CN112807239A - Multi-anti-aging repairing stock solution type cosmetic containing plukenetia volubilis linneo and preparation method of multi-anti-aging repairing stock solution type cosmetic - Google Patents
Multi-anti-aging repairing stock solution type cosmetic containing plukenetia volubilis linneo and preparation method of multi-anti-aging repairing stock solution type cosmetic Download PDFInfo
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Abstract
The invention relates to the technical field of cosmetics, and relates to a pluriparia multi-anti-aging repair stock solution type cosmetic and a preparation method thereof, wherein the stock solution type cosmetic comprises 53-57 parts of group A raw materials and 25-31 parts of anti-aging group raw materials; the anti-aging group raw materials comprise a plukenetia volubilis linneo component, and the plukenetia volubilis linneo component is plukenetia volubilis linneo oil and/or plukenetia volubilis linneo oil microemulsion; the group A raw materials comprise the following components in parts by weight: 44-48 parts of water, 2.5-3.2 parts of glycerol glucoside, 0.8-1.2 parts of PEG/PPG-17/6 copolymer, 2.8-3.5 parts of butanediol, 2.0-2.5 parts of trehalose and 0.5-1.0 part of glycerol. The invention has the beneficial effects that: the raw liquid cosmetic has reasonable formula design, can effectively permeate into the muscle bottom, starts the powerful functions of skin repair, activation and cell regeneration, combines a biological transdermal technology, has strong activity and high absorptivity, solves various skin aging problems such as skin sagging and wrinkles, and recovers the young state of the skin.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a pluriparia-anti-aging repairing stock solution type cosmetic and a preparation method thereof.
Background
Aging is a spontaneous inevitable process of living beings over time, is a complex natural phenomenon, and is an irresistible natural process of life, skin aging is a result of the combined action of internal and external factors, and sagging and wrinkles of the skin are manifestations of skin aging. With the age, the moisture in the skin is reduced, the collagen fibers become thin, the elasticity of the elastin is reduced, and the regular network structure formed by the interaction of the collagen and the elastin in the original dermis is gradually disintegrated, and finally wrinkles and sagging are caused. In view of the principle and process of skin sagging and wrinkle formation, anti-sagging and anti-wrinkle active ingredients commonly used in cosmetics mainly include active ingredients that promote skin moisturization and repair skin barrier function, such as hyaluronic acid; and components for resisting oxidative damage, such as vitamin E.
At present, common anti-sagging and anti-wrinkle stock solution cosmetics in the market mostly adopt macromolecular raw materials, are thick and sticky, are difficult to be absorbed through skin, can form a thick film on skin after being used, and cause poor skin breathability, and can cause skin allergy and inflammation due to factors such as allergic constitution, environmental change, resistance reduction of endocrine disorder, nervous life and work rhythm, unbalanced diet, abnormal life and rest, night stay, germ infection and the like.
Disclosure of Invention
In order to solve the problems, the invention provides a pluriparia-resistant repair stock solution cosmetic and a preparation method thereof.
The technical scheme of the invention is as follows: the pluriparia senilis-resistant repair stock solution cosmetic is characterized in that: the composite material comprises the following raw materials in parts by mass: 53-57 parts of group A raw materials and 25-31 parts of anti-aging raw materials.
Further, the anti-aging group raw material comprises a plukenetia volubilis linneo component, and the plukenetia volubilis linneo component is plukenetia volubilis linneo oil and/or plukenetia volubilis linneo oil microemulsion.
Further, the anti-aging group raw materials also comprise one or more of monkey tree seed oil, peony seed oil, samara oil, acer truncatum seed oil, rhus chinensis fruit oil, prinsepia utilis royle oil and green coffee bean oil;
furthermore, the anti-aging raw materials comprise the following components in parts by weight: 10-13 parts of plukenetia volubilis linneo oil, 3-8 parts of Paeonia suffruticosa seed oil, 1-2 parts of peony seed oil, 3-6 parts of samara oil, 2-5 parts of acer truncatum seed oil, 2-5 parts of Rhus chinensis Mill fruit oil, 1-6 parts of Prinsepia utilis linne oil and 3-5 parts of green coffee bean oil.
Further, the group A raw materials comprise the following components in parts by weight: 44-48 parts of water, 2.5-3.2 parts of glycerol glucoside, 0.8-1.2 parts of PEG/PPG-17/6 copolymer, 2.8-3.5 parts of butanediol, 2.0-2.5 parts of trehalose and 0.5-1.0 part of glycerol.
Further, the pluriparia anti-aging repair stock solution cosmetic also comprises 2-2.5 parts of group B raw materials, wherein the group B raw materials comprise the following components in parts by weight: 1.8-2.2 parts of 1, 3-propylene glycol and 0.25-0.32 part of carbomer sodium.
Further, the pluriparia anti-aging repair stock solution cosmetic also comprises 3.0-3.5 parts of group C raw materials, wherein the group C raw materials comprise the following components in parts by weight: 2.8-3.5 parts of 1, 3-propylene glycol and 0.35-0.6 part of p-hydroxyacetophenone.
Furthermore, the pluriparia anti-aging repair stock solution cosmetic also comprises 4-4.5 parts of group D raw materials, wherein the group D raw materials comprise the following components in parts by weight: 1.5-2.5 parts of water, 0.1-0.2 part of small molecular hyaluronic acid, 0.15-0.25 part of butanediol, 0.05-0.1 part of chamomile extract, 0.05-0.1 part of mint leaf extract, 0.05-0.1 part of pelargonium graveolens extract, 0.02-0.05 part of purslane extract, 0.05-0.1 part of aloe barbadensis leaf extract, 0.05-0.1 part of sophora flavescens root extract, 0.05-0.1 part of peony root extract, 0.05-0.1 part of loquat leaf extract, 0.02-0.05 part of selaginella tamariscina extract and 0.02-0.05 part of cacumen biotae extract.
Further, the pluriparia anti-aging repair stock solution cosmetic also comprises 35-40 parts of group E raw materials, wherein the group E raw materials comprise the following components in parts by weight: 0.3-0.5 part of panthenol, 28-35 parts of acetyl hexapeptide-8, 1.0-1.5 parts of oligopeptide-1, 1.0-1.5 parts of oligopeptide-3, 0.8-1.2 parts of oligopeptide-5, 0.8-1.2 parts of oligopeptide-2, 0.35-0.6 part of apple fruit cell culture extract and 0.35-0.6 part of 1, 2-hexanediol.
A preparation method of a pluriparia anti-aging repair stock solution cosmetic is characterized by comprising the following steps: the method comprises the following steps:
step one, sequentially adding the raw materials of the group A into a batching pot, stirring and heating the raw materials to 85-90 ℃ for complete dissolution, keeping the temperature for 30 minutes, and stirring at the rotating speed of 25-30 rpm;
step two, cooling and stirring the temperature of the batching pot in the step one to 80-85 ℃, adding the raw materials of the group B, stirring and homogenizing until the raw materials are completely dissolved and transparent, and stirring at the rotating speed of 30-35 rpm;
step three, continuously cooling and stirring the temperature of the batching pot in the step two to 55-60 ℃, adding the pre-dissolved C group raw materials and uniformly stirring, wherein the stirring speed is 20-25 rpm;
step four, cooling and stirring the temperature of the batching pot in the step three to 38-42 ℃, adding the group D raw materials and the group E raw materials, and uniformly stirring at the stirring speed of 15-20rpm to finish the preparation.
Further, before the first step, a pretreatment step is further included, and the pretreatment step specifically refers to: thoroughly cleaning and sterilizing production equipment, and calibrating the production equipment;
and/or
A detection step is further included after the fourth step, wherein the detection step specifically refers to: stopping the machine, sampling and detecting, and filtering and discharging after the detection is qualified.
The invention has the beneficial effects that: the invention mainly adopts the components of the embelia laeta, hyaluronic acid with the molecular weight of 4000da, acetyl hexapeptide-8, glycerol glucoside, oligopeptide-1, oligopeptide-3, oligopeptide-5, oligopeptide-2, apple fruit cell culture extract, peony root extract, aloe barbadensis leaf extract, loquat leaf extract, chamomile extract, selaginella tamariscina extract, cacumen biotae extract, purslane extract, pelargonium graveolens extract, golden yellow chamomile extract, sophora flavescens root extract and other natural source components, the raw liquid cosmetic has reasonable formula design, can effectively permeate into the muscle bottom, starts the powerful functions of skin repair, activation and cell regeneration, combines a biological transdermal technology, has strong activity and high absorptivity, solves various skin aging problems such as skin sagging and wrinkles, and recovers the young state of the skin.
Drawings
Fig. 1 is a flow chart of a preparation method of the pluripto anti-aging repairing stock solution cosmetic of the invention:
FIG. 2 is a photograph of in vitro test of a pluriparia anti-aging repairing stock solution cosmetic of the present invention;
wherein (A) a blank stock solution day0 is used; (B) use blank stock day 15; (C) the pluriparia senilis-resistant repair stock solution cosmetic day0 is used; (D) the pluriparia senilism-resistant repair stock solution cosmetic day15 is used.
Detailed Description
The multi-anti-aging repairing stock solution cosmetic of the plukenetia volubilis linneo and the preparation method thereof are described in detail below with reference to the accompanying drawings and examples.
The technical scheme of the invention is as follows: the pluriparia-anti-aging repair stock solution cosmetic comprises the following raw materials in parts by mass: 53-57 parts of group A raw materials and 25-31 parts of anti-aging raw materials.
The anti-aging group raw material comprises a plukenetia volubilis linneo component, and the plukenetia volubilis linneo component is plukenetia volubilis linneo oil and/or plukenetia volubilis linneo oil microemulsion.
The plukenetia volubilis linneo, the academic name plukenetia volubilis linneo, belongs to perennial woody liana plants of the euphorbiaceae family, and grows in tropical rainforests in south America Andes mountain areas with the altitude of 80-1700 m. In the end of 2008, Puer integrated biological resource development limited company in Yunnan province starts to introduce provenance, and the Puer is planted in Puer city and Xishuangbanna in 2009 and is mainly distributed in Puer and Xishuangbanna areas and the like, and the planting area reaches more than 5 ten thousand mu. The plukenetia volubilis linneo nut is rich in nutrition, is rich in protein, unsaturated fatty acid, vitamin E, calcium, phosphorus, iron and other mineral substances, has important functional effects in the aspects of promoting bone growth and nervous system development, beautifying and resisting aging, improving digestive system functions, preventing cardiovascular diseases, preventing cancers, preventing diabetes and the like, and has formal notice of plukenetia volubilis linneo oil as a national new resource food in 2013 in 1 month.
The Plukenetia volubilis linneo oil is prepared by cold pressing and primary pressing, wherein the cold pressing and primary pressing process comprises the steps of selecting seeds, cleaning, drying, shelling, crushing, cold pressing once and filtering. The vegetable oil prepared by the cold pressing preliminary pressing mode is different from the refined vegetable oil, the cold pressing preliminary pressing vegetable seed oil contains more unsaturated oil, various vitamins such as sterol, carotene, plant flavone, plant polyphenol and the like, has the effect of promoting the generation of hyaluronic acid, collagen and elastin of the skin, can keep the skin elastic, keep away from wrinkles and present a healthy and young skin state.
The microemulsion is a transparent or semitransparent solution system which is formed spontaneously by a water phase, an oil phase, a surfactant and a cosurfactant according to a proper proportion, has low viscosity, isotropy and stable thermodynamics and has a particle size of 10-100 nm. The microemulsion has the advantages of good stability, simple operation, high bioavailability, etc., and can increase the solubility of plant essential oil in water.
The anti-aging group also comprises one or more of Paeonia suffruticosa seed oil, peony seed oil, samara oil, Acer Truncatum Bunge seed oil, Rhus chinensis Mill fruit oil, Prinsepia utilis Royle oil, and green coffee bean oil;
the anti-aging composition comprises the following raw materials in parts by weight: 10-13 parts of plukenetia volubilis linneo oil, 3-8 parts of Paeonia suffruticosa seed oil, 1-2 parts of peony seed oil, 3-6 parts of samara oil, 2-5 parts of acer truncatum seed oil, 2-5 parts of Rhus chinensis Mill fruit oil, 1-6 parts of Prinsepia utilis linne oil and 3-5 parts of green coffee bean oil.
The group A raw materials comprise the following components in parts by weight: 44-48 parts of water, 2.5-3.2 parts of glycerol glucoside, 0.8-1.2 parts of PEG/PPG-17/6 copolymer, 2.8-3.5 parts of butanediol, 2.0-2.5 parts of trehalose and 0.5-1.0 part of glycerol.
The pluriparia anti-aging repair stock solution cosmetic also comprises 2-2.5 parts of group B raw materials, wherein the group B raw materials comprise the following components in parts by weight: 1.8-2.2 parts of 1, 3-propylene glycol and 0.25-0.32 part of carbomer sodium.
The pluripotency anti-aging repair stock solution cosmetic also comprises 3.0-3.5 parts of group C raw materials, wherein the group C raw materials comprise the following components in parts by weight: 2.8-3.5 parts of 1, 3-propylene glycol and 0.35-0.6 part of p-hydroxyacetophenone.
The pluriparia anti-aging repair stock solution cosmetic also comprises 4-4.5 parts of a group D raw material, wherein the group D raw material comprises the following components in parts by weight: 1.5-2.5 parts of water, 0.1-0.2 part of small molecular hyaluronic acid, 0.15-0.25 part of butanediol, 0.05-0.1 part of chamomile extract, 0.05-0.1 part of mint leaf extract, 0.05-0.1 part of pelargonium graveolens extract, 0.02-0.05 part of purslane extract, 0.05-0.1 part of aloe barbadensis leaf extract, 0.05-0.1 part of sophora flavescens root extract, 0.05-0.1 part of peony root extract, 0.05-0.1 part of loquat leaf extract, 0.02-0.05 part of selaginella tamariscina extract and 0.02-0.05 part of cacumen biotae extract.
The pluriparia anti-aging repair stock solution cosmetic also comprises 35-40 parts of group E raw materials, wherein the group E raw materials comprise the following components in parts by weight: 0.3-0.5 part of panthenol, 28-35 parts of acetyl hexapeptide-8, 1.0-1.5 parts of oligopeptide-1, 1.0-1.5 parts of oligopeptide-3, 0.8-1.2 parts of oligopeptide-5, 0.8-1.2 parts of oligopeptide-2, 0.35-0.6 part of apple fruit cell culture extract and 0.35-0.6 part of 1, 2-hexanediol.
A preparation method of the pluriparia anti-aging repair stock solution cosmetic comprises the following steps:
step one, sequentially adding the group A raw materials and the anti-aging raw materials into a batching pot, stirring and heating to 85-90 ℃ for complete dissolution, keeping the temperature for 30 minutes, and stirring at the rotating speed of 25-30 rpm;
step two, cooling and stirring the temperature of the batching pot in the step one to 80-85 ℃, adding the raw materials of the group B, stirring and homogenizing until the raw materials are completely dissolved and transparent, and stirring at the rotating speed of 30-35 rpm;
step three, continuously cooling and stirring the temperature of the batching pot in the step two to 55-60 ℃, adding the pre-dissolved C group raw materials and uniformly stirring, wherein the stirring speed is 20-25 rpm;
step four, cooling and stirring the temperature of the batching pot in the step three to 38-42 ℃, adding the group D raw materials and the group E raw materials, and uniformly stirring at the stirring speed of 15-20rpm to finish the preparation.
The method also comprises a pretreatment step before the first step, wherein the pretreatment step specifically comprises the following steps: thoroughly cleaning and sterilizing production equipment, and calibrating the production equipment;
a detection step is further included after the fourth step, wherein the detection step specifically refers to: stopping the machine, sampling and detecting, and filtering and discharging after the detection is qualified.
