CN112574475A - Brittle wall material for cigarette blasting bead - Google Patents
Brittle wall material for cigarette blasting bead Download PDFInfo
- Publication number
- CN112574475A CN112574475A CN202011530676.3A CN202011530676A CN112574475A CN 112574475 A CN112574475 A CN 112574475A CN 202011530676 A CN202011530676 A CN 202011530676A CN 112574475 A CN112574475 A CN 112574475A
- Authority
- CN
- China
- Prior art keywords
- wall material
- cigarette
- parts
- brittle wall
- brittle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000011324 bead Substances 0.000 title claims abstract description 25
- 239000000463 material Substances 0.000 title claims abstract description 25
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 17
- 238000005422 blasting Methods 0.000 title claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 239000002738 chelating agent Substances 0.000 claims abstract description 5
- 229910052751 metal Inorganic materials 0.000 claims abstract description 5
- 239000002184 metal Substances 0.000 claims abstract description 5
- 239000003755 preservative agent Substances 0.000 claims abstract description 5
- 230000002335 preservative effect Effects 0.000 claims abstract description 5
- 239000004094 surface-active agent Substances 0.000 claims abstract description 5
- 239000000499 gel Substances 0.000 claims description 12
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 10
- 229920002148 Gellan gum Polymers 0.000 claims description 8
- 235000010492 gellan gum Nutrition 0.000 claims description 8
- 239000000216 gellan gum Substances 0.000 claims description 8
- 229920001817 Agar Polymers 0.000 claims description 6
- 239000004368 Modified starch Substances 0.000 claims description 6
- 229920000881 Modified starch Polymers 0.000 claims description 6
- 239000008272 agar Substances 0.000 claims description 6
- 235000010418 carrageenan Nutrition 0.000 claims description 6
- 239000000679 carrageenan Substances 0.000 claims description 6
- 229920001525 carrageenan Polymers 0.000 claims description 6
- 229940113118 carrageenan Drugs 0.000 claims description 6
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims description 6
- 235000019426 modified starch Nutrition 0.000 claims description 6
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 6
- 239000011780 sodium chloride Substances 0.000 claims description 5
- 239000000126 substance Substances 0.000 claims description 5
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 4
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 3
- 239000004288 Sodium dehydroacetate Substances 0.000 claims description 3
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 claims description 3
- 229960002216 methylparaben Drugs 0.000 claims description 3
- 239000004302 potassium sorbate Substances 0.000 claims description 3
- 235000010241 potassium sorbate Nutrition 0.000 claims description 3
- 229940069338 potassium sorbate Drugs 0.000 claims description 3
- 235000019259 sodium dehydroacetate Nutrition 0.000 claims description 3
- 229940079839 sodium dehydroacetate Drugs 0.000 claims description 3
- DSOWAKKSGYUMTF-GZOLSCHFSA-M sodium;(1e)-1-(6-methyl-2,4-dioxopyran-3-ylidene)ethanolate Chemical compound [Na+].C\C([O-])=C1/C(=O)OC(C)=CC1=O DSOWAKKSGYUMTF-GZOLSCHFSA-M 0.000 claims description 3
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 2
- 229920001213 Polysorbate 20 Polymers 0.000 claims description 2
- 229920001214 Polysorbate 60 Polymers 0.000 claims description 2
- 239000001110 calcium chloride Substances 0.000 claims description 2
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 claims description 2
- 235000010486 polyoxyethylene sorbitan monolaurate Nutrition 0.000 claims description 2
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 2
- 229920000053 polysorbate 80 Polymers 0.000 claims description 2
- 239000001103 potassium chloride Substances 0.000 claims description 2
- 235000011164 potassium chloride Nutrition 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- 235000010268 sodium methyl p-hydroxybenzoate Nutrition 0.000 claims description 2
- 238000010521 absorption reaction Methods 0.000 abstract description 7
- 241000208125 Nicotiana Species 0.000 abstract description 5
- 235000002637 Nicotiana tabacum Nutrition 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 231100000956 nontoxicity Toxicity 0.000 abstract 1
- 238000003756 stirring Methods 0.000 description 9
- 238000010438 heat treatment Methods 0.000 description 6
- 239000011259 mixed solution Substances 0.000 description 6
