CN112889924A - Milk tablet for preventing dental caries and its preparation method - Google Patents
Milk tablet for preventing dental caries and its preparation method Download PDFInfo
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- CN112889924A CN112889924A CN202110148778.7A CN202110148778A CN112889924A CN 112889924 A CN112889924 A CN 112889924A CN 202110148778 A CN202110148778 A CN 202110148778A CN 112889924 A CN112889924 A CN 112889924A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/18—Milk in dried and compressed or semi-solid form
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C3/00—Preservation of milk or milk preparations
- A23C3/08—Preservation of milk or milk preparations by addition of preservatives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
- A23C9/1522—Inorganic additives, e.g. minerals, trace elements; Chlorination or fluoridation of milk; Organic salts or complexes of metals other than natrium or kalium; Calcium enrichment of milk
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
- A23C9/156—Flavoured milk preparations ; Addition of fruits, vegetables, sugars, sugar alcohols or sweeteners
Abstract
The invention discloses a milk tablet for preventing decayed teeth and a preparation method thereof. The preparation method is simple, the production cost is low, the prepared milk tablet is complete, the yield is high, the product quality is stable and controllable, and the milk tablet is suitable for common consumers and is particularly suitable for children and teenagers in the growth period to eat.
Description
Technical Field
The invention belongs to the technical field of health-care food, and relates to a milk tablet, in particular to a milk tablet for preventing decayed teeth and a preparation method thereof.
Background
The milk tablet is a sheet milk product prepared by taking fresh milk or milk powder as a main raw material and adding a proper amount of auxiliary materials, and mixing and tabletting, the nutritional ingredients of the milk tablet comprise protein, fat, carbohydrate and the like, and the milk tablet is very popular with consumers due to rich nutrition, direct eating, convenient carrying, long shelf life, deliciousness and palatability.
Dental caries is a multi-factor dynamic infectious disease mainly comprising bacteria, can simultaneously affect the growth of deciduous teeth and permanent teeth, and can not only cause pain to patients and affect the normal eating of the patients, but also affect the normal growth and development of the patients to a certain extent. Caries has a high incidence in adolescents, and in recent years, the incidence of caries in adolescents in China tends to rise year by year.
The invention discloses a Chinese patent application with the publication number of 'CN 112136896A', and discloses a 'nutrition supplementing and modulating milk tablet and a preparation method thereof', wherein the invention takes milk powder, xylitol, tricalcium phosphate, albumen powder, edible essence, fruit and vegetable powder and a nutritional agent as raw materials, and is prepared by uniformly mixing and tabletting; although the nutritional agent is added into the milk tablet, the nutritional ingredients required by human bodies can be well supplemented, but the invention does not consider the oral problems possibly caused by eating the milk tablet.
The invention discloses a Chinese patent application with publication number 'CN 110115292A' and discloses 'a probiotic milk tablet for preventing decayed teeth and a preparation method thereof', wherein the probiotic milk tablet is prepared by taking whole milk powder, skim milk powder, probiotic powder, xylitol powder, sodium carboxymethylcellulose and magnesium stearate as raw materials, culturing probiotics, centrifuging high-concentration probiotic suspension, freeze-drying in vacuum to prepare bacterial powder, mixing the probiotic powder with milk powder and auxiliary materials, and granulating; although the invention can prevent dental caries, the invention has single nutrient component and is difficult to meet the nutritional and health requirements of consumers.
Disclosure of Invention
The invention aims to provide a milk tablet which has rich nutrition, good taste and dental caries prevention;
another object of the present invention is to provide a method for preparing the above mentioned anticarious milk tablet.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
the milk tablet for preventing the decayed teeth comprises the following raw materials of effective components in parts by weight: 80-90 parts of milk powder, 5-15 parts of erythritol, 1-3 parts of xylitol, 0.5-1.5 parts of tricalcium phosphate, 0.02-0.04 part of lactoferrin, 0.15-0.35 part of vitamin complex and 0.1-0.3 part of mineral complex.
As a limitation of the invention, the raw materials for preparing the effective components of the milk tablet also comprise 1-4 parts of green tea extract by weight.
As a further limitation of the present invention, the green tea extract is prepared by the steps of: crushing green tea, adding the crushed green tea into 60-70% acetone aqueous solution by mass percent, leaching for 10-30 min, centrifuging, concentrating the obtained supernatant to be thick paste, washing for 2-5 times, concentrating, and drying to obtain the green tea extract.
In still another more specific aspect of the present invention, the ratio of the ground green tea to the aqueous acetone solution is 1 kg: 8-10L; the washing is with ethanol.
As another limitation of the present invention, the multivitamin composition is composed of 0.1 to 0.2 parts by weight of vitamin A and 0.05 to 0.15 parts by weight of vitamin C.
As a third definition of the invention, the complex mineral includes zinc and iron.
As a further limitation of the invention, the composite mineral substance is composed of 0.05-0.15 parts by weight of ferrous sulfate and 0.05-0.15 parts by weight of zinc sulfate.
In the fourth limitation of the invention, the raw materials for preparing the effective components of the milk tablet also comprise 0.05 to 0.15 parts of butter essence by weight.
The invention also provides a preparation method of the milk tablet for preventing the decayed tooth, which is to evenly mix and tablet the raw materials to obtain the milk tablet for preventing the decayed tooth.
As a limitation of the invention, the raw materials are sieved by a sieve of 60-120 meshes before being uniformly mixed.
Due to the adoption of the technical scheme, compared with the prior art, the invention has the technical progress that:
(1) the added erythritol is a natural active substance and has the characteristics of low hygroscopicity, high thermal stability, high tolerance, zero calorific value, harmonious sweet taste, no increase of blood sugar and caries resistance, and the added erythritol can improve the palatability of the milk tablet, reduce the sweet and greasy feeling of the milk tablet in the eating process, increase the refreshing taste, inhibit bacteria in the oral cavity and delay the moisture absorption and deterioration of the milk tablet in the placing process due to lower hygroscopicity;
(2) the added green tea extract is rich in tea polyphenol, caffeine, aromatic oil, mineral substances, amino acids, vitamins and other nutrient substances, so that the health-care effects of improving the immunity, reducing blood fat, sterilizing, detoxifying and the like of the milk tablet are increased, and more importantly, the green tea extract is added into the milk tablet, so that the taste of the milk tablet can be adjusted, the refreshing taste is increased, and the quality guarantee period of the milk tablet is prolonged;
(3) the added erythritol has an inhibiting effect on growth, adhesion and acid production of oral pathogenic bacteria, beneficial ingredients such as fluorine and tea polyphenol in the green tea extract have the effects of inhibiting bacteria, reducing enamel demineralization, promoting enamel remineralization, inhibiting salivary amylase and the like, and the synergistic caries prevention effect is achieved by combining the two, so that the caries prevention performance of the milk tablet is remarkably improved;
(4) the added compound vitamins comprise vitamine A and vitamine C which are extremely important and easy to lack and are necessary for human body, the vitamine A is beneficial to the development of children eyesight, and the vitamine C has an anti-oxidation effect and can prevent the oxidation of effective components in the milk tablet; the added compound mineral contains zinc element and iron element, and the added zinc and iron are beneficial to the intelligence development of children brains; the tricalcium phosphate added in the invention is a safe nutrition enhancer and an excipient, and can prevent or treat the symptom of calcium deficiency of human bodies, help the formation of the milk tablets and improve the yield of the milk tablets when being added into the milk tablets;
(5) the preparation method is simple, the production cost is low, the prepared milk tablet is complete, the yield is high, and the product quality is stable and controllable;
in conclusion, the milk tablet with rich nutrition, good taste and caries prevention is prepared by taking milk powder as a main raw material, particularly adding erythritol, a green tea extract, compound vitamins and compound minerals, mixing materials and tabletting.
The invention is used for providing the milk tablet for preventing the decayed tooth, and the milk tablet is suitable for common consumers, in particular suitable for children and teenagers in the growth period.
Drawings
The invention is described in further detail below with reference to the figures and the embodiments.
FIG. 1 is a graph showing the evaluation of caries in mice in example 9 of the present invention.
