CN114617292B - Novel bead-explosion wall material for cigarettes and preparation method thereof - Google Patents
Novel bead-explosion wall material for cigarettes and preparation method thereof Download PDFInfo
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- CN114617292B CN114617292B CN202210467022.3A CN202210467022A CN114617292B CN 114617292 B CN114617292 B CN 114617292B CN 202210467022 A CN202210467022 A CN 202210467022A CN 114617292 B CN114617292 B CN 114617292B
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- 239000000463 material Substances 0.000 title claims abstract description 39
- 238000004880 explosion Methods 0.000 title claims abstract description 28
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims abstract description 23
- 239000005060 rubber Substances 0.000 claims abstract description 44
- 239000011324 bead Substances 0.000 claims abstract description 43
- 239000000843 powder Substances 0.000 claims abstract description 37
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000004014 plasticizer Substances 0.000 claims abstract description 19
- 239000003755 preservative agent Substances 0.000 claims abstract description 17
- 230000002335 preservative effect Effects 0.000 claims abstract description 17
- 239000000049 pigment Substances 0.000 claims abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims abstract description 6
- 229920001817 Agar Polymers 0.000 claims description 18
- 239000008272 agar Substances 0.000 claims description 18
- 235000010419 agar Nutrition 0.000 claims description 18
- 235000010418 carrageenan Nutrition 0.000 claims description 16
- 239000000679 carrageenan Substances 0.000 claims description 16
- 229920001525 carrageenan Polymers 0.000 claims description 16
- 229940113118 carrageenan Drugs 0.000 claims description 16
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 16
- 229920002148 Gellan gum Polymers 0.000 claims description 14
- 235000010492 gellan gum Nutrition 0.000 claims description 14
- 239000000216 gellan gum Substances 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 13
- PEDCQBHIVMGVHV-UHFFFAOYSA-N glycerol group Chemical group OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 8
- 239000004288 Sodium dehydroacetate Substances 0.000 claims description 3
- 235000011187 glycerol Nutrition 0.000 claims description 3
- 229940079839 sodium dehydroacetate Drugs 0.000 claims description 3
- 235000019259 sodium dehydroacetate Nutrition 0.000 claims description 3
- DSOWAKKSGYUMTF-GZOLSCHFSA-M sodium;(1e)-1-(6-methyl-2,4-dioxopyran-3-ylidene)ethanolate Chemical group [Na+].C\C([O-])=C1/C(=O)OC(C)=CC1=O DSOWAKKSGYUMTF-GZOLSCHFSA-M 0.000 claims description 3
- 239000002245 particle Substances 0.000 abstract description 7
- 230000009172 bursting Effects 0.000 abstract description 6
- 239000000084 colloidal system Substances 0.000 abstract description 5
- 239000000243 solution Substances 0.000 description 11
- 230000000052 comparative effect Effects 0.000 description 8
- 239000000499 gel Substances 0.000 description 8
- 239000003292 glue Substances 0.000 description 8
- 239000000047 product Substances 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 229920002752 Konjac Polymers 0.000 description 3
- 235000010489 acacia gum Nutrition 0.000 description 3
- 239000001785 acacia senegal l. willd gum Substances 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 239000002360 explosive Substances 0.000 description 3
- 239000001341 hydroxy propyl starch Substances 0.000 description 3
- 235000013828 hydroxypropyl starch Nutrition 0.000 description 3
- 235000010485 konjac Nutrition 0.000 description 3
- 239000006187 pill Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000005303 weighing Methods 0.000 description 3
- 108010010803 Gelatin Proteins 0.000 description 2
- 229920001938 Vegetable gum Polymers 0.000 description 2
- 238000005422 blasting Methods 0.000 description 2
- 239000002775 capsule Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 229920000159 gelatin Polymers 0.000 description 2
- 239000008273 gelatin Substances 0.000 description 2
- 235000019322 gelatine Nutrition 0.000 description 2
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- 230000002195 synergetic effect Effects 0.000 description 2
- 239000001993 wax Substances 0.000 description 2
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 description 1
- 241000220479 Acacia Species 0.000 description 1
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- 229920001353 Dextrin Polymers 0.000 description 1
- 239000004375 Dextrin Substances 0.000 description 1
- 239000001856 Ethyl cellulose Substances 0.000 description 1
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 1
- 206010016807 Fluid retention Diseases 0.000 description 1
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- 235000010643 Leucaena leucocephala Nutrition 0.000 description 1
- 229920000881 Modified starch Polymers 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 108010073771 Soybean Proteins Proteins 0.000 description 1
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- 102000007544 Whey Proteins Human genes 0.000 description 1
- 108010046377 Whey Proteins Proteins 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 235000013871 bee wax Nutrition 0.000 description 1
- 239000012166 beeswax Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000005018 casein Substances 0.000 description 1
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 1
- 235000021240 caseins Nutrition 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 229920006184 cellulose methylcellulose Polymers 0.000 description 1
- 239000000701 coagulant Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 235000019425 dextrin Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 235000019325 ethyl cellulose Nutrition 0.000 description 1
- 229920001249 ethyl cellulose Polymers 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 235000019426 modified starch Nutrition 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 231100000956 nontoxicity Toxicity 0.000 description 1
- 229920001542 oligosaccharide Polymers 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 235000010413 sodium alginate Nutrition 0.000 description 1
- 239000000661 sodium alginate Substances 0.000 description 1
- 229940005550 sodium alginate Drugs 0.000 description 1
- 229940001941 soy protein Drugs 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 238000009210 therapy by ultrasound Methods 0.000 description 1
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- 235000013311 vegetables Nutrition 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 235000021119 whey protein Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Paper (AREA)
- Manufacturing Of Cigar And Cigarette Tobacco (AREA)
Abstract
The invention discloses a novel cigarette explosion bead wall material and a preparation method thereof, wherein the wall material comprises the following raw materials in parts by weight: 35-40 parts of rubber powder, 0.1-0.3 part of preservative, 5-10 parts of plasticizer, 0.1-0.3 part of pigment and 1150 parts of water. The explosion beads prepared by dripping the wall materials have good crushing strength, and do not soften when stored for a period of time in an open environment. And the rubber strength and the bursting strength can be adjusted by freely adjusting the proportion of each colloid, so that the method can be suitable for bursting beads with different particle sizes.
Description
Technical Field
The invention relates to the technical field of bead blasting wall materials for cigarettes, in particular to a novel bead blasting wall material for cigarettes and a preparation method thereof.
Background
The explosive beads, also called as fragrant pills, brittle capsules and beads, are sealed brittle capsules formed by wrapping essence and spice with a suitable wall material, and are mainly applied to cigarette products. The explosion bead consists of a rubber sheet and core liquid, wherein the rubber sheet is used for wrapping and sealing the core liquid. The rubber is broken when reaching the triggering condition, and the core liquid component is released to realize the purposes of enhancing fragrance, preserving moisture and the like.
At present, the explosion beads for cigarettes mainly adopt a water phase-coated oil phase system. For coating the ester soluble content, the general requirements are that the material has stable performance, no toxicity, no side effect, no irritation, compatibility, no influence on the functions of essence and spice, and the viscosity, permeability, certain strength, plasticity and the like which meet the requirements, and common wall materials are vegetable gums (acacia, sodium alginate, carrageenan and the like), starch and derivatives thereof (various types of dextrin, oligosaccharide, starch derivatives and the like, have good emulsifying property, film forming property and confidentiality, are good wall materials for embedding the essence), proteins (gelatin, casein, soy protein, whey protein and the like), various cellulose derivatives (CMC, ethylcellulose, methylcellulose substances and the like), waxes (insect wax, paraffin wax, beeswax and the like) and the like.
At present, most of wall materials of the explosion beads for cigarettes adopt hydrophilic colloid raw materials such as gelatin, vegetable gum, vegetable polysaccharide, polyethylene glycol and the like, are easy to soften and even mould in a humid environment, and gradually lose brittleness and lose the breaking sound of the explosion beads.