- 238000005303 weighing Methods 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 238000001914 filtration Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 230000010355 oscillation Effects 0.000 description 3
- 238000004220 aggregation Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000003349 gelling agent Substances 0.000 description 2
- 239000003292 glue Substances 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 229920001661 Chitosan Polymers 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 235000010489 acacia gum Nutrition 0.000 description 1
- 239000001785 acacia senegal l. willd gum Substances 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 229950006191 gluconic acid Drugs 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 239000002085 irritant Substances 0.000 description 1
- 231100000021 irritant Toxicity 0.000 description 1
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 230000009044 synergistic interaction Effects 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L5/00—Compositions of polysaccharides or of their derivatives not provided for in groups C08L1/00 or C08L3/00
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/16—Halogen-containing compounds
- C08K2003/162—Calcium, strontium or barium halides, e.g. calcium, strontium or barium chloride
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to the field of tobacco production, in particular to a brittle wall material for cigarette bead blasting, which is characterized by comprising the following raw materials in parts by weight: 5-10 parts of gel, 0.5-1.0 part of metal chelating agent, 0.1-0.5 part of surfactant, 0.1-0.5 part of preservative and 88-93 parts of water. The brittle wall material produced by using the formula has the advantages of good stability, capability of effectively reducing phenomena of moisture absorption softening, adhesion and the like of the bead blasting for cigarettes, no pungent smell, safety and no toxicity.
Description
Technical Field
The invention relates to the field of tobacco production, in particular to a brittle wall material for a cigarette bead.
Background
The bead is widely applied to the field of tobacco manufacturing, a smoker can break the bead by pinching with hands in the cigarette smoking process to enable essence in the bead to overflow, and the flavor components in the essence are released in the mainstream smoke of the cigarette, so that the effects of increasing flavor and keeping moisture can be achieved, and the taste level of the tobacco is enriched.
The blasting beads in the prior art are mostly made of brittle wall materials and are mainly prepared from raw materials such as gelatin, Arabic gum, vegetable polysaccharide, chitosan and the like according to a certain proportion. The components are mainly hydrophilic glue raw materials, and when the humidity of the preservation environment of the popping beads is higher, the glue skin can absorb moisture in the air, the phenomena of moisture absorption softening, adhesion, permeation and the like are caused, and the brittleness of the popping beads is reduced. Especially, after the tobacco is smoked for a period of time, the mainstream smoke released in the burning process contains certain water vapor, so that the moisture absorption and softening phenomena of the exploded bead are more obvious and sometimes even can not be broken, the use experience of smokers is seriously influenced, and the actual application effect of the exploded bead is reduced.
Disclosure of Invention
The invention aims to provide a brittle wall material for a cigarette blasting bead, which has good stability, can effectively reduce the phenomena of moisture absorption softening, adhesion and the like of the cigarette blasting bead, has no pungent smell, and is safe and nontoxic.
The technical scheme for realizing the aim of the invention is that the brittle wall material for the cigarette blasting bead is characterized by comprising the following raw materials in parts by weight: 5-10 parts of gel, 0.5-1.0 part of metal chelating agent, 0.1-0.5 part of surfactant, 0.1-0.5 part of preservative and 88-93 parts of water.
The gel comprises the following raw materials in percentage by weight: 5-10% of carrageenan, 35-40% of gellan gum, 50-55% of agar and 1-5% of modified starch.
And the metal chelating agent is a mixture of one or more salt substances selected from sodium chloride, potassium chloride, calcium chloride and the like.
And the surfactant is one or more compounds selected from Tween-20, Tween-60 and Tween-80.
And the preservative is one or more selected from sodium dehydroacetate, methyl paraben and potassium sorbate.
The water is pure water, and the resistivity of the water is 10-15 megaohms.
