CN112841378A - Black rice anthocyanin food for improving sleep and preparation method thereof - Google Patents
Black rice anthocyanin food for improving sleep and preparation method thereof Download PDFInfo
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- CN112841378A CN112841378A CN202110193798.6A CN202110193798A CN112841378A CN 112841378 A CN112841378 A CN 112841378A CN 202110193798 A CN202110193798 A CN 202110193798A CN 112841378 A CN112841378 A CN 112841378A
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- black rice
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- 241000371652 Curvularia clavata Species 0.000 title claims abstract description 39
- 229930002877 anthocyanin Natural products 0.000 title claims abstract description 39
- 235000010208 anthocyanin Nutrition 0.000 title claims abstract description 39
- 239000004410 anthocyanin Substances 0.000 title claims abstract description 39
- 150000004636 anthocyanins Chemical class 0.000 title claims abstract description 39
- 235000013305 food Nutrition 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title description 7
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims abstract description 22
- 239000000284 extract Substances 0.000 claims abstract description 19
- 235000009508 confectionery Nutrition 0.000 claims abstract description 15
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 13
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 13
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims abstract description 12
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000000811 xylitol Substances 0.000 claims abstract description 12
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims abstract description 12
- 229960002675 xylitol Drugs 0.000 claims abstract description 12
- 235000010447 xylitol Nutrition 0.000 claims abstract description 12
- 229920000168 Microcrystalline cellulose Polymers 0.000 claims abstract description 11
- 235000019359 magnesium stearate Nutrition 0.000 claims abstract description 11
- 235000019813 microcrystalline cellulose Nutrition 0.000 claims abstract description 11
- 239000008108 microcrystalline cellulose Substances 0.000 claims abstract description 11
- 229940016286 microcrystalline cellulose Drugs 0.000 claims abstract description 11
- 239000000843 powder Substances 0.000 claims abstract description 8
- 238000007908 dry granulation Methods 0.000 claims description 16
- 239000007888 film coating Substances 0.000 claims description 13
- 238000009501 film coating Methods 0.000 claims description 13
- 239000000463 material Substances 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 8
- 239000008187 granular material Substances 0.000 claims description 7
- 230000000694 effects Effects 0.000 abstract description 11
- 238000012795 verification Methods 0.000 abstract description 2
- 239000003814 drug Substances 0.000 description 11
- 239000000047 product Substances 0.000 description 9
- 208000013738 Sleep Initiation and Maintenance disease Diseases 0.000 description 7
- 206010022437 insomnia Diseases 0.000 description 7
- 238000005550 wet granulation Methods 0.000 description 6
- 239000000243 solution Substances 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 239000011248 coating agent Substances 0.000 description 4
- 238000000576 coating method Methods 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 229940079593 drug Drugs 0.000 description 3
- 230000036541 health Effects 0.000 description 3
- 230000006872 improvement Effects 0.000 description 3
- 230000007774 longterm Effects 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000002560 therapeutic procedure Methods 0.000 description 3
- 231100000331 toxic Toxicity 0.000 description 3
- 230000002588 toxic effect Effects 0.000 description 3
- 238000005303 weighing Methods 0.000 description 3
- 206010059866 Drug resistance Diseases 0.000 description 2
- 235000005911 diet Nutrition 0.000 description 2
- 235000015872 dietary supplement Nutrition 0.000 description 2
- 206010013663 drug dependence Diseases 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 230000004799 sedative–hypnotic effect Effects 0.000 description 2
- 208000019116 sleep disease Diseases 0.000 description 2
- 208000011117 substance-related disease Diseases 0.000 description 2
- 239000013589 supplement Substances 0.000 description 2
- 206010067482 No adverse event Diseases 0.000 description 1
- 206010062519 Poor quality sleep Diseases 0.000 description 1
- 206010057040 Temperature intolerance Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 230000000378 dietary effect Effects 0.000 description 1
- 239000002552 dosage form Substances 0.000 description 1
- 235000006694 eating habits Nutrition 0.000 description 1
- 230000000517 effect on sleep Effects 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000005562 fading Methods 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 230000008543 heat sensitivity Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 230000004630 mental health Effects 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 230000002688 persistence Effects 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 235000019422 polyvinyl alcohol Nutrition 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 208000020685 sleep-wake disease Diseases 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/364—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/42—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds characterised by the carbohydrates used, e.g. polysaccharides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/48—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/50—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by shape, structure or physical form, e.g. products with supported structure
- A23G3/54—Composite products, e.g. layered, coated, filled
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Microbiology (AREA)
- Nutrition Science (AREA)
- Molecular Biology (AREA)
- Botany (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The sleep-improving black rice anthocyanin food comprises the following components in parts by weight: 45-50 parts of xylitol, 30-37 parts of black rice extract, 15-20 parts of microcrystalline cellulose, 0.5-1 part of magnesium stearate and 0.5-2 parts of polyvinyl alcohol. The black rice extract is dried powder with anthocyanin content of 25-35%; the food type is a tablet candy type. Through the verification of the administration of people, the black rice anthocyanin food has the effect of improving sleep.
Description
Technical Field
The invention relates to a black rice anthocyanin food for improving sleep and a preparation method thereof, belonging to the technical field of foods.
Background
Modern people are under great stress, work and life are in a tension state, and many people have insomnia. According to the 'world sleep day' survey issued by the psychiatry of the Chinese medical society, it is shown that four and a half of people in China have sleep disorders, in other words, about 5 hundred million people in China have poor sleep, and the number is increasing continuously. At the same time, we can see that people of all ages have a need to change the insomnia condition.
According to survey, a plurality of consumers still adopt no so-called attitude to insomnia at present, and the part of people belongs to people with insomnia but without medicines, and is a huge potential consumer group of the market. With the improvement of people's knowledge about sleep and health consciousness, the market demand for improving sleep products will gradually increase in a period of time in the future.
Clinically, the treatment of severe insomnia and long-term sleep disorder is the first choice for taking sedative hypnotic drugs. Can generate a plurality of toxic and side effects such as drug resistance, addiction and the like after long-term use. The damage to the physical and mental health of the patient is great. The health care product for improving sleep has various varieties and unsatisfactory effect. The traditional Chinese medicine theory considers that the medicine supplement is not like food supplement, food is safe without toxic and side effects, people without contraindications have no use limit, the food therapy is more convenient, the food therapy is constant in dosage and the food supplement dosage, the effect is not achieved without the persistence, and people cannot do the food therapy according to modern living conditions and dietary habits. However, modern high-tech biotechnology helps us to realize the highest bound of the theory of traditional Chinese medicine, so that the development of a pressed food product which is safer to use, has more prominent effect and no adverse reaction and has the effect of improving sleep is urgent.
The black rice anthocyanin (type of tablet candy) food has the characteristics of quick absorption and quick response in the aspect of improving sleep, and the current experiment shows that the effect of a patient with serious insomnia is obvious after taking the product for about one month, and the effect of the patient with slight insomnia is obvious after taking the product for one week. And compared with the medicine, the medicine belongs to pure natural components and has no side effect.
Disclosure of Invention
The invention aims to provide a black rice anthocyanin food for improving sleep and a preparation method thereof, solves the problems of drug resistance, addiction and other toxic and side effects caused by long-term administration of sedative hypnotic drugs, and injects scientific and technological vitality for industrialization and large-scale injection of diet health products under the guidance of the traditional Chinese medicine 'dietotherapy theory'.
The technical scheme of the invention is as follows:
the black rice anthocyanin food for improving sleep is prepared from the following raw and auxiliary materials in parts by weight: 45-50 parts of xylitol, 30-37 parts of black rice extract, 15-20 parts of microcrystalline cellulose, 0.5-1 part of magnesium stearate and 0.5-2 parts of polyvinyl alcohol.
The black rice extract is dried powder with anthocyanin content of 25-35%;
the food type is a tablet candy type.
A preparation method of a black rice anthocyanin food for improving sleep comprises the following steps:
putting xylitol, black rice extract and microcrystalline cellulose into a mixer according to a ratio, mixing for 20-30 minutes, then performing dry granulation by using a dry granulator to prepare granules of 16-18 meshes, adding magnesium stearate according to the formula ratio, uniformly mixing by using the mixer, then performing tabletting by using a tabletting machine to prepare tablets of 0.6 g/tablet, and performing film coating on the tablets by using polyvinyl alcohol in a film coating device to prepare the black rice anthocyanin food of the tabletting candy type.