Therefore, developing a bead wall material with good stability and capable of providing coating performance and water resistance is a problem to be solved urgently.
Disclosure of Invention
In order to solve the technical problems, the invention provides a novel wall material of the explosion beads for cigarettes and a preparation method thereof, wherein the explosion beads prepared by dripping the wall material have good crushing strength, and do not soften when being stored for a period of time in an open environment. And the rubber strength and the bursting strength can be adjusted by freely adjusting the proportion of each colloid, so that the method can be suitable for bursting beads with different particle sizes.
In order to achieve the technical effects, the invention provides the following technical scheme:
the novel cigarette explosion bead wall material comprises the following raw materials in parts by weight: 35-40 parts of rubber powder, 0.1-0.3 part of preservative, 5-10 parts of plasticizer, 0.1-0.3 part of pigment and 1150 parts of water.
The further technical scheme is that the rubber powder consists of the following raw materials in parts by weight: 20-25 parts of agar, 10-15 parts of gellan gum and 1-3 parts of carrageenan.
According to a further technical scheme, the plasticizer is glycerol.
According to a further technical scheme, the preservative is sodium dehydroacetate.
The further technical proposal is that the water is pure water, and the TDS is less than or equal to 10.
The preparation method of the novel cigarette bead explosion wall material comprises the following steps: according to the weight portions, 35 to 40 portions of rubber powder, 0.1 to 0.3 portion of preservative, 5 to 10 portions of plasticizer and 0.1 to 0.3 portion of pigment are weighed, 1150 portions of water are added into a liquid preparation tank, the water is heated to 70 to 80 ℃, the plasticizer, the preservative and the pigment are sequentially added under the condition of continuous stirring, the rubber powder is added after stirring for 2 to 5 minutes, the liquid preparation tank is closed after the rubber powder is added, and stirring reaction is carried out for 80 to 100 minutes at 80+/-2 ℃.
According to a further technical scheme, the stirring frequency is 50HZ.
The further technical scheme is that the rubber powder consists of the following raw materials in parts by weight: 20-25 parts of agar, 10-15 parts of gellan gum and 1-3 parts of carrageenan.
The rubber powder consists of agar, gellan gum and carrageenan, and firstly, the agar has good stability, is difficult to degrade at room temperature and can have good storability; in addition, the agar has the largest characteristic of having gel property, even if the concentration is 0.004% of the agar solution, the agar solution can form gel at normal temperature, and the gel strength is the largest at the same concentration compared with other substances capable of forming gel. The agar forms gel without any coagulant aid, which is one of the reasons why no other additives are needed; the gellan gum can play a role with lower dosage. Is stable under the conditions of heating and low pH and is not easy to be hydrolyzed. The viscosity of the gellan gum is rapidly reduced when the temperature is increased, but the viscosity can be completely recovered after cooling, thereby facilitating the process of dissolving the gum and dripping pills; secondly, the gellan gum is sensitive to ions and can be suitable for strengthening technology; moreover, the gellan gum has good compatibility with other gums and other ingredients, and the prepared system has good flavor release; the carrageenan has thickening property, can be used for adjusting the viscosity of the glue solution, and the viscosity of the glue solution is important for the success of the dripping pill process; secondly, carrageenan can produce synergistic effect with other colloids, and the elasticity and water retention of the gel are improved.
Compared with the prior art, the invention has the following beneficial effects: the invention adopts the synergistic effect of agar, gellan gum and carrageenan, reduces the use amount of the rubber powder, and the proportion of the rubber powder in the whole formula is only about 3 percent, and the wall material prepared by the formula can effectively lock the internal core liquid of the explosion beads for cigarettes, can ensure that the fragrance is not lost during storage, and has wide raw material sources, safety and sanitation. The explosion beads prepared by dripping the wall materials of the formula have good crushing strength and can not be softened after being stored for a period of time in an open environment. And the rubber strength and the bursting strength can be adjusted by freely adjusting the proportion of each colloid, so that the method can be suitable for bursting beads with different particle sizes.
Detailed Description
The invention is further illustrated and described below in connection with specific examples.
Example 1
The novel cigarette explosion bead wall material comprises the following components in parts by weight: 3.8 parts of rubber powder, 0.02 part of preservative, 1 part of plasticizer, 0.01 part of pigment and 115 parts of water. Wherein the rubber powder comprises 20 parts of agar, 15 parts of gellan gum and 3 parts of carrageenan. The viscosity of the glue solution was 75.2 mpa.s.
The preparation method comprises the following steps: the adhesive powder, the plasticizer, the preservative, the pigment and the water are weighed according to the weight parts. Adding water into the liquid preparation tank, and starting heating. When the water temperature in the tank is heated to 70 ℃ (the digital thermometer is displayed as standard), the stirring function of the liquid preparation tank is started, the rotating speed frequency is regulated to 50HZ, and the purified water can not overflow from the observation port too fast. Adding the weighed materials into a liquid preparation tank according to the sequence (plasticizer, pigment and rubber powder), adding and stirring the plasticizer and the pigment for 2-5 minutes, adding the rubber powder, slowly and uniformly adding the rubber powder, adding for at least 2 minutes, washing residual materials in containers such as a beaker and the like with pure water after the rubber powder adding is completed, pouring the washed residual materials into the liquid preparation tank for stirring and mixing, ensuring that the formula materials completely enter the rubber solution, and closing a rubber melting cover. The reaction was stirred at 80.+ -. 2 ℃ for 90 minutes. The glue solution with qualified viscosity value is filtered by a 80-mesh standard sample sieve after being evenly stirred and mixed, and the glue solution can be used for producing dripping.
A total of 10 samples are selected and detected, the pressure average value of the explosion beads of the finished product is 14.37N, the SD value is 1.584 on average, and the particle size average value is 2.71mm (small beads).
Example 2
The novel cigarette explosion bead wall material comprises the following components in parts by weight: 3.8 parts of rubber powder, 0.02 part of preservative, 1 part of plasticizer, 0.01 part of pigment and 115 parts of water. Wherein the rubber powder comprises 22 parts of agar, 15 parts of gellan gum and 1 part of carrageenan. The viscosity of the glue solution was 79.6 mpa.s. The preparation method is the same as in example 1.
10 batches of samples are selected and detected, the average pressure value of the explosion beads of the finished product is 15.58N, the average SD value is 1.85, and the average particle size is 3.12mm (middle beads).
Example 3
The novel cigarette explosion bead wall material comprises the following components in parts by weight: 3.5 parts of rubber powder, 0.01 part of preservative, 1 part of plasticizer, 0.02 part of pigment and 115 parts of water. Wherein the rubber powder comprises 25 parts of agar, 15 parts of gellan gum and 3 parts of carrageenan. The viscosity of the glue solution is 200 mpa.s. The preparation method is the same as in example 1.
10 batches of samples are selected and detected, the pressure average value of the explosion beads of the finished product is 16.01N, the SD value is 2.3 on average, and the particle size average value is 3.18mm (middle beads).
Example 4
The novel cigarette explosion bead wall material comprises the following components in parts by weight: 4.0 parts of rubber powder, 0.01 part of preservative, 1 part of plasticizer, 0.02 part of pigment and 115 parts of water. Wherein the composition of the gel powder is 23 parts of agar, 15 parts of gellan gum and 3 parts of carrageenan. The viscosity of the glue solution is 108 mpa.s. The preparation method is the same as in example 1.
10 batches of samples are selected and detected, the average pressure value of the explosion beads of the finished product is 15.09N, the average SD value is 2.50, and the average particle size is 3.12mm.
Comparative example 1
The wall material of the explosion bead for the cigarette comprises the following components in parts by weight: 10 parts of rubber powder, 0.5 part of preservative, 0.5 part of plasticizer, 0.5 part of embrittling agent and 88.5 parts of water. Wherein the rubber powder comprises 50 parts of agar, 20 parts of carrageenan, 20 parts of Arabic gum, 5 parts of hydroxypropyl starch and 5 parts of konjak gum.