Detailed Description
EXAMPLE 1 preparation of a milk tablet for preventing dental caries
The embodiment is a preparation method of a milk tablet for preventing decayed teeth, which is sequentially carried out according to the following steps:
s1, preparing a green tea extract
Pulverizing 10kg of green tea in a pulverizer, adding the pulverized green tea into 90L of 70 wt% acetone water solution (the ratio of the pulverized green tea to the acetone water solution is 1 kg: 9L), and extracting at 25 deg.C for 20min to obtain material A1;
centrifuging the material A1, collecting the supernatant, repeatedly leaching the residue for 2 times (the same operation as the above leaching process), and mixing the supernatants to obtain material B1;
concentrating the material B1 under reduced pressure to obtain paste, washing with ethanol for 3 times, evaporating, concentrating, and freeze drying to obtain green tea extract;
s2, sieving
Sieving the milk powder, xylitol, erythritol and green tea extract with 110 mesh sieve respectively;
s3, mixing materials
Weighing 80kg of milk powder, 8kg of erythritol, 1kg of green tea extract, 1kg of xylitol, 1kg of tricalcium phosphate, 0.02kg of lactoferrin, 0.2kg of compound vitamin (comprising 0.1kg of vitamin A and 0.1kg of vitamin C), 0.2kg of compound mineral (comprising 0.05kg of ferrous sulfate and 0.15kg of zinc sulfate) and 0.05kg of cream essence, and uniformly stirring to obtain a material C1;
s4, tabletting
And putting the material C1 into a tablet machine to be pressed into tablets, namely the milk tablet for preventing the decayed teeth is marked as N1.
Example 2-8 preparation method of anti-caries milk tablet
Examples 2 to 8 are methods for preparing a milk tablet for preventing dental caries, and the methods are substantially the same as those in example 1, except for the differences in the amount of raw materials and process parameters, which are specifically shown in the following table:
table 1 summary of the raw material amounts and process parameters in examples 2 to 8
Comparative examples 1 'to 3'
Comparative example 1 ' is essentially the same as example 1 except that comparative example 1 ' does not have green tea extract added and the resulting milk tablet is labeled N1 ';
comparative example 2 ' is essentially the same as example 1 except that comparative example 2 ' does not have added erythritol and the resulting milk tablet is labeled N2 ';
comparative example 3 ' is essentially the same as example 1 except that comparative example 3 ' replaces erythritol with glucose and the resulting milk slice is labeled N3 '.
EXAMPLE 9 Effect test
(I) sensory testing
Please refer to 15 professional product research and development and dairy product appraisers to taste the N1-N8 milk tablets provided in examples 1-8 and the N1 '-N3' milk tablets provided in comparative examples 1 'to 3', and perform sensory evaluation on the mouthfeel and state of the milk tablets according to the scoring criteria in table 2, and calculate the average value of the sensory evaluation results of the milk tablets in each group, and the results are shown in table 3:
TABLE 2 sensory test evaluation criteria
TABLE 3 summary of sensory test results
As can be seen from the above table, the overall preference of the milk tablets N1-N8 is over 85 points, and each group of milk tablets has good taste, flavor, appearance and tissue state; the overall preference of the N1 'and N2' milk tablets is over 80 points, and the scores of mouthfeel and flavor are slightly lower; the N3' milk tablet has poor mouthfeel and flavor, and the score of the milk tablet does not reach 80.
Experiment on influence of milk tablet on oral health of mice
Grouping experiments: selecting 24 weaning SD rats with age of 23d, randomly dividing into 4 groups, namely a control group, an experimental group 1, an experimental group 2 and an experimental group 3, wherein each group comprises 6 rats with half of male and female;
administering 0.5mL of ampicillin sodium (dissolved in water) per SD rat every day during the age of 23-25d rats for killing bacteria in the oral cavity of SD rat, during which SD rat normal feed and water are normally fed;
inoculating cariogenic bacteria: feeding SD rats with cariogenic feed Diet2000# and 5% sucrose water from 25d of age, and inoculating 107CFU/mL of streptococcus mutans (streptococcus mutans is one of main cariogenic bacteria) into the oral cavity of each rat once a day during 26-30 d of age of the rat, wherein each inoculation is 1 mL; the main components of the cariogenic feed Diet2000# are as follows:
TABLE 4 main ingredient table of cariogenic Diet Diet2000#
And (3) experimental intervention: from the age of 31d rats, after feeding SD rats with cariogenic Diet, Diet2000# and 5% sucrose water, experimental group 1 was additionally fed daily with milk tablets N1 provided in example 1; experimental group 2 was additionally fed daily with the milk slices N1' provided in comparative example 1; experimental group 3 was additionally fed daily with the milk slices N2' provided in comparative example 1; each SD rat is fed with the corresponding milk tablet at a dose of 2g/kg (measured by weight of the SD rat) per day; the control group was not fed any additional samples, and so on for 6 consecutive weeks.
