easy to accomplish industrialized production；The product is by the way of green plant addition, by vast need The person of asking is received, and is had a vast market foreground.

Realize the technical scheme is that

A kind of green onion salt, the green onion salt include that the weight ratio of salt and green onion raw material salt and green onion raw material is (0.01-99.99): (0.01-99.99).

One or more of the green onion powder, Herba Alii fistulosi extract of dusting after the green onion raw material is wet green onion, is dry, Herba Alii fistulosi extract is selected from Green onion is through the extraction method, steam distillation, supercritical CO of squeezing the juice₂Extraction method, ultrasound assisted extraction method, soxhlet extraction, enzymatic hydrolysis mention It one of follows the example of or the Herba Alii fistulosi extract of a variety of extractions.

Herba Alii fistulosi extract main component are as follows: allicin, mercaptan, trisulfide, caffeic acid, sinapic acid, cinnamic acid, citrate, It is cycloalliin, prostaglandin A, tolbutamide similar substance, diallyl disulfide, trace elements of selenium, methylsulphur fourth arteries and veins, different red Green onion A prime, eleutherin, different eleutherin, cupreol, 8- hydroxyl -3,4- dimethoxy-l- methyl-anthraquinone -2- carboxylic acid first Ester, 4- hydroxyl eleutherin, hongconin, 4,8- dihydroxy -3- methoxyl group-l- methyl-anthraquinone -2- carboxylate methyl ester, Dihydro-eleutherinol, l are 3,6- trihydroxy -8- tectoquinone, the mucous matter of bulb, crude fat, thick protein, thick Fiber, nitrogen-free extracts, pentosan, polysaccharide, cellulose, hemicellulose, protopectin, water soluble pectin, vitamin C, Hu Luo Bu Su, vitamin B1, vitamin B2, vitamin A, nicotinic acid, oxalic acid, lipid, linolenic acid, linoleic acid, palmitinic acid, oleic acid, Arachidic acid, ubiquinone-9 and 2,3-dimethoxy-5-methyl-6-decaprenyl-1,4-benzoquinone, allicin, allyl sulfide, sweet-scented osmanthus skin alcohol, spiraeoside, embroider line glucoside, Quercetin -3, 4- diglucoside, protein, calcium, phosphorus, iron, vitamin C 15, thiamine, riboflavin, the Multiple components such as niacin.

The green onion is selected from white green onion, red green onion, onion, shallot, shallot, Hu green onion, spring onion, chive, continuous green onion, fiery green onion, four seasons green onion, thin The one or more of rice green onion, building green onion.

The salt is one of sea salt, lake salt, well salt, rock salt or lake salt or a variety of, can be crude salt, refined salt or Add various microelements or one or more of nutrition, the extraordinary salt of flavor substance；Can be salt compounded of iodine, (propiodal can be The edible inorganic iodide such as Potassiumiodate, potassium iodide and the rich organic propiodal of iodine: as kelp, seaweed, thallus laminariae, seaweed, fresh hairtail, One of extracts containing iodine of the food containing iodine such as blood clam is dry, clam is dry, dried scallop, mussel, sea cucumber, jellyfish, lobster are several, use Preceding elder generation's dusting is to 60 ~ 200 mesh), it is also possible to no salt compounded of iodine.The purity of Sodium Chloride in Salt is 98% or more, and partial size is 0.07 ~ 1.0 Mm, whiteness are 55% ~ 95% microcrystal grain.

Also contain anticaking agent in the green onion salt, the content of anticaking agent is 0.0001-0.005wt%, and anticaking agent is selected from citric acid One or more of iron ammonium, potassium ferrocyanide, sodium ferrocyanide, tartaric acid iron, calcium silicates, silica, calcium silicates.

The salt is no salt compounded of iodine or iodizedsalt, and the propiodal of the iodizedsalt is that edible inorganic iodide or rich iodine are organic Propiodal.

The preparation method is mechanical mixing or concentrated crystallization.

The purposes of the health green onion salt can change according to the adjustment of salt and green onion ratio: health green onion salt when salt content is higher Application method is similar with common table salt；It is direct-edible when salt content is lower.It can be with according to different health green onion salt of formula As edible salt and seasoning salt.

Wherein the pretreating process of dry green onion powder and Herba Alii fistulosi extract is as follows:

1, pulverization process

(1) green onion is dried under suitable condition, obtains dry green onion；

(2) dry green onion is carried out being ground to 20 ~ 2000 mesh, obtains dry green onion powder.

2, Herba Alii fistulosi extract juicing extraction method

(1) green onion is squeezed out the effective component in green onion by oil press.