The preparation method comprises the following steps: firstly, weighing rubber powder components according to parts by weight, and uniformly mixing to obtain rubber powder; then weighing 90% of chitosan and 10% of citric acid according to weight percentage, and uniformly mixing to obtain the embrittling agent; secondly, weighing 10 parts of the gel, 0.5 part of sodium dehydroacetate, 0.5 part of glycerol, 0.5 part of embrittling agent and 88.5 parts of water according to parts by weight, uniformly mixing, placing in a heating container, heating to 70 ℃ under the condition of continuous stirring, continuously preserving heat and stirring for 2 hours, and obtaining a mixed solution after the materials are fully dissolved; finally, filtering the mixed solution, removing bubbles through ultrasonic treatment, and preserving heat at 75 ℃ for later use, wherein the obtained liquid substance is the explosion bead wall material in the embodiment.
Comparative example 2
The wall material of the explosion bead for the cigarette comprises the following components in parts by weight: 5 parts of rubber powder, 0.1 part of preservative, 1 part of plasticizer, 0.9 part of embrittling agent and 93 parts of water. Wherein the rubber powder comprises 60 parts of agar, 10 parts of carrageenan, 10 parts of Arabic gum, 10 parts of hydroxypropyl starch and 10 parts of konjak gum.
The preparation method is the same as that of comparative example 1
Comparative example 3
The wall material of the explosion bead for the cigarette comprises the following components in parts by weight: 10 parts of rubber powder, 0.5 part of preservative, 0.5 part of plasticizer, 1 part of embrittling agent and 88 parts of water. Wherein the rubber powder comprises 40 parts of agar, 20 parts of carrageenan, 20 parts of Arabic gum, 10 parts of hydroxypropyl starch and 10 parts of konjak gum.
The preparation method is the same as that of comparative example 1
The final product and the control group of the explosive beads obtained in each example were stored in an open environment with humidity of 40%, 50%, 60%, 70%, 80% for 3 days, and then the moisture content in the explosive bead rubber was tested.
TABLE 1 moisture content of the beaded products in open Environment
| Humidity of the water | 40％ | 50％ | 60％ | 70％ | 80％ |
| Comparative example 1 | 0.72 | 0.86 | 0.98 | 1.15 | 1.29 |
| Comparative example 2 | 0.71 | 0.83 | 0.97 | 1.12 | 1.25 |
| Comparative example 3 | 0.65 | 0.79 | 0.94 | 1.09 | 1.27 |
| Example 1 | 0.62 | 0.74 | 0.89 | 1.04 | 1.20 |
| Example 2 | 0.60 | 0.71 | 0.87 | 1.03 | 1.18 |
| Example 3 | 0.70 | 0.84 | 0.96 | 1.10 | 1.24 |
| Example 4 | 0.68 | 0.81 | 0.94 | 1.08 | 1.22 |
Although the invention has been described herein with reference to the above-described illustrative embodiments thereof, the above-described embodiments are merely preferred embodiments of the present invention, and the embodiments of the present invention are not limited by the above-described embodiments, it should be understood that numerous other modifications and embodiments can be devised by those skilled in the art that will fall within the scope and spirit of the principles of this disclosure.
Claims (7)
1. The novel cigarette explosion bead wall material is characterized by comprising the following raw materials in parts by weight: 35-40 parts of rubber powder, 0.1-0.3 part of preservative, 5-10 parts of plasticizer, 0.1-0.3 part of pigment and 1150 parts of water;
the rubber powder consists of the following raw materials in parts by weight: 20-25 parts of agar, 10-15 parts of gellan gum,
1-3 parts of carrageenan.
2. The novel cigarette bead wall material according to claim 1, wherein the plasticizer is glycerin.
3. The novel cigarette bead wall material according to claim 1, wherein the preservative is sodium dehydroacetate.
4. The novel cigarette bead wall material according to claim 1, wherein the water is pure water, and the TDS is less than or equal to 10.
5. The preparation method of the novel cigarette bead-explosion wall material is characterized by comprising the following steps of: according to the weight portions, 35 to 40 portions of rubber powder, 0.1 to 0.3 portion of preservative, 5 to 10 portions of plasticizer and 0.1 to 0.3 portion of pigment are weighed, 1150 portions of water are added into a liquid preparation tank, the water is heated to 70 to 80 ℃, the plasticizer, the preservative and the pigment are sequentially added under the condition of continuous stirring, the rubber powder is added after stirring for 2 to 5 minutes, the liquid preparation tank is closed after the rubber powder is added, and stirring reaction is carried out for 80 to 100 minutes at 80+/-2 ℃.
6. The method for preparing a novel cigarette bead wall material according to claim 5, wherein the stirring frequency is 50HZ.
7. The preparation method of the novel cigarette bead wall material according to claim 5, wherein the rubber powder comprises the following raw materials in parts by weight: 20-25 parts of agar, 10-15 parts of gellan gum and 1-3 parts of carrageenan.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210467022.3A CN114617292B (en) | 2022-04-29 | 2022-04-29 | Novel bead-explosion wall material for cigarettes and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210467022.3A CN114617292B (en) | 2022-04-29 | 2022-04-29 | Novel bead-explosion wall material for cigarettes and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN114617292A CN114617292A (en) | 2022-06-14 |
| CN114617292B true CN114617292B (en) | 2024-02-06 |
Family
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Family Applications (1)
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| CN202210467022.3A Active CN114617292B (en) | 2022-04-29 | 2022-04-29 | Novel bead-explosion wall material for cigarettes and preparation method thereof |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110396225A (en) * | 2019-08-06 | 2019-11-01 | 河南金瑞香精香料有限公司 | A kind of quick-fried pearl wall material and preparation method thereof and dripping pill method |
| CN110897194A (en) * | 2019-11-15 | 2020-03-24 | 湖北中烟工业有限责任公司 | Bead blasting wall material for cigarettes and preparation method thereof |
| CN111289342A (en) * | 2020-03-20 | 2020-06-16 | 云南中烟工业有限责任公司 | Bead blasting wall material capable of regulating and controlling burst pressure and measuring method of burst pressure |
| CN111454490A (en) * | 2020-04-14 | 2020-07-28 | 中国科学院化学研究所 | Composition for preparing edible plant plasma membrane and application thereof |
| CN112574475A (en) * | 2020-12-22 | 2021-03-30 | 武汉市昱宸峰科技有限公司 | Brittle wall material for cigarette blasting bead |
| WO2021143150A1 (en) * | 2020-01-13 | 2021-07-22 | 云南南中科技有限公司 | Explosion bead for flavored cigarettes and preparation method therefor |
-
2022
- 2022-04-29 CN CN202210467022.3A patent/CN114617292B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110396225A (en) * | 2019-08-06 | 2019-11-01 | 河南金瑞香精香料有限公司 | A kind of quick-fried pearl wall material and preparation method thereof and dripping pill method |
| CN110897194A (en) * | 2019-11-15 | 2020-03-24 | 湖北中烟工业有限责任公司 | Bead blasting wall material for cigarettes and preparation method thereof |
| WO2021143150A1 (en) * | 2020-01-13 | 2021-07-22 | 云南南中科技有限公司 | Explosion bead for flavored cigarettes and preparation method therefor |
| CN111289342A (en) * | 2020-03-20 | 2020-06-16 | 云南中烟工业有限责任公司 | Bead blasting wall material capable of regulating and controlling burst pressure and measuring method of burst pressure |
| CN111454490A (en) * | 2020-04-14 | 2020-07-28 | 中国科学院化学研究所 | Composition for preparing edible plant plasma membrane and application thereof |
| CN112574475A (en) * | 2020-12-22 | 2021-03-30 | 武汉市昱宸峰科技有限公司 | Brittle wall material for cigarette blasting bead |
Non-Patent Citations (1)
| Title |
|---|
| 基于植物胶的爆珠壁材配方设计及其工艺优化;于浩;王艳梅;孙东亮;王志勇;袁霆;王琦琦;刘哲;李玉辉;;中国烟草学报;第26卷(第2期);全文 * |
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