And (4) measuring the result: killing SD rats when the rats age 72 days, taking jaw bone specimens, cleaning and drying, soaking in 0.4% of a ziurenine solution for 12h for dyeing, taking out and cleaning, performing half-cutting along the nearly middle of the molar surfaces of the upper jaw and the lower jaw to the sagittal direction by using ultrathin carborundum tablets with the thickness of 0.1mm and the diameter of 25mm, and after cleaning and drying, scoring the smooth surfaces of the molar surfaces and the carious lesions of the fossa of the rats under a stereomicroscope according to a Keyes scoring method so as to evaluate the cariostatic condition of each group of milk tablets;
keyes scoring method:
(1) grinding mouse teeth according to caries range, and grinding mouse cheek, tongue and adjacent surface
Dividing the facial fossa into a plurality of tooth surface scoring units (shown in table 5), scoring according to the caries condition of each tooth surface, wherein the higher the scoring is, the larger the caries damage range is, and the worse the caries inhibiting effect of the milk tablet is;
(2) classification into 4 levels according to the depth of damage: the grade E caries lesion is limited to enamel, Ds grade caries lesion and enamel and dentin outer layer 1/4, and 1/4 to 3/4 of inner and Dm grade caries lesion and dentin thickness, and 3/4 of Dx grade caries lesion depth exceeding dentin thickness, even the full layer of dentin is affected;
the caries lesion status of each group of SD rats was scored and graded accordingly, and the results are shown in FIG. 1:
TABLE 5 Keyes method mouse molar tooth surface unit fraction distribution
a: lst, 2nd and 3rd represent first, second and third mouse molars respectively
b: the proximal surface of the second rat molar includes a mesial surface and a distal surface
As can be seen from the attached figure 1, in caries lesions of grade E, grade Ds, grade Dm and grade Dx, the scores of the experimental groups 1-3 are lower than those of the control group in different degrees, wherein the score of the experimental group 1 is obviously lower than those of the experimental group 2 and the experimental group 3, the score of the experimental group 2 is slightly lower than that of the experimental group 3, but the difference is not large, and the milk slices of N1, N1 'and N2' have the function of resisting caries, but the degrees are different, and the anti-caries effect is better than that of the milk slice of N1 provided by the embodiment 1.
In conclusion, the milk tablet for preventing the decayed tooth provided by the invention is rich in nutrient substances and has good mouthfeel and decayed tooth resistance.
Although the present invention has been described in detail with reference to the above embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described above, or equivalents may be substituted for elements thereof. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the scope of the claims of the present invention.
Claims (10)
1. The milk tablet for preventing the decayed teeth is characterized in that the raw materials for preparing the effective components of the milk tablet comprise the following components in parts by weight: 80-90 parts of milk powder, 5-15 parts of erythritol, 1-3 parts of xylitol, 0.5-1.5 parts of tricalcium phosphate, 0.02-0.04 part of lactoferrin, 0.15-0.35 part of vitamin complex and 0.1-0.3 part of mineral complex.
2. The anti-caries milk tablet as claimed in claim 1, wherein the raw materials for preparing the effective components further comprise 1-4 parts by weight of green tea extract.
3. The anti-caries milk tablet as claimed in claim 2, wherein the green tea extract is obtained by crushing green tea, adding the obtained green tea crushed material into 60-70% by mass of an acetone aqueous solution, extracting for 10-30 min, centrifuging, concentrating the obtained supernatant to be paste, washing for 2-5 times, concentrating and drying.
4. The anti-caries milk slice as claimed in claim 3, wherein the ratio of the green tea crushed material to the acetone aqueous solution is 1 kg: 8-10L; the washing is with ethanol.
5. The caries prevention milk tablet according to any one of claims 1 to 4, wherein the vitamin complex is composed of 0.1 to 0.2 parts by weight of vitamin A and 0.05 to 0.15 parts by weight of vitamin C.
6. The caries-preventing milk slice according to any one of claims 1 to 4, wherein the composite mineral contains zinc and iron.
