CN106036609A - Blueberry chewable tablets and preparation method thereof - Google Patents
Blueberry chewable tablets and preparation method thereof Download PDFInfo
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- CN106036609A CN106036609A CN201610364118.1A CN201610364118A CN106036609A CN 106036609 A CN106036609 A CN 106036609A CN 201610364118 A CN201610364118 A CN 201610364118A CN 106036609 A CN106036609 A CN 106036609A
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Abstract
The invention provides a preparation method of blueberry chewable tablets. The blueberry chewable tablets are prepared from the following raw materials and component in parts by weight: 30-70 parts of blueberry fruit powder, 15-20 parts of milk powder, 7-10 parts of cane sugar, 1-3 parts of lactobacilli powder, 1-3 parts of bifidobacteria powder and 0.3-1 part of magnesium stearate. The distinctive blueberry chewable tablets prepared by the preparation method reserve the specific nutrient components and the specific physiological functions of blueberries, contain amino acids, mineral substances and B-group vitamin needed for human bodies, and are high in nutrient value; the blueberry chewable tablets provide a large quantity of lactic acid bacteria and bifidobacteria, so that the blueberry chewable tablets have the effects of strengthening the functions of the stomach and the intestines, and besides, the situation that bean curd residues produce sourness through lactic acid bacteria fermentation is avoided; inorganic selenium is transformed into organic selenium through microzymes, so that the content of the organic selenium is increased; and the autolysis characteristic of yeast is utilized, so that the fruit powder contains a large quantity of small peptide substances.
Description
Technical field
The present invention relates to a kind of blueberry chewable tablet product, be specifically related to the preparation method of blueberry chewable tablet, belong to food
Manufacture field.
Background technology
Blue berry has another name called blue berry, belongs to Ericaceae Vaccinium plant, and fruit is bluish violet, Blueberry averagely weigh 0.5～
2.5g, maximum weight 5g, edible rate is 100%, sweet and sour palatability, and has fragrant refreshing pleasant fragrance, for eating good merchantable brand raw.Blue berry contains
Multiple abundant aminoacid, trace element, anthocyanidin and the polyphenols such as anthocyanin and catechuic acid, wherein vaccinium oxycoccus pigment
Non-oxidizability is very strong, ophthalmology and cardiovascular and cerebrovascular disease is had preferable curative effect, can play the multiple efficacies such as aesthetic health care；Vitamin
Content is general, but vitamin E and pyridoxol content are relatively high；Flavonoid substances accounts for the 0.5% of dry weight, and this kind of material has fall blood
Pressure, vessel softening, prevent the effects such as arteriosclerosis, blood sugar lowering, minimizing cholesterol accumulation, and fruit juice is for carcinogen nitrous
Amine has capacity of decomposition.But owing to blue berry is perishable, it is not easy to storage and transport, limit the market sale week of blue berry
Phase, in order to meet the demand of people, market occurs in that blue berry fruit juice, fruit jam and solid beverage, can the inconvenience of existing blue berry product
In carrying, and blue berry seed and blue berry peel are all eliminated, and blue berry rich in anthocyanidin most be exactly peel, not only blue berry money
The waste in source, is also the loss of nutritional labeling.
A kind of blueberry chewable tablet of the Introduction To Cn Patent of Publication No. CN103070338A, described chewable tablet its formula group
Becoming: blue berry extract powder, white sugar, citric acid, maltodextrin, water soluble dietary fiber, flavoring orange essence, magnesium stearate etc. becomes
Point, size-reduced, mixing, pelletize, dry, the production technology such as compacting, the chewable tablet made, this method is the lowest to blue berry utilization rate, spy
It not that lipid soluble ingredients is not utilized effectively.
The Introduction To Cn Patent of Publication No. CN104473084A a kind of blueberry peel, slag multivitamin nutrient chewable tablet and preparation
Method, step is as follows: blue berry screens, and cleans and after blanch process, squeezes the juice.Take part blue berry fruit juice stand-by after pasteurization；
The blueberry peel after squeezing the juice, slag is through microwave vacuum drying and pulverizes, and grinds to form the blueberry powder of 100 mesh sieves.Take institute nutritious
Strengthening supplement, filler, correctives, wetting agent, lubricant are standby after pulverizing 150 mesh sieves.Take above-mentioned blueberry powder
30.0g, 12.2g microcrystalline Cellulose, 5.6g carboxymethyl cellulose, 15.2g maltodextrin, 1.0g phylloxanthin, 2.6g tea polyphenols,
6.0g xylitol, 4.0g fructose, 3.0g oligofructose, 3.0g stachyose, 6.0g maltose alcohol, 2.4g citric acid mix homogeneously；
Spraying adds blue berry fruit juice mix and blend and pelletizes, and being incremented by 30～50 DEG C heats up is dried granule, is dried in granule and adds
Enter 1.0g magnesium stearate, mix, feeding of sieving tablet machine, tabletted, make chewable tablet, described blueberry peel, slag are many
Dimension nutrient chewable tablet；Every weight is 0.6g/ sheet.This chewable tablet exists the process of blue berry seed thorough, in use
Feel the most coarse, do not meet Chinese consumption habit.
The Introduction To Cn Patent of Publication No. CN104544077A a kind of blue berry probiotic bacteria chewable tablet and manufacture method, step
Rapid as follows: the blue berry after cleaning is dried by changing temperature-pressure-difference and puffing, the technological parameter of changing temperature-pressure-difference and puffing: blue after hot air drying
Certain kind of berries moisture content 22%～24%, swelling temperature 80 DEG C, 25min dead time, evacuation temperature 65 DEG C～70 DEG C, vacuum be～
0.092MPa～～0.094MPa, be vacuum dried time 1.2h～1.4h, dried dried fruits water content is 3%～4%.Will be dry
Blue berry dried fruits after dry puts in pulverizer and is crushed to 80 mesh～100 mesh, i.e. obtains blueberry powder base material.In advance by adjuvant Fructus Hordei Germinatus
After the size-reduced machine of sugar alcohol, Sorbitol and citric acid is pulverized, cross 80 mesh～100 mesh sieves, with blueberry powder base material after crushed,
The Concha Ostreae powder being spray-dried puts in mixer together and mixes.After material is mixed in mixer, it is slowly added to
The ethanol of concentration of wetting agent 60%～70%, adjusts humidity of materials, makes soft material, and the soft durometer of soft material is typically pinched can become with hands
Group, light pressure then dissipates preferably.Being put in oscillating granulator by the soft material made and carry out pelletize, pelletize crosses 8 mesh～10 mesh after completing
Sieve；Being placed in by wet grain in 65 DEG C～70 DEG C of air dry ovens and be dried, 25min～30min stirs once, to accelerate rate of drying,
Dry terminal is down to 3%～5% with pellet moisture and is advisable.The stearic acid of its weight 0.6%～0.8% is added in dry granule
Magnesium, as lubricant, is simultaneously introduced the Bifidobacteria powder mix homogeneously that raw material weight ratio is 1～3, sends in tablet machine and presses
Sheet, irradiates 20min～30min under ultraviolet light by the tablet pressed and carries out sterilizing, pack in time, be finished product.This chewable tablet
There is also and blue berry seed is processed thoroughly, in use feel the most coarse, blue berry sarcocarp is not processed, make blue berry
The poor dispersion of fruit powder.
Summary of the invention
Poor for the mouthfeel of blueberry fresh fruit own, containing a large amount of fruit seeds in existing blueberry chewable tablet, blueberry powder viscosity is too high,
Blueberry pigment utilizes the problems such as too low, the present invention to provide a kind of blueberry chewable tablet and processing method thereof, can preserve to greatest extent
Blueberry pigment, fruit powder good dispersion are beneficial to tabletting, add again local flavor and the taste of chewable tablet, good palatability, cost simultaneously
Low, added value is high, and nutritious, make product have raising immunity, defying age, anticancer, prevent and treat hypertension, heart disease etc.
Health-care effect, is all-ages health food.
The present invention provide blueberry chewable tablet, be made up of with following weight portion the most each raw material composition: blueberry powder 30～
70 parts, milk powder 15～20 parts, sucrose 7～10 parts, lactobacillus mycopowder 1～3 parts, Bifidobacteria powder 1～3 parts, magnesium stearate
0.3～1 part.
Second object of the present invention is to provide the manufacture method of above-mentioned blueberry powder product, and it specifically comprises the following steps that
A, blueberry pomace is mixed with soybean cake powder or peanut cake powder, after the weight water such as addition, add pectase and albumen
Enzyme is stirred uniformly, and adjusting pH is 4～5, and enzymolysis 2～5h is put in fermentation tank, obtained enzymolysis solution, 100～110 DEG C of sterilizings
After 10～30min standby.
B, adding 2～5% sucrose, 0.5～5% yeast in enzymolysis solution, stir laggard aerobe fermentation of acting charitably, temperature
Controlling at 28～30 DEG C, fermentation time is 2～4 days, after 1mol/L salt acid for adjusting pH to 1～3,50～70 DEG C of insulations to 12
～20h obtains fermentation liquid.
C, by fermentation liquid with after filtered through gauze 2 times, then filter 1 time through microfilter, regulate with 1mol/L sodium hydroxide
After filtrate pH to 4.5～5.5, obtain blueberry pomace fermentation liquid.
D, by blueberry pomace fermentation liquid, water, Blueberry pigment, maltodextrin, stabilizer mix homogeneously by a certain percentage, obtain
Blue berry mixed liquor, wherein blueberry pomace fermentation liquid 30～80 parts, water 5～20 parts, Blueberry pigment 10～15 parts, maltodextrin 10～
30 parts, sodium carboxymethyl cellulose 0.2～1 part.
E, will allotment after blue berry mixed liquor be spray-dried, inlet temperature is 165 DEG C～185 DEG C, and leaving air temp is
65 DEG C～85 DEG C；The rotating speed 450 of sampling pump～700 revs/min, sample introduction pressure limit, 1～2MPa, obtains blueberry powder.
Amount g of blueberry pomace described in above-mentioned a step is 3～10:1 with the weight g ratio of soybean cake powder or peanut cake powder.
Pectase usage amount described in above-mentioned a step is 200～1000g/100kg blueberry pomaces, and wherein 1g pectase is lived
Power requires at more than 3000IU, can buy from market purchasing and obtain, the pectase that Jining and letter Bioisystech Co., Ltd produce.
Protease usage amount described in above-mentioned a step is 500～800g/100kg blueberry pomace, wherein 1g prolease activities
Require at more than 2000IU, can buy from market purchasing and obtain, the albumen that Dong Henghua road biology science and technology limited Company produces
Enzyme.
% described in above-mentioned steps refers to solid masses kg and liquor capacity L ratio.
Filtered through gauze described in above-mentioned step c refers to 2～3 layers of filtered through gauze, the pore size filter of microfilter be 0.6～
1.0μm。
Above-mentioned soybean cake powder or peanut cake powder refer to the leftover bits and pieces after oils and fats.
Above-mentioned yeast, lactobacillus, bacillus bifidus bacterium can directly buy acquisition, it is also possible to trained by conventional strain
Breeding method obtains bacterium solution or mycopowder.
Third object of the present invention is to provide the preparation method of above-mentioned Blueberry pigment and blueberry pomace, and its concrete steps are such as
Under:
(1) select without rot blue berry raw material clean, under the conditions of 45～55 DEG C air-dry, keep blue berry moisture be 30～
40%, blue berry is smashed to pieces, making beating, obtain blueberry pulp.
(2) blueberry pulp is added a certain amount of ethanol water, with 0.1mol/L salt acid for adjusting pH value to 2.5～5, super
Sound wave extraction 24h～48h, filters, repeats secondary, and merging filtrate, blueberry pomace is standby.
(3) filtrate carries out being evaporated to the 1/10～1/50 of original volume below 50 DEG C, and upper XDA-8 macroporous resin is inhaled
Attached, with the 50 of 3BV～15BV～80% ethanol water carry out gradient elution, collect to obtain eluent.
(4) eluent is evaporated to do below 50 DEG C, obtains Blueberry pigment.
Adding the volume L of ethanol water described in above-mentioned (2) step with the quality kg ratio of blueberry pulp is 1～4:1；Its
Middle ethanol water refers to 30～70% ethanol water.
The compound method of above-mentioned 30% ethanol water is: 30mL ethanol mixes after adding 70mL water.
Filter described in above-mentioned (2) step and refer to 2～3 layers of filtered through gauze.
Described in above-mentioned (3) step, BV refers to column volume.
70% ethanol water described in above-mentioned (3) step refers to that 70mL ethanol mixes after adding 30mL water.
Technique effect:
1, having distinctive blueberry chewable tablet, it remains nutritional labeling specific to blue berry and physiological function, contains again
The aminoacid of human body needs, mineral, vitamin B group, be of high nutritive value.
2, provide substantial amounts of lactic acid bacteria, double bacillus, there is enhancing action of enterogastric function, avoid Glycine max (L.) Merr. to pass through simultaneously
Lactic acid bacteria fermentation produces tart flavour.
3, utilize conversion of saccharomycetes inorganic selenium for organic selenium, to improve the content of organic selenium in fruit powder, utilize again yeast certainly
Molten feature, makes in fruit powder containing substantial amounts of little peptide material.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below with the embodiment of the present invention, but do not limit this with this
Invention.
Embodiment 1
Select the 200kg blue berry raw material without rotting to clean, air-dry under the conditions of 45～55 DEG C, make blue berry moisture control
30～40%, blue berry is smashed to pieces, making beating, obtain blueberry pulp.Taking 150L blueberry pulp, 70% ethanol adding 300L is water-soluble
Liquid, with 0.1mol/L salt acid for adjusting pH value to 4, ultrasonic-leaching 45h, 3 layers of filtered through gauze, repeat secondary, merging filtrate, gained
Blueberry pomace standby, the filtrate of gained is evaporated to the 1/30 of original volume below 50 DEG C, and upper XDA-8 macroporous resin is inhaled
Attached, with the 40 of 12BV～80% ethanol water carry out gradient elution, collect to obtain eluent, eluent reduced pressure below 50 DEG C
It is concentrated to dryness, obtains Blueberry pigment.
Embodiment 2
100kg blueberry pomace is mixed with 30kg soybean cake powder, after adding 130kg water, adds 500g pectase and 600g
Protease is stirred uniformly, and adjusting pH is 4.5, and enzymolysis 4h puts in fermentation tank, obtains enzymolysis solution, 100～110 DEG C of sterilizings
After 20min standby.In enzymolysis solution, add 10kg sucrose, 5g sodium selenite, 5kg yeast, be sealed into after stirring and act charitably
Aerobe fermentation 4 days, after 1mol/L salt acid for adjusting pH to 2, obtains fermentation liquid 70 DEG C of insulations to 18h.By fermentation liquid with 3 layers of gauze
After filtering 2 times, then the microfilter that via hole diameter is 0.8 μm filters 1 time, regulates filtrate pH to 4.5 with 1mol/L sodium hydroxide
After, obtain blueberry pomace fermentation liquid.Take 600g blueberry pomace fermentation liquid, 100g water, 150g Blueberry pigment, 200g maltodextrin, 5g
Sodium carboxymethyl cellulose, obtains blue berry mixed liquor.Being spray-dried by blue berry mixed liquor after allotment, inlet temperature is 165
DEG C～185 DEG C, leaving air temp is 65 DEG C～85 DEG C；The rotating speed 450 of sampling pump～700 revs/min, sample introduction pressure limit 1～
2MPa, obtains blueberry powder.Take blueberry powder 5kg, 1.6kg milk powder, 0.8kg sucrose, 0.2kg lactobacillus mycopowder, 0.3kg double
Discrimination bacillus mycopowder, 0.1kg magnesium stearate, after mixing, tabletting obtains blueberry chewable tablet.
Embodiment 3
200kg blueberry pomace is mixed with 50kg soybean cake powder, adds after 250kg water, add 1.2kg pectase and
1.5kg protease is stirred uniformly, and adjusting pH is 4.5, and enzymolysis 4h puts in fermentation tank, after 100～110 DEG C of sterilizing 20min
Obtain enzymolysis solution.In enzymolysis solution, add 25kg sucrose, 15g sodium selenite, 10kg yeast, be sealed into after stirring and act charitably
Aerobe fermentation 3 days, after 1mol/L salt acid for adjusting pH to 1.5, obtains fermentation liquid 60 DEG C of insulations to 15h.By fermentation liquid with 3 layers of yarn
After cloth filters 2 times, then the microfilter that via hole diameter is 1.0 μm filters 1 time, regulates filtrate pH to 5 with 1mol/L sodium hydroxide
After, obtain blueberry pomace fermentation liquid.Take 1kg blueberry pomace fermentation liquid, 150g water, 300g Blueberry pigment, 350g maltodextrin, 10g
Sodium carboxymethyl cellulose, obtains blue berry mixed liquor.Being spray-dried by blue berry mixed liquor after allotment, inlet temperature is 165
DEG C～185 DEG C, leaving air temp is 65 DEG C～85 DEG C；The rotating speed 450 of sampling pump～700 revs/min, sample introduction pressure limit 1～
2MPa, obtains blueberry powder.Take blueberry powder 5kg, 1.6kg milk powder, 0.8kg sucrose, 0.2kg lactobacillus mycopowder, 0.3kg double
Discrimination bacillus mycopowder, 0.1kg magnesium stearate, after mixing, tabletting obtains blueberry chewable tablet.
Comparative examples 1
100kg blueberry fresh fruit is mixed with 30kg soybean cake powder, after adding 130kg water, adds 500g pectase and 600g
Protease is stirred uniformly, and adjusting pH is 4.5, and enzymolysis 4h puts in fermentation tank, obtains enzymolysis solution, 100～110 DEG C of sterilizings
After 20min standby.In enzymolysis solution, add 10kg sucrose, 5g sodium selenite, 5kg yeast, be sealed into after stirring and act charitably
Aerobe fermentation 4 days, after 3 layers of filtered through gauze 2 times, then the microfilter that via hole diameter is 0.8 μm filters 1 time, uses 1mol/L hydrogen-oxygen
After changing sodium regulation filtrate pH to 4.5, obtain blueberry pomace fermentation liquid.Take 600g blueberry pomace fermentation liquid, 100g water, 200g Fructus Hordei Germinatus paste
Essence, 5g sodium carboxymethyl cellulose, obtain blue berry mixed liquor.Blue berry mixed liquor after allotment is spray-dried, inlet temperature
Being 165 DEG C～185 DEG C, leaving air temp is 65 DEG C～85 DEG C；The rotating speed 450 of sampling pump～700 revs/min, sample introduction pressure limit is 1
～2MPa, obtain blueberry powder.Take blueberry powder 5kg, 1.6kg milk powder, 0.8kg sucrose, 0.2kg lactobacillus mycopowder, 0.3kg
Bifidobacteria powder, 0.1kg magnesium stearate, after mixing, tabletting obtains blueberry chewable tablet.
Attached: the antioxidation contrast of various products
Precision weighs DPPH8.0mg, and with anhydrous alcohol solution and be settled in 200mL brown volumetric flask, obtaining concentration is
The DPPH solution of 0.004%, keeps in Dark Place, standby.After various sample 5g room temperatures are placed a period of time, DPPH reagent is used to enter
The mensuration of row antioxidation is shown in Table 1.
Table 1 various blueberry drink product is to DPPH antioxidation
Attached: DPPH method measures antioxidative concrete grammar: take respectively different trial each sample solution (0.24,0.48,
0.72,0.96,1.20mg/mL) 1.0mL, puts in 10mL centrifuge tube, adds the DPPH solution of 3.0mL, and room temperature lucifuge is reacted
30min, simultaneously with dehydrated alcohol as blank, measures light absorption value at 517nm wavelength.Calculate DPPH by following equation freely to remove
Rate.
The free clearance rate of DPPH (%)=A0-(AS-Ac)/A0× 100%
In formula, A0The absorbance of 1.0mL distilled water+3.0mLDPPH solution
ASThe absorbance of 1.0mL sample solution+3.0mLDPPH solution
AcThe absorbance of 1.0mL sample solution+3.0mL dehydrated alcohol
To test in triplicate, try to achieve the most on duty for the day of clearance rate.
Claims (8)
1. the present invention provides a kind of blueberry chewable tablet, is made up of with following weight portion the most each raw material composition: blueberry powder 30～
70 parts, milk powder 15～20 parts, sucrose 7～10 parts, lactobacillus mycopowder 1～3 parts, Bifidobacteria powder 1～3 parts, magnesium stearate
0.3～1 part.
2. the process of claim 1 wherein the manufacture method of blueberry powder product, it specifically comprises the following steps that
A, blueberry pomace is mixed with soybean cake powder or peanut cake powder, after the weight water such as addition, add pectase and protease enters
Row stirs, and adjusting pH is 4～5, and enzymolysis 2～5h is put in fermentation tank, obtained enzymolysis solution, 100～110 DEG C of sterilizings 10～
After 30min standby.
