CN106722770A

CN106722770A - A kind of new celery salt and preparation method thereof

Info

Publication number: CN106722770A
Application number: CN201611192031.7A
Authority: CN
Inventors: 米立伟; 刘宁; 崔世忠; 周松峰; 张风; 张一风; 陈卫华
Original assignee: Zhongyuan University of Technology
Current assignee: Zhongyuan University of Technology
Priority date: 2016-11-09
Filing date: 2016-12-21
Publication date: 2017-05-31

Abstract

The invention discloses a kind of new celery salt and preparation method thereof., as main body, by different modes be added in salt appropriate celery nutrients using different extractions, preparation technology by the present invention from salt, also can in right amount add anticaking agent, obtains edible celery product salt.The product that the present invention is prepared have functions that step-down, it is hypoglycemic, antitumor, anti-oxidant, mend iron blood-nourishing, pre- anti-cancer, protection cardiovascular system, protection liver, anti-oxidant calm the nerves.This invention is by with wide practical value and market prospects.

Description

A kind of new celery salt and preparation method thereof

Technical field

The present invention particularly belongs to food dressing field, is related to the extraction process of vegetable ingredients and a kind of system of celery salt Standby technology.

Background technology

Salt, is one of important substance needed for human survival, and Main Ingredients and Appearance is sodium chloride（NaCl）.Ancients are initially boiling The method of seawater has obtained sea salt.As people constantly deepen to recognize to salt, salt has become the mankind as edible flavouring Life and the indispensable necessity of diet.

In recent years, the disease serious crisis such as cancer, hypertension, high fat of blood the healthy of the mankind.According to research institution Issue《The year two thousand twenty health medical treatment prediction address》It has been shown that, China's Hypertensive Population quantity is higher than 160,000,000, people with hyperlipidemia number Amount is higher than 100,000,000, and Health risk has been broken out comprehensively in China, and China is into global first " three high "（Hypertension, high fat of blood is high Blood sugar）State, except having a strong impact on hundreds of millions of Chinese people's health and lives, will also cause huge production rate to be lost, so that aggravating national warp Ji burden.

As the mankind show meals and disease correlation studies, some foods have step-down, mend iron blood-nourishing, pre- anti-cancer, Oxidation resistant effect, obtains active ingredient by people's common concern from food.Celery is that a kind of common Umbelliferae is planted Thing, flavonoid compound is contained in celery nutrients, is distributed widely in Thymelaeceae, Verenaceae, Spikemoss plant, energy Enough effectively prevention kinds cancers, such as stomach cancer, lung cancer, colon cancer, breast cancer, while also having step-down, anti-oxidant, tranquilizing and allaying excitement Effect, with other Flavonoid substances（Kaempferia galamga flavones）Compare, the features such as with low toxicity, without mutagenesis.Current existing addition celery In the product salt of dish nutrients, there is the product salt that with the addition of Celeryseed extract, the celery that its raw material sources is used with the present invention Base of leaf has significant difference；Have in addition using the plant salt of celery nutrients, its main component has notable difference with the present invention, and originally The preparation process condition of invention is gentle, process cleans contamination-free, and active constituent content is higher in celery nutrients, there is good Development prospect.

This patent passes through the simple directly method such as mechanical mixing, condensing crystallizing mixing method by celery nutrients and salt Uniformly mixed according to a certain percentage, prepared a kind of new celery salt, the product is had step-down, mends iron blood-nourishing, pre- anti-cancer Disease, anti-oxidant effect calmed the nerves, and the preparation method have that operation is simple, energy consumption is low, environmental protection, production life cycle are short, honest and clean The advantages of valency, it is easy to received by numerous clients.

The content of the invention

The purpose of the present invention is salt product category on supplement existing market, and realization is reached pre- by edible celery product salt Anti-cancer, step-down mend the purpose of iron.The preparation method of this kind of salt has process is simple, raw material natural harmless, environmental protection, cost Low advantage, it is easy to accomplish large-scale production；The primary raw material of the product is constituted from plant, and natural nuisance-free is easily needed The person of asking receives, with wide market prospects.

In order to solve the above technical problems, the present invention uses technical scheme as described below：A kind of new celery salt, the celery The main component of dish salt is salt and celery nutrients, and the content of celery nutrients is 0.09-33.4wt% in celery salt.

Celery nutrients is the one kind in celery powder and celery nutrition extract, and celery powder is made up of celery crushed after being dried Powder, celery nutrition extract is circumfluence method, leaching method, centrifugal process, enzyme process, supercritical methanol technology, any in microwave ultrasound method The material that method is extracted；One or more of celery nutrient source in Thymelaeceae, Verenaceae, Spikemoss plant.

The celery nutrients is apiolin, and the content of apiolin is 0.09-3 wt%.

Also contain anticaking agent in the new celery salt, the content of anticaking agent is 0.0006-0.0025wt%.

Anticaking agent derives from ferric citrate, potassium ferrocyanide, sodium ferrocyanide, tartaric acid iron, silica, calcium silicates In one or more.

The salt is that the propiodal of the iodizedsalt is that edible inorganic iodide or rich iodine are organic without salt compounded of iodine or iodizedsalt Propiodal.

One or more be chosen in sea salt, lake salt, well salt, rock salt or lake salt of the salt, chlorine in the salt The purity for changing sodium is more than 98%, and particle diameter is 0.07-1.0 mm, and whiteness is 55%-95% microcrystal grains.

The salt be chosen for crude salt, purified salt, crush washing salt, evaporate brine day and Cardia Salt or add it is various micro One or more in element or nutrition, the extraordinary salt of flavor substance, the purity of the Sodium Chloride in Salt is more than 98%, Particle diameter is 0.07-1.0 mm, and whiteness is 55%-95% microcrystal grains.