(2) green onion effective component obtained above is filtered, filters out solid residue, recycle filtrate.

(3) the obtained filtrate of recycling is descended into drying under proper condition, then spontaneous nucleation is ground to 20 ~ 2000 mesh, both Obtain Herba Alii fistulosi extract.

3, Herba Alii fistulosi extract steam distillation

(1) green onion powder is weighed, is placed in round-bottomed flask, distilled water is added, it is slightly boiled to be heated to oil mass after connecting steam distillation device Until not increasing, green onion effective component distillation is obtained.

(2) green onion effective component is dried, spontaneous nucleation under proper condition, is then ground to 20 ~ 2000 mesh, both obtained green onion and mentioned Take object.

4, Herba Alii fistulosi extract supercritical CO₂Extraction method

(1) green onion powder is weighed, first a period of time preset in the state of middle pressure, room temperature；

(2) under higher extracting pressure, under certain extraction temperature, supercritical CO is utilized₂Dynamic circulation extraction is carried out, reduction is passed through Extract is precipitated in separating still in pressure and temperature, obtains green onion effective component.

(3) green onion effective component is descended into drying under proper condition, then spontaneous nucleation grinds to 20 ~ 2000 mesh, both obtains green onion Extract.

5, Herba Alii fistulosi extract ultrasound assisted extraction method

(1) green onion powder is weighed, is put in conical flask, uses petroleum ether as solvent, is extracted under ultrasonication, is filtered.

(2) petroleum ether is continuously added in the conical flask for filling filter residue as solvent, is extracted under ultrasonication, is filtered. And merge filtrate twice.

(3) petroleum ether is recycled in rotary evaporation, obtains green onion effective component.

(4) green onion effective component is descended into drying under proper condition, then spontaneous nucleation grinds to 20 ~ 2000 mesh, both obtains green onion Extract.

6, Herba Alii fistulosi extract soxhlet extraction

(1) green onion powder is weighed, is wrapped with filter paper, is placed in Soxhlet extraction cylinder, petroleum ether is added, extracts.

(2) extracting solution recycles petroleum ether in rotary evaporation, obtains green onion effective component.

7, Herba Alii fistulosi extract zymohydrolysis extracting method

(1) green onion powder is weighed, water is added and is heated, stirring heat preservation appropriate time adds complex enzyme (cellulase, pectase etc.), in acid Under the conditions of property, digested in warm water

(2) add buck to adjust pH to alkalescent in the green onion powder after enzymatic hydrolysis, extract 3 times, be then centrifuged in boiling water, collect centrifugation Liquid.

(3) above-mentioned centrifugate is concentrated in Rotary Evaporators, obtains green onion effective component.

8, Herba Alii fistulosi extract microwave loss mechanisms

(1) claim to remove green onion powder, be put into microwave extraction tank, and ethyl alcohol is added.

(2) instrument is opened, regulation power, time carry out microwave abstracting.

(3) after the completion of extracting, cooling extracting solution, and by its condensing crystallizing, obtain brown viscous liquid.

(4) it by above-mentioned brown viscous liquid, is dried, and grinds to 20 ~ 2000 mesh, both obtain Herba Alii fistulosi extract.

By 0.01% ~ 99.99% part of edible salt, 99.99% ~ 0.01% part of green onion raw material, with suitable anticaking agent (ironic citrate One or more of ammonium, potassium ferrocyanide, sodium ferrocyanide, tartaric acid iron, calcium silicates, silica, calcium silicates) and 1 × 10^-5~4×10^-5The propiodal (in terms of iodine) of part carries out uniformly mixing by suitable addition manner to get green onion salt compounded of iodine.

The beneficial effects of the present invention are:

(1) invention, which is put forward for the first time, is added to green onion in salt, prepares healthy green onion salt, has filled up the sky in the field in a way It is white.

(2) by adding vegetable ingredients green onion and its extract in daily flavouring salt, when avoiding individually eating green onion It bring alliaceous odour taste and is difficult to ensure successional drawback, in the long run, more has duration using green onion salt.In addition, green onion and its mentioning It takes the addition of object to increase content of nitrite, raising immunity, promotion blood of the salt in removing toxic substances seasoning, reduction gastric juice to follow Ring, prevention senile dementia, the effect of reducing bad cholesterol, relieving fatigue etc..

(3) the healthy green onion salt for developing green onion in conjunction with salt product, highlights the peculiar taste and color of green onion.It can expire significantly Diversified demand of the sufficient consumer in terms of culinary art, promotes the mouthfeel of dish.

(4) green onion can enrich the effect of salt, and change green onion and salt ratio, which is directly used as eating Salt and seasoning salt.