The anti-sagging and anti-wrinkle stock solution cosmetic disclosed by the invention is fresh and cool in texture, easy to absorb through skin, good in skin air permeability after being used, not easy to be allergic, and capable of relieving skin allergy and inflammation caused by factors such as allergic constitution, environmental change, resistance reduction of endocrine disorder, tension life and work rhythm, unbalanced diet, abnormal life and rest, night stay, germ infection and the like.
Example 1
The pluriparia senilis-resistant repair stock solution cosmetic is characterized in that: the composite material comprises the following raw materials in parts by mass: 53-57 parts of group A raw materials and 25-31 parts of anti-aging raw materials.
Example 2
The pluriparia senilis-resistant repair stock solution cosmetic is characterized in that: the composite material comprises the following raw materials in parts by mass: 53-57 parts of group A raw materials and 25-31 parts of anti-aging raw materials.
The anti-aging group raw material comprises a plukenetia volubilis linneo component, and the plukenetia volubilis linneo component is plukenetia volubilis linneo oil and/or plukenetia volubilis linneo oil microemulsion.
Example 3
The pluriparia-anti-aging repair stock solution cosmetic comprises the following raw materials in parts by mass: 53-57 parts of group A raw materials and 25-31 parts of anti-aging raw materials.
The anti-aging group raw material comprises a plukenetia volubilis linneo component, and the plukenetia volubilis linneo component is plukenetia volubilis linneo oil and/or plukenetia volubilis linneo oil microemulsion.
The anti-aging group also comprises one or more of Paeonia suffruticosa seed oil, peony seed oil, samara oil, Acer Truncatum Bunge seed oil, Rhus chinensis Mill fruit oil, Prinsepia utilis Royle oil, and green coffee bean oil;
the anti-aging composition comprises the following raw materials in parts by weight: 10-13 parts of plukenetia volubilis linneo oil, 3-8 parts of Paeonia suffruticosa seed oil, 1-2 parts of peony seed oil, 3-6 parts of samara oil, 2-5 parts of acer truncatum seed oil, 2-5 parts of Rhus chinensis Mill fruit oil, 1-6 parts of Prinsepia utilis linne oil and 3-5 parts of green coffee bean oil.
Example 4
The technical scheme of the method comprises the following technical scheme in addition to any one of the technical schemes 1 to 3:
the group A raw materials comprise the following components in parts by weight: 44-48 parts of water, 2.5-3.2 parts of glycerol glucoside, 0.8-1.2 parts of PEG/PPG-17/6 copolymer, 2.8-3.5 parts of butanediol, 2.0-2.5 parts of trehalose and 0.5-1.0 part of glycerol.
Example 5
Besides any technical scheme of 1-4, the method also comprises the following technical scheme:
the pluriparia anti-aging repair stock solution cosmetic also comprises 2-2.5 parts of group B raw materials, wherein the group B raw materials comprise the following components in parts by weight: 1.8-2.2 parts of 1, 3-propylene glycol and 0.25-0.32 part of carbomer sodium.
Example 6
Besides any technical scheme of 1-5, the method also comprises the following technical scheme:
the pluripotency anti-aging repair stock solution cosmetic also comprises 3.0-3.5 parts of group C raw materials, wherein the group C raw materials comprise the following components in parts by weight: 2.8-3.5 parts of 1, 3-propylene glycol and 0.35-0.6 part of p-hydroxyacetophenone.
Example 7
Besides any technical scheme of 1-6, the method also comprises the following technical scheme:
the pluriparia anti-aging repair stock solution cosmetic also comprises 4-4.5 parts of a group D raw material, wherein the group D raw material comprises the following components in parts by weight: 1.5-2.5 parts of water, 0.1-0.2 part of small molecular hyaluronic acid, 0.15-0.25 part of butanediol, 0.05-0.1 part of chamomile extract, 0.05-0.1 part of mint leaf extract, 0.05-0.1 part of pelargonium graveolens extract, 0.02-0.05 part of purslane extract, 0.05-0.1 part of aloe barbadensis leaf extract, 0.05-0.1 part of sophora flavescens root extract, 0.05-0.1 part of peony root extract, 0.05-0.1 part of loquat leaf extract, 0.02-0.05 part of selaginella tamariscina extract and 0.02-0.05 part of cacumen biotae extract.
Example 9
Besides any technical scheme of 1-7, the method also comprises the following technical scheme:
the pluriparia anti-aging repair stock solution cosmetic also comprises 35-40 parts of group E raw materials, wherein the group E raw materials comprise the following components in parts by weight: 0.3-0.5 part of panthenol, 28-35 parts of acetyl hexapeptide-8, 1.0-1.5 parts of oligopeptide-1, 1.0-1.5 parts of oligopeptide-3, 0.8-1.2 parts of oligopeptide-5, 0.8-1.2 parts of oligopeptide-2, 0.35-0.6 part of apple fruit cell culture extract and 0.35-0.6 part of 1, 2-hexanediol.
Example 10
A preparation method of the pluriparia anti-aging repair stock solution cosmetic comprises the following steps:
step 101, sequentially adding the group A raw materials and the anti-aging raw materials into a batching pot, stirring and heating to 85-90 ℃ for complete dissolution, keeping the temperature for 30 minutes, and stirring at the rotating speed of 25-30 rpm;
wherein, the component and the weight part of each component of the group A raw materials are as follows: 44-48 parts of water, 2.5-3.2 parts of glycerol glucoside, 0.8-1.2 parts of PEG/PPG-17/6 copolymer, 2.8-3.5 parts of butanediol, 2.0-2.5 parts of trehalose and 0.5-1.0 part of glycerol.
The anti-aging composition comprises the following raw materials in parts by weight: 10-13 parts of plukenetia volubilis linneo oil, 3-8 parts of Paeonia suffruticosa seed oil, 1-2 parts of peony seed oil, 3-6 parts of samara oil, 2-5 parts of acer truncatum seed oil, 2-5 parts of Rhus chinensis Mill fruit oil, 1-6 parts of Prinsepia utilis linne oil and 3-5 parts of green coffee bean oil.
Step 102, cooling and stirring the temperature of the batching pot in the step 101 to 80-85 ℃, adding the raw materials in the group B, stirring and homogenizing until the raw materials are completely dissolved and transparent, and stirring at the rotating speed of 30-35 rpm;
the component of the B group of raw materials and the weight portion of each component are as follows: 1.8-2.2 parts of 1, 3-propylene glycol and 0.25-0.32 part of carbomer sodium.
Step 103, continuously cooling and stirring the temperature of the dosing pot in the step 102 to 55-60 ℃, adding the pre-dissolved C group raw materials, and uniformly stirring at the stirring speed of 20-25 rpm;
the group C raw materials comprise the following components in parts by weight: 2.8-3.5 parts of 1, 3-propylene glycol and 0.35-0.6 part of p-hydroxyacetophenone.
Step 104, cooling and stirring the temperature of the dosing pot in the step 103 to 38-42 ℃, adding the group D raw materials and the group E raw materials, and uniformly stirring at the stirring speed of 15-20rpm to finish the preparation;
the group D raw materials comprise the following components in parts by weight: 1.5-2.5 parts of water, 0.1-0.2 part of small molecular hyaluronic acid, 0.15-0.25 part of butanediol, 0.05-0.1 part of chamomile extract, 0.05-0.1 part of mint leaf extract, 0.05-0.1 part of pelargonium graveolens extract, 0.02-0.05 part of purslane extract, 0.05-0.1 part of aloe barbadensis leaf extract, 0.05-0.1 part of sophora flavescens root extract, 0.05-0.1 part of peony root extract, 0.05-0.1 part of loquat leaf extract, 0.02-0.05 part of selaginella tamariscina extract and 0.02-0.05 part of cacumen biotae extract.
The group E raw materials comprise the following components in parts by weight: 0.3-0.5 part of panthenol, 28-35 parts of acetyl hexapeptide-8, 1.0-1.5 parts of oligopeptide-1, 1.0-1.5 parts of oligopeptide-3, 0.8-1.2 parts of oligopeptide-5, 0.8-1.2 parts of oligopeptide-2, 0.35-0.6 part of apple fruit cell culture extract and 0.35-0.6 part of 1, 2-hexanediol.
Example 11
A preparation method of the pluriparia anti-aging repair stock solution cosmetic comprises the following steps:
step 201: thoroughly cleaning and sterilizing production equipment, and calibrating the production equipment;
202, sequentially adding the group A raw materials and the anti-aging raw materials into a batching pot, stirring and heating to 85-90 ℃ to completely dissolve, keeping the temperature for 30 minutes, and stirring at the rotating speed of 25-30 rpm;
wherein, the component and the weight part of each component of the group A raw materials are as follows: 44-48 parts of water, 2.5-3.2 parts of glycerol glucoside, 0.8-1.2 parts of PEG/PPG-17/6 copolymer, 2.8-3.5 parts of butanediol, 2.0-2.5 parts of trehalose and 0.5-1.0 part of glycerol.
The anti-aging composition comprises the following raw materials in parts by weight: 10-13 parts of plukenetia volubilis linneo oil, 3-8 parts of Paeonia suffruticosa seed oil, 1-2 parts of peony seed oil, 3-6 parts of samara oil, 2-5 parts of acer truncatum seed oil, 2-5 parts of Rhus chinensis Mill fruit oil, 1-6 parts of Prinsepia utilis linne oil and 3-5 parts of green coffee bean oil.
Step 203, cooling and stirring the temperature of the batching pot in the step 202 to 80-85 ℃, adding the raw materials in the group B, stirring and homogenizing until the raw materials are completely dissolved and transparent, and stirring at the rotating speed of 30-35 rpm;
the component of the B group of raw materials and the weight portion of each component are as follows: 1.8-2.2 parts of 1, 3-propylene glycol and 0.25-0.32 part of carbomer sodium.
Step 204, continuously cooling and stirring the temperature of the dosing pot in the step 203 to 55-60 ℃, adding the pre-dissolved C group raw materials, and uniformly stirring at the stirring speed of 20-25 rpm;
the group C raw materials comprise the following components in parts by weight: 2.8-3.5 parts of 1, 3-propylene glycol and 0.35-0.6 part of p-hydroxyacetophenone.
Step 205, cooling and stirring the temperature of the batching pot in the step 204 to 38-42 ℃, adding the group D raw materials and the group E raw materials, and uniformly stirring at the stirring speed of 15-20rpm to finish the preparation;
the group D raw materials comprise the following components in parts by weight: 1.5-2.5 parts of water, 0.1-0.2 part of small molecular hyaluronic acid, 0.15-0.25 part of butanediol, 0.05-0.1 part of chamomile extract, 0.05-0.1 part of mint leaf extract, 0.05-0.1 part of pelargonium graveolens extract, 0.02-0.05 part of purslane extract, 0.05-0.1 part of aloe barbadensis leaf extract, 0.05-0.1 part of sophora flavescens root extract, 0.05-0.1 part of peony root extract, 0.05-0.1 part of loquat leaf extract, 0.02-0.05 part of selaginella tamariscina extract and 0.02-0.05 part of cacumen biotae extract.