Described preparation method is mechanical mixing, is comprised the following steps that：

1）Celery nutrients is dried into 4-12 hour at 60-150 DEG C, then control moisture be ground to 60- in 2%-20% 200 mesh；

2）By step 1）In the celery nutrients that treats, anticaking agent and salt carry out mechanical mixture and obtain powdered celery Salt.

Described preparation method comprises the following steps for condensing crystallizing method：

2）Appropriate pure water is measured, after being heated to micro-boiling, salt is slowly added to, be configured to saturated aqueous solution, stirred in machinery Mixing down makes all salinities fully dissolve；

3）By step 1）In celery nutrients and anticaking agent be slowly added to step 2 under mechanical stirring）Prepared salt is satisfied And the aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that celery nutrients, anticaking agent are in salt saturated aqueous solution In be uniformly dispersed；

4）After celery nutrients and anticaking agent are uniformly dispersed in salt saturated aqueous solution, continuing mechanical agitation, will mix The temperature control of liquid slowly steams moisture at 60-100 DEG C, by celery nutrients, anticaking agent and salt condensing crystallizing, to paste It is placed in during shape in 60 DEG C -100 DEG C of air dry oven and steams residual moisture, obtains block celery salt；

5）To step 4）In the block celery salt that obtains carry out pulverization process, obtain powdered celery salt.

Direct mechanical mixing gained celery salt is powder-product, can calibrate quantitative salt product as non-, or by shaping Or packing obtains calibrating quantitative salt product；Condensing crystallizing mixing method gained celery salt can carry out screening and classify according to salt particle size To calibration quantitative salt product, or non-calibration quantitative salt product are obtained after grinding.

Using above technical scheme, the beneficial effects of the invention are as follows：

1st, the invention is by extracting celery nutrients, and is added to the method in salt, prepares new celery salt, to a certain degree On filled up the salt species in the field.

2nd, by adding vegetable ingredients celery nutrients in daily flavouring salt, it is to avoid independent edible celery institute The mouthfeel of generation is single and is difficult to ensure that successional problem, in the long run, more has continuation using celery salt.It is of the invention used Celery nutrients, concentrate nutriment contained by celery, have more preferable health care preventive effect, the cancer using crowd can be reduced The occurrence probability of the disease such as disease and hypertension.

3rd, the preparation process is simple of celery salt of the present invention, strong operability, low cost, with market development potential, conscientiously may be used OK.

4th, the beneficial effects of the invention are as follows there is provided a kind of new celery salt and preparation method thereof.Natural plant extracts Rationally it is added in salt, on the basis of salt outward appearance is kept, highlights the peculiar taste and color and luster of apiolin.Can expire significantly Diversified demand of the sufficient consumer in terms of culinary art, lifts the mouthfeel of dish.

The beneficial effects of the invention are as follows there is provided a kind of new celery salt and preparation method thereof, vegetable ingredients celery battalion Foster thing is added in salt, has farthest played the health-care effect of celery nutrients, people is being used salt, reaches tune While taste purpose, moreover it is possible to promote the healthy of itself.

Specific embodiment

Present aspect is described in further detail below by embodiment, following examples be explanation of the invention and The invention is not limited in following examples.

Embodiment 1

Preparation technology without iodine celery salt in the present embodiment comprises the steps：

1）Circumfluence method prepares celery nutrients

A. the pretreatment of celery：500 grams of commercially available celery impurity eliminations are cleaned, is shredded (including leaf, stem) into 0.5 × 0.2cm²It is small Block, add water 2L, and at 80 DEG C, refluxing extraction 2 hours crosses 4 layers of filtered through gauze to water temperature；Filter residue adds water 1L, by the identical bar of preceding method Part carries out refluxing extraction again, and filtrate carries out suction filtration after merging, and vacuum is 0.85 MPa during suction filtration, and filtrate concentrates at 80 DEG C Dry, grind to form the powder of 100 mesh；

B. above-mentioned powder is dried 16 hours at 60 DEG C, control moisture below 2%, i.e. celery nutrients；

With apiolin, amino acid, calcium constituent, ferro element as primary product, extracted amount divides the celery nutrients that the above method is obtained Wei not 8.2g/kg（Celery）, 0.2g/kg（Celery）, 0.02g/kg（Celery）, 0.01g/kg（Celery）；

2）Mechanical mixing prepares celery salt

According to following percentage by weight preparation raw material：The celery nutrients of 0.09wt%, balance of salt（Sea salt is raw material）；

A. celery nutrients is dried into 12 hours at 60 DEG C, then control moisture be ground to 60 mesh 2%；

B. by step 1）In the celery nutrients and the salt that treat carry out mechanical mixture and obtain powdered celery salt.

Embodiment 2

1）Circumfluence method prepares celery nutrients

A. the pretreatment of celery：500 grams of commercially available celery impurity eliminations are cleaned, is shredded (including leaf, stem) into 0.5 × 0.2cm²It is small Block, plus the L of 80% ethanol water 2, at 80 DEG C, refluxing extraction 2 hours is filtered water temperature while hot；Filtrate carries out suction filtration, true during suction filtration Reciprocal of duty cycle is 0.85 MPa, and filtrate concentrate drying at 80 DEG C grinds to form the powder of 100 mesh；

B. above-mentioned powder is dried into 18 hours at 60 DEG C, control moisture is below 2%；That is celery nutrients；

The celery nutrients that the above method is obtained with apiolin, amino acid, calcium constituent, ferro element, vitamin B2 as primary product, Extracted amount is respectively 13.5g/kg（Celery）, 1.2g/kg（Celery）, 0.01g/kg（Celery）, 0.01g/kg（Celery）, 0.01g/ kg（Celery）；

2）Condensing crystallizing method prepares celery salt

According to following percentage by weight preparation raw material：Take celery nutrients, the potassium ferrocyanide of 0.001wt%, the surplus of 1.5wt% It is salt（Rock salt is raw material）；