The invention uses xylitol, black rice extract, microcrystalline cellulose, magnesium stearate and polyvinyl alcohol as raw and auxiliary materials, and prepares the black rice anthocyanin (tabletting candy type) food through mixing, dry granulation, tabletting and film coating, wherein the content of the black rice anthocyanin in each black rice anthocyanin (tabletting candy type) food is more than or equal to 50 mg, and more than 300 mg is recommended to be eaten every day for improving the sleep effect.
The invention has the beneficial effects that:
1. the black rice extract dry powder with the anthocyanin content of 25-35% is adopted, the black rice extract dry powder belongs to the range of high-purity black rice anthocyanin (plant extract), the anthocyanin content of the commercially available common black rice extract is more than 5-20%, only individual manufacturers can achieve the anthocyanin content of about 30%, and the sleep improvement effect is excellent by taking the black rice extract with the anthocyanin content of about 30% as a raw material through verification of people.
2. The combination of the components of the formula can meet the requirements of dry granulation equipment process parameters, and the wet granulation equipment and the preparation process are almost used in the large-scale production of the tabletted candies, because the dry granulation has special requirements on raw and auxiliary materials which are required to be in a dry powder state, and the raw and auxiliary materials can be directly extruded and bonded into tablets by the dry granulation equipment under the formula components, xylitol and black rice extracts in the invention are raw materials, magnesium stearate is a lubricant required by the tabletting process, polyvinyl alcohol is film coating powder, and the requirement of the dry granulation process parameters can be realized by introducing single auxiliary material microcrystalline cellulose with a proper proportion, so that the invention is an innovation in the preparation process of the tabletted candies rich in anthocyanins, and the dry granulation has the improvement compared with the traditional and conventional wet granulation: the drying step in wet granulation is omitted, the heat sensitivity loss of anthocyanin and the softening and sugar melting phenomena of xylitol in the drying step are avoided, ethanol with a certain concentration is almost required to be introduced for granulation in the wet granulation for tabletting candy dosage forms due to the existence of sugar, the prepared tablets often retain unpleasant alcohol smell due to ethanol residue caused by the wet granulation, the tablets prepared by the dry granulation have no peculiar smell, the essential process step after the wet granulation is the drying process of the granules, and the drying process is omitted by adopting the dry granulation.
3. The progress of adopting the film coating for the anthocyanin type tabletting candy food is as follows: the anthocyanin is prevented from being oxidized and degraded by contacting air by isolating the tablet from air, and the anthocyanin is prevented from being stained with hands directly in the taking process or falling off powder and fading in bottled transportation, so that the tablet is more attractive.
The high-purity black rice anthocyanin-rich tabletted candy type food prepared by using the black rice extract as a main raw material can be used as a dietary health-care food to supplement a human body, and the modern high-tech biotechnology helps us to realize the highest boundary of the traditional Chinese medicine theory, so that the dietotherapy theory of the traditional Chinese medicine is practically developed. Can be certainly accepted by wide consumers.
Detailed Description
In order to make the technical solution of the present invention clear, the following is further described with reference to specific embodiments.
The first embodiment is as follows:
1. weighing the ingredients: 50 parts of xylitol, 30 parts of black rice extract (30 percent of anthocyanin content), 17 parts of microcrystalline cellulose, 1 part of magnesium stearate, 2 parts of polyvinyl alcohol and other raw and auxiliary materials are accurately weighed.
2. Mixing: 50 parts of xylitol, 30 parts of black rice extract (the content of anthocyanin is 30 percent), 17 parts of microcrystalline cellulose and the like are weighed and put into a mixer to be mixed for 20 minutes.
3. And (3) dry granulation: and (3) performing dry granulation on the uniformly mixed materials in a dry granulation machine to prepare 18-mesh granules.
4. Tabletting: the granules prepared in the above procedure were mixed with 1 part of magnesium stearate and tabletted on a tabletting machine with tablet weight of 0.6 g/tablet.
