CN112402297A - Semi-transparent cream-like cosmetic composition and preparation method thereof - Google Patents

Semi-transparent cream-like cosmetic composition and preparation method thereof Download PDF

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Publication number
CN112402297A
CN112402297A CN202011524369.4A CN202011524369A CN112402297A CN 112402297 A CN112402297 A CN 112402297A CN 202011524369 A CN202011524369 A CN 202011524369A CN 112402297 A CN112402297 A CN 112402297A
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Prior art keywords
parts
cosmetic composition
translucent
translucent cream
polydimethylsiloxane
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Inventor
张用伟
师国康
赵文轩
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Zhejiang Biyouti Cosmetics Co ltd
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Zhejiang Biyouti Cosmetics Co ltd
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Priority to CN202011524369.4A priority Critical patent/CN112402297A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • A61K8/894Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a polyoxyalkylene group, e.g. cetyl dimethicone copolyol
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/895Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/26Optical properties
    • A61K2800/262Transparent; Translucent
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/48Thickener, Thickening system
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Emergency Medicine (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a translucent cream-like cosmetic composition, which comprises a sun-screening agent and a thickening agent in parts by mass, wherein the sun-screening agent comprises 5-7.5 parts of ethylhexyl methoxycinnamate, 4-8 parts of homosalate, 2-6 parts of ethylhexyl salicylate, 2-6 parts of octocrylene and 1-3 parts of bis-ethylhexyloxyphenol methoxyphenyl triazine; the thickening agent comprises 1-2 parts of trihydroxystearin, 20-35 parts of PEG-10 polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and 10-20 parts of polydimethylsiloxane cross-linked polymer. The translucent sunscreen product is high in sunscreen index, light, thin and not greasy, has the effect of pre-makeup emulsion, and can well provide a makeup foundation for a subsequent makeup layer.