A. celery nutrients is dried into 11 hours at 70 DEG C, then control moisture be ground to 80 mesh 5%；

B. appropriate pure water is measured, after being heated to micro-boiling, salt is slowly added to, be configured to saturated aqueous solution, stirred in machinery Mixing down makes all salinities fully dissolve；

C. by step 1）In celery nutrients and potassium ferrocyanide be slowly added to step 2 under mechanical stirring）Prepared food The salt loading aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that celery nutrients and potassium ferrocyanide are full in salt It is uniformly dispersed with the aqueous solution；

D. after celery nutrients and potassium ferrocyanide are uniformly dispersed in salt saturated aqueous solution, mechanical agitation is being continued, will The temperature control of mixed liquor slowly steams moisture at 60 DEG C, by celery nutrients, potassium ferrocyanide and salt condensing crystallizing, It is placed in during to pasty state in 60 DEG C of air dry oven and steams residual moisture, obtains block celery salt；

E. to step 5）In the block celery salt that obtains carry out pulverization process, obtain powdered celery salt.

Embodiment 3

1）Leaching method prepares celery nutrients

A. the pretreatment of celery：500 grams of commercially available celery impurity eliminations are cleaned, is shredded (including leaf, stem) into 0.5 × 0.2cm²It is small Block, crushes in plant pulverizer；

B. take the celery sample after crushing to be added to the water, leaching 6 hours is stirred under 300 revs/min of speed, 4 layers of yarn are crossed afterwards , again be added to the water celery after extracting by cloth, and such as above-mentioned step leaches twice again；

C. merge leaching liquid, original 50% be concentrated at 80 DEG C, after be centrifuged, 4000 revs/min of rotating speed, 60 after filtering Dried at DEG C, grind to form 100 mesh powders, i.e. celery nutrients；

With apiolin, amino acid, vitamin B2 as primary product, extracted amount is respectively the celery nutrients that the above method is obtained 10.5g/kg（Celery）, 1.6g/kg（Celery）, 0.01g/kg（Celery）；

2）Condensing crystallizing method prepares celery salt

According to following percentage by weight preparation raw material：Take the celery nutrients of the 5.5wt%, sodium ferrocyanide of 0.0015wt%, remaining It is salt to measure（Lake salt is raw material）；

A. celery nutrients is dried into 10 hours at 80 DEG C, then control moisture be ground to 150 mesh 10%；

C. by step 1）In celery nutrients, sodium ferrocyanide be slowly added to step 2 under mechanical stirring）Prepared food The salt loading aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that celery nutrients and sodium ferrocyanide are full in salt It is uniformly dispersed with the aqueous solution；

D. after celery nutrients and sodium ferrocyanide are uniformly dispersed in salt saturated aqueous solution, mechanical agitation is being continued, will The temperature control of mixed liquor slowly steams moisture at 80 DEG C, by celery nutrients, sodium ferrocyanide and salt condensing crystallizing, It is placed in during to pasty state in 80 DEG C of air dry oven and steams residual moisture, obtains block celery salt；

Embodiment 4

1）Leaching method prepares celery nutrients

A. the pretreatment of celery：500 grams of Selaginella tamariscina impurity eliminations are cleaned, 0.5 × 0.2cm is chopped into²Fritter, in plant pulverizer Middle crushing；

B. take in the Selaginella tamariscina sample addition 2L water after crushing, leaching 6 hours is stirred under 300 revs/min of speed, 4 layers are crossed afterwards Gauze, adds Selaginella tamariscina after extracting in 1 L water again, and such as above-mentioned step leaches twice again；

C. merge leaching liquid, original 60% be concentrated at 80 DEG C, after be centrifuged, 5000 revs/min of rotating speed, 50 after filtering Dried at DEG C, grind to form the powder of 200 mesh, i.e. celery nutrients；

With apiolin, vitamin B2, calcium constituent as primary product, extracted amount is respectively the celery nutrients that the above method is obtained 3.8g/kg（Celery）, 0.02g/kg（Celery）, 0.01g/kg（Celery）；

2）Mechanical mixing prepares celery salt

According to following percentage by weight preparation raw material：It is the celery nutrients of 10.0wt%, the tartaric acid iron of 0.0018wt%, balance of Salt（50% well salt and 50% lake salt are raw material）；

A. celery nutrients is dried into 8 hours at 100 DEG C, then control moisture be ground to 160 mesh 16%；

B. by step 1）In the celery nutrients that treats, tartaric acid iron and salt carry out mechanical mixture and obtain powdered celery Dish salt.

Embodiment 5

1）Leaching method prepares celery nutrients

A. the pretreatment of celery：500 grams of commercially available celery impurity eliminations are cleaned, 0.5 × 0.2cm is chopped into²Fritter, crushes in plant Crushed in machine；

B. take in 70% ethanol water of 2 L of celery sample addition after crushing, stirred under 300 revs/min of speed Leaching 5 hours, crosses 4 layers of gauze, adds celery again after extracting in 1 L ethanol waters, and such as above-mentioned step leaches secondary again；

C. merge leaching liquid, original 60% be concentrated at 70 DEG C, after be centrifuged, 4000 revs/min of rotating speed, 60 after filtering Dried at DEG C, grind to form the powder of 100 mesh, i.e. celery nutrients；

With apiolin, amino acid, vitamin B2 as primary product, extracted amount is respectively the celery nutrients that the above method is obtained 9.5g/kg（Celery）, 1.0g/kg（Celery）, 0.02g/kg（Celery）.

2）Mechanical mixing prepares celery salt

According to following percentage by weight preparation raw material：It is the celery nutrients of 15.0wt%, the silica of 0.0018wt%, balance of Salt（Crude salt is raw material）；

A. celery nutrients is dried into 8 hours at 120 DEG C, then control moisture be ground to 180 mesh 18%；

B. by step 1）In the celery nutrients that treats, silica and salt carry out mechanical mixture and obtain powdered celery Dish salt.