Specific embodiment

Below in conjunction with the embodiment of the present invention, technical solution of the present invention is clearly and completely described, it is clear that institute The embodiment of description is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, Those of ordinary skill in the art's every other embodiment obtained under that premise of not paying creative labor, belongs to this hair The range of bright protection.

Embodiment 1

Preparation process without iodine health green onion salt in the present embodiment in turn includes the following steps.

(1) by green onion drying and crushing, be sieved to obtain green onion powder；

(2) 99 parts of salt is weighed, which is sea salt, and wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 Mm, whiteness are 55% ~ 95% microcrystal grain.

(3) 1 part of green onion powder obtained in step (1) is weighed, by itself and the weighed salt of step (2) and suitable ironic citrate Ammonium carries out mechanical mixture and obtains powdered no iodine health green onion salt.

Embodiment 2

(2) 90 parts of salt is weighed, which is lake salt, and wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 Mm, whiteness are 55% ~ 95% microcrystal grain.

(3) 10 parts of green onion powder obtained in step (1) are weighed, by itself and the weighed salt of step (2) and suitable citric acid Iron ammonium carries out mechanical mixture and obtains powdered no iodine health green onion salt.

Embodiment 3

The preparation process of healthy green onion salt compounded of iodine in turn includes the following steps in the present embodiment.

(2) 85 parts of salt is weighed, which is well salt, and wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 Mm, whiteness are 55% ~ 95% microcrystal grain.

(3) 15 parts of green onion powder obtained in step (1) and 1 × 10 are weighed^-5(in terms of iodine, iodine is from acid iodide for part propiodal Potassium uses preceding first dusting to 60 ~ 200 mesh), it is subjected to machinery with the weighed salt of step (2) and suitable potassium ferrocyanide It is mixed to get powdered healthy green onion salt compounded of iodine.

Embodiment 4

(2) 80 parts of salt is weighed, which is rock salt, and wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 Mm, whiteness are 55% ~ 95% microcrystal grain.

(3) measure suitable pure water, be heated to it is slightly boiled after, step (2) load weighted salt is slowly added to, is configured to Saturated aqueous solution dissolves all salinities sufficiently.

(4) 20 parts of green onion powder obtained in step (1) and suitable anticaking agent are weighed, is slowly added to step under mechanical stirring (3) the salt saturated aqueous solution prepared by, and continue to stir 0.5 h or more in slight boiling condition, guarantee green onion powder and potassium ferrocyanide It is uniformly dispersed in salt saturated aqueous solution.

(5) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled 60 ~ 100^oC slowly steams moisture Out, by green onion powder, salt and anticaking agent condensing crystallizing, until being placed in 60 when paste^oC~100 ^oResidue is steamed in the air dry oven of C Moisture obtains bulk without iodine health green onion salt.

(6) to bulk obtained in step (5) without iodine health green onion salt, quantitative screening is carried out according to blocky size, is determined Scalar quantity is without iodine health green onion salt.

Embodiment 5

(2) 75 parts of salt is weighed, which is lake salt, and wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 Mm, whiteness are 55% ~ 95% microcrystal grain.

(3) 25 parts of green onion powder obtained in step (1) and 2 × 10 are weighed^-5Part propiodal (in terms of iodine, from mussel and The extract containing iodine of lobster uses preceding first dusting to 60 ~ 200 mesh), by itself and the weighed salt of step (2) and suitable ferrous iron Cymag carries out mechanical mixture and obtains powdered healthy green onion salt compounded of iodine.

Embodiment 6

(2) 70 parts of salt is weighed, which is sea salt and lake salt, and wherein the purity of sodium chloride is 98% or more, partial size 0.07 ~ 1.0 mm, whiteness are 55% ~ 95% microcrystal grain.

(3) 30 parts of processed green onion powder and 3 × 10 are weighed in step (1)^-5(in terms of iodine, iodine is from iodine for part propiodal Sour potassium and potassium iodide use preceding first dusting to 60 ~ 200 mesh), by itself and the weighed salt of step 2 and suitable sodium ferrocyanide It carries out mechanical mixture and obtains powdered healthy green onion salt compounded of iodine.

(4) it to powdered health green onion salt compounded of iodine quantitatively forms obtained in step (3) or sample dispenses, obtains surely gauged Healthy green onion salt compounded of iodine.

The calibration that is prepared in the present embodiment quantitative healthy green onion salt compounded of iodine, can take green onion according to different crowd and salt Demand carries out quantitative use, easy can control daily usage amount.

Embodiment 7

(2) 65 parts of salt is weighed, which can be sea salt and lake salt, and wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, whiteness are 55% ~ 95% microcrystal grain.

