CN109619528A - A kind of natto salt and preparation method thereof - Google Patents
A kind of natto salt and preparation method thereof Download PDFInfo
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- CN109619528A CN109619528A CN201811509250.2A CN201811509250A CN109619528A CN 109619528 A CN109619528 A CN 109619528A CN 201811509250 A CN201811509250 A CN 201811509250A CN 109619528 A CN109619528 A CN 109619528A
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- Prior art keywords
- natto
- salt
- iodine
- extract
- weighed
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- 235000013557 nattō Nutrition 0.000 title claims abstract description 364
- 150000003839 salts Chemical class 0.000 title claims abstract description 307
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- 239000002994 raw material Substances 0.000 claims abstract description 21
- 238000000034 method Methods 0.000 claims abstract description 16
- 239000000203 mixture Substances 0.000 claims abstract description 3
- 235000002639 sodium chloride Nutrition 0.000 claims description 343
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 150
- 229910052740 iodine Inorganic materials 0.000 claims description 149
- 239000011630 iodine Substances 0.000 claims description 149
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 81
- 239000000843 powder Substances 0.000 claims description 63
- 239000003795 chemical substances by application Substances 0.000 claims description 46
- 239000011780 sodium chloride Substances 0.000 claims description 45
- UOZDOLIXBYLRAC-UHFFFAOYSA-L [2-hydroxy-3-(trimethylazaniumyl)propyl]-trimethylazanium;diiodide Chemical compound [I-].[I-].C[N+](C)(C)CC(O)C[N+](C)(C)C UOZDOLIXBYLRAC-UHFFFAOYSA-L 0.000 claims description 38
- 239000013081 microcrystal Substances 0.000 claims description 36
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- 239000002245 particle Substances 0.000 claims description 22
- NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 claims description 18
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- KBPZVLXARDTGGD-UHFFFAOYSA-N 2,3-dihydroxybutanedioic acid;iron Chemical compound [Fe].OC(=O)C(O)C(O)C(O)=O KBPZVLXARDTGGD-UHFFFAOYSA-N 0.000 claims description 4
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 4
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- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 101710162629 Trypsin inhibitor Proteins 0.000 description 1
- 229940122618 Trypsin inhibitor Drugs 0.000 description 1
- 241001464837 Viridiplantae Species 0.000 description 1
- 229930003451 Vitamin B1 Natural products 0.000 description 1
- 229930003779 Vitamin B12 Natural products 0.000 description 1
- 229930003471 Vitamin B2 Natural products 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 108010028144 alpha-Glucosidases Proteins 0.000 description 1
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 1
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 235000019418 amylase Nutrition 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000002457 bidirectional effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000037182 bone density Effects 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 235000019504 cigarettes Nutrition 0.000 description 1
- AGVAZMGAQJOSFJ-WZHZPDAFSA-M cobalt(2+);[(2r,3s,4r,5s)-5-(5,6-dimethylbenzimidazol-1-yl)-4-hydroxy-2-(hydroxymethyl)oxolan-3-yl] [(2r)-1-[3-[(1r,2r,3r,4z,7s,9z,12s,13s,14z,17s,18s,19r)-2,13,18-tris(2-amino-2-oxoethyl)-7,12,17-tris(3-amino-3-oxopropyl)-3,5,8,8,13,15,18,19-octamethyl-2 Chemical compound [Co+2].N#[C-].[N-]([C@@H]1[C@H](CC(N)=O)[C@@]2(C)CCC(=O)NC[C@@H](C)OP(O)(=O)O[C@H]3[C@H]([C@H](O[C@@H]3CO)N3C4=CC(C)=C(C)C=C4N=C3)O)\C2=C(C)/C([C@H](C\2(C)C)CCC(N)=O)=N/C/2=C\C([C@H]([C@@]/2(CC(N)=O)C)CCC(N)=O)=N\C\2=C(C)/C2=N[C@]1(C)[C@@](C)(CC(N)=O)[C@@H]2CCC(N)=O AGVAZMGAQJOSFJ-WZHZPDAFSA-M 0.000 description 1
- ACTIUHUUMQJHFO-UPTCCGCDSA-N coenzyme Q10 Chemical compound COC1=C(OC)C(=O)C(C\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CCC=C(C)C)=C(C)C1=O ACTIUHUUMQJHFO-UPTCCGCDSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 235000019621 digestibility Nutrition 0.000 description 1
- 208000010643 digestive system disease Diseases 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229950003499 fibrin Drugs 0.000 description 1
- 235000019152 folic acid Nutrition 0.000 description 1
- 239000011724 folic acid Substances 0.000 description 1
- 229960000304 folic acid Drugs 0.000 description 1
- 208000018685 gastrointestinal system disease Diseases 0.000 description 1
- 235000006539 genistein Nutrition 0.000 description 1
- TZBJGXHYKVUXJN-UHFFFAOYSA-N genistein Natural products C1=CC(O)=CC=C1C1=COC2=CC(O)=CC(O)=C2C1=O TZBJGXHYKVUXJN-UHFFFAOYSA-N 0.000 description 1
- 229940045109 genistein Drugs 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 235000009569 green tea Nutrition 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 229960000367 inositol Drugs 0.000 description 1
- CDAISMWEOUEBRE-GPIVLXJGSA-N inositol Chemical compound O[C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@H](O)[C@@H]1O CDAISMWEOUEBRE-GPIVLXJGSA-N 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 150000002496 iodine Chemical class 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- LVPMIMZXDYBCDF-UHFFFAOYSA-N isocinchomeronic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)N=C1 LVPMIMZXDYBCDF-UHFFFAOYSA-N 0.000 description 1
- 229940118199 levulan Drugs 0.000 description 1
- 229920005610 lignin Polymers 0.000 description 1
- 229960004488 linolenic acid Drugs 0.000 description 1
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 1
- 235000019421 lipase Nutrition 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000000874 microwave-assisted extraction Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 229920001542 oligosaccharide Polymers 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- 235000020665 omega-6 fatty acid Nutrition 0.000 description 1
- 229940033080 omega-6 fatty acid Drugs 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000019161 pantothenic acid Nutrition 0.000 description 1
- 239000011713 pantothenic acid Substances 0.000 description 1
- 229940055726 pantothenic acid Drugs 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 229940085127 phytase Drugs 0.000 description 1
- 235000002949 phytic acid Nutrition 0.000 description 1
- 239000000467 phytic acid Substances 0.000 description 1
- 229940068041 phytic acid Drugs 0.000 description 1
- 229920002643 polyglutamic acid Polymers 0.000 description 1
- 229920001184 polypeptide Polymers 0.000 description 1
- 102000004196 processed proteins & peptides Human genes 0.000 description 1
- 235000019419 proteases Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- GJAWHXHKYYXBSV-UHFFFAOYSA-N pyridinedicarboxylic acid Natural products OC(=O)C1=CC=CN=C1C(O)=O GJAWHXHKYYXBSV-UHFFFAOYSA-N 0.000 description 1
- 150000003233 pyrroles Chemical class 0.000 description 1
- ADXCEOBGDCQCKM-UHFFFAOYSA-N quinoline-2,3-dione Chemical compound C1=CC=CC2=NC(=O)C(=O)C=C21 ADXCEOBGDCQCKM-UHFFFAOYSA-N 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000000837 restrainer Substances 0.000 description 1
- 229960002477 riboflavin Drugs 0.000 description 1
- 235000017709 saponins Nutrition 0.000 description 1
- CDAISMWEOUEBRE-UHFFFAOYSA-N scyllo-inosotol Natural products OC1C(O)C(O)C(O)C(O)C1O CDAISMWEOUEBRE-UHFFFAOYSA-N 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 229940082787 spirulina Drugs 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229960003495 thiamine Drugs 0.000 description 1
- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 235000010384 tocopherol Nutrition 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- 229960001295 tocopherol Drugs 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 239000002753 trypsin inhibitor Substances 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 description 1
- 235000010374 vitamin B1 Nutrition 0.000 description 1
- 239000011691 vitamin B1 Substances 0.000 description 1
- 235000019163 vitamin B12 Nutrition 0.000 description 1
- 239000011715 vitamin B12 Substances 0.000 description 1
- 235000019164 vitamin B2 Nutrition 0.000 description 1
- 239000011716 vitamin B2 Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/40—Table salts; Dietetic salt substitutes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Beans For Foods Or Fodder (AREA)
Abstract
The invention discloses a kind of natto salt and preparation method thereof, belong to food seasoning field.The present invention cleverly selects salt as carrier using natto and salt as primary raw material, and suitable natto and its extract are added by different modes, is uniformly mixed, Series Health natto product salt is made.According to the optimization of formulation condition, which can be used as edible salt and seasoning salt.The healthy natto salt prepared using technology path of the invention is had salt itself and rendered palatable the function of seasoning, and has the distinctive healthcare function of natto.Easy to operate, raw material sources are extensive, at low cost and environmentally friendly, and product stability is good, are convenient for large-scale industrial production.The method can control the content of natto nutriment in product, suitable for the preparation containing the natural drugs active ingredients salt such as other nattos and its derivative by the ratio of control natto and salt.
Description
Technical field
The present invention particularly belongs to food dressing field, is related to nutritive salt of vegetable ingredients and preparation method thereof.
Background technique
Natto is that soybean is manufactured after bacillus natto to ferment, a variety of rich in amino acid, organic acid, oligosaccharide etc.
The nutritional ingredient being easily absorbed by the body, while also containing several physiological active substances, as Nattokinase, superoxide dismutase,
Isoflavones, saponin(e element, tocopherol, vitamin etc..Since ancient times, natto is used as always dietotherapeutic food civil.Largely grind
Study carefully and show that natto has the function of a variety of medicine healthy sofas, often eats adjustable stomach, the intestines problems such as prevent constipation, diarrhea,
Bone density is improved, pre- preventing bone rarefaction can dissolve outmoded thrombus patch with bidirectional modulation blood pressure, adjust blood lipid, can eliminate tired
Labor, synthesis improve the immunity of the human body, can play the role of keeping fit and healthy, prevent disease.
Salt be all from ancient times to the present people life it is essential, be to one of most important substance of human survival, and
The daily salinity of general population is 5 ~ 8 grams.Thus it is guaranteed that, as the carrier of edible health care product, increasing while salt seasons
Its health-care efficacy is added to have become the research hotspot of food seasoning field.There are spirulina salt, mushroom salt etc. in China market at present
Plant salt product, but these product salts can only play seasoning and promote fragrant effect, be unable to satisfy the needs for improving human health.Certainly,
Also there is patent report that green tea powder is added in commodity salt and prepare health-care salt, but the health-care salt haves the defects that poor taste.
This patent is by simple method uniformly mixed pretreated natto powder with salt according to a certain percentage, system
Standby natto salt healthy out, which, which has, adjusts stomach, reduces cholesterol, thrombus, reduces blood pressure, promote to digest, improve
The health-care efficacies such as immunity, anti-aging, pre- preventing bone rarefaction, can also be improved the shelf-life of natto, plays and brings out the best in each other
Effect, and the preparation method has many advantages, such as that process is simple, low energy consumption, environmentally protective, production life cycle is short, cheap, be easy to by
Customers are received.
According to the inventors knowledge, report is had no at present natto is added in salt, or prepared mouthfeel and health-care effect
Good vegetalitas eats the related patents and document of natto salt.
Summary of the invention
The purpose of the present invention is research and develop a kind of natto salt for high-incidence diseases such as current gastrointestinal disease, hypertension.This method
Have many advantages, such as that easy to operate, with short production cycle, product quality is good, environmentally protective, low energy consumption, cheap, it is easy to accomplish industrialization
Production；The product is received by vast demander, is had a vast market foreground by the way of green plant addition.
In order to solve the above technical problems, the present invention uses technical solution as described below:
A kind of natto salt, the natto salt include the natto of the edible salt of 0.01 ~ 99.99 parts by weight, 99.99 ~ 0.01 parts by weight
Raw material and 1 × 10-5~4×10-4The anticaking agent of part.
In terms of iodine, the natto salt further includes 1 × 10-5~4×10-5The propiodal of parts by weight.
The natto raw material selects the natto particle after the natto fermented, drying, smashed natto powder, natto extraction
One or more of object.
The natto extract passes through juicing extraction method, steam distillation, supercritical CO2Extraction method, ultrasonic wave added mention
It follows the example of, soxhlet extraction or zymohydrolysis extracting method extract.
The edible salt is using sea salt, lake salt, well salt, rock salt, lake salt, crude salt, refined salt, the various microelements of addition or battalion
One or more of feeding, extraordinary salt of flavor substance, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0
Mm, whiteness are 55% ~ 95% microcrystal grain.
The antagonist is selected from ferric citrate, potassium ferrocyanide, sodium ferrocyanide, tartaric acid iron, calcium silicates, titanium dioxide
One or more of silicon, calcium silicates.
The propiodal is using inorganic iodide or the organic propiodal of rich iodine.
The inorganic iodide uses Potassiumiodate or potassium iodide；The richness organic propiodal of iodine uses Thallus Laminariae (Thallus Eckloniae) extract, seaweed
Extract, thallus laminariae extract, seaweed extract, fresh band fish extracts, blood clam dry extracts, clam dry extracts, dried scallop extract,
One of mussel extract, sea cucumber extract, jellyfish extract, lobster extract are several, using preceding first dusting to 60 ~
200 mesh.
The natto salt the preparation method comprises the following steps: by edible salt, natto raw material and anticaking agent pass through suitable addition manner
Uniformly mixing is carried out to get no iodine natto salt.
The natto salt suitably adds the preparation method comprises the following steps: edible salt, natto raw material and anticaking agent and propiodal are passed through
Add mode carries out uniformly mixing to get natto salt compounded of iodine.
It is specific the preparation method is as follows:
The selection and pretreatment of one, natto raw material
The selection of natto raw material can be natto particle, smashed natto powder, natto after the natto fermented, drying and extract
One or more of object.
Wherein the pretreating process of natto powder and natto extract is as follows:
1, pulverization process
(1) natto fermented is dried under suitable condition, obtains dry natto particle；
(2) it carries out dry natto particle to be ground to 20 ~ 2000 mesh, obtains natto powder.
2, natto extract juicing extraction method
(1) natto fermented is squeezed out the effective component in natto by oil press.
(2) natto effective component obtained above is filtered, filters out solid residue, recycle filtrate.
(3) filtrate that recycling obtains is descended into drying under proper condition, then spontaneous nucleation grinds to 20 ~ 2000 mesh, obtains
Natto extract.
3, natto extract steam distillation
(1) natto powder is weighed, is placed in round-bottomed flask, distilled water is added, it is slightly boiled to be heated to oil after connecting steam distillation device
Until amount does not increase, natto effective component distillation is obtained.
(2) natto effective component is descended into drying under proper condition, then spontaneous nucleation grinds to 20 ~ 2000 mesh, must receive
Beans extract.
4, natto extract supercritical CO2Extraction method
(1) natto powder is weighed, first a period of time preset in the state of middle pressure, room temperature；
(2) under higher extracting pressure, under certain extraction temperature, supercritical CO is utilized2Dynamic circulation extraction is carried out, reduction is passed through
Extract is precipitated in separating still in pressure and temperature, obtains natto effective component.
(3) natto effective component is descended into drying under proper condition, then spontaneous nucleation grinds to 20 ~ 2000 mesh, must receive
Beans extract.
5, natto extract ultrasound assisted extraction method
(1) natto powder is weighed, is put in conical flask, uses petroleum ether as solvent, is extracted under ultrasonication, is filtered.
(2) petroleum ether is continuously added in the conical flask for filling filter residue as solvent, is extracted under ultrasonication, is filtered.
And merge filtrate twice.
(3) petroleum ether is recycled in rotary evaporation, obtains natto effective component.
(4) natto effective component is dried, spontaneous nucleation under proper condition, then grinds to 20 ~ 2000 mesh, obtains natto
Extract.
6, natto extract soxhlet extraction
(1) natto powder is weighed, is wrapped with filter paper, is placed in Soxhlet extraction cylinder, petroleum ether is added, extracts.
(2) extracting solution recycles petroleum ether in rotary evaporation, obtains natto effective component.
(3) natto effective component is descended into drying under proper condition, then spontaneous nucleation grinds to 20 ~ 2000 mesh, must receive
Beans extract.
7, natto extract zymohydrolysis extracting method
(1) natto powder is weighed, water is added and is heated, stirring heat preservation appropriate time adds complex enzyme (cellulase, pectase etc.),
Under acid condition, digested in warm water
(2) add buck to adjust pH to alkalescent the natto powder after enzymatic hydrolysis, extract 3 times, be then centrifuged in boiling water, collect centrifugation
Liquid.
(3) above-mentioned centrifugate is concentrated in Rotary Evaporators, obtains natto effective component.
(4) natto effective component is descended into drying under proper condition, then spontaneous nucleation grinds to 20 ~ 2000 mesh, both obtained
Natto extract.
8, natto extract microwave loss mechanisms
(1) claim to remove natto powder, be put into microwave extraction tank, and ethyl alcohol is added.
(2) instrument is opened, regulation power, time carry out microwave abstracting.
(3) after the completion of extracting, cooling extracting solution, and by its condensing crystallizing, obtain brown viscous liquid.
(4) it by above-mentioned brown viscous liquid, is dried, and grinds to 20 ~ 2000 mesh, obtain natto extract.
The main component of natto extract includes Bacillus natto, Nattokinase, levulan, natto γ-polyglutamic acid, paddy ammonia
Sour polypeptide, saponin, isoflavones, unsaturated fatty acid, lecithin, folic acid, dietary fibre, farnoquinone, dipyridine acid, high resiliency
Protein, elastase, pyridinedicarboxylic acid, vitamin B1, vitamin B2, vitamin 6, vitamin B12, pantothenic acid, cigarette (Yan) acid,
Lignanoid, lecithin, cephalin, phosphatide phenol inositol, daidzein, linoleic acid, linolenic acid, omega-fatty acid, ω -6 fatty acid,
Mucoprotein, protease, amylase, lipase, cellulase, levansucrase, glutamate-transpeptidase are (GTP, urase, high-elastic
Property protease, phytase, pectase, trypsin inhibitor (STI), angiotensin converting enzyme-inhibiting peptide, FAS/ turn over element, more
Amine, alpha-glucosidase restrainer, superoxide dismutase, catalase, glutathione peroxidase, Co-Q10, Hu
Radish element, genistein, Genistin, trihydroxy -2- aminobenzoic acid, 2,3-, 2,5- and 3,4-Dihydroxybenzoic acid, amino
Glucose, 6- hydroxyl daidzein, 8- hydroxy dye lignin, 8- hydroxyl daidzein, X cancer-resisting substance, phytosterol, phytic acid, pyrroles's quinoline
The microelements such as numerous nutriments such as quinoline quinone and calcium, magnesium, phosphorus, potassium, iron, zinc, selenium, copper, manganese, molybdenum, chromium, nickel, vanadium, iodine.
The selection of two, salt: salt is selected to can be any salt that sea salt, lake salt, well salt, rock salt, lake salt etc. have found
Kind；It can be one of the extraordinary salt or several of crude salt, refined salt or the various microelements of addition or nutrition, flavor substance
Kind；Can be salt compounded of iodine (propiodal can be the edible inorganic iodide such as Potassiumiodate, potassium iodide and the rich organic propiodal of iodine: as kelp,
The food containing iodine such as seaweed, thallus laminariae, seaweed, fresh hairtail, blood clam are dry, clam is dry, dried scallop, mussel, sea cucumber, jellyfish, lobster are mentioned containing iodine
One of object or several is taken, preceding first dusting to 60 ~ 200 mesh is used), it is also possible to no salt compounded of iodine.The wherein purity of sodium chloride
It is 98% or more, partial size is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain.
Three, are by 0.01% ~ 99.99% part of edible salt, 99.99% ~ 0.01% part of natto raw material, with 1 × 10-5~4×10-4
Part anticaking agent (ferric citrate, potassium ferrocyanide, sodium ferrocyanide, tartaric acid iron, calcium silicates, silica, in calcium silicates
It is one or more of) uniformly mix to get no iodine natto salt by suitable addition manner；Or by 0.01% ~ 99.99% part
Edible salt, 99.99% ~ 0.01% part of natto raw material, with 1 × 10-5~4×10-4Part anticaking agent (ferric citrate, potassium ferrocyanide,
One or more of sodium ferrocyanide, tartaric acid iron, calcium silicates, silica, calcium silicates) and 1 × 10-5~4×10-5Part
Propiodal (in terms of iodine) carries out uniformly mixing by suitable addition manner to get natto salt compounded of iodine.
Preferably, there is less impurity to guarantee to be made natto salt, preferably prepare healthy natto salt, the salt
But any salt kind that sea salt, lake salt, well salt, rock salt, lake salt etc. have found；It is various micro- to can be crude salt, refined salt or addition
Secondary element or one or more of nutrition, the extraordinary salt of flavor substance；Can be salt compounded of iodine, (propiodal can be Potassiumiodate, iodine
Change the edible inorganic iodides such as potassium and the organic propiodal of rich iodine: as kelp, seaweed, thallus laminariae, seaweed, fresh hairtail, blood clam do, clam
One of extract containing iodine of the food containing iodine such as dry, dried scallop, mussel, sea cucumber, jellyfish, lobster is several, uses preceding first powder
Change to 60 ~ 200 mesh), it is also possible to no salt compounded of iodine.Wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, whiteness
For 55% ~ 95% microcrystal grain.
The health natto salt is divided into no iodine natto salt and natto salt compounded of iodine whether can be according to the addition of propiodal.
The purposes of the health natto salt can change according to the adjustment of salt and natto ratio: the higher Shi Jiankang of salt content
Natto salt application method is similar with common table salt；It is direct-edible when salt content is lower.It is received according to different health of formula
Beans salt can be used as edible salt and seasoning salt.
The beneficial effects of the present invention are:
Natto is added in salt 1. the invention is put forward for the first time, healthy natto salt is prepared, has filled up the field in a way
Blank.
2. by adding natto in daily flavouring salt, bring stink when avoiding individually eating natto, and receive
The preparation process of beans is relatively complicated, the duration is longer, in the long run, more has duration and generality using healthy natto salt.This hair
Bright natto used is not only to be possessed the nutritive value of soya bean by fermentation gained by soya bean, be rich in farnoquinone, raising albumen
The digestibility of matter, it is often more important that fermentation process produces several physiological active substances, has and dissolves internal fibrin
And other adjust the health-care effect of physiological function.
3. the healthy natto salt that natto is developed in conjunction with salt product, highlights the peculiar taste and color of natto.It can
Meet diversified demand of the consumer in terms of culinary art significantly, promotes the mouthfeel of dish.
4. natto can enrich the effect of salt, salt can increase the shelf-life of natto, can play and bring out the best in each other
Effect, and change natto and salt ratio, which is directly used as edible salt and seasoning salt.
5, the beneficial effects of the invention are as follows a kind of natto salt and preparation method thereof is provided, vegetable ingredients natto is added
In salt, the health-care effect of natto has been played to the greatest extent, is made people while reaching seasoning purpose using salt, is promoted
Itself health.
Specific embodiment
Combined with specific embodiments below, the present invention will be further described.It should be understood that following embodiment is merely to illustrate this
The person skilled in the art of the range of invention and is not intended to limit the present invention, the field can make one according to the content of foregoing invention
A little nonessential modifications and adaptations.
Embodiment 1
Preparation process without iodine health natto salt in the present embodiment in turn includes the following steps.
(1) natto is crushed, be sieved to obtain natto powder；
(2) weigh 99 parts of salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness be 55% ~
95% microcrystal grain.
(3) 1 part of natto powder obtained in step (1) is weighed, by itself and the weighed salt of step (2) and 1 × 10-5Part resistive connection
Agent carries out mechanical mixture and obtains powdered no iodine health natto salt.
Embodiment 2
Preparation process without iodine health natto salt in the present embodiment in turn includes the following steps.
(1) natto is crushed, be sieved to obtain natto powder；
(2) weigh 90 parts of salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness be 55% ~
95% microcrystal grain.
(3) 10 parts of natto powder obtained in step (1) are weighed, by itself and the weighed salt of step (2) and 2 × 10-5Part is anti-
Knot agent carries out mechanical mixture and obtains powdered no iodine health natto salt.
Embodiment 3
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto is crushed, be sieved to obtain natto powder；
(2) weigh 85 parts of salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness be 55% ~
95% microcrystal grain.
(3) 15 parts of natto powder obtained in step (1) and 1 × 10 are weighed-5(in terms of iodine, iodine is from iodine for part propiodal
Sour potassium uses preceding first dusting to 60 ~ 200 mesh), by itself and the weighed salt of step (2) and 3 × 10-5Part anticaking agent carries out mechanical
It is mixed to get powdered healthy natto salt compounded of iodine.
Embodiment 4
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto is crushed, be sieved to obtain natto powder；
(2) weigh 80 parts of salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness be 55% ~
95% microcrystal grain.
(3) measure suitable pure water, be heated to it is slightly boiled after, step (2) load weighted salt is slowly added to, is configured to
Saturated aqueous solution dissolves all salinities sufficiently.
(4) 20 parts of natto powder obtained in step (1) and 4 × 10 are weighed-5Part anticaking agent, is slowly added under mechanical stirring
Salt saturated aqueous solution prepared by step (3), and continue to stir 0.5 h or more in slight boiling condition, guarantee natto powder and resistive connection
Agent is uniformly dispersed in salt saturated aqueous solution.
(5) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled at 60 ~ 100 DEG C, is slowly steamed moisture
Out, by natto powder, salt and anticaking agent condensing crystallizing, residue is steamed until being placed in 60 ~ 100 DEG C of air dry oven when paste
Moisture obtains bulk without iodine health natto salt.
(6) to bulk obtained in step (5) without iodine health natto salt, quantitative screening is carried out according to blocky size, is obtained
Calibration is quantitative without iodine health natto salt.
Embodiment 5
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto is crushed, be sieved to obtain natto powder；
(2) 75 parts of salt salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain.
(3) 25 parts of natto powder obtained in step (1) is weighed and with 2 × 10-5Part propiodal is (in terms of iodine, from light
The extract containing iodine of dish and lobster uses preceding first dusting to 60 ~ 200 mesh), by itself and the weighed salt of step (2) and 5 × 10-5
Part anticaking agent carries out mechanical mixture and obtains powdered healthy natto salt compounded of iodine.
Embodiment 6
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto is crushed, be sieved to obtain natto powder；
(2) weigh 70 parts of salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness be 55% ~
95% microcrystal grain.
(3) 30 parts of processed natto powder and 3 × 10 are weighed in step (1)-5Part propiodal (in terms of iodine, iodine from
Potassiumiodate and potassium iodide use preceding first dusting to 60 ~ 200 mesh), by itself and the weighed salt of step 2 and 6 × 10-5Part anticaking agent
It carries out mechanical mixture and obtains powdered healthy natto salt compounded of iodine.
(4) to powdered health natto salt compounded of iodine quantitatively forms obtained in step (3) or sample dispenses, it is quantitative to obtain calibration
Healthy natto salt compounded of iodine.
The quantitative healthy natto salt compounded of iodine of the calibration being prepared in the present embodiment, can take and eat to natto according to different crowd
The demand of salt carries out quantitative use, easy can control daily usage amount.
Embodiment 7
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto is crushed, be sieved to obtain natto powder；
(2) 65 portions of salt are weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95%
Microcrystal grain.
(3) measure suitable pure water, be heated to it is slightly boiled after, step (2) load weighted salt is slowly added to, is configured to
Saturated aqueous solution dissolves all salinities sufficiently.
(4) 35 parts of natto powder obtained in step (1), 4 × 10 are weighed-5Part propiodal (in terms of iodine, from kelp,
The extract containing iodine of seaweed and dried scallop uses preceding first dusting to 60 ~ 200 mesh) and 7 × 10-5Part anticaking agent, delays under mechanical stirring
Slowly salt saturated aqueous solution prepared by step (3) is added, and continues to stir 0.5 h or more in slight boiling condition, guarantees natto powder
It is uniformly dispersed in salt saturated aqueous solution.
(5) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled at 60 ~ 100 DEG C, is slowly steamed moisture
Out, by natto powder, propiodal, anticaking agent and salt condensing crystallizing, until being placed in 60 when pasteoC~100 oIt is steamed in the air dry oven of C
Residual moisture out obtains blocky healthy natto salt compounded of iodine.
(6) pulverization process is carried out to the healthy natto salt compounded of iodine of bulk obtained in step (5), obtains powdered healthy natto iodine
Salt.
Health natto salt compounded of iodine made from the present embodiment is made using concentrated crystallization, and natto powder is allowed to be scattered in chlorination
Inside sodium particle, so that the two dispersion is more uniform, it can greatly reduce because dispersing uneven bring usage amount error.
Embodiment 8
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto is crushed, be sieved to obtain natto powder；
(2) 60 portions of salt are weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95%
Microcrystal grain.
(3) 40 parts of processed natto powder and 2 × 10 are weighed in step (1)-5Part propiodal is (in terms of iodine, from sea
Band, seaweed and thallus laminariae extract containing iodine, use preceding elder generation's dusting to 60 ~ 200 mesh), by it with the weighed salt of step (2) and
8×10-5Part anticaking agent carries out mechanical mixture and obtains powdered healthy natto salt compounded of iodine.
Embodiment 9
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto is crushed, be sieved to obtain natto powder；
(2) weigh 98 parts of salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness be 55% ~
95% microcrystal grain.
(3) 2 parts of processed natto powder and 3 × 10 are weighed in step (1)-5(in terms of iodine, iodine is from fresh for part propiodal
The extract containing iodine that hairtail, blood clam are dry and clam is dry uses preceding elder generation's dusting to 60 ~ 200 mesh), by it with the weighed salt of step (2) and
9×10-5Part anticaking agent carries out mechanical mixture and obtains powdered healthy natto salt compounded of iodine.
(4) to powdered health natto salt compounded of iodine quantitatively forms obtained in step (3) or sample dispenses, it is quantitative to obtain calibration
Healthy natto salt compounded of iodine.
The quantitative healthy natto salt compounded of iodine of the calibration being prepared in the present embodiment, can be according to different crowd to natto and salt
Demand carry out quantitative use, easy can control daily usage amount.
Embodiment 10
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto is dry, obtain natto particle.
(2) 10 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain.
(3) 90 parts of processed natto particle and 1 × 10 are weighed in step (1)-5(in terms of iodine, iodine comes from part propiodal
In dried scallop, mussel and the extract containing iodine of sea cucumber, preceding first dusting to 60 ~ 200 mesh is used), by itself and step (2) weighed salt
With 1 × 10-4Part anticaking agent carries out mechanical mixture and obtains powdered healthy natto salt compounded of iodine.
Embodiment 11
Preparation process without iodine health natto salt in the present embodiment in turn includes the following steps.
(1) natto is dry, obtain natto particle.
(2) 1 part of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain.
(3) measure suitable pure water, be heated to it is slightly boiled after, step (2) load weighted salt is slowly added to, is configured to
Saturated aqueous solution dissolves all salinities sufficiently.
(4) 99 parts of natto particle obtained in step (1) are weighed, is slowly added to prepared by step 3) under mechanical stirring
Salt saturated aqueous solution, and continue to stir 0.5 h or more in slight boiling condition, guarantee natto particle, anticaking agent and salt saturated water
It is uniformly mixed in solution.
(5) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled at 60 ~ 100 DEG C, is slowly steamed moisture
Out, by natto particle and salt condensing crystallizing, residual moisture is steamed until being placed in 60 ~ 100 DEG C of air dry oven when paste, is obtained
To bulk without iodine health natto salt.
(6) to bulk obtained in step (5) without iodine health natto salt, quantitative screening is carried out according to blocky size, is obtained
Calibration is quantitative without iodine health natto salt.
Embodiment 12
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto is dry, obtain natto particle；
(2) 0.01 part of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, whiteness 55%
~ 95% microcrystal grain.
(3) 99.99 parts of natto particle obtained in step (1) is weighed and with 2 × 10-5Part propiodal (in terms of iodine, comes from
In the extract containing iodine of mussel and lobster, preceding first dusting to 60 ~ 200 mesh is used), it is carried out with the weighed salt of step (2)
Mechanical mixture obtains powdered healthy natto salt compounded of iodine.
Embodiment 13
Preparation process without iodine health natto salt in the present embodiment in turn includes the following steps.
(1) natto that selection ferments is spare as raw material.
(2) 1 part of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain.
(3) measure suitable pure water, be heated to it is slightly boiled after, step (2) load weighted salt is slowly added to, is configured to
Saturated aqueous solution dissolves all salinities sufficiently.
(4) 99 parts of natto fermented in step (1) are weighed, are slowly added under mechanical stirring prepared by step (3)
Salt saturated aqueous solution, and continue to stir 0.5h or more in slight boiling condition, guarantee in natto, anticaking agent and salt saturated aqueous solution
It is uniformly mixed.
(5) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled 60 ~ 100oC slowly steams moisture
Out, by natto particle and salt condensing crystallizing, until paste, obtains no iodine health natto salt.
Embodiment 14
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto that selection ferments is spare as raw material.
(2) 98 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain.
(3) 2 parts of the natto that ferments in step (1) and 3 × 10 are weighed-5(in terms of iodine, iodine is from fresh band for part propiodal
The extract containing iodine that fish, blood clam are dry and clam is dry uses preceding first dusting to 60 ~ 200 mesh), by itself and the weighed salt of step (2) and 2
×10-4Part anticaking agent carries out mechanical mixture and obtains powdered healthy natto salt compounded of iodine.
(4) to powdered health natto salt compounded of iodine quantitatively forms obtained in step (3) or sample dispenses, it is quantitative to obtain calibration
Healthy natto salt compounded of iodine.
The quantitative healthy natto salt compounded of iodine of the calibration being prepared in the present embodiment, can be according to different crowd to natto and salt
Demand carry out quantitative use, easy can control daily usage amount.
Embodiment 15
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) choosing natto extract is raw material, spare；
(2) weigh 80 parts of salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness be 55% ~
95% microcrystal grain.
(3) measure suitable pure water, be heated to it is slightly boiled after, step (2) load weighted salt is slowly added to, is configured to
Saturated aqueous solution dissolves all salinities sufficiently.
(4) 20 parts of natto extract obtained in step (1) and 3 × 10 are weighed-4Part anticaking agent, under mechanical stirring slowly
Be added salt saturated aqueous solution prepared by step (3), and continue to stir 0.5 h or more in slight boiling condition, guarantee natto powder and
Anticaking agent is uniformly dispersed in salt saturated aqueous solution.
(5) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled at 60 ~ 100 DEG C, is slowly steamed moisture
Out, by natto powder, salt and anticaking agent condensing crystallizing, remaining water is steamed until being placed in 60 ~ 100 DEG C of air dry oven when paste
Point, bulk is obtained without iodine health natto salt.
(6) to bulk obtained in step (5) without iodine health natto salt, quantitative screening is carried out according to blocky size, is obtained
Calibration is quantitative without iodine health natto salt.
Embodiment 16
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) it chooses natto powder and natto extract is raw material, it is spare.
(2) 10 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain.
(3) 90 parts of processed natto powder and natto extract and 1 × 10 are weighed in step (1)-5Part propiodal is (with iodine
Meter, iodine use preceding first dusting to 60 ~ 200 mesh from dried scallop, mussel and the extract containing iodine of sea cucumber), by itself and step (2)
Weighed salt and 4 × 10-4Part anticaking agent carries out mechanical mixture and obtains powdered healthy natto salt compounded of iodine.
Embodiment 17
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) choosing natto powder, the natto fermented and natto extract is raw material, spare；
(2) weigh 70 parts of salt, wherein the purity of sodium chloride be 98% or more, partial size be 0.07 ~ 1.0 mm, whiteness be 55% ~
95% microcrystal grain.
(3) 30 parts of natto powder in step (1), the natto fermented and natto extract and 3 × 10 are weighed-5Part propiodal (with
Iodine meter, iodine use preceding first dusting to 60 ~ 200 mesh from Potassiumiodate and potassium iodide), by itself and step (2) weighed food
Salt and 3.5 × 10-4Part anticaking agent carries out mechanical mixture and obtains powdered healthy natto salt compounded of iodine.
(4) to powdered health natto salt compounded of iodine quantitatively forms obtained in step (3) or sample dispenses, it is quantitative to obtain calibration
Healthy natto salt compounded of iodine.
The quantitative healthy natto salt compounded of iodine of the calibration being prepared in the present embodiment, can take and eat to natto according to different crowd
The demand of salt carries out quantitative use, easy can control daily usage amount.
Embodiment 18
Preparation process without iodine health natto salt in the present embodiment in turn includes the following steps.
(1) natto is crushed, be sieved to obtain natto powder；
(2) 99.99 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain.
(3) 0.01 part of natto powder obtained in step (1) is weighed, by itself and the weighed salt of step (2) and 2.5 × 10-4
Part anticaking agent carries out mechanical mixture and obtains powdered no iodine health natto salt.
Embodiment 19
Preparation process without iodine health natto salt in the present embodiment in turn includes the following steps.
(1) natto that selection ferments is spare as raw material.
(2) 0.01 part of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, whiteness
For 55% ~ 95% microcrystal grain.
(3) measure suitable pure water, be heated to it is slightly boiled after, step (2) load weighted salt is slowly added to, is configured to
Saturated aqueous solution dissolves all salinities sufficiently.
(4) 99.99 parts of natto fermented in step (1) are weighed, are slowly added to prepared by step 3) under mechanical stirring
Salt saturated aqueous solution, and slight boiling condition continue stir 0.5 h or more, guarantee natto, anticaking agent and salt saturation it is water-soluble
It is uniformly mixed in liquid.
(5) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled 60 ~ 100oC slowly steams moisture
Out, by natto particle and salt condensing crystallizing, until paste, obtains no iodine health natto salt.
Embodiment 20
Preparation process without iodine health natto salt in the present embodiment in turn includes the following steps.
(1) natto that selection ferments is spare as raw material.
(2) 0.05 part of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, whiteness
For 55% ~ 95% microcrystal grain.
(3) measure suitable pure water, be heated to it is slightly boiled after, step (2) load weighted salt is slowly added to, is configured to
Saturated aqueous solution dissolves all salinities sufficiently.
(4) 99.95 parts of natto fermented in step (1) are weighed, are slowly added to prepared by step 3) under mechanical stirring
Salt saturated aqueous solution, and slight boiling condition continue stir 0.5 h or more, guarantee natto, anticaking agent and salt saturation it is water-soluble
It is uniformly mixed in liquid.
(5) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled 60 ~ 100oC slowly steams moisture
Out, by natto particle and salt condensing crystallizing, until paste, obtains no iodine health natto salt.
Embodiment 21
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto is crushed, be sieved to obtain natto powder；
(2) 99.97 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain.
(3) 0.03 part of processed natto powder and 2 × 10 are weighed in step (1)-5Part propiodal (in terms of iodine, from
The extract containing iodine of kelp, seaweed and thallus laminariae uses preceding first dusting to 60 ~ 200 mesh), by itself and step (2) weighed salt
With 1.5 × 10-4Part anticaking agent carries out mechanical mixture and obtains powdered healthy natto salt compounded of iodine.
Embodiment 22
The preparation process of healthy natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto is crushed, be sieved to obtain natto powder；
(2) 0.04 part of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, whiteness 55%
~ 95% microcrystal grain.
(3) 99.96 parts of processed natto powder and 2 × 10 are weighed in step (1)-5Part propiodal (in terms of iodine, from
The extract containing iodine of kelp, seaweed and thallus laminariae uses preceding first dusting to 60 ~ 200 mesh), by itself and step (2) weighed salt
It carries out mechanical mixture and obtains powdered healthy natto salt compounded of iodine.
Embodiment 23
Preparation process without iodine natto salt in the present embodiment in turn includes the following steps.
(1) natto fermented is dried at 60 DEG C, obtains dry natto particle；
(2) it is sieved with 100 mesh sieve after being ground dry natto particle, obtains natto powder.
(3) 98 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain weighs 2 parts of natto powder obtained in step (2), it is carried out mechanical mixture with anticaking agent and obtains powder
Shape without iodine turmeric salt.
Embodiment 24
Preparation process without iodine natto salt in the present embodiment in turn includes the following steps.
(1) natto that will be fermented is squeezed out the natto effective component in turmeric by oil press.
(2) natto effective component obtained above is filtered, filters out solid residue, recycle filtrate.
(3) filtrate that recycling obtains is descended into drying under proper condition, then spontaneous nucleation is ground, sieve with 100 mesh sieve, both
Obtain natto extract.
(4) 90 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain weighs 10 parts of turmeric effective extract matter obtained in step (3), by itself and 2.5 × 10-5Part resistive connection
Agent carries out mechanical mixture and obtains powdered no iodine turmeric salt.
(5) powdered no iodine turmeric salt obtained in step (4) is quantitatively formed or sample dispenses, obtained surely gauged
Without iodine turmeric salt.
The calibration being prepared in the present embodiment is quantitative without iodine turmeric salt, can be according to different crowd to Turmeric P.E matter
Quantitative use is carried out with the demand of salt, easy can control daily amount.
Embodiment 25
The preparation process of natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) 100 g natto powders are weighed, are placed in 1000 mL round-bottomed flasks, 500 mL water are added, connect steam distillation
It is slightly boiled to be heated to natto distillation being obtained, through anhydrous Na until oil mass do not increase after device2SO4After drying, obtain natto effectively at
Point.
(2) natto effective component is dry at 60 DEG C, then spontaneous nucleation grinds, sieves with 100 mesh sieve, and has both obtained natto and has mentioned
Take object.
(3) 85 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain weighs 15 parts of natto extract obtained in step (2) and 1 × 10-5Part propiodal (in terms of iodine, iodine
From Potassiumiodate, preceding first dusting is used), by itself and 4.5 × 10-5Part anticaking agent carries out mechanical mixture and obtains powdered natto
Salt compounded of iodine.
Embodiment 26
The preparation process of natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) present 10 MPa of pressure of 200 g natto powders, preset 15 min in the state of 30 DEG C of temperature are weighed；
It (2) is 30 MPa in extracting pressure, extraction temperature is 45 DEG C, CO2Flow is 40 L h-1, the item of 120 min of extraction time
Dynamic circulation extraction is carried out under part, and extract is precipitated in separating still by reducing pressure and temperature, obtains natto effective component.
(3) natto effective component is dry at 60 DEG C, then spontaneous nucleation grinds, sieves with 100 mesh sieve, and has both obtained natto and has mentioned
Take object.
(4) 80 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain, is dissolved in distilled water, be heated to it is slightly boiled after, load weighted salt is slowly added to, saturated water is configured to
Solution dissolves all salinities sufficiently.
(5) 20 parts of natto extract and 5.5 × 10 are weighed obtained in step (3)-5Part anticaking agent, delays under mechanical stirring
It is slow that salt saturated aqueous solution prepared by step 4) is added, and continue to stir 0.5 h or more in slight boiling condition, guarantee that natto extracts
Object and anticaking agent are uniformly dispersed in salt saturated aqueous solution.
(6) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled 60oC or more slowly steams moisture
Out, by natto extract, salt and anticaking agent condensing crystallizing, until being placed in 60 when pasteoResidue is steamed in the air dry oven of C
Moisture obtains bulk without iodine natto salt product.
(7) to bulk obtained in step (6) without iodine natto salt, quantitative screening is carried out according to blocky size, is calibrated
Quantitatively without iodine natto salt.Or after crushing, quantitative molding is carried out according to the step (5) in embodiment 2 or sample dispenses, is determined
Gauged no iodine natto salt.
Embodiment 27
The preparation process of natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) claim 20 g natto powders, be put in the conical flask of 500 mL, use 200 mL petroleum ethers as solvent, make in ultrasound
With 30 min of lower extraction, filtering.
(2) 200 mL petroleum ethers are continuously added in the conical flask for filling filter residue as solvent, are extracted under ultrasonication
30 min, filtering.And merge filtrate twice.
(3) petroleum ether is recycled in 45 DEG C of rotary evaporations, obtains natto effective component.
(4) by natto effective component, at 60 DEG C then lower drying, spontaneous nucleation grind, sieve with 100 mesh sieve, and both obtain natto
Extract.
(5) 75 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain weighs 25 parts of natto extract obtained in step (4) and with 2 × 10-5Part propiodal (in terms of iodine,
From the extract containing iodine of mussel and lobster, preceding first dusting to 60 ~ 200 mesh is used), it is subjected to mechanical mixture with anticaking agent
Obtain powdered natto salt compounded of iodine.
Embodiment 28
The preparation process of natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) claim 20 g natto powders, wrapped, be placed in Soxhlet extraction cylinder with filter paper, 300 mL petroleum ethers are added, are mentioned at 85 DEG C
Take 6 h.
(2) extracting solution is in 45oC rotary evaporation recycles petroleum ether, obtains natto effective component.
(3) by natto effective component, at 60 DEG C then lower drying, spontaneous nucleation grind, sieve with 100 mesh sieve, and both obtain natto
Extract.
(4) 70 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain weighs in step (3) 30 parts of processed natto extract and 3 × 10-5Part propiodal (in terms of iodine,
Iodine uses preceding first dusting from Potassiumiodate and potassium iodide), by itself and 6.5 × 10-5Part anticaking agent carries out mechanical mixture and obtains powder
The natto salt compounded of iodine of last shape.
(5) powdered natto salt compounded of iodine obtained in step (4) is quantitatively formed or sample dispenses, obtain surely gauged receive
Beans salt compounded of iodine.
The calibration being prepared in the present embodiment quantifies natto salt compounded of iodine, can be according to different crowd to natto extract and food
The demand of salt carries out quantitative use, easy can control daily amount.
Embodiment 29
The preparation process of natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) claim 40 g natto powders, water is added to be warming up to 90 DEG C, stirring 2 h of heat preservation add complex enzyme (cellulase, pectase
Deng), in acid condition, digested in warm water
(2) add buck to adjust pH to alkalescent the natto powder after enzymatic hydrolysis, extract 3 times, be then centrifuged in boiling water, collect centrifugation
Liquid.
(3) above-mentioned centrifugate is concentrated in Rotary Evaporators, obtains natto effective component.
(4) natto effective component being descended into drying under proper condition, then spontaneous nucleation is ground, it sieves with 100 mesh sieve, both
Natto extract.
(5) 65 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain, is dissolved in distilled water, be heated to it is slightly boiled after, load weighted salt is slowly added to, saturated water is configured to
Solution dissolves all salinities sufficiently.
(6) 35 parts of natto extract, 4 × 10 obtained in step (4) are weighed-5Part propiodal is (in terms of iodine, from sea
Band, seaweed and dried scallop extract containing iodine, use preceding elder generation's dusting to 60 ~ 200 mesh) and 8.5 × 10-5Part anticaking agent, is stirred in machinery
It mixes down and is slowly added to salt saturated aqueous solution prepared by step (5), and continue to stir 0.5 h or more in slight boiling condition, guarantee
Natto extract is uniformly dispersed in salt saturated aqueous solution.
(7) continue under conditions of mechanical stirring, the temperature of mixed liquor is controlled 60oC or more slowly steams moisture
Out, by natto extract, propiodal, anticaking agent and salt condensing crystallizing, until being placed in 60 when pasteoIt is steamed in the air dry oven of C
Residual moisture obtains blocky natto salt compounded of iodine.
(8) pulverization process is carried out to bulk natto salt compounded of iodine obtained in step (7), obtains powdered natto salt compounded of iodine.
Natto salt compounded of iodine made from the present embodiment is made using concentrated crystallization, and natto extract is allowed to be scattered in chlorination
Inside sodium particle, so that the two dispersion is more uniform, it can greatly reduce because dispersing uneven bring amount error.
Embodiment 30
The preparation process of natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto that will be fermented, is dried under suitable condition, obtains dry natto particle；
(2) dry natto particle is ground, obtains natto powder.
(3) 60 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain weighs in step (2) 40 parts of processed natto powder and 2 × 10-5Part propiodal (in terms of iodine, comes from
In the extract containing iodine of kelp, seaweed and thallus laminariae, preceding first dusting is used), by itself and 9.5 × 10-5Part anticaking agent carries out mechanical
It is mixed to get powdered natto salt compounded of iodine.
Embodiment 31
The preparation process of natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) natto that will be fermented is squeezed out the natto effective component in natto by oil press.
(2) natto effective component obtained above is filtered, filters out solid residue, recycle filtrate.
(3) filtrate that recycling obtains is descended into drying under proper condition, then spontaneous nucleation is ground, both obtained natto and extracted
Object.
(4) 98 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain weighs in step (3) 1 part of processed natto extract and 3 × 10-5Part propiodal (in terms of iodine,
Iodine uses preceding first dusting from fresh hairtail, the extract containing iodine that blood clam does and clam is dry), by itself and 2.8 × 10-4Part anticaking agent into
Row mechanical mixture obtains powdered natto salt compounded of iodine.
(5) powdered natto salt compounded of iodine obtained in step (4) is quantitatively formed or sample dispenses, obtain surely gauged receive
Beans salt compounded of iodine.
The calibration being prepared in the present embodiment quantifies natto salt compounded of iodine, can be according to different crowd to natto extract and food
The demand of salt carries out quantitative use, easy can control daily amount.
Embodiment 32
The preparation process of natto salt compounded of iodine in turn includes the following steps in the present embodiment.
(1) 100 g natto powders are weighed, are placed in 1000 mL round-bottomed flasks, 500 mL water are added, connect steam distillation
It is slightly boiled to be heated to obtaining natto effective component until oil mass do not increase after device.
(2) 98 parts of salt is weighed, wherein the purity of sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is
55% ~ 95% microcrystal grain weighs in step (1) 0.5 part of processed natto effective component and 1 × 10-5Part propiodal is (with iodine
Meter, iodine use preceding first dusting to 60 ~ 200 mesh from dried scallop, mussel and the extract containing iodine of sea cucumber), by itself and 7.5 × 10-5
Part anticaking agent carries out mechanical mixture and obtains powdered natto salt compounded of iodine.
Basic principles and main features and advantages of the present invention of the invention have been shown and described above.The skill of the industry
Art personnel it should be appreciated that the present invention is not limited to the above embodiments, the above embodiments and description only describe
The principle of the present invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these
Changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and
Its equivalent thereof.
Claims (10)
1. a kind of natto salt, it is characterised in that: the natto salt includes the edible salt of 0.01 ~ 99.99 parts by weight, 99.99 ~ 0.01
The natto raw material of parts by weight and 1 × 10-5~4×10-4Anticaking agent.
2. natto salt according to claim 1, it is characterised in that: further include 1 × 10 in terms of iodine-5~4×10-5Weight
The propiodal of part.
3. natto salt according to claim 1 or 2, it is characterised in that: the natto raw material is selected the natto fermented, done
One or more of natto particle, smashed natto powder, natto extract after dry.
4. natto salt according to claim 3, it is characterised in that: the natto extract is steamed by juicing extraction method, water
Steam distillation method, supercritical CO2Extraction method, ultrasound assisted extraction method, soxhlet extraction or zymohydrolysis extracting method extract.
5. natto salt according to claim 1 or 2, it is characterised in that: the edible salt uses sea salt, lake salt, well salt, rock
Salt, lake salt, crude salt, refined salt, the various microelements of addition or one or more of nutrition, the extraordinary salt of flavor substance,
The purity of middle sodium chloride is 98% or more, and partial size is 0.07 ~ 1.0 mm, and whiteness is 55% ~ 95% microcrystal grain.
6. natto salt according to claim 1 or 2, it is characterised in that: the antagonist is selected from ferric citrate, ferrous cyanogen
Change one or more of potassium, sodium ferrocyanide, tartaric acid iron, calcium silicates, silica, calcium silicates.
7. natto salt according to claim 1 or 2, it is characterised in that: the propiodal is had using inorganic iodide or rich iodine
Machine propiodal.
8. natto salt according to claim 7, it is characterised in that: the inorganic iodide uses Potassiumiodate or potassium iodide；
The richness organic propiodal of iodine is extracted using Thallus Laminariae (Thallus Eckloniae) extract, marine algae extract, thallus laminariae extract, seaweed extract, fresh hairtail
Object, blood clam dry extracts, clam dry extracts, dried scallop extract, mussel extract, sea cucumber extract, jellyfish extract, lobster are extracted
One of object is several, uses preceding first dusting to 60 ~ 200 mesh.
9. the preparation method of natto salt according to claim 1, it is characterised in that: by edible salt, natto raw material and resistive connection
Agent carries out uniformly mixing by suitable addition manner to get no iodine natto salt.
10. the preparation method of natto salt according to claim 2, it is characterised in that: by edible salt, natto raw material and resistive connection
Agent and propiodal uniformly mix to get natto salt compounded of iodine by suitable addition manner.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110150626A (en) * | 2019-07-02 | 2019-08-23 | 中盐工程技术研究院有限公司 | A kind of edible salt and preparation method thereof adding novel anticaking agent |
| CN112544888A (en) * | 2020-12-11 | 2021-03-26 | 天津市尖峰天然产物研究开发有限公司 | Preparation method of natto extract rich in spermidine |
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| CN112544888A (en) * | 2020-12-11 | 2021-03-26 | 天津市尖峰天然产物研究开发有限公司 | Preparation method of natto extract rich in spermidine |
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Application publication date: 20190416 |