Embodiment 6

1）Enzyme process prepares celery nutrients

B. take crush after celery sample add 1 L water in, using the cellulase of 0.15mg/mL mass concentrations, 0.20mg/ The complex enzyme of mL pectases composition by mass degradations such as the cellulose in celery cell wall and cytoplasm, hemicellulose 1 hour, Hydrolysis temperature is 50 DEG C, pH=4.5；

C. the solution after enzymolysis is filtered, is centrifuged, 4000 revs/min of rotating speed, dried at 60 DEG C after filtering, ground to form The powder of 100 mesh, i.e. celery nutrients；

With apiolin, vitamin B2, ferro element as primary product, extracted amount is respectively the celery nutrients that the above method is obtained 1.2g/kg（Celery）, 0.02g/kg（Celery）, 0.01g/kg（Celery）；

2）Mechanical mixing prepares celery salt

According to following percentage by weight preparation raw material：The celery nutrients of 20.0wt%, the calcium silicates of 0.0020wt%, balance of food Salt（Purified salt is raw material）；

A. celery nutrients is dried into 6 hours at 130 DEG C, then control moisture be ground to 200 mesh 20%；

B. by step 1）In the celery nutrients that treats, calcium silicates and salt carry out mechanical mixture and obtain powdered celery Salt.

Embodiment 7

1）Supercritical CO₂Extraction prepares celery nutrients

A. the pretreatment of celery：500 grams of commercially available celery impurity eliminations are cleaned, 0.5 × 0.2cm is chopped into²Fritter, in Plant Powder Crushed in broken machine；

B. taking the celery sample after crushing carries out supercritical CO₂Extract, extraction conditions is；The MPa of extracting pressure 25, extraction temperature 50 DEG C, it is 35% as entrainer, consumption to use absolute ethyl alcohol, and extraction time is 4 hours, CO₂Flow 3.5 L/ minutes.Obtain Concentrate is dried, and grinds to form the powder of 100 mesh, i.e. celery nutrients；

With apiolin, vitamin B2 as primary product, extracted amount is respectively 9.6g/kg to the celery nutrients that the above method is obtained （Celery）, 0.02g/kg（Celery）；

2）Condensing crystallizing method prepares celery salt

According to following percentage by weight preparation raw material：Take the celery nutrients of 33.4.0wt%, the potassium ferrocyanide of 0.001wt% and 0.0025wt% ferric citrates, balance of salt（60% crushing washing salt and evaporate brine for 40% is raw material）；

A. celery nutrients is dried into 5 hours at 70 DEG C, then control moisture be ground to 110 mesh 20%；

C. by step 1）In celery nutrients, potassium ferrocyanide and ferric citrate be slowly added to step under mechanical stirring 2）Prepared salt saturated aqueous solution, and continue to stir 0.5 more than h in slight boiling condition, it is ensured that celery nutrients, ferrous cyanogen Change potassium and ferric citrate is uniformly dispersed in salt saturated aqueous solution；

D. after celery nutrients, potassium ferrocyanide and ferric citrate are uniformly dispersed in salt saturated aqueous solution, continuing Mechanical agitation, by the temperature control of mixed liquor at 100 DEG C, slowly steams moisture, by celery nutrients, potassium ferrocyanide and Ferric citrate and salt condensing crystallizing, are placed in 100 DEG C of air dry oven during to pasty state and steam residual moisture, obtain block Shape celery salt；

Embodiment 8

The preparation technology of celery salt in turn includes the following steps in the present embodiment：

1）After maintaining 121 DEG C to maintain sterilizing in 20 minutes in autoclave sterilization pot 300 parts of celery nutrients, done at 40 DEG C Dry 4 hours, obtain product A；

2）1000 parts are taken without iodine common salt, the salt includes that 30% crude salt, 50% purified salt, 20% crush washing salt, by 1000 parts without iodine Salt mixes 6 hours with product A consistent mechanicals, that is, obtain a kind of celery salt.

Embodiment 9

1）200 parts of celery nutrients are dissolved fully in 400 part of 70% ethanol water, product A is obtained；

2）1000 parts are taken without iodine common salt, the salt is the extraordinary salt for adding selenium（The raw material of extraordinary salt is lake salt）, by salt It is laid in drying pallet, the product A is uniformly sprayed on salt with the speed of 5 parts/minute, 40 DEG C is heated to pallet And kept for 24 hours, be less than 5% to moisture, that is, obtain a kind of celery salt.

Embodiment 10

1）By 200 parts of celery nutrients and 0.03 part of Potassiumiodate ultrasonic disperse in water, ultrasonic power is 30 KHzs, gained Dispersion liquid is product A；

2）1000 parts are taken without iodine common salt, the salt include 60% evaporate brine day and 40% Cardia Salt（Both raw materials are pond Salt）, 1000 parts being laid in without iodine common salt in drying pallet, product A is uniformly sprayed on salt with the speed of 10 parts/minute, And be heated to 60 DEG C and kept for 6 hours, be less than 5% to moisture, that is, obtain a kind of celery salt.

Embodiment 11

1）By 200 parts of celery nutrients, 0.03 part of Potassiumiodate and 1000 parts without iodine common salt（Add the extraordinary salt of zinc, special type food Salt is lake salt）The ultrasonic disperse in water, ultrasonic power is 40 KHzs, and gained dispersion liquid is product A;

2）By product A, freeze-day with constant temperature is crystallized for 48 hours at 80 DEG C, obtains crystallization block product B;

3）Product B is ground and is crushed to 300 mesh, obtain a kind of celery salt.