(4) 35 parts of green onion powder obtained in step (1), 4 × 10 are weighed^-5Part propiodal is (in terms of iodine, from kelp, sea The extract containing iodine of algae and dried scallop uses preceding first dusting to 60 ~ 200 mesh) and suitable anticaking agent, slowly add under mechanical stirring Enter salt saturated aqueous solution prepared by step (3), and continue to stir 0.5 h or more in slight boiling condition, guarantees green onion powder in salt It is uniformly dispersed in saturated aqueous solution.

(5) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled 60 ~ 100^oC slowly steams moisture Out, by green onion powder, propiodal, sodium ferrocyanide and salt condensing crystallizing, until being placed in 60 when paste^oC~100 ^oIn the air dry oven of C Residual moisture is steamed, blocky healthy green onion salt compounded of iodine is obtained.

(6) pulverization process is carried out to the healthy green onion salt compounded of iodine of bulk obtained in step (5), obtains powdered healthy green onion salt compounded of iodine.

Health green onion salt compounded of iodine made from the present embodiment is made using concentrated crystallization, and green onion powder is allowed to be scattered in sodium chloride Intragranular portion can greatly be reduced so that the two dispersion is more uniform because dispersing uneven bring usage amount error.

Embodiment 8

(2) 60 parts of salt is weighed, which is sea salt, lake salt and well salt, and wherein the purity of sodium chloride is 98% or more, partial size For 0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain.

(3) 40 parts of processed green onion powder and 2 × 10 are weighed in step (1)^-5Part propiodal (in terms of iodine, from kelp, The extract containing iodine of seaweed and thallus laminariae uses preceding first dusting to 60 ~ 200 mesh), it with the weighed salt of step (2) and is fitted The tartaric acid iron of amount carries out mechanical mixture and obtains powdered healthy green onion salt compounded of iodine.

Embodiment 9

(2) 98 parts of salt is weighed, which is sea salt, well salt and rock salt, and wherein the purity of sodium chloride is 98% or more, partial size For 0.07 ~ 1.0 mm, whiteness is 55% ~ 95% microcrystal grain.

(3) 2 parts of processed green onion powder and 3 × 10 are weighed in step (1)^-5(in terms of iodine, iodine is from fresh band for part propiodal The extract containing iodine that fish, blood clam are dry and clam is dry uses preceding first dusting to 60 ~ 200 mesh), it with the weighed salt of step (2) and is fitted The tartaric acid iron of amount carries out mechanical mixture and obtains powdered healthy green onion salt compounded of iodine.

The quantitative healthy green onion salt compounded of iodine of the calibration being prepared in the present embodiment, can be according to different crowd to the need of green onion and salt The amount of asking carries out quantitative use, easy can control daily usage amount.

Embodiment 10

(1) green onion is dry, obtain dry green onion.

(2) weigh 10 parts of salt, which is sea salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness are 55% ~ 95% microcrystal grain.

(3) 90 parts of processed dry green onion and 1 × 10 are weighed in step (1)^-5(in terms of iodine, iodine is from dry for part propiodal Shellfish, mussel and sea cucumber extract containing iodine, use preceding first dusting to 60 ~ 200 mesh), it with the weighed salt of step (2) and is fitted The calcium silicates of amount carries out mechanical mixture and obtains powdered healthy green onion salt compounded of iodine.

Embodiment 11

(1) green onion is dry, obtain dry green onion.

(2) 1 part of salt is weighed, which is rock salt and lake salt, and wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, whiteness are 55% ~ 95% microcrystal grain.

(4) 99 parts of dry green onion obtained in step (1) are weighed, is slowly added to salt prepared by step 3) under mechanical stirring Saturated aqueous solution, and continue to stir 0.5 h or more in slight boiling condition, guarantee to mix in dry green onion, anticaking agent and salt saturated aqueous solution It closes uniform.

(5) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled 60^oC slowly steams moisture, will Dry green onion and salt condensing crystallizing, until being placed in 60 when paste^oResidual moisture is steamed in the air dry oven of C, obtains bulk without iodine Healthy green onion salt.

Embodiment 12

(1) green onion is dry, obtain dry green onion；

(2) 0.01 part of salt is weighed, which is crude salt, and wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 Mm, whiteness are 55% ~ 95% microcrystal grain.

(3) 99.99 parts of dry green onion obtained in step (1) is weighed and with 2 × 10^-5Part propiodal is (in terms of iodine, from light The extract containing iodine of dish and lobster uses preceding first dusting to 60 ~ 200 mesh), it is subjected to machinery with the weighed salt of step (2) It is mixed to get powdered healthy green onion salt compounded of iodine.