The group E raw materials comprise the following components in parts by weight: 0.3-0.5 part of panthenol, 28-35 parts of acetyl hexapeptide-8, 1.0-1.5 parts of oligopeptide-1, 1.0-1.5 parts of oligopeptide-3, 0.8-1.2 parts of oligopeptide-5, 0.8-1.2 parts of oligopeptide-2, 0.35-0.6 part of apple fruit cell culture extract and 0.35-0.6 part of 1, 2-hexanediol.
Example 12
A preparation method of the pluriparia anti-aging repair stock solution cosmetic comprises the following steps:
301, sequentially adding the group A raw materials and the anti-aging raw materials into a batching pot, stirring and heating to 85-90 ℃ to completely dissolve, keeping the temperature for 30 minutes, and stirring at the rotating speed of 25-30 rpm;
wherein, the component and the weight part of each component of the group A raw materials are as follows: 44-48 parts of water, 2.5-3.2 parts of glycerol glucoside, 0.8-1.2 parts of PEG/PPG-17/6 copolymer, 2.8-3.5 parts of butanediol, 2.0-2.5 parts of trehalose and 0.5-1.0 part of glycerol.
The anti-aging composition comprises the following raw materials in parts by weight: 10-13 parts of plukenetia volubilis linneo oil, 3-8 parts of Paeonia suffruticosa seed oil, 1-2 parts of peony seed oil, 3-6 parts of samara oil, 2-5 parts of acer truncatum seed oil, 2-5 parts of Rhus chinensis Mill fruit oil, 1-6 parts of Prinsepia utilis linne oil and 3-5 parts of green coffee bean oil.
Step 302, cooling and stirring the temperature of the batching pot in the step 301 to 80-85 ℃, adding the raw materials in the group B, stirring and homogenizing until the raw materials are completely dissolved and transparent, and stirring at the rotating speed of 30-35 rpm;
the component of the B group of raw materials and the weight portion of each component are as follows: 1.8-2.2 parts of 1, 3-propylene glycol and 0.25-0.32 part of carbomer sodium.
Step 303, continuously cooling and stirring the temperature of the batching pot in the step 302 to 55-60 ℃, adding the pre-dissolved C group raw materials, and uniformly stirring at the stirring speed of 20-25 rpm;
the group C raw materials comprise the following components in parts by weight: 2.8-3.5 parts of 1, 3-propylene glycol and 0.35-0.6 part of p-hydroxyacetophenone.
Step 304, cooling and stirring the temperature of the batching pot in the step 303 to 38-42 ℃, adding the group D raw materials and the group E raw materials, and uniformly stirring at the stirring speed of 15-20rpm to finish the preparation;
the group D raw materials comprise the following components in parts by weight: 1.5-2.5 parts of water, 0.1-0.2 part of small molecular hyaluronic acid, 0.15-0.25 part of butanediol, 0.05-0.1 part of chamomile extract, 0.05-0.1 part of mint leaf extract, 0.05-0.1 part of pelargonium graveolens extract, 0.02-0.05 part of purslane extract, 0.05-0.1 part of aloe barbadensis leaf extract, 0.05-0.1 part of sophora flavescens root extract, 0.05-0.1 part of peony root extract, 0.05-0.1 part of loquat leaf extract, 0.02-0.05 part of selaginella tamariscina extract and 0.02-0.05 part of cacumen biotae extract.
The group E raw materials comprise the following components in parts by weight: 0.3-0.5 part of panthenol, 28-35 parts of acetyl hexapeptide-8, 1.0-1.5 parts of oligopeptide-1, 1.0-1.5 parts of oligopeptide-3, 0.8-1.2 parts of oligopeptide-5, 0.8-1.2 parts of oligopeptide-2, 0.35-0.6 part of apple fruit cell culture extract and 0.35-0.6 part of 1, 2-hexanediol.
And 305, stopping sampling and detecting after the preparation is finished, and filtering and discharging after the detection is qualified.
Example 13
A preparation method of the pluriparia anti-aging repair stock solution cosmetic comprises the following steps:
step 401: thoroughly cleaning and sterilizing production equipment, and calibrating the production equipment;
step 402, adding the group A raw materials and the anti-aging raw materials into a batching pot in sequence, stirring and heating to 85-90 ℃ for complete dissolution, keeping the temperature for 30 minutes, and stirring at the rotating speed of 25-30 rpm;
wherein, the component and the weight part of each component of the group A raw materials are as follows: 44-48 parts of water, 2.5-3.2 parts of glycerol glucoside, 0.8-1.2 parts of PEG/PPG-17/6 copolymer, 2.8-3.5 parts of butanediol, 2.0-2.5 parts of trehalose and 0.5-1.0 part of glycerol.
The anti-aging composition comprises the following raw materials in parts by weight: 10-13 parts of plukenetia volubilis linneo oil, 3-8 parts of Paeonia suffruticosa seed oil, 1-2 parts of peony seed oil, 3-6 parts of samara oil, 2-5 parts of acer truncatum seed oil, 2-5 parts of Rhus chinensis Mill fruit oil, 1-6 parts of Prinsepia utilis linne oil and 3-5 parts of green coffee bean oil.