Embodiment 12

1）350 parts of celery nutrients and 0.01 part of Potassiumiodate are mechanically mixed directly, product A is obtained；

2）1000 parts are taken without iodine common salt, the salt includes the extraordinary salt of the extraordinary salt of 30% addition zinc and 70% addition calcium, will Product A and 1000 parts are uniform by mechanical mixture without iodine common salt, are laid in afterwards in drying pallet, and 40 DEG C are heated to pallet simultaneously Drying in 8 hours is kept, product B is obtained；

3）Product B is carried out the operation of metering process, the salt of fixed mass, the metering process is eaten every time with instant edible person Operation include:Weigh 1.5 grams of product B and insert tabletted in the mould of specific standard, obtain quantitative celery salt finished product.

Embodiment 13

The present embodiment is that iodine reinforcing agent derives from following steps with the difference of embodiment 10：

1）The pretreatment of marine alga：Marine alga is dried into 24 hours at 60 DEG C, control moisture uses stainless steel scissors below 2% It is cut into 0.5 × 0.2cm²Fritter after, in plant pulverizer crush；

2）Take in the seaweed sample 1 L water of addition after crushing, water temperature is 50 DEG C, and refluxing extraction 6 hours is filtered while hot, and filter residue adds 1 L water carries out secondary back extraction by preceding method, and filtrate merges, and it is rich iodine solution to obtain filtrate, after 80 DEG C of concentrate dryings 48 hours, Grind to form 100 mesh powders, i.e. iodine reinforcing agent；

The iodine reinforcing agent that the above method is obtained is with I^-, organic iodine, IO₃ ^-It is primary product, extracted amount is respectively 6.6g/kg（Sea Algae）, 1.2g/kg（Marine alga）、0.12g/kg（Marine alga）.

Embodiment 14

1）The pretreatment of marine alga：Marine alga is dried into 12 hours at 60 DEG C, control moisture is cut below 2% with stainless steel scissors Into 0.5 × 0.2cm²Fritter after, in plant pulverizer crush；

2）Take in the seaweed sample 2 L water of addition after crushing, leaching 8 hours is stirred under 350 revs/min of rotating speeds, cross 4 layers of yarn Cloth, adds marine alga after extracting in 1L water again, and such as above-mentioned step leaches secondary again；

3) merge leaching liquid, original 50% is concentrated at 60 DEG C, after be centrifuged, 4000 revs/min of rotating speed, 60 after filtering Dried at DEG C, grind to form the powder of 100 mesh, i.e. iodine reinforcing agent.

The iodine reinforcing agent that the above method is obtained is with I^-, organic iodine, IO₃ ^-It is primary product, extracted amount is respectively 7.1g/kg （Marine alga）, 0.2g/kg（Marine alga）、0.32g/kg（Marine alga）.

Embodiment 15

1）The pretreatment of marine alga：Marine alga is dried into 24 hours at 60 DEG C, control moisture is cut below 2% with stainless steel scissors Into 0.5 × 0.2cm²Fritter after, in plant pulverizer crush；

2）Take the seaweed sample after crushing to be added to the water, ultrasonic disperse 2 hours under being stirred at 200 revs/min, ultrasonic power is 20 KHz, dispersion liquid crosses 4 layers of gauze, and during marine alga to add 1L water again after extracting, such as ultrasonic extraction is once again for above-mentioned step；

3) merge leaching liquid, original 60% is concentrated at 70 DEG C, after be centrifuged, 3000 revs/min of rotating speed, 80 after filtering Dried at DEG C, grind to form the powder of 100 mesh, i.e. iodine reinforcing agent.

The iodine reinforcing agent that the above method is obtained is with I^-, organic iodine, IO₃ ^-It is primary product, extracted amount is respectively 8.1g/kg （Marine alga）, 3.7g/kg（Marine alga）、0.42g/kg（Marine alga）.

Embodiment 16

Celery powder is made after celery is dried, according to following percentage by weight preparation raw material：The celery powder of 20.0wt%, The calcium silicates of 0.0020wt%, balance of salt（Purified salt is raw material）；Afterwards celery salt is mixed to get by three kinds.

Embodiment 17

Preparation technology without iodine celery salt in the present embodiment in turn includes the following steps：

1）The apiolin of the plant extract of the commercialization that will be bought（From Thymelaeceae）6 hours are dried at 80 DEG C, so Grinding sieving, obtains the powder below 100 mesh afterwards, standby；

2）Weigh 10kg salt（As obtained by sea salt as raw material）；

3）Weigh step 1）In treat apiolin 0.1g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Last shape without iodine celery salt.

Embodiment 18

1）The apiolin of the plant extract of the commercialization that will be bought（From Verenaceae）12 hours are dried at 60 DEG C, Then grinding sieving, obtains the powder below 100 mesh, standby；

2）Weigh 10kg salt（As obtained by lake salt as raw material）；

3）Weigh step 1）In treat apiolin 5g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Shape without iodine celery salt.

Embodiment 19

1）The apiolin of the plant extract of the commercialization that will be bought（From Selaginaceae）8 hours are dried at 100 DEG C, so Grinding sieving, obtains the powder below 200 mesh afterwards, standby；

2）Weigh 10kg salt（As obtained by well salt as raw material）；

3）Weigh step 1）In treat apiolin 1g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Shape without iodine celery salt.

Embodiment 20

1）The apiolin of the plant extract of the commercialization that will be bought dries 7 hours at 120 DEG C, and then grinding sieving, obtains Powder to below 150 mesh, it is standby；

2）Weigh 10kg salt（As obtained by well salt as raw material）；

3）Weigh step 1）In treat apiolin 20g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Last shape without iodine celery salt.

Embodiment 21

1）The apiolin of the plant extract of the commercialization that will be bought dries 6 hours at 80 DEG C, and then grinding sieving, obtains Powder below 100 mesh, it is standby；

2）Weigh 10kg salt（As obtained by lake salt as raw material）；

3）Weigh step 1）In treat apiolin 0.2g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Last shape without iodine celery salt；

4）To step 3）In powdered quantitatively the shaping without iodine celery salt that obtains obtain 0.6g sheet salt particles, obtain calibration quantitative Without iodine celery salt.

The calibration being prepared from the present embodiment is quantitative without iodine celery salt, can be according to different crowd to apiolin and salt Demand quantitatively used, being capable of the daily usage amount of easy control.

Embodiment 22

1）The apiolin of the plant extract of the commercialization that will be bought（From Verenaceae）4 hours are dried at 80 DEG C, Then grinding sieving, obtains the powder below 100 mesh, standby；

2）Weigh 10kg salt（As obtained by lake salt as raw material）；

3）Weigh step 1）In treat apiolin 0.6g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Last shape without iodine celery salt；

4）To step 3）In powdered quantitatively the shaping without iodine celery salt that obtains obtain the spherical salt particles of 0.5g, obtain calibration fixed Amount without iodine celery salt.

Embodiment 23

1）The apiolin of the plant extract of the commercialization that will be bought dries 5 hours at 120 DEG C, and then grinding sieving, obtains Powder to below 200 mesh, it is standby；

2）Weigh 10kg salt（As obtained by sea salt as raw material）；

3）Weigh step 1）In treat apiolin 5g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Shape without iodine celery salt；

4）To step 3）In powdered quantitatively the shaping without iodine celery salt that obtains obtain 0.2g sheet salt particles, obtain calibration quantitative Without iodine celery salt.

Embodiment 24

1）The apiolin of the plant extract of the commercialization that will be bought dries 9 hours at 60 DEG C, and then grinding sieving, obtains Powder below 100 mesh, it is standby；

2）Weigh 10kg salt（As obtained by well salt as raw material）；

3）Weigh step 1）In treat apiolin 20g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Last shape without iodine celery salt；

4）To step 3）In powdered quantitatively the shaping without iodine celery salt that obtains obtain 0.1g sheet salt particles, obtain calibration quantitative Without iodine celery salt.

Embodiment 25

1）The apiolin of the plant extract of the commercialization that will be bought（From Thymelaeceae）8 hours are dried at 90 DEG C, so Grinding sieving, obtains the powder below 100 mesh afterwards, standby；

2）Weigh 10kg salt（As obtained by rock salt as raw material）；

3）Weigh step 1）In treat apiolin 1g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Shape without iodine celery salt；

4）To step 3）In powdered quantitatively the shaping without iodine celery salt that obtains obtain 0.5g sheet salt particles, obtain calibration quantitative Without iodine celery salt.

Embodiment 26

2）Weigh 10kg salt（As obtained by well salt as raw material）；

3）Appropriate pure water is measured, after being heated to micro-boiling, by step 2）Load weighted salt is slowly added to, and is configured to saturation water Solution, makes all salinities fully dissolve under mechanical stirring；

4）Weigh step 1）In treat apiolin 0.5g, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied And the aqueous solution, continue to stir 0.5 more than h, it is ensured that apiolin is uniformly dispersed in salt saturated aqueous solution；

5）After apiolin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor Temperature control slowly steams moisture at 70 DEG C, by apiolin and salt condensing crystallizing, 80 DEG C of air blast is placed in during to pasty state Residual moisture is steamed in drying box, bulk is obtained without iodine celery salt；

6）To step 5）In obtain bulk carry out pulverization process without iodine celery salt, obtain powdered without iodine celery salt.

The present embodiment is obtained to be obtained without iodine celery salt using condensing crystallizing method so that apiolin can be scattered in sodium chloride Inside particle so that both are scattered more uniform, can greatly reduce because of the uneven usage amount error brought of dispersion.

Embodiment 27

The preparation technology of iodine celery salt is added in turn include the following steps in the present embodiment：

1）The apiolin of the plant extract of the commercialization that will be bought dries 12 hours at 60 DEG C, and then grinding sieving, obtains Powder to below 60 mesh, it is standby；

2）Weigh 10kg salt（As obtained by well salt as raw material）；

4）Weigh step 1）In treat apiolin 1g, step 3 is slowly added under mechanical stirring）Prepared salt saturation The aqueous solution, continues to stir 2 more than h, it is ensured that apiolin is uniformly dispersed in salt saturated aqueous solution；

5）After apiolin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor Temperature control slowly steams moisture at 100 DEG C, by apiolin and salt condensing crystallizing, 90 DEG C of air blast is placed in during to pasty state Residual moisture is steamed in drying box, block plus iodine celery salt product are obtained, wherein propiodal is edible inorganic iodide；

6）To step 5）In after the bulk that obtains plus iodine celery salt crushed as the powdery product below 60 mesh, quantitative shaping is obtained 0.2g slabbing salt particles, obtain surely gauged plus iodine celery salt.

Embodiment 28

1）The apiolin of the plant extract of the commercialization that will be bought dries 9 hours at 80 DEG C, standby；

2）Weigh 10kg salt（As obtained by sea salt as raw material）；

4）Weigh step 1）In treat apiolin 0.1g, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied And the aqueous solution, continue to stir 2 more than h, it is ensured that apiolin is uniformly dispersed in salt saturated aqueous solution；

5）After apiolin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor Temperature control steams moisture at 80 DEG C, is placed in during to pasty state in 100 DEG C of air dry oven and steams residual moisture, obtains block Shape adds iodine celery salt product, and wherein propiodal is the organic propiodal of rich iodine；

6）To step 5）In after the bulk that obtains plus iodine celery salt crushed as the powdery product below 100 mesh, be quantitatively molded To 0.5g slabbing salt particles, surely gauged plus iodine celery salt is obtained.

Embodiment 29

1）The apiolin of the plant extract of the commercialization that will be bought dries 6 hours at 70 DEG C, standby；

2）Weigh 10kg salt（As obtained by lake salt as raw material）；

4）Weigh step 1）In treat apiolin 2g, step 3 is slowly added under mechanical stirring）Prepared salt saturation The aqueous solution, continues to stir 1 more than h, it is ensured that apiolin is uniformly dispersed in salt saturated aqueous solution；

5）After apiolin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor Temperature control steams moisture at 80 DEG C, is placed in during to pasty state in 70 DEG C of air dry oven and steams residual moisture, obtains bulk Without iodine celery salt product；

Embodiment 30

1）The apiolin of the plant extract of the commercialization that will be bought dries 6 hours at 80 DEG C, standby；

2）Weigh 10kg salt（As obtained by lake salt as raw material）；

4）Weigh step 1）In treat apiolin 15g, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied And the aqueous solution, continue to stir 2 more than h, it is ensured that apiolin is uniformly dispersed in salt saturated aqueous solution；

5）After apiolin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor Temperature control steams moisture at 80 DEG C, is placed in during to pasty state in 80 DEG C of air dry oven and steams residual moisture, obtains bulk Without iodine celery salt product；

6）To step 5）In obtain bulk carry out pulverization process without iodine celery salt, obtain powdered without iodine celery salt；

7）To step 6）In powdered quantitatively the shaping without iodine celery salt that obtains obtain 0.1g sheet salt particles, obtain calibration quantitative Without iodine celery salt.

Embodiment 31

2）Weigh 10kg iodic salts（Salt as obtained by lake salt as raw material）；

Embodiment 32

2）Weigh 10kg iodic salts（Salt as obtained by well salt as raw material）；

3）Weigh step 1）In treat apiolin 20g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Last shape plus iodine celery salt.

Embodiment 33

1）The apiolin of the plant extract of the commercialization that will be bought dries 4 hours at 150 DEG C, and then grinding sieving, obtains Powder to below 200 mesh, it is standby；

2）Weigh 10kg iodic salts（Salt as obtained by sea salt as raw material）；

3）Weigh step 1）In treat apiolin 0.5g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Last shape plus iodine celery salt.

Embodiment 34

2）Weigh 10kg iodic salts（Salt as obtained by sea salt as raw material）；

3）Weigh step 1）In treat apiolin 0.2g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Last shape plus iodine celery salt；

4）To step 3）In obtain powdered plus iodine celery salt be quantitatively molded and obtain the spherical salt particles of 0.5g, obtain calibration fixed Measure plus iodine celery salt.

The calibration being prepared from the present embodiment quantitatively adds iodine celery salt, can be according to different crowd to apiolin and salt Demand quantitatively used, being capable of the daily usage amount of easy control.

Embodiment 35

3）Weigh step 1）In treat apiolin 20g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Last shape plus iodine celery salt；

4）To step 3）In obtain powdered plus iodine celery salt be quantitatively molded and obtain 0.1g sheet salt particles, obtain calibration quantitative Plus iodine celery salt.

Embodiment 36

1）The apiolin of the plant extract of the commercialization that will be bought dries 12 hours at 60 DEG C, and then grinding sieving, obtains Powder to below 80 mesh, it is standby；

3）Weigh step 1）In treat apiolin 1g, by itself and step 2）The salt for weighing carries out mechanical mixture and obtains powder Shape plus iodine celery salt；

4）To step 3）In obtain powdered plus iodine celery salt be quantitatively molded and obtain 0.2g sheet salt particles, obtain calibration quantitative Plus iodine celery salt.

Embodiment 37

The preparation technology of iodine celery salt is added in turn include the following steps in the present embodiment:

5）After apiolin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor Temperature control steams moisture at 80 DEG C, is placed in during to pasty state in 70 DEG C of air dry oven and steams residual moisture, obtains bulk Plus iodine celery salt；

6）To step 5）In the bulk that obtains plus iodine celery salt carry out pulverization process, obtain powdered plus iodine celery salt.

Embodiment 38

1）The apiolin of the plant extract of the commercialization that will be bought dries 5 hours at 120 DEG C, standby；

4）Weigh step 1）In treat apiolin 20g, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied And the aqueous solution, continue to stir 3 more than h, it is ensured that apiolin is uniformly dispersed in salt saturated aqueous solution；

5）After apiolin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor Temperature control steams moisture at 90 DEG C, is placed in during to pasty state in 80 DEG C of air dry oven and steams residual moisture, obtains bulk Plus iodine celery salt；

Embodiment 39

1）The apiolin of the plant extract of the commercialization that will be bought dries 4 hours at 120 DEG C, standby；

2）Weigh 10kg iodic salts（Salt as obtained by sea salt as raw material）；

5）After apiolin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor Temperature control steams moisture at 80 DEG C, is placed in during to pasty state in 80 DEG C of air dry oven and steams residual moisture, obtains bulk Plus iodine celery salt；

Embodiment 40

1）The apiolin of the plant extract of the commercialization that will be bought dries 6 hours at 100 DEG C, standby；

2）Weigh 10kg iodic salts（Salt as obtained by sea salt as raw material）；

4）Weigh step 1）In treat apiolin 200g, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied And the aqueous solution, continue to stir 3 more than h, it is ensured that apiolin is uniformly dispersed in salt saturated aqueous solution；

Embodiment 41

1）The apiolin of the plant extract of the commercialization that will be bought dries 4 hours at 80 DEG C, standby；

2）Weigh 10kg iodic salts（Salt as obtained by rock salt as raw material）；

4）Weigh step 1）In treat apiolin 2g, step 3 is slowly added under mechanical stirring）Prepared salt saturation The aqueous solution, continues to stir 2 more than h, it is ensured that apiolin is uniformly dispersed in salt saturated aqueous solution；

5）After apiolin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor Temperature control steams moisture at 70 DEG C, is placed in during to pasty state in 80 DEG C of air dry oven and steams residual moisture, obtains bulk Plus iodine celery salt；

Embodiment 42

1）The apiolin of the plant extract of the commercialization that will be bought dries 4 hours at 90 DEG C, standby；

2）Weigh 10kg iodic salts（Salt as obtained by sea salt as raw material）；

4）Weigh step 1）In treat apiolin 30g, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied And the aqueous solution, continue to stir 2 more than h, it is ensured that apiolin is uniformly dispersed in salt saturated aqueous solution；

5）After apiolin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor Temperature control steams moisture at 80 DEG C, is placed in during to pasty state in 70 DEG C of air dry oven and steams residual moisture, obtains bulk Celery salt product；

6）To step 5）In the block celery salt that obtains carry out pulverization process, obtain powdered plus iodine celery salt；

7）To step 6）In obtain powdered plus iodine celery salt be quantitatively molded and obtain 0.2g sheet salt particles, obtain calibration quantitative Plus iodine celery salt.