Embodiment 13

(1) selection green onion is spare as raw material.

(2) weigh 1 part of salt, which is refined salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness are 55% ~ 95% microcrystal grain.

(4) 99 parts of green onion are weighed in step (1), is slowly added to salt saturated water prepared by step (3) under mechanical stirring Solution, and continue to stir 0.5 h or more in slight boiling condition, guarantee to be uniformly mixed in green onion, calcium silicates and salt saturated aqueous solution.

(5) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled 80^oC slowly steams moisture, will Dry green onion and salt condensing crystallizing, until paste, obtains no iodine health green onion salt.

Embodiment 14

(1) directly selection green onion is spare as raw material.

(2) 98 parts of salt is weighed, which adds the extraordinary salt of various microelements or nutrition, flavor substance, The purity of middle sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain.

(3) 2 parts of green onion and 3 × 10 are weighed in step (1)^-5Part propiodal (in terms of iodine, iodine is from fresh hairtail, blood clam is dry and The dry extract containing iodine of clam uses preceding first dusting to 60 ~ 200 mesh), by itself and the weighed salt of step (2) and suitable dioxy SiClx carries out mechanical mixture and obtains powdered healthy green onion salt compounded of iodine.

Embodiment 15

(1) choosing Herba Alii fistulosi extract is raw material, spare；

(2) 80 parts of salt is weighed, which is crude salt and refined salt, and wherein the purity of sodium chloride is 98% or more, partial size 0.07 ~ 1.0 mm, whiteness are 55% ~ 95% microcrystal grain.

(4) 20 parts of Herba Alii fistulosi extract obtained in step (1) and suitable anticaking agent are weighed, is slowly added under mechanical stirring Salt saturated aqueous solution prepared by step (3), and continue to stir 0.5 h or more in slight boiling condition, guarantee green onion powder and titanium dioxide Silicon is uniformly dispersed in salt saturated aqueous solution.

(5) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled 80^oC slowly steams moisture, will Green onion powder, salt and anticaking agent condensing crystallizing, until being placed in 80 when paste^oResidual moisture is steamed in the air dry oven of C, obtains block Shape is without iodine health green onion salt.

Embodiment 16

(1) it chooses green onion powder and Herba Alii fistulosi extract is raw material, it is spare.

(3) 90 parts of processed green onion powder and Herba Alii fistulosi extract and 1 × 10 are weighed in step (1)^-5Part propiodal (in terms of iodine, Iodine uses preceding first dusting to 60 ~ 200 mesh from dried scallop, mussel and the extract containing iodine of sea cucumber), it is weighed with step (2) Salt and suitable silica carry out mechanical mixture obtain powdered healthy green onion salt compounded of iodine.

Embodiment 17

(1) choosing green onion powder, green onion and Herba Alii fistulosi extract is raw material, spare；

(2) 70 parts of salt is weighed, which is lake salt, and wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 Mm, whiteness are 55% ~ 95% microcrystal grain.

(3) 30 parts of green onion powder in step (1), green onion and Herba Alii fistulosi extract and 3 × 10 are weighed^-5(in terms of iodine, iodine comes from part propiodal In Potassiumiodate and potassium iodide, preceding first dusting to 60 ~ 200 mesh is used), by itself and the weighed salt of step (2) and suitable silicic acid Calcium carries out mechanical mixture and obtains powdered healthy green onion salt compounded of iodine.

Embodiment 18

(2) 99.99 parts of salt is weighed, which is well salt, rock salt, lake salt, and wherein the purity of sodium chloride is 98% or more, grain Diameter is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain.

(3) 0.01 part of green onion powder obtained in step (1) is weighed, by itself and the weighed salt of step (2) and suitable silicic acid Calcium carries out mechanical mixture and obtains powdered no iodine health green onion salt.

Embodiment 19

(1) selection green onion is spare as raw material.

(2) 0.01 part of salt is weighed, which is sea salt, lake salt, well salt, rock salt, and wherein the purity of sodium chloride is 98% More than, partial size is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain.

(4) 99.99 parts of green onion are weighed in step (1), is slowly added to the saturation of salt prepared by step 3) under mechanical stirring Aqueous solution, and continue to stir 0.5 h or more in slight boiling condition, guarantee to be uniformly mixed in green onion, calcium silicates and salt saturated aqueous solution.

(5) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled 100^oC slowly steams moisture, By dry green onion and salt condensing crystallizing, until paste, obtains no iodine health green onion salt.

Embodiment 20

(1) selection green onion is spare as raw material.

(2) 0.05 part of salt is weighed, which is crude salt, and wherein the purity of sodium chloride is 98% or more, partial size 0.07 ~ 1.0 mm, whiteness are 55% ~ 95% microcrystal grain.