Step 403, cooling and stirring the temperature of the batching pot in the step one to 80-85 ℃, adding the raw materials in the group B, stirring and homogenizing until the raw materials are completely dissolved and transparent, and stirring at the rotating speed of 30-35 rpm;
the component of the B group of raw materials and the weight portion of each component are as follows: 1.8-2.2 parts of 1, 3-propylene glycol and 0.25-0.32 part of carbomer sodium.
Step 404, continuously cooling and stirring the temperature of the batching pot in the step 403 to 55-60 ℃, adding the pre-dissolved C group raw materials, and uniformly stirring at the stirring speed of 20-25 rpm;
the group C raw materials comprise the following components in parts by weight: 2.8-3.5 parts of 1, 3-propylene glycol and 0.35-0.6 part of p-hydroxyacetophenone.
Step 405, cooling and stirring the temperature of the batching pot in the step 404 to 38-42 ℃, adding the group D raw materials and the group E raw materials, and uniformly stirring at the stirring speed of 15-20rpm to finish the preparation;
the group D raw materials comprise the following components in parts by weight: 1.5-2.5 parts of water, 0.1-0.2 part of small molecular hyaluronic acid, 0.15-0.25 part of butanediol, 0.05-0.1 part of chamomile extract, 0.05-0.1 part of mint leaf extract, 0.05-0.1 part of pelargonium graveolens extract, 0.02-0.05 part of purslane extract, 0.05-0.1 part of aloe barbadensis leaf extract, 0.05-0.1 part of sophora flavescens root extract, 0.05-0.1 part of peony root extract, 0.05-0.1 part of loquat leaf extract, 0.02-0.05 part of selaginella tamariscina extract and 0.02-0.05 part of cacumen biotae extract.
The group E raw materials comprise the following components in parts by weight: 0.3-0.5 part of panthenol, 28-35 parts of acetyl hexapeptide-8, 1.0-1.5 parts of oligopeptide-1, 1.0-1.5 parts of oligopeptide-3, 0.8-1.2 parts of oligopeptide-5, 0.8-1.2 parts of oligopeptide-2, 0.35-0.6 part of apple fruit cell culture extract and 0.35-0.6 part of 1, 2-hexanediol.
And 406, stopping sampling and detecting after preparation is finished, and filtering and discharging after the detection is qualified.
Example 14
The multi-anti-aging repairing stock solution cosmetic of the plukenetia volubilis linneo comprises the following components in parts by weight:
the preparation method of the pluriparia anti-aging repair stock solution cosmetic comprises the following steps:
1. thoroughly cleaning and sterilizing production equipment, and calibrating the production equipment;
2. sequentially adding the raw materials of the group A into a batching pan, stirring and heating to 85-90 ℃ to completely dissolve, keeping the temperature for 30 minutes, and stirring at the rotating speed of 25-30 rpm;
3. cooling and stirring the temperature of the batching pot in the step 2 to 80-85 ℃, adding the raw materials of the group B, stirring and homogenizing until the raw materials are completely dissolved and transparent, and stirring at the rotating speed of 30-35 rpm;
4. continuously cooling and stirring the temperature of the batching kettle in the step 3 to 55-60 ℃, adding the pre-dissolved C group raw materials, and uniformly stirring at the stirring speed of 20-25 rpm;
5. cooling and stirring the temperature of the batching pot in the step 4 to 38-42 ℃, adding the group D raw materials and the group E raw materials, and uniformly stirring at the stirring speed of 15-20 rpm;
6. stopping the machine, sampling and detecting, and filtering and discharging after the detection is qualified.
Comparative test
FIG. 2 is a photograph of in vitro test of a pluriparia anti-aging repairing stock solution cosmetic of the present invention;
wherein (A) a blank stock solution day0 is used; (B) use blank stock day 15; (C) the pluriparia senilis-resistant repair stock solution cosmetic day0 is used; (D) the pluriparia senilism-resistant repair stock solution cosmetic day15 is used.
The subjects respectively adopt blank stock solution and multiple anti-aging repair stock solution containing plukenetia volubilis linneo to wipe around the eyes once in the morning and at night, and silicon imprints are obtained before and after 15 days of tests. The silicon imprints were analyzed by confocal scanning microscopy to assess changes in the skin surface before and after use. The test showed a significant reduction in wrinkle depth after 15 days with multiple anti-aging repair stock solutions.
The above description is only an embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can easily conceive of changes or substitutions within the technical scope of the present invention, and all such changes or substitutions are included in the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the claims.
Claims (11)
1. The pluriparia senilis-resistant repair stock solution cosmetic is characterized in that: the composite material comprises the following raw materials in parts by mass: 53-57 parts of group A raw materials and 25-31 parts of anti-aging raw materials.
2. The multi-anti-aging repairing stock solution type cosmetic of plukenetia volubilis linneo according to claim 1, which is characterized in that: the anti-aging group raw material comprises a plukenetia volubilis linneo component, and the plukenetia volubilis linneo component is plukenetia volubilis linneo oil and/or plukenetia volubilis linneo oil microemulsion.
3. The multi-anti-aging repairing stock solution type cosmetic of plukenetia volubilis linneo according to claim 2, which is characterized in that: the anti-aging group raw materials also comprise one or more of Paeonia suffruticosa seed oil, peony seed oil, samara oil, Acer Truncatum Bunge seed oil, Rhus chinensis Mill fruit oil, Prinsepia utilis Royle oil and green coffee bean oil.