Description

Semi-transparent cream-like cosmetic composition and preparation method thereof
Technical Field
The invention relates to a cosmetic composition and a preparation method thereof, in particular to a translucent cream-shaped cosmetic composition and a preparation method thereof.
Background
At present, sun-screening and pre-makeup creams are widely used for the face, the sun-screening has the effect of protecting the skin from being damaged by ultraviolet rays, and the pre-makeup creams can make the makeup effect more appropriate and longer; the conventional application method is to sequentially use sunscreen cream, pre-make-up emulsion, foundation liquid and the like after basic skin care. Most sunscreens are affected by sunscreens, and are significantly greasy in both oil-in-water and water-in-oil formulations.
Moreover, the existing sunscreen creams are generally prepared by emulsification, and in order to obtain a good sunscreen effect, the sunscreen creams have a heavy feeling when used, are heavy in skin burden, and cannot replace pre-makeup creams.
Disclosure of Invention
The invention aims to provide a translucent cream-like cosmetic composition and a preparation method thereof. The product is a semitransparent sunscreen product with high sun protection index, is lighter, thinner and not greasy, has the effect of pre-makeup emulsion, and can well provide a makeup foundation for a subsequent makeup layer.
The technical scheme of the invention is as follows: a translucent cream-like cosmetic composition is characterized in that: the sunscreen agent comprises, by mass, 5-7.5 parts of ethylhexyl methoxycinnamate, 4-8 parts of homosalate, 2-6 parts of ethylhexyl salicylate, 2-6 parts of octocrylene and 1-3 parts of bis-ethylhexyloxyphenol methoxyphenyl triazine; the thickening agent comprises 1-2 parts of trihydroxystearin, 20-35 parts of PEG-10 polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and 10-20 parts of polydimethylsiloxane cross-linked polymer.
In order to provide the effects of lubrication, moisture retention, protection, gloss enhancement and the like for the skin, the translucent cream cosmetic composition also comprises 40-48 parts of an emollient, 0.2-1 part of a skin conditioner, 0.5-6 parts of an active ingredient and 0.1-2 parts of a preservative by mass.
In the aforementioned translucent cream cosmetic composition, the emollient includes isohexadecane, cyclopentadimethylsiloxane, isododecane, phenyl polytrimethylsiloxane, polydimethylsiloxane, and isononyl isononanoate. Its function is to provide lubrication and protection to the skin surface. The mass ratio of the isohexadecane, the cyclopentadecyldimethylsiloxane, the isododecane, the phenyl polytriethylsiloxane, the polydimethylsiloxane and the isononyl isononanoate is 1: 3: 3: 1: 2: 2.5.
in the translucent cream cosmetic composition, the skin conditioner comprises ethylhexyl glycerin and octyl glycol, and the mass ratio of the ethylhexyl glycerin to the octyl glycol is 1: 1. it has effects of moistening skin and helping antisepsis.
In the translucent cream cosmetic composition, the active ingredient is the white chingma seed oil, so that the skin can be moisturized and the luster of the skin can be increased.
In the translucent cream cosmetic composition, the preservative is glyceryl caprylate. It has the effects of inhibiting growth and reproduction of microorganism, and keeping stable property of cosmetic.
The preparation method of the translucent cream-like cosmetic composition comprises the following steps:
firstly, mixing and heating a sun-screening agent and a thickening agent, completely and uniformly mixing, and then cooling to room temperature to obtain a phase A;
② mixing the emollient, the skin conditioner, the thickening agent, the active ingredient and the preservative uniformly to obtain phase B.
And thirdly, putting the A phase product into the B phase, starting stirring, and homogenizing.
In the preparation method of the translucent cream-like cosmetic composition, in the step I, the heating temperature is 100-160 ℃, and the heating time is 5-10 min.
In the preparation method of the translucent cream-like cosmetic composition, in the third step, the stirring time is 2-5min, and the stirring speed is 2500-3500 rpm/min; the homogenization time is 1-2min, and the homogenization speed is 1000-1200 rpm/min.
Compared with the prior art, several types of sunscreens are screened out and combined and are compatible with thickeners such as screened trihydroxystearin, PEG-10 polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and the like, so that a semitransparent cream system, namely semitransparent protective cream, can be formed, and the protective cream belongs to a pure oil system and has sunscreen and pre-makeup effects. The product has semitransparent appearance, can be prepared without emulsification, has small skin burden, is light and thin without oily feeling after being used, can cover and decorate the defects of uneven skin color, pores and darkness on the skin, and improves the water-moist glossiness of the skin, thereby realizing the effect of pre-makeup emulsion. The cosmetic composition disclosed by the invention is high in sun-screening index, good in stability, not easy to produce oil, moderate in viscosity, lighter in skin feel and not easy to rub mud.
Detailed Description
The present invention is further illustrated by the following examples, which are not to be construed as limiting the invention.
Examples are given. A translucent cream-like cosmetic composition comprises a sun-screening agent and a thickening agent according to parts by mass, wherein the sun-screening agent comprises 5-7.5 parts of ethylhexyl methoxycinnamate, 4-8 parts of homosalate, 2-6 parts of ethylhexyl salicylate, 2-6 parts of octocrylene and 1-3 parts of bis-ethylhexyloxyphenol methoxyphenyl triazine; the thickening agent comprises 1-2 parts of trihydroxystearin, 20-35 parts of PEG-10 polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and 10-20 parts of polydimethylsiloxane cross-linked polymer. Also comprises 40 to 48 portions of emollient, 0.2 to 1 portion of skin conditioner, 0.5 to 6 portions of active ingredients and 0.1 to 2 portions of preservative. The emollient comprises 1: 3: 3: 1: 2: 2.5 of isohexadecane, cyclopentadimethylsiloxane, isododecane, phenyl polytriethylsiloxane, polydimethylsiloxane and isononyl isononanoate. The skin conditioner comprises 1:1 parts of ethylhexyl glycerin and parts of octyl glycol. The active ingredient is white Potentilla chinensis seed oil. The preservative is glyceryl caprylate.
The preparation method of the translucent cream cosmetic composition comprises the following steps:
firstly, mixing and heating a sun-screening agent and a thickening agent, completely and uniformly mixing, and then cooling to room temperature to obtain a phase A; the heating temperature is 100-160 ℃, and the heating time is 5-10 min.
② mixing the emollient, the skin conditioner, the thickening agent, the active ingredient and the preservative uniformly to obtain phase B.
And thirdly, putting the A phase product into the B phase, starting stirring, and homogenizing. The stirring time is 2-5min, and the stirring speed is 2500-; the homogenization time is 1-2min, and the homogenization speed is 1000-1200 rpm/min.
Examples of the experiments. A group of formulas in the formula range is selected to prepare an experimental example. And the amount of sunscreen (octocrylene) in the experimental examples was adjusted to give comparative examples 1 and 2; in addition, based on the experimental examples, two different sunscreens (butyl methoxydibenzoylmethane and 4-methylbenzylidenecamphor) were added to give comparative examples 3 and 4, respectively. The details are shown in the following table.
Figure BDA0002850353050000041
The viