CN112675243A - Anti-inflammatory analgesic medicinal liquor and preparation method thereof - Google Patents
Anti-inflammatory analgesic medicinal liquor and preparation method thereof Download PDFInfo
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Abstract
The invention provides anti-inflammatory analgesic medicinal liquor which comprises the following raw materials in parts by weight: 3-5 parts of coreopsis tinctoria extract, 2-8 parts of cactus extract, 7-12 parts of pseudo-ginseng, 10-25 parts of groundsel root extract, 50-60 parts of wine liquid and 10-15 parts of deionized water liquid. The anti-inflammatory and analgesic medicinal liquor has the effects of clearing heat and detoxicating, diminishing inflammation and relieving pain, and drawing out toxic materials and promoting tissue regeneration, and has good curative effects on lumbar disc herniation, hyperosteogeny, scapulohumeral periarthritis, cervical vertebra pain, contusion, sprain and other diseases.
Description
Technical Field
The invention relates to the technical field of medicinal liquor, and particularly relates to anti-inflammatory and analgesic medicinal liquor and a preparation method thereof.
Background
Diseases such as lumbocrural pain, arm pain, scapulohumeral periarthritis, sciatica and the like are common diseases which are troubled for a long time, and the normal life of people can be influenced when the diseases are serious. Especially, sciatica has high incidence and great harmfulness, which causes inconvenience in movement and even incapability in severe cases. At present, a plurality of medicines and methods for treating the diseases exist, but the medicines and the methods have the defects of unobvious treatment effect, long treatment course and the like, and cause pain to patients in treatment.
In view of the above, the present invention is particularly proposed.
Disclosure of Invention
The invention aims to provide the anti-inflammatory and analgesic medicinal liquor, which is prepared by matching the chamomile extract, the cactus extract, the pseudo-ginseng and the extract of the rhizomadia, extracting and mixing the effective components through liquor, so that the effective components of the raw materials can play a role extremely, the effects of clearing away heat and toxic materials, diminishing inflammation, relieving pain, drawing out toxin and promoting tissue regeneration can be achieved, and the medicinal liquor has good curative effects on lumbar disc herniation, hyperosteogeny, scapulohumeral periarthritis, cervical vertebra pain, contusion, sprain and other diseases.
The second purpose of the invention is to provide the preparation method of the medicinal liquor, the preparation method is simple to operate and convenient to prepare, the medicinal effects of the components are fully exerted through specific steps and process parameters, and the prepared medicinal liquor has quick response and good curative effect and has good therapeutic effect on lumbar disc herniation, hyperosteogeny, scapulohumeral periarthritis, cervical vertebra pain, contusion, sprain and other diseases.
In order to achieve the above purpose of the present invention, the following technical solutions are adopted:
the invention provides anti-inflammatory analgesic medicinal liquor which comprises the following raw materials in parts by weight: 3-5 parts of coreopsis tinctoria extract, 2-8 parts of cactus extract, 7-12 parts of pseudo-ginseng, 10-25 parts of groundsel root extract, 50-60 parts of wine liquid and 10-15 parts of deionized water liquid.
Preferably, 3-5 parts of coreopsis tinctoria extract, 4-6 parts of cactus extract, 9-10 parts of pseudo-ginseng, 15-20 parts of groundsel root-growing extract, 53-57 parts of wine liquid and 12-14 parts of deionized water liquid.
Preferably, the traditional Chinese medicine composition comprises 4 parts of coreopsis tinctoria extract, 5 parts of cactus extract, 9 parts of pseudo-ginseng, 18 parts of groundsel root-growing extract, 55 parts of wine liquid and 13 parts of deionized water liquid.
Preferably, the wine liquid is self-brewed white spirit by the traditional process. Further, the alcohol content is 50 degrees.
The diseases such as lumbar disc herniation, hyperosteogeny, scapulohumeral periarthritis, cervical vertebra pain, contusion and sprain and the like are common diseases, but the treatment effect on the diseases is not obvious, the treatment course is long, the diseases are easy to repeat, and the pain is caused to the treatment of patients.
In order to solve the problems, the invention provides the medicinal liquor, the medicinal liquor adopts a specific process to ensure that the medicinal effect of active ingredients is exerted to the utmost extent, alcohol fully enters the medicinal material cells to fully dissolve the active ingredients, the diffusion and replacement of the active ingredients are promoted, the leaching speed and the leaching effect are improved, the medicines are mutually complemented and promoted, the prepared medicinal liquor has the effects of clearing away heat and toxic materials, diminishing inflammation, relieving pain, drawing out toxin and promoting granulation, and has good curative effects on lumbar disc herniation, hyperosteogeny, scapulohumeral periarthritis, cervical vertebra pain, contusion, sprain and other diseases.
Among the components, the inula japonicas has the functions of detoxifying, relieving pain, diminishing inflammation, relieving itching and reducing swelling; cactus is a plant of the cactus genus of the cactaceae family, and is firstly carried in Ben Cao gang mu Shi Yi (supplement to compendium of materia Medica) by Zhao Ming Dynasty in China as a medicinal herb. According to the book record, the cactus is light in taste and cold in nature, has the functions of promoting qi and blood circulation, clearing away heat and toxic materials, relieving swelling and pain, invigorating spleen and relieving diarrhea, soothing nerves and promoting urination, and can be taken orally and externally used for treating various diseases. The theory of traditional Chinese medicine considers that the fleshy stem has the effects of clearing away heat and toxic materials, removing blood stasis and detumescence, invigorating stomach, easing pain, promoting granulation and expelling pus, and promoting qi and blood circulation. It is commonly indicated for gastric and duodenal ulcer, acute dysentery and cough in folks. It is used externally to treat epidemic parotitis, mastitis, carbuncle, furuncle, swelling, snake bite, burn and scald. Modern medical research shows that the compound has wide pharmacological activity, such as bacteriostasis, anti-inflammation, immunity enhancement, stomach strengthening, blood sugar reducing, antivirus, gastric ulcer resisting, anticancer, fatigue resisting, anoxia resisting, stress resisting, procoagulant, mutagenesis resisting, lipid peroxidation resisting, aging resisting, pain relieving, cholesterol level reducing and male mouse sexual function improving. Meanwhile, acute toxicity tests show that the traditional Chinese medicine composition has small toxic and side effects; pseudo-ginseng: has bitter taste and cool nature, and has effects of dispelling blood stasis, stopping bleeding, clearing away heat and toxic materials, dispelling pathogenic wind heat, and relieving swelling and pain; the herba Farfarae is a plant of the genus of herba Farfarae of Crassulaceae, and has the following properties: bland, slightly sour, astringent and cool. The main treatment is as follows: detoxify and detumescence, activate blood and alleviate pain, remove toxicity and promote granulation. It is used externally to treat carbuncle, sore, swelling, mastitis, erysipelas, felon, traumatic hemorrhage, traumatic injury, fracture, burn, scald and otitis media.
The preparation method of the coreopsis extract comprises the following steps: pulverizing flos Gynurae Divaricatae, adding 30-70 wt% ethanol aqueous solution 10-15 times of flos Gynurae Divaricatae, extracting with ethanol under reflux for 3-4 times, each time extracting with ethanol for 30-40min, mixing extractive solutions, filtering, adsorbing with macroporous adsorbent resin, eluting with the adsorbed resin, and concentrating the eluate until the solution content is less than 3% to obtain flos Gynurae Divaricatae extract.
Preparation of cactus extract: selecting dry cactus powder, placing into an extraction tank, adding 18-22 times of water and 0.8-1.5% of cellulase, heating to 45-55 deg.C, maintaining the temperature, adjusting pH to 4-6, performing enzymolysis for 50-70min, cooling to 22-26 deg.C, stirring at 2 lattices for 1.5-2.5h, centrifuging for 8-12min with a 4000r/min centrifuge, mixing the supernatants, adding 4-6% of active carbon, standing for 20-30h, centrifuging to remove active carbon, and mixing the water extracts.
The method for extracting the extract of the rhizomes fallen to the ground comprises the following steps of; pulverizing appropriate amount of herba Centellae, sieving to obtain powder, adding 0.2mo1/L NaOH water solution, mixing at solid-to-liquid ratio of 1:10, hot-soaking at 80 deg.C for 2 hr, repeating for 2 times, filtering, adding 3% hydrochloric acid into the filtrate to adjust pH to 7, centrifuging at 4000r/min, and removing supernatant to obtain precipitate as herba Centellae extract.
The invention also provides a preparation method of the anti-inflammatory and analgesic medicinal liquor, which comprises the following steps:
dissolving a chamomile extract and a cactus extract in wine to obtain a solution A;
adding the pseudo-ginseng and the extract of the rhizoctonia falling into the ground into deionized water and stirring to obtain a solution B;
and step three, mixing the solution A and the solution B, adding the preservative, uniformly stirring, and filling.
Preferably, the dissolving temperature in the first step is 20-25 ℃, and the dissolving time is 165-171 h.
Preferably, the stirring speed in the second step is 200-300r/min, and the stirring temperature is 75-85 ℃.
Preferably, the addition amount of the preservative in the third step is 3% of the mass of the mixed solution A and solution B.
Preferably, the preservative is sodium benzoate.
Preferably, the stirring temperature in the third step is 20-30 ℃, the stirring speed is 250-350r/min, and the stirring time is 15-25 min.
According to the preparation method, the effective components in the chamomile extract, the cactus extract, the pseudo-ginseng and the extract of the rhizomadia falling to the ground are dissolved in advance by preparing the solution A and the solution B, so that the diffusion and replacement of the effective components are promoted, the leaching speed and the leaching effect are improved, and the solution A and the solution B are mixed at a specific temperature and a stirring speed, so that the alcohol is promoted to enter the medicinal material cells, and the solubility of the effective components is improved; the shelf life of the medicinal liquor is prolonged by adding the preservative; the whole preparation method is simple to operate and high in preparation efficiency.
Compared with the prior art, the invention has the beneficial effects that:
the medicinal liquor disclosed by the invention has the beneficial effects that the medicinal effect of active ingredients is brought into full play by adopting a specific process, alcohol fully enters medicinal material cells, the active ingredients are fully dissolved, the diffusion and replacement of the active ingredients are promoted, the leaching speed and the leaching effect are improved, the medicines are mutually complemented and promoted, the prepared medicinal liquor has the effects of clearing away heat and toxic materials, diminishing inflammation, relieving pain, drawing out toxin and promoting granulation, and has good curative effects on diseases such as lumbar disc herniation, hyperosteogeny, scapulohumeral periarthritis, cervical vertebra pain, contusion, sprain and the like.
Detailed Description
Embodiments of the present invention will be described in detail below with reference to examples, but it will be understood by those skilled in the art that the following examples are only illustrative of the present invention and should not be construed as limiting the scope of the present invention. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available commercially.
Example 1
First, the following components were weighed: 3g of coreopsis tinctoria extract, 2g of cactus extract, 7g of pseudo-ginseng, 10g of groundsel root-growing extract, 50g of wine liquid and 10g of deionized water liquid.
Then dissolving the chamomile extract and the cactus extract at the temperature of 20 ℃ for 165h to obtain a solution A;
simultaneously, adding the panax notoginseng and the extract of the rhizomes fallen to the ground into deionized water, and stirring and mixing at the temperature of 75 ℃ and the speed of 200r/min to obtain a solution B;
and finally, mixing the solution A and the solution B at the temperature of 20 ℃, adding a preservative, stirring at the speed of 250r/min for 15min, and filling the prepared medicinal liquor after stirring.
Example 2
First, the following components were weighed: 3g of coreopsis tinctoria extract, 4g of cactus extract, 9g of pseudo-ginseng, 15g of groundsel root-growing extract, 53g of wine liquid and 12g of deionized water liquid.
Then dissolving the chamomile extract and the cactus extract at the temperature of 20 ℃ for 165h to obtain a solution A;
simultaneously, adding the panax notoginseng and the extract of the rhizomes fallen to the ground into deionized water, and stirring and mixing at the temperature of 80 ℃ and the speed of 220r/min to obtain a solution B;
and finally, mixing the solution A and the solution B at 25 ℃, adding a preservative, stirring at the speed of 270r/min for 15min, and filling the prepared medicinal liquor after stirring.
Example 3
First, the following components were weighed: 4g of coreopsis tinctoria extract, 5g of cactus extract, 9g of pseudo-ginseng, 18g of groundsel root-growing extract, 55g of wine liquid and 13g of deionized water liquid.
Dissolving the Callicarpa Inophylla extract and the radix et caulis Opuntiae Dillenii extract at 25 deg.C for 168 hr to obtain solution A;
simultaneously, adding the panax notoginseng and the extract of the rhizomes fallen to the ground into deionized water, and stirring and mixing at the temperature of 80 ℃ and the speed of 250r/min to obtain a solution B;
and finally, mixing the solution A and the solution B at 25 ℃, adding a preservative, stirring at the speed of 300r/min for 20min, and filling the prepared medicinal liquor after stirring.
Example 4
First, the following components were weighed: 5g of coreopsis tinctoria extract, 6g of cactus extract, 10g of pseudo-ginseng, 20g of groundsel root-growing extract, 57g of wine liquid and 14g of deionized water liquid.
Dissolving the Callicarpa Inophylla extract and the radix et caulis Opuntiae Dillenii extract at 25 deg.C for 171 hr to obtain solution A;
simultaneously, adding the panax notoginseng and the extract of the rhizomes fallen to the ground into deionized water, and stirring and mixing at the temperature of 80 ℃ and the speed of 300r/min to obtain a solution B;
and finally, mixing the solution A and the solution B at the temperature of 30 ℃, adding a preservative, stirring at the speed of 350r/min for 25min, and filling the prepared medicinal liquor after stirring.
Example 5
First, the following components were weighed: 5g of coreopsis tinctoria extract, 8g of cactus extract, 12g of pseudo-ginseng, 25g of groundsel root extract, 60g of wine liquid and 15g of deionized water liquid.
Dissolving the Callicarpa Inophylla extract and the radix et caulis Opuntiae Dillenii extract at 25 deg.C for 171 hr to obtain solution A;
simultaneously, adding the panax notoginseng and the extract of the rhizomes fallen to the ground into deionized water, and stirring and mixing at the temperature of 85 ℃ and the speed of 300r/min to obtain a solution B;
and finally, mixing the solution A and the solution B at the temperature of 30 ℃, adding a preservative, stirring at the speed of 350r/min for 25min, and filling the prepared medicinal liquor after stirring.
Comparative example 1
The procedure in this example was the same as in example 3 except that no cactus extract was added.
Comparative example 2
The procedure in this example was the same as in example 3 except that 10g of cactus extract was added.
Comparative example 3
The procedure in this example was the same as in example 3 except that no extract of Fall Potentilla root was added.
Comparative example 4
The procedure in this example was the same as in example 3 except that 50g of extract of Fall Potentilla japonica was added.
Comparative example 5
The procedure in this example was the same as in example 3 except that no Calliopsis japonicus extract was added.
Comparative example 6
The procedure in this example was the same as in example 3 except that 30g of the Calliopsis japonicus extract was added.
Comparative example 7
The procedure in this example was the same as in example 3 except that no notoginseng was added.
Comparative example 8
The procedure in this example was the same as in example 3 except that 20g of notoginseng was added.
Comparative example 9
The components used in this example were the same as in example 3, except for the preparation steps.
The preparation steps are as follows: mixing herba Gynurae Divaricatae extract, radix et caulis Opuntiae Dillenii extract, Notoginseng radix, herba Salviae Plebeiae extract, wine solution and deionized water solution at 25 deg.C under stirring.
Examples of the experiments
The statistics of the chemical solutions and the scores of examples 1 to 5 and comparative examples 1 to 9 are shown in the following table 1:
1400 patients are selected clinically, and the symptoms are as follows: swelling and pain caused by various diseases such as lumbar disc herniation, hyperosteogeny, scapulohumeral periarthritis, cervical vertebra pain, contusion, sprain and the like. The separation into 14 groups: 100 people per group.
The application method comprises the following steps: the 14 groups of cases correspond to examples 1-5 and comparative examples 1-9 respectively, and are applied once a day in the morning and at night, kept for 30 minutes once and then cleaned, and 7 days is a treatment course.
The curative effect standard is as follows: significant effect, effective and ineffective.
(1) The effect is shown: after 1 course of treatment, the symptoms completely disappear, and no recurrence occurs within three months;
(2) the method has the following advantages: after being applied for 1 course of treatment, the symptoms are obviously improved, swelling and pain basically disappear, and the symptoms completely disappear after being applied for 2 courses of treatment; and no recurrence occurs within three months;
(3) and (4) invalidation: after 1 course of application, the symptoms are not improved or aggravated.
The test results are given in the following table:
test results
As can be seen from the above table, the drug solutions according to the examples of the present invention have excellent therapeutic effects. And the best results were obtained with the composition of example 3.
Comparing example 3 with comparative examples 1-2, it can be seen that the efficacy is not exerted when cactus extract is not added or when cactus extract is added too much, indicating that the best efficacy can be ensured only when the components of cactus extract are limited to a certain range.
Comparing example 3 with comparative examples 3-4, it can be seen that the efficacy is not good when the extract of radices sileris is not added or when the extract of radices sileris is added too much, which indicates that the best efficacy can be ensured only when the components of the extract of radices sileris are limited to a certain range.
Comparing example 3 with comparative examples 5 to 6, it can be seen that the efficacy is not favorably exhibited when the tanacetum parthenium extract is not added or the amount of the tanacetum parthenium extract is excessively increased, indicating that the best efficacy can be ensured only when the components of the tanacetum parthenium extract are limited to a certain range.
Comparing example 3 with comparative examples 7-8, it can be seen that the efficacy is not favorably exerted when no notoginseng is added or when too much notoginseng is added, indicating that the best efficacy can be ensured only when the notoginseng components are limited to a certain range.
Comparing example 3 with comparative example 9, it can be seen that the curative effect of example 3 is far better than that of comparative example 9, which shows that the prepared medicinal liquor can be ensured to have good curative effect only by adopting the specific steps and process parameters of the invention for preparation.
In a word, the anti-inflammatory and analgesic medicinal liquor has the effects of clearing away heat and toxic materials, diminishing inflammation, relieving pain, drawing out toxic materials and promoting tissue regeneration, and has good curative effects on lumbar disc herniation, hyperosteogeny, scapulohumeral periarthritis, cervical vertebra pain, contusion, sprain and other diseases.
While particular embodiments of the present invention have been illustrated and described, it would be obvious that various other changes and modifications can be made without departing from the spirit and scope of the invention. It is therefore intended to cover in the appended claims all such changes and modifications that are within the scope of this invention.
Claims (10)
1. The anti-inflammatory and analgesic medicinal liquor is characterized by comprising the following raw materials in parts by weight: 3-5 parts of coreopsis tinctoria extract, 2-8 parts of cactus extract, 7-12 parts of pseudo-ginseng, 10-25 parts of groundsel root extract, 50-60 parts of wine liquid and 10-15 parts of deionized water liquid.
2. The anti-inflammatory and analgesic medicinal liquor as claimed in claim 1, wherein the extracts of camomile 3-5 parts, cactus 4-6 parts, notoginseng 9-10 parts, extract of radices sileris 15-20 parts, wine 53-57 parts and deionized water 12-14 parts.
3. The anti-inflammatory and analgesic medicinal liquor as claimed in claim 1, wherein the extract of camomile is 4 parts, the extract of cactus is 5 parts, the extract of notoginseng is 9 parts, the extract of rhizomadesis falling is 18 parts, the liquor is 55 parts and the deionized water is 13 parts.
4. The anti-inflammatory and analgesic medicinal liquor as claimed in claim 1, wherein the liquor is a traditional-process self-brewed white liquor.
5. The method for preparing the anti-inflammatory and analgesic medicinal liquor as claimed in any one of claims 1 to 4, comprising the steps of:
dissolving a chamomile extract and a cactus extract in wine to obtain a solution A;
adding the pseudo-ginseng and the extract of the rhizoctonia falling into the ground into deionized water and stirring to obtain a solution B;
and step three, mixing the solution A and the solution B, adding the preservative, uniformly stirring, and filling.
6. The anti-inflammatory and analgesic medicinal liquor as claimed in claim 5, wherein the dissolving temperature in the first step is 20-25 ℃, and the dissolving time is 165-171 h.
7. The anti-inflammatory and analgesic medicinal liquor as claimed in claim 5, wherein the stirring speed in the second step is 200-300r/min, and the stirring temperature is 75-85 ℃.
8. The anti-inflammatory and analgesic medicinal liquor as claimed in claim 5, wherein the amount of the preservative added in the step three is 3% of the mass of the mixture of the solution A and the solution B.
9. The anti-inflammatory and analgesic medicinal liquor as claimed in claim 5, wherein the preservative is sodium benzoate.
10. The anti-inflammatory and analgesic medicinal liquor as claimed in claim 5, wherein the stirring temperature in the third step is 20-30 ℃, the stirring speed is 250-350r/min, and the stirring time is 15-25 min.
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Citations (3)
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| CN103952268A (en) * | 2013-10-04 | 2014-07-30 | 史文革 | Pseudo-ginseng health care wine |
| CN108379323A (en) * | 2018-05-29 | 2018-08-10 | 文峰 | A kind of preparation method and applications for treating spur ointment |
| CN109303811A (en) * | 2018-11-23 | 2019-02-05 | 重庆市嘉利酒业有限公司 | The exterior-applied medical wine of activating microcirculation and removing stasis medicinal anti-inflammatory analgetic |
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2021
- 2021-01-14 CN CN202110049506.1A patent/CN112675243A/en active Pending
Patent Citations (3)
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|---|---|---|---|---|
| CN103952268A (en) * | 2013-10-04 | 2014-07-30 | 史文革 | Pseudo-ginseng health care wine |
| CN108379323A (en) * | 2018-05-29 | 2018-08-10 | 文峰 | A kind of preparation method and applications for treating spur ointment |
| CN109303811A (en) * | 2018-11-23 | 2019-02-05 | 重庆市嘉利酒业有限公司 | The exterior-applied medical wine of activating microcirculation and removing stasis medicinal anti-inflammatory analgetic |
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