Embodiment 43

1）The apiolin of the plant extract of the commercialization that will be bought dries 7 hours at 120 DEG C, standby；

4）Weigh step 1）In treat apiolin 1g, step 3 is slowly added under mechanical stirring）Prepared salt saturation The aqueous solution, continues to stir 4 more than h, it is ensured that apiolin is uniformly dispersed in salt saturated aqueous solution；

5）After apiolin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor Temperature control steams moisture at 60 DEG C, is placed in during to pasty state in 80 DEG C of air dry oven and steams residual moisture, obtains bulk Celery salt product；

7）To step 6）In obtain powdered plus iodine celery salt be quantitatively molded and obtain the spherical salt particles of 0.5g, obtain calibration fixed Measure plus iodine celery salt.

Embodiment 44

4）Weigh step 1）In treat apiolin 200g, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied And the aqueous solution, continue to stir 4 more than h, it is ensured that apiolin is uniformly dispersed in salt saturated aqueous solution；

5）After apiolin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor Temperature control steams moisture at 70 DEG C, is placed in during to pasty state in 70 DEG C of air dry oven and steams residual moisture, obtains bulk Celery salt；

7）To step 6）In obtain powdered plus iodine celery salt be quantitatively molded and obtain 0.1g sheet salt particles, obtain calibration quantitative Plus iodine celery salt.

Embodiment 45

5）After apiolin is uniformly dispersed in salt saturated aqueous solution, under conditions of mechanical agitation is continued, by mixed liquor Temperature control steams moisture at 70 DEG C, is placed in during to pasty state in 70 DEG C of air dry oven and steams residual moisture, obtains bulk Plus iodine celery salt；

6）To step 5）In the bulk that obtains plus iodine celery salt carry out pulverization process, obtain powdered plus iodine celery salt；

Embodiment 46

2）Weigh 10kg iodic salts（Salt as obtained by sea salt as raw material）；

4）Weigh step 1）In treat apiolin 50g, step 3 is slowly added under mechanical stirring）Prepared salt is satisfied And the aqueous solution, continue to stir 2 more than h, it is ensured that apiolin is uniformly dispersed in salt saturated aqueous solution；

7）To step 6）In obtain powdered plus iodine celery salt be quantitatively molded and obtain 0.1g sheet salt particles, calibrated Quantitative plus iodine celery salt.

Although the present invention is disclosed as above with embodiment, it is not limited to protection scope of the present invention, any ripe The technical staff of this technology is known, in the change made without departing from the spirit and scope of the invention and retouching, this all should be belonged to The protection domain of invention.

Claims

1. a kind of new celery salt, it is characterised in that：The main component of the celery salt is salt and celery nutrients, celery salt The content of middle celery nutrients is 0.09-33.4wt%.

2. new celery salt according to claim 1, it is characterised in that：Celery nutrients is that celery powder and celery nutrition are carried Take the one kind in thing, celery powder is the powder that celery crushed after being dried is made, celery nutrition extract be circumfluence method, leaching method, The material that either method in centrifugal process, enzyme process, supercritical methanol technology, microwave ultrasound method is extracted；Celery nutrient source in Thymelaeceae, One or more in Verenaceae, Spikemoss plant.

3. new celery salt according to claim 2, it is characterised in that：The celery nutrients is apiolin, apiolin Content be 0.09-3 wt%.

4. new celery salt according to claim 1, it is characterised in that：Also contain anticaking agent in the new celery salt, The content of anticaking agent is 0.0006-0.0025wt%.

5. new celery salt according to claim 4, it is characterised in that：Anticaking agent is from ferric citrate, ferrous cyanogen Change potassium, sodium ferrocyanide, tartaric acid iron, silica, one or more in calcium silicates.

6. the new celery salt according to claim 1 or 2 or 3 or 4, it is characterised in that：The salt is without salt compounded of iodine or adds Salt compounded of iodine, the propiodal of the iodizedsalt is edible inorganic iodide or the organic propiodal of rich iodine.

7. the new celery salt according to claim 1 or 2 or 3 or 4, it is characterised in that：The salt be chosen for sea salt, One or more in lake salt, well salt, rock salt or lake salt, the purity of the Sodium Chloride in Salt is more than 98%, and particle diameter is 0.07-1.0 mm, whiteness is 55%-95% microcrystal grains.

8. the new celery salt stated according to claim 1 or 2 or 3 or 4, it is characterised in that：The salt is chosen for crude salt, essence Salt manufacturing, crush washing salt, evaporate brine day and Cardia Salt or add it is various trace element or nutrition, the extraordinary salt of flavor substance in One or more, the purity of the Sodium Chloride in Salt is more than 98%, and particle diameter is 0.07-1.0 mm, and whiteness is 55%-95% Microcrystal grain.

9. the preparation method of the new celery salt described in claim 1 or 2 or 3 or 4, it is characterised in that described preparation method It is mechanical mixing, comprises the following steps that：

10. the preparation method of the new celery salt described in claim 1 or 2 or 3 or 4, it is characterised in that described preparation method For condensing crystallizing method comprises the following steps：