CN112609456A - 一种防毡缩呢子大衣的制备方法 - Google Patents
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- 229960002154 guar gum Drugs 0.000 claims abstract description 6
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- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 claims abstract description 6
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- 239000001397 quillaja saponaria molina bark Substances 0.000 claims abstract description 6
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- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical compound C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 claims abstract description 6
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Abstract
本发明公开了一种防毡缩呢子大衣的制备方法，将己二酸、乙基三乙氧基硅烷、邻羟基苯甲酸酯、丙烯酸乙酯、十二烷基三甲氧基硅烷、瓜尔胶羟丙基三甲基氯化铵、十二烷基磺酸钠己二胺、甲基环硅氧烷、双端羧基聚乙二醇份投入反应器中，氮气保护下升温反应，然后加入二癸基二甲基氯化铵、天然皂甙、异丙醇钛、亚磷酸，真空反应2‑3h，反应后降温至70℃，停止反应，得到整理剂；将呢子大衣浸泡于整理剂中浸轧，浸轧后的呢子大衣烘干，烘干后再焙烘。本发明生产工艺简单，制作成本低，整理得到的呢子大衣具有优良的防毡缩性能和高强力保留率，同时还可以保持呢子大衣原有柔韧性和手感，耐水洗，安全无害的特点。
Description
技术领域
本发明涉及一种防毡缩呢子大衣的制备方法。
技术背景
随着时代的发展，人们生活水平的不断提高，健康与时尚是人们追求的一种消费方式。现有的普通面料已经不能满足人们的需求。舒适性、多功能、易护理的服装越来越受到消费者的青睐。因此消费者对织物面料的舒适性、多功能、易护理的要求也越来越高。呢子大衣，一种较厚较密的毛织品。其面料由于风格新颖别致，挺括中不失柔软，朴实中又不失时尚，粗犷中蕴涵典雅，故在秋冬市场十分走俏。呢子面料不能水洗，水洗容易掉毛、缩水和变形。在生活节奏极其紧张的今天，人们不愿花太多心思和时间在服装护理上。因此纺织企业不断从其他技术领域引进借鉴各种新技术，以提高加工深度，通过整理获得更舒适性、多功能、易护理的产品。整理是通过化学或物理的主法改善面料的外观和手感、增进服用性能或赋予特殊功能的工艺过程。随着人类对环境污染和破坏的关注，对健康越来越重视，提倡“低碳”经济，后整理技术要求进行环保“绿色”加工，生产“清洁”、“低碳”的纺织产品。因此本发明提出一种低能耗、无污染的防毡缩呢子大衣的制备方法。
发明内容
本发明的目的在于针对现有技术的不足，提供了一种防毡缩呢子大衣的制备方法。
本发明的目的是通过以下技术方案实现的：
一种防毡缩呢子大衣的制备方法，所述方法包括以下步骤：
步骤1、按重量份数比，将己二酸13-18份、乙基三乙氧基硅烷8-10份、邻羟基苯甲酸酯4-9份、丙烯酸乙酯4-7份、十二烷基三甲氧基硅烷1-3份、瓜尔胶羟丙基三甲基氯化铵2-6份、十二烷基磺酸钠己二胺2-4份、甲基环硅氧烷4-7份、双端羧基聚乙二醇1-5份投入反应器中，氮气保护下升温至170-200℃，保温0.5-1h，然后加入二癸基二甲基氯化铵3-7份、天然皂甙12-16份、异丙醇钛3-6份、亚磷酸1-5份，升温至240-260℃，在0.04-0.08MPa下真空反应2-3h，反应后降温至70℃，停止反应，得到整理剂；
步骤2、将呢子大衣浸泡于整理剂中，浸泡后的呢子大衣在室温下进行浸轧工艺，浸泡时间0.5-2h，轧车转速为0.18-0.32m/s，压力1.4-2.6Mpa，浸轧后的呢子大衣放入烘箱中烘干，再将烘干后的呢子大衣放入170-200℃的焙烘箱中1-2分钟。
所述步骤2中浸轧工艺为二浸二轧工艺，其浸轧温度：20-50℃，轧余率：80-90%。
所述步骤2中烘干温度为120-160℃，烘干时间为1-5分钟。
所述整理剂的浓度为30-100g/L。
所述焙烘温度为185℃，焙烘时间为1.5分钟。
有益效果：本发明制备的产品的生产工艺简单，制作成本低，整理得到的呢子大衣具有优良的防毡缩性能和高强力保留率，同时还可以保持呢子大衣原有柔韧性和手感，耐水洗，安全无害的特点。
具体实施方式
本发明所述的实例是对本发明的说明而不能限制本发明，在与本发明相当的含义和范围内的任何改变和调整，都应认为是在本发明的范围内。
实施例1
一种防毡缩呢子大衣的制备方法，所述方法包括以下步骤：
步骤1、按重量份数比，将己二酸13份、乙基三乙氧基硅烷8份、邻羟基苯甲酸酯4份、丙烯酸乙酯4份、十二烷基三甲氧基硅烷1份、瓜尔胶羟丙基三甲基氯化铵2份、十二烷基磺酸钠己二胺2份、甲基环硅氧烷4份、双端羧基聚乙二醇1份投入反应器中，氮气保护下升温至170℃，保温0.5h，然后加入二癸基二甲基氯化铵3份、天然皂甙12份、异丙醇钛3份、亚磷酸1份，升温至240℃，在0.04MPa下真空反应2h，反应后降温至70℃，停止反应，得到整理剂；
步骤2、将整理剂和水混合后搅拌均匀得到整理液，整理剂的浓度为30g/L，将呢子大衣浸泡于整理液中，浸泡后的呢子大衣在室温下进行浸轧工艺，浸轧工艺为二浸二轧工艺，其浸轧温度：20℃，轧余率：80%，浸泡时间0.5h，轧车转速为0.18m/s，压力1.4Mpa，浸轧后的呢子大衣放入烘箱中烘干，烘干温度为120℃，烘干时间为1分钟，再将烘干后的呢子大衣放入170℃的焙烘箱中1分钟。
实施例2
一种防毡缩呢子大衣的制备方法，所述方法包括以下步骤：
步骤1、按重量份数比，将己二酸15份、乙基三乙氧基硅烷9份、邻羟基苯甲酸酯6份、丙烯酸乙酯5份、十二烷基三甲氧基硅烷2份、瓜尔胶羟丙基三甲基氯化铵4份、十二烷基磺酸钠己二胺3份、甲基环硅氧烷6份、双端羧基聚乙二醇3份投入反应器中，氮气保护下升温至180℃，保温1h，然后加入二癸基二甲基氯化铵7份、天然皂甙16份、异丙醇钛4份、亚磷酸3份，升温至250℃，在0.06MPa下真空反应2.5h，反应后降温至70℃，停止反应，得到整理剂；
步骤2、将整理剂和水混合后搅拌均匀得到整理液，整理剂的浓度为60g/L，将呢子大衣浸泡于整理液中，浸泡后的呢子大衣在室温下进行浸轧工艺，浸轧工艺为二浸二轧工艺，其浸轧温度：30℃，轧余率：85%，浸泡时间1h，轧车转速为0.22m/s，压力1.8Mpa，浸轧后的呢子大衣放入烘箱中烘干，烘干温度为140℃，烘干时间为3分钟，再将烘干后的呢子大衣放入185℃的焙烘箱中1.5分钟。
实施例3
一种防毡缩呢子大衣的制备方法，所述方法包括以下步骤：
步骤1、按重量份数比，将己二酸18份、乙基三乙氧基硅烷10份、邻羟基苯甲酸酯9份、丙烯酸乙酯7份、十二烷基三甲氧基硅烷3份、瓜尔胶羟丙基三甲基氯化铵6份、十二烷基磺酸钠己二胺4份、甲基环硅氧烷7份、双端羧基聚乙二醇5份投入反应器中，氮气保护下升温至200℃，保温1h，然后加入二癸基二甲基氯化铵7份、天然皂甙16份、异丙醇钛6份、亚磷酸5份，升温至260℃，在0.08MPa下真空反应3h，反应后降温至70℃，停止反应，得到整理剂；
步骤2、将整理剂和水混合后搅拌均匀得到整理液，整理剂的浓度为100g/L，将呢子大衣浸泡于整理液中，浸泡后的呢子大衣在室温下进行浸轧工艺，浸轧工艺为二浸二轧工艺，其浸轧温度，50℃，轧余率：90%，浸泡时间2h，轧车转速为0..32m/s，压力2.6Mpa，浸轧后的呢子大衣放入烘箱中烘干，烘干温度为160℃，烘干时间为5分钟，再将烘干后的呢子大衣放入200℃的焙烘箱中2分钟。
Claims (5)
1.一种防毡缩呢子大衣的制备方法，其特征在于所述方法包括以下步骤：
步骤1、按重量份数比，将己二酸13-18份、乙基三乙氧基硅烷8-10份、邻羟基苯甲酸酯4-9份、丙烯酸乙酯4-7份、十二烷基三甲氧基硅烷1-3份、瓜尔胶羟丙基三甲基氯化铵2-6份、十二烷基磺酸钠己二胺2-4份、甲基环硅氧烷4-7份、双端羧基聚乙二醇1-5份投入反应器中，氮气保护下升温至170-200℃，保温0.5-1h，然后加入二癸基二甲基氯化铵3-7份、天然皂甙12-16份、异丙醇钛3-6份、亚磷酸1-5份，升温至240-260℃，在0.04-0.08MPa下真空反应2-3h，反应后降温至70℃，停止反应，得到整理剂；
步骤2、将呢子大衣浸泡于整理剂中，浸泡后的呢子大衣在室温下进行浸轧工艺，浸泡时间0.5-2h，轧车转速为0.18-0.32m/s，压力1.4-2.6Mpa，浸轧后的呢子大衣放入烘箱中烘干，再将烘干后的呢子大衣放入170-200℃的焙烘箱中1-2分钟。
2.根据权利要求1所述的一种防毡缩呢子大衣的制备方法，其特征在于：所述步骤2中浸轧工艺为二浸二轧工艺，其浸轧温度：20-50℃，轧余率：80-90%。
3.根据权利要求1所述的一种防毡缩呢子大衣的制备方法，其特征在于：所述步骤2中烘干温度为120-160℃，烘干时间为1-5分钟。
4.根据权利要求1所述的一种防毡缩呢子大衣的制备方法，其特征在于：所述整理剂的浓度为30-100g/L。
5.根据权利要求1所述的一种防毡缩呢子大衣的制备方法，其特征在于：所述焙烘温度为185℃，焙烘时间为1.5分钟。
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