4. The multi-anti-aging repairing stock solution type cosmetic of plukenetia volubilis linneo according to claim 3, which is characterized in that: the anti-aging composition comprises the following raw materials in parts by weight: 10-13 parts of plukenetia volubilis linneo oil, 3-8 parts of Paeonia suffruticosa seed oil, 1-2 parts of peony seed oil, 3-6 parts of samara oil, 2-5 parts of acer truncatum seed oil, 2-5 parts of Rhus chinensis Mill fruit oil, 1-6 parts of Prinsepia utilis linne oil and 3-5 parts of green coffee bean oil.
5. The multi-anti-aging repairing stock solution cosmetic as claimed in any one of claims 1 to 4, which is characterized in that: the group A raw materials comprise the following components in parts by weight: 44-48 parts of water, 2.5-3.2 parts of glycerol glucoside, 0.8-1.2 parts of PEG/PPG-17/6 copolymer, 2.8-3.5 parts of butanediol, 2.0-2.5 parts of trehalose and 0.5-1.0 part of glycerol.
6. The multi-anti-aging repairing stock solution type cosmetic of plukenetia volubilis linneo according to claim 5, which is characterized in that: the pluriparia anti-aging repair stock solution cosmetic also comprises 2-2.5 parts of a group B raw material, wherein the group B raw material comprises the following components in parts by weight: 1.8-2.2 parts of 1, 3-propylene glycol and 0.25-0.32 part of carbomer sodium.
7. The multi-anti-aging repairing stock solution type cosmetic of plukenetia volubilis linneo according to claim 6, which is characterized in that: the pluriparia anti-aging repair stock solution cosmetic also comprises 3.0-3.5 parts of group C raw materials, wherein the group C raw materials comprise the following components in parts by weight: 2.8-3.5 parts of 1, 3-propylene glycol and 0.35-0.6 part of p-hydroxyacetophenone.
8. The multi-anti-aging repairing stock solution type cosmetic of plukenetia volubilis linneo according to claim 7, which is characterized in that: the pluriparia anti-aging repair stock solution cosmetic also comprises 4-4.5 parts of a group D raw material, wherein the group D raw material comprises the following components in parts by weight: 1.5-2.5 parts of water, 0.1-0.2 part of small molecular hyaluronic acid, 0.15-0.25 part of butanediol, 0.05-0.1 part of chamomile extract, 0.05-0.1 part of mint leaf extract, 0.05-0.1 part of pelargonium graveolens extract, 0.02-0.05 part of purslane extract, 0.05-0.1 part of aloe barbadensis leaf extract, 0.05-0.1 part of sophora flavescens root extract, 0.05-0.1 part of peony root extract, 0.05-0.1 part of loquat leaf extract, 0.02-0.05 part of selaginella tamariscina extract and 0.02-0.05 part of cacumen biotae extract.
9. The multi-anti-aging repairing stock solution type cosmetic of plukenetia volubilis linneo according to claim 5, which is characterized in that: the pluriparia anti-aging repair stock solution cosmetic also comprises 35-40 parts of group E raw materials, wherein the group E raw materials comprise the following components in parts by weight: 0.3-0.5 part of panthenol, 28-35 parts of acetyl hexapeptide-8, 1.0-1.5 parts of oligopeptide-1, 1.0-1.5 parts of oligopeptide-3, 0.8-1.2 parts of oligopeptide-5, 0.8-1.2 parts of oligopeptide-2, 0.35-0.6 part of apple fruit cell culture extract and 0.35-0.6 part of 1, 2-hexanediol.
10. A preparation method of a pluriparia anti-aging repair stock solution cosmetic is characterized by comprising the following steps: the method comprises the following steps:
step one, sequentially adding the group A raw materials and the anti-aging raw materials into a batching pot, stirring and heating to 85-90 ℃ for complete dissolution, keeping the temperature for 30 minutes, and stirring at the rotating speed of 25-30 rpm;
step two, cooling and stirring the temperature of the batching pot in the step one to 80-85 ℃, adding the raw materials of the group B, stirring and homogenizing until the raw materials are completely dissolved and transparent, and stirring at the rotating speed of 30-35 rpm;
step three, continuously cooling and stirring the temperature of the batching pot in the step two to 55-60 ℃, adding the pre-dissolved C group raw materials and uniformly stirring, wherein the stirring speed is 20-25 rpm;
step four, cooling and stirring the temperature of the batching pot in the step three to 38-42 ℃, adding the group D raw materials and the group E raw materials, and uniformly stirring at the stirring speed of 15-20rpm to finish the preparation.
11. The preparation method of the pluriparia multi-anti-aging repairing stock solution type cosmetic according to claim 9, which is characterized by comprising the following steps: the method also comprises a pretreatment step before the first step, wherein the pretreatment step specifically comprises the following steps: thoroughly cleaning and sterilizing production equipment, and calibrating the production equipment;
and/or
A detection step is further included after the fourth step, wherein the detection step specifically refers to: stopping the machine, sampling and detecting, and filtering and discharging after the detection is qualified.
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CN107281005A (en) * | 2017-05-25 | 2017-10-24 | 珀莱雅化妆品股份有限公司 | A kind of preparation method of the nanometer emulsified liquid of anti-wrinkle composition and its PIT |
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