7. The anti-caries milk tablet of claim 6, wherein the composite mineral substance is composed of ferrous sulfate 0.05-0.15 parts by weight and zinc sulfate 0.05-0.15 parts by weight.
8. The anti-caries milk slice as claimed in any one of claims 1 to 4 and 7, wherein the effective component of the milk slice is prepared from 0.05 to 0.15 parts by weight of butter essence.
9. The preparation method of the milk tablet for preventing the decayed tooth according to any one of claims 1 to 8, wherein the milk tablet for preventing the decayed tooth is obtained by uniformly mixing and tabletting raw materials.
10. The preparation method of the milk tablet for preventing the decayed tooth according to claim 9, wherein the raw materials are sieved by a sieve of 60-120 meshes before being uniformly mixed.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202110148778.7A CN112889924A (en) | 2021-02-03 | 2021-02-03 | Milk tablet for preventing dental caries and its preparation method |
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| CN202110148778.7A CN112889924A (en) | 2021-02-03 | 2021-02-03 | Milk tablet for preventing dental caries and its preparation method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114097889A (en) * | 2021-11-30 | 2022-03-01 | 内蒙古伊利实业集团股份有限公司 | Low-viscosity tooth milk tablet and preparation method thereof |
| CN114601003A (en) * | 2022-04-08 | 2022-06-10 | 辽宁大学 | Sugar-free anti-caries dessert |
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| WO2002080946A1 (en) * | 2001-04-02 | 2002-10-17 | Wakamoto Pharmaceutical Co.,Ltd. | Compositions for preventing and/or treating oral diseases |
| CN1698839A (en) * | 2005-06-22 | 2005-11-23 | 徐永福 | Xylitol green tea preparation for clearing mouth smell and preventing decayed tooth and its preparation process |
| CN105076403A (en) * | 2014-05-07 | 2015-11-25 | 保龄宝生物股份有限公司 | Dental caries resistant milk product containing erythritol |
| CN105770191A (en) * | 2015-10-21 | 2016-07-20 | 云南白药天颐茶品有限公司 | Composition having function of reducing activity of periodontal pathogens as well as preparation method and application of the composition |
| CN111296617A (en) * | 2020-04-24 | 2020-06-19 | 中国农业大学 | Erythritol alkalescent chewing gum for preventing dental caries and preparation method thereof |
| CN112136896A (en) * | 2020-08-25 | 2020-12-29 | 石家庄君乐宝乳业有限公司 | Nutrition-supplementing modified milk tablet and preparation method thereof |
-
2021
- 2021-02-03 CN CN202110148778.7A patent/CN112889924A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002080946A1 (en) * | 2001-04-02 | 2002-10-17 | Wakamoto Pharmaceutical Co.,Ltd. | Compositions for preventing and/or treating oral diseases |
| CN1698839A (en) * | 2005-06-22 | 2005-11-23 | 徐永福 | Xylitol green tea preparation for clearing mouth smell and preventing decayed tooth and its preparation process |
| CN105076403A (en) * | 2014-05-07 | 2015-11-25 | 保龄宝生物股份有限公司 | Dental caries resistant milk product containing erythritol |
| CN105770191A (en) * | 2015-10-21 | 2016-07-20 | 云南白药天颐茶品有限公司 | Composition having function of reducing activity of periodontal pathogens as well as preparation method and application of the composition |
| CN111296617A (en) * | 2020-04-24 | 2020-06-19 | 中国农业大学 | Erythritol alkalescent chewing gum for preventing dental caries and preparation method thereof |
| CN112136896A (en) * | 2020-08-25 | 2020-12-29 | 石家庄君乐宝乳业有限公司 | Nutrition-supplementing modified milk tablet and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114097889A (en) * | 2021-11-30 | 2022-03-01 | 内蒙古伊利实业集团股份有限公司 | Low-viscosity tooth milk tablet and preparation method thereof |
| CN114601003A (en) * | 2022-04-08 | 2022-06-10 | 辽宁大学 | Sugar-free anti-caries dessert |
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Address after: 050000 No. 68 stone Copper Road, Hebei, Shijiazhuang Applicant after: JUNLEBAO Dairy Group Co.,Ltd. Address before: 050000 No. 68 stone Copper Road, Hebei, Shijiazhuang Applicant before: THE SHIJIAZHUANG JUNLEBAO DAIRY Co.,Ltd. |
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