(4) 99.95 parts of green onion are weighed in step (1), is slowly added to the saturation of salt prepared by step 3) under mechanical stirring Aqueous solution, and continue to stir 0.5 h or more in slight boiling condition, guarantee to be uniformly mixed in green onion, calcium silicates and salt saturated aqueous solution.

Embodiment 21

(2) 99.97 parts of salt is weighed, which is refined salt and the special type for adding various microelements or nutrition, flavor substance Salt, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain.

(3) 0.03 part of processed green onion powder and 2 × 10 are weighed in step (1)^-5Part propiodal is (in terms of iodine, from sea Band, seaweed and thallus laminariae extract containing iodine, use preceding elder generation's dusting to 60 ~ 200 mesh), by it with the weighed salt of step (2) and Suitable silica carries out mechanical mixture and obtains powdered healthy green onion salt compounded of iodine.

Embodiment 22

(2) 0.04 part of salt is weighed, which is sea salt, and wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 Mm, whiteness are 55% ~ 95% microcrystal grain.

(3) 99.96 parts of processed green onion powder and 2 × 10 are weighed in step (1)^-5Part propiodal is (in terms of iodine, from sea Band, seaweed and thallus laminariae extract containing iodine, use preceding elder generation's dusting to 60 ~ 200 mesh), by its with step (2) weighed salt into Row mechanical mixture obtains powdered healthy green onion salt compounded of iodine.

Embodiment 23

Preparation process without iodine green onion salt in the present embodiment in turn includes the following steps.

(1) by green onion 60^oIt is dried under C, obtains dry green onion；

(2) it is sieved with 100 mesh sieve after being ground dry green onion, obtains green onion powder.

(3) weighing 98 parts of salt, (salt is sea salt and crude salt, and wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, whiteness are 55% ~ 95% microcrystal grain), 2 parts of green onion powder obtained in step (2) are weighed, by itself and ironic citrate Ammonium carries out mechanical mixture and obtains powdered no iodine turmeric salt.

Embodiment 24

(1) green onion is squeezed out the green onion effective component in turmeric by oil press.

(3) filtrate that recycling obtains is descended into drying under proper condition, then spontaneous nucleation is ground, sieve with 100 mesh sieve, both Obtain Herba Alii fistulosi extract.

(4) weigh 90 parts salt (salt is sea salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness be 55% ~ 95% microcrystal grain), weigh 10 parts of turmeric effective extract matter obtained in step (3), by its with Ferric citrate carries out mechanical mixture and obtains powdered no iodine turmeric salt.

(5) powdered no iodine turmeric salt obtained in step (4) is quantitatively formed or sample dispenses, obtained surely gauged Without iodine turmeric salt.

The calibration being prepared in the present embodiment is quantitative without iodine turmeric salt, can be according to different crowd to Turmeric P.E matter Quantitative use is carried out with the demand of salt, easy can control daily amount.

Embodiment 25

The preparation process of green onion salt compounded of iodine in turn includes the following steps in the present embodiment.

(1) 100 g green onion powder are weighed, are placed in 1000 mL round-bottomed flasks, 500 mL water, connection steam distillation dress is added It postpones, it is slightly boiled to be heated to green onion distillation being obtained, through anhydrous Na until oil mass do not increase₂SO₄After drying, green onion effective component is obtained.

(2) by green onion effective component 60^oThen the lower drying of C, spontaneous nucleation grind, sieve with 100 mesh sieve, both obtained green onion and extracted Object.

(3) weigh 85 parts salt (salt is lake salt kind, wherein the purity of sodium chloride be 98% or more, partial size 0.07 ~ 1.0 mm, whiteness are 55% ~ 95% microcrystal grain), weigh 15 parts of Herba Alii fistulosi extract obtained in step (2) and 1 × 10^-5Part propiodal (in terms of iodine, iodine uses preceding first dusting from Potassiumiodate), carries out mechanical mixture with ferric citrate for it and obtains powder The green onion salt compounded of iodine of shape.

Embodiment 26

(1) present 10 MPa of pressure of 200 g green onion powder, temperature 30 are weighed^oPreset 15 min in the state of C；

It (2) is 30 MPa, extraction temperature 45 in extracting pressure^oC, CO₂Flow is 40 L h^-1, 120 min's of extraction time Under the conditions of carry out dynamic circulation extraction, by reduce pressure and temperature extract is precipitated in separating still, obtain green onion effective component.

(3) by green onion effective component 60^oDry under C, then spontaneous nucleation grinds, sieves with 100 mesh sieve, and has both obtained green onion and has extracted Object.

(4) weigh 80 parts salt (salt is sea salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness be 55% ~ 95% microcrystal grain), be dissolved in distilled water, be heated to it is slightly boiled after, load weighted salt is slowly added Enter, be configured to saturated aqueous solution, dissolves all salinities sufficiently.

(5) 20 parts of Herba Alii fistulosi extract and ferric citrate obtained in step (3) are weighed, is slowly added to walk under mechanical stirring It is rapid 4) prepared by salt saturated aqueous solution, and continue to stir 0.5 h or more in slight boiling condition, guarantee Herba Alii fistulosi extract and citric acid Iron ammonium is uniformly dispersed in salt saturated aqueous solution.

(6) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled 60^oC or more slowly steams moisture Out, by Herba Alii fistulosi extract, salt and ferric citrate condensing crystallizing, until being placed in 60 when paste^oIt is steamed in the air dry oven of C surplus Remaining moisture obtains bulk without iodine green onion salt product.

(7) to bulk obtained in step (6) without iodine green onion salt, quantitative screening is carried out according to blocky size, it is fixed to obtain calibration Amount is without iodine green onion salt.Or after crushing, quantitative molding is carried out according to the step (5) in embodiment 2 or sample dispenses, it is fixed to obtain calibration Amount without iodine green onion salt.

Embodiment 27

(1) claim 20 g green onion powder, be put in the conical flask of 500 mL, use 200 mL petroleum ethers as solvent, in ultrasonication 30 min of lower extraction, filtering.

(2) 200 mL petroleum ethers are continuously added in the conical flask for filling filter residue as solvent, are extracted under ultrasonication 30 min, filtering.And merge filtrate twice.

(3) in 45^oC rotary evaporation recycles petroleum ether, obtains green onion effective component.

(4) by green onion effective component 60^oThen the lower drying of C, spontaneous nucleation grind, sieve with 100 mesh sieve, both obtained green onion and extracted Object.

(5) weigh 75 parts salt (salt is sea salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness are 55% ~ 95% microcrystal grain), weigh 25 parts of Herba Alii fistulosi extract obtained in step (4) and with 2 × 10^-5Part propiodal (in terms of iodine, from the extract containing iodine of mussel and lobster, using preceding first dusting to 60 ~ 200 mesh), by itself and citric acid Iron ammonium carries out mechanical mixture and obtains powdered green onion salt compounded of iodine.

Embodiment 28

(1) claim 20 g green onion powder, wrapped, be placed in Soxhlet extraction cylinder with filter paper, 300 mL petroleum ethers of addition, 85^oIt is mentioned under C Take 6 h.

(2) extracting solution is in 45^oC rotary evaporation recycles petroleum ether, obtains green onion effective component.

(4) weigh 70 parts salt (salt adds the extraordinary salt of various microelements or nutrition, flavor substance, The purity of middle sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain), weigh step (3) In 30 parts of processed Herba Alii fistulosi extract and 3 × 10^-5(in terms of iodine, iodine is before Potassiumiodate and potassium iodide, use for part propiodal First dusting), it is subjected to mechanical mixture with ferric citrate and obtains powdered green onion salt compounded of iodine.

(5) powdered green onion salt compounded of iodine obtained in step (4) is quantitatively formed or sample dispenses, obtain surely gauged green onion iodine Salt.

The calibration being prepared in the present embodiment quantifies green onion salt compounded of iodine, can be according to different crowd to Herba Alii fistulosi extract and salt Demand carries out quantitative use, easy can control daily amount.

Embodiment 29

(1) claim 40 g green onion powder, water is added to be warming up to 90^oC, stirring 2 h of heat preservation, adds complex enzyme (cellulase, pectase Deng), in acid condition, digested in warm water

(4) green onion effective component is dried under proper condition, then spontaneous nucleation is ground, sieve with 100 mesh sieve, and has both been obtained green onion and has been mentioned Take object.

(5) weigh 65 parts salt (salt is crude salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness be 55% ~ 95% microcrystal grain), be dissolved in distilled water, be heated to it is slightly boiled after, load weighted salt is slowly added Enter, be configured to saturated aqueous solution, dissolves all salinities sufficiently.

(6) 35 parts of Herba Alii fistulosi extract, 4 × 10 obtained in step (4) are weighed^-5Part propiodal is (in terms of iodine, from sea Band, seaweed and dried scallop extract containing iodine, use preceding elder generation's dusting to 60 ~ 200 mesh) and ferric citrate, delay under mechanical stirring Slowly salt saturated aqueous solution prepared by step (5) is added, and continues to stir 0.5 h or more in slight boiling condition, guarantees that green onion is extracted Object is uniformly dispersed in salt saturated aqueous solution.

(7) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled 60^oC or more slowly steams moisture Out, by Herba Alii fistulosi extract, propiodal, ferric citrate and salt condensing crystallizing, until being placed in 60 when paste^oIt is steamed in the air dry oven of C Residual moisture out obtains blocky green onion salt compounded of iodine.

(8) pulverization process is carried out to bulk green onion salt compounded of iodine obtained in step (7), obtains powdered green onion salt compounded of iodine.

Green onion salt compounded of iodine made from the present embodiment is made using concentrated crystallization, and Herba Alii fistulosi extract is allowed to be scattered in sodium chloride Intragranular portion can greatly be reduced so that the two dispersion is more uniform because dispersing uneven bring amount error.

Embodiment 30

(1) green onion is dried under suitable condition, obtains dry green onion；

(2) dry green onion is ground, obtains green onion powder.

(3) weigh 60 parts salt (salt is lake salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness are 55% ~ 95% microcrystal grain), weigh in step (2) 40 parts of processed green onion powder and 2 × 10^-5Part propiodal (with Iodine meter uses preceding first dusting from the extract containing iodine of kelp, seaweed and thallus laminariae), by itself and ferric citrate into Row mechanical mixture obtains powdered green onion salt compounded of iodine.

Embodiment 31

(1) green onion is squeezed out the green onion effective component in green onion by oil press.

(3) filtrate that recycling obtains is descended into drying under proper condition, then spontaneous nucleation is ground, both obtain Herba Alii fistulosi extract.

(4) weigh 98 parts salt (salt is rock salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness are 55% ~ 95% microcrystal grain), weigh in step (3) 1 part of processed Herba Alii fistulosi extract and 3 × 10^-5Part propiodal (in terms of iodine, iodine uses preceding first dusting from fresh hairtail, the extract containing iodine that blood clam does and clam is dry), by itself and citric acid Iron ammonium carries out mechanical mixture and obtains powdered green onion salt compounded of iodine.

Embodiment 32

(1) 100 g green onion powder are weighed, are placed in 1000 mL round-bottomed flasks, 500 mL water, connection steam distillation dress is added It postpones, it is slightly boiled to be heated to obtaining green onion effective component until oil mass do not increase.

(2) weigh 98 parts salt (salt be add nutrition, flavor substance extraordinary salt, wherein sodium chloride is pure Degree is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain), weigh processed green onion in step (1) 0.5 part of effective component and 1 × 10^-5(in terms of iodine, iodine makes part propiodal from dried scallop, mussel and the extract containing iodine of sea cucumber With preceding first dusting to 60 ~ 200 mesh), it is subjected to mechanical mixture with ferric citrate and obtains powdered green onion salt compounded of iodine.

The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.

Claims

1. a kind of green onion salt, it is characterised in that: the green onion salt includes salt and green onion raw material, and the weight ratio of salt and green onion raw material is (0.01-99.99): (0.01-99.99).

2. green onion salt according to claim 1, it is characterised in that: the green onion powder of dusting, green onion after the green onion raw material is wet green onion, is dry One or more of extract, Herba Alii fistulosi extract are selected from green onion through the extraction method, steam distillation, supercritical CO of squeezing the juice₂Extraction method, One of ultrasound assisted extraction method, soxhlet extraction, zymohydrolysis extracting method or the Herba Alii fistulosi extract of a variety of extractions.

3. green onion salt according to claim 2, it is characterised in that: the green onion be selected from white green onion, red green onion, onion, shallot, shallot, Hu green onion, spring onion, chive, continuous green onion, fiery green onion, four seasons green onion, thin rice green onion, building green onion one or more.

4. green onion salt according to claim 1, it is characterised in that: the salt is sea salt, lake salt, well salt, rock salt or lake salt One of or it is a variety of, the purity of Sodium Chloride in Salt is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% micro- Brilliant particle.

5. green onion salt according to claim 1, it is characterised in that: also contain anticaking agent, the content of anticaking agent in the green onion salt For 0.0001-0.005wt%, anticaking agent is selected from lemon acid iron ammonium, potassium ferrocyanide, sodium ferrocyanide, tartaric acid iron, calcium silicates, two One or more of silica, calcium silicates.

6. green onion salt according to claim 1, it is characterised in that: the salt is no salt compounded of iodine or iodizedsalt, the iodizedsalt Propiodal be edible inorganic iodide or the rich organic propiodal of iodine.

7. the preparation method of green onion salt described in any one of claims 1-6, it is characterised in that: the preparation method is mechanical mixed Legal or concentrated crystallization.