The principle of the invention is as follows: the gel in the formula takes agar as a main raw material and is reasonably compounded with gellan gum, carrageenan and modified starch. Through the synergistic interaction among the four colloids, the wall material has certain brittleness and strength. The gellan gum is prepared from beta-1, 3-D glucose, beta-1, 4-D-gluconic acid and alpha-1, 4-L-rhamnose according to a molar ratio of 2: 1: 1, low temperature exists in a double helix structure, and high temperature exists in a single strand form. After the gellan gum is dissolved in water, an automatic aggregation phenomenon can be generated among molecules to form a double-spiral structure, and a three-dimensional network structure can be formed by further aggregation, so that water molecules are conveniently trapped to generate a gel phenomenon, and therefore the formed bead has good stability and still has good brittleness after moisture absorption.
The invention has the advantages that: 1. the wall material prepared by the formula can not generate the phenomena of moisture absorption, softening, adhesion and the like after being stored for a period of time in a normal temperature environment; when the bead is broken by hand, a crisp sound can be heard. 2. The material is stable, non-toxic, free of side effect, non-irritant and does not affect the taste of the essence and the spice.
Drawings
FIG. 1 is a schematic diagram showing the water content of a brittle wall material of a bead for cigarette in an open environment.
Detailed Description
Referring to fig. 1, the present invention will be further explained with reference to examples.
The first embodiment,
Firstly, weighing 1 g of carrageenan, 3.5 g of gellan gum, 5 g of agar and 5 g of modified starch, and uniformly mixing to obtain a gel; weighing 1 g of sodium chloride, 800.5 g of tween-sodium, 0.5 g of sodium dehydroacetate and 88 g of pure water, uniformly mixing with 10 g of prepared gel, placing in a heating container, continuously stirring, heating to 90 ℃ in the stirring process, continuously keeping the temperature and stirring for 1.5 hours, and obtaining a mixed solution after the materials are fully dissolved; and finally, filtering the mixed solution, removing bubbles through ultrasonic oscillation, and keeping the temperature at 90 ℃ for later use, wherein the obtained liquid substance is the brittle wall material.
Example II,
Firstly, weighing 0.8 g of carrageenan, 3.2 g of gellan gum, 3.6 g of agar and 0.4 g of modified starch, and uniformly mixing to obtain 8 g of gel; weighing 0.8 g of sodium chloride, 0.5 g of tween-800.3 g of potassium sorbate and 90.4 g of pure water, uniformly mixing with 8 g of prepared gel, placing in a heating container, continuously stirring, heating to 85 ℃ in the stirring process, continuously keeping the temperature and stirring for 2 hours, and obtaining a mixed solution after the materials are fully dissolved; and finally, filtering the mixed solution, removing bubbles by ultrasonic oscillation to obtain a liquid substance which is a brittle wall material, and preserving heat at 85 ℃ for later use.
Example III,
Firstly, weighing 0.25 g of carrageenan, 2 g of gellan gum, 2.65 g of agar and 0.1 g of modified starch, and uniformly mixing to obtain 5 g of gel; weighing 0.5 g of sodium chloride, 800.1 g of tween-1, 0.1 g of methyl paraben and 94.3 g of pure water, uniformly mixing with 5 g of prepared gel, placing in a heating container, continuously stirring, heating to 80 ℃ in the stirring process, continuously preserving heat and stirring for 5 hours, and obtaining a mixed solution after the materials are fully dissolved; and finally, filtering the mixed solution, removing bubbles by ultrasonic oscillation to obtain a liquid substance which is a brittle wall material, and preserving heat at 80 ℃ for later use.
In the above examples, if the amount of the gelling agent is less than 6 parts by weight, the gelling time is long and the rubber is not easily molded, and if the amount is more than 10 parts by weight, the gelling time is too fast and the viscosity is high and the dripping is not easily caused. Therefore, the dosage of the optional gelling agent is 5-10 parts, and more preferably 6-8 parts. The water content of the brittle wall material prepared by the formula in an open environment is obviously lower than that of the product in the prior art, the waterproof effect is good, and the phenomena of moisture absorption, softening, adhesion and the like can not occur by combining with the figure 1.