5. Film coating: preparing 15% coating solution by using 2 parts of polyvinyl alcohol and carrying out film coating on the tablets pressed in the above steps by using the prepared polyvinyl alcohol coating solution in film coating equipment.
6. Obtaining a finished product: the black rice anthocyanin (type of pressed candy) food is obtained according to the steps, and the anthocyanin content in the finished product is 54 mg/tablet.
Example two:
1. weighing the ingredients: accurately weighing 45 parts of xylitol, 36 parts of black rice extract (the anthocyanin content is 35%), 16 parts of microcrystalline cellulose, 1 part of magnesium stearate, 2 parts of polyvinyl alcohol and other raw and auxiliary materials.
2. Mixing: and putting 45 parts of the weighed xylitol, 36 parts of the black rice extract (the anthocyanin content is 35 percent), 16 parts of microcrystalline cellulose and the like into a mixer for mixing for 20 minutes.
3. And (3) dry granulation: and (3) performing dry granulation on the uniformly mixed materials in a dry granulation machine to prepare 18-mesh granules.
4. Tabletting: the granules prepared in the above procedure were mixed with 1 part of magnesium stearate and tabletted on a tabletting machine with tablet weight of 0.6 g/tablet.
5. Film coating: preparing 15% coating solution by using 2 parts of polyvinyl alcohol and carrying out film coating on the tablets pressed in the above steps by using the prepared polyvinyl alcohol coating solution in film coating equipment.
6. Obtaining a finished product: the black rice anthocyanin (type of pressed candy) food is obtained according to the steps, and the anthocyanin content in the finished product is 75 mg/tablet.
Claims (3)
1. The black rice anthocyanin food for improving sleep is characterized in that: the health-care food is prepared from the following raw and auxiliary materials in parts by weight: 45-50 parts of xylitol, 30-37 parts of black rice extract, 15-20 parts of microcrystalline cellulose, 0.5-1 part of magnesium stearate and 0.5-2 parts of polyvinyl alcohol;
the fructus Zizaniae Caduciflorae extract is dried powder with anthocyanin content of 25-35%.
2. The black rice anthocyanin food for improving sleep as set forth in claim 1, wherein: the food type is a tablet candy type.
3. The method for preparing a black rice anthocyanin food for improving sleep as set forth in claim 1 or 2, wherein: the method comprises the following steps:
putting xylitol, black rice extract and microcrystalline cellulose into a mixer according to a ratio, mixing for 20-30 minutes, then performing dry granulation by using a dry granulator to prepare granules of 16-18 meshes, adding magnesium stearate according to the formula ratio, uniformly mixing by using the mixer, then performing tabletting by using a tabletting machine to prepare tablets of 0.6 g/tablet, and performing film coating on the tablets by using polyvinyl alcohol in a film coating device to prepare the black rice anthocyanin food of the tabletting candy type.
Priority Applications (1)
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CN202110193798.6A CN112841378A (en) | 2021-02-21 | 2021-02-21 | Black rice anthocyanin food for improving sleep and preparation method thereof |
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CN202110193798.6A CN112841378A (en) | 2021-02-21 | 2021-02-21 | Black rice anthocyanin food for improving sleep and preparation method thereof |
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CN202110193798.6A Pending CN112841378A (en) | 2021-02-21 | 2021-02-21 | Black rice anthocyanin food for improving sleep and preparation method thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2023034196A1 (en) * | 2021-08-30 | 2023-03-09 | Kitt Bio, Inc. | Ribes nigrum for use in enhancing sleep quality |
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CN107019132A (en) * | 2017-04-20 | 2017-08-08 | 王清华 | A kind of black rice beverage and preparation method thereof |
CN111955580A (en) * | 2020-09-21 | 2020-11-20 | 罗通山 | Black rice tea |
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2021
- 2021-02-21 CN CN202110193798.6A patent/CN112841378A/en active Pending
Patent Citations (4)
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CN1939296A (en) * | 2005-09-29 | 2007-04-04 | 中国人民解放军军事医学科学院毒物药物研究所 | Theapolyphenol composition and its preparation |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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WO2023034196A1 (en) * | 2021-08-30 | 2023-03-09 | Kitt Bio, Inc. | Ribes nigrum for use in enhancing sleep quality |
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