B, adding 2～5% sucrose, 0.5～5% yeast in enzymolysis solution, stir laggard aerobe fermentation of acting charitably, and temperature controls
At 28～30 DEG C, fermentation time is 2～4 days, after 1mol/L salt acid for adjusting pH to 1～3,50～70 DEG C of insulations to 12～
20h obtains fermentation liquid.
C, by fermentation liquid with after filtered through gauze 2 times, then filter 1 time through microfilter, regulate filtrate with 1mol/L sodium hydroxide
After pH to 4.5～5.5, obtain blueberry pomace fermentation liquid.
D, by blueberry pomace fermentation liquid, water, Blueberry pigment, maltodextrin, stabilizer mix homogeneously by a certain percentage, obtain blue berry
Mixed liquor, wherein blueberry pomace fermentation liquid 30～80 parts, water 5～20 parts, Blueberry pigment 10～15 parts, maltodextrin 10～30
Part, sodium carboxymethyl cellulose 0.2～1 part.
E, will allotment after blue berry mixed liquor be spray-dried, inlet temperature is 165 DEG C～185 DEG C, and leaving air temp is 65 DEG C
～85 DEG C；The rotating speed 450 of sampling pump～700 revs/min, sample introduction pressure limit, 1～2MPa, obtains blueberry powder.
3. the method for claim 2, wherein the weight g ratio of amount g of blueberry pomace described in a step and soybean cake powder or peanut cake powder
Example is 3～10:1.
4. the method for claim 2, wherein pectase usage amount described in a step is 200～1000g/100kg blueberry pomaces,
Wherein 1g pectinase activity requires at more than 3000IU, can buy from market purchasing and obtain, Jining and the letter limited public affairs of biotechnology
The pectase that department produces.
5. the method for claim 2, wherein protease usage amount described in a step is 500～800g/100kg blueberry pomaces, its
Middle 1g prolease activity requires at more than 2000IU, can buy from market purchasing and obtain, Dong Henghua road biotechnology Limited Liability
The protease that company produces.
6. the method for claim 2, wherein filtered through gauze described in step c refers to 2～3 layers of filtered through gauze, microfilter
Pore size filter is 0.6～1.0 μm.
7. the method for claim 1～6, wherein said Blueberry pigment and the preparation method of blueberry pomace, it specifically comprises the following steps that
(1) select without rot blue berry raw material clean, under the conditions of 45～55 DEG C air-dry, keep blue berry moisture be 30～
40%, blue berry is smashed to pieces, making beating, obtain blueberry pulp.
(2) blueberry pulp is added a certain amount of ethanol water, with 0.1mol/L salt acid for adjusting pH value to 2.5～5, ultrasound wave
Extraction 24h～48h, filters, and repeats secondary, and merging filtrate, blueberry pomace is standby.
(3) filtrate carries out being evaporated to the 1/10～1/50 of original volume below 50 DEG C, upper XDA-8 macroporous resin adsorption,
With the 50 of 3BV～15BV～80% ethanol water carry out gradient elution, collect to obtain eluent.
(4) eluent is evaporated to do below 50 DEG C, obtains Blueberry pigment.
8. the method for claim 7, wherein adds the volume L of ethanol water and the quality of blueberry pulp described in step (2)
Kg ratio is 1～4:1；Wherein ethanol water refers to 30～70% ethanol water.
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| CN107372836A (en) * | 2017-08-10 | 2017-11-24 | 山东阳春羊奶乳业有限公司 | A kind of sea-buckthorn blueberry goat milk piece and preparation method thereof |
| CN107712249A (en) * | 2017-11-27 | 2018-02-23 | 威海百合生物技术股份有限公司 | A kind of pressed candy and preparation method thereof |
| CN107744113A (en) * | 2017-09-28 | 2018-03-02 | 黑龙江绿知都生物科技开发有限公司 | A kind of compound aid digestion chewable tablets of children special-purpose blueberry |
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| CN107772463A (en) * | 2017-12-12 | 2018-03-09 | 贵阳学院 | A kind of blueberry pomace ferment lozenge |
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Application publication date: 20161026 |