Claims (6)
1. The brittle wall material for the cigarette bead blasting is characterized by comprising the following raw materials in parts by weight:
5-10 parts of gel, 0.5-1.0 part of metal chelating agent, 0.1-0.5 part of surfactant, 0.1-0.5 part of preservative and 88-93 parts of water.
2. The fragile wall material of the popping bead for the cigarette as claimed in claim 1, wherein the gel comprises the following raw materials by weight percent: 5-10% of carrageenan, 35-40% of gellan gum, 50-55% of agar and 1-5% of modified starch.
3. The brittle wall material for cigarette blasting beads according to claim 1, characterized in that: the metal chelating agent is a mixture of one or more salt substances selected from sodium chloride, potassium chloride, calcium chloride and the like.
4. The brittle wall material for cigarette blasting beads according to claim 1, characterized in that: the surfactant is one or more compounds selected from Tween-20, Tween-60 and Tween-80.
5. The brittle wall material for cigarette blasting beads according to claim 1, characterized in that: the preservative is one or more selected from sodium dehydroacetate, methyl paraben and potassium sorbate.
6. The brittle wall material for cigarette blasting beads according to claim 1, characterized in that: the water is pure water, and the resistivity of the water is 10-15 megaohms.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011530676.3A CN112574475A (en) | 2020-12-22 | 2020-12-22 | Brittle wall material for cigarette blasting bead |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011530676.3A CN112574475A (en) | 2020-12-22 | 2020-12-22 | Brittle wall material for cigarette blasting bead |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112574475A true CN112574475A (en) | 2021-03-30 |
Family
ID=75139043
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011530676.3A Pending CN112574475A (en) | 2020-12-22 | 2020-12-22 | Brittle wall material for cigarette blasting bead |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112574475A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114617292A (en) * | 2022-04-29 | 2022-06-14 | 四川三联新材料有限公司 | Novel bead blasting wall material for cigarettes and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109393555A (en) * | 2018-12-07 | 2019-03-01 | 云南巴菰生物科技有限公司 | A kind of preparation method of the cigarette capsule with degrading resistance property |
| CN109549249A (en) * | 2018-12-11 | 2019-04-02 | 云南巴菰生物科技有限公司 | A kind of preparation method of cigarette preservation antioxidation capsule |
| CN110897194A (en) * | 2019-11-15 | 2020-03-24 | 湖北中烟工业有限责任公司 | Bead blasting wall material for cigarettes and preparation method thereof |
| WO2020148924A1 (en) * | 2019-01-18 | 2020-07-23 | 三生医薬株式会社 | Seamless capsule, and filter and smoking device including same |
-
2020
- 2020-12-22 CN CN202011530676.3A patent/CN112574475A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109393555A (en) * | 2018-12-07 | 2019-03-01 | 云南巴菰生物科技有限公司 | A kind of preparation method of the cigarette capsule with degrading resistance property |
| CN109549249A (en) * | 2018-12-11 | 2019-04-02 | 云南巴菰生物科技有限公司 | A kind of preparation method of cigarette preservation antioxidation capsule |
| WO2020148924A1 (en) * | 2019-01-18 | 2020-07-23 | 三生医薬株式会社 | Seamless capsule, and filter and smoking device including same |
| CN110897194A (en) * | 2019-11-15 | 2020-03-24 | 湖北中烟工业有限责任公司 | Bead blasting wall material for cigarettes and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114617292A (en) * | 2022-04-29 | 2022-06-14 | 四川三联新材料有限公司 | Novel bead blasting wall material for cigarettes and preparation method thereof |
| CN114617292B (en) * | 2022-04-29 | 2024-02-06 | 四川三联新材料有限公司 | Novel bead-explosion wall material for cigarettes and preparation method thereof |
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Application publication date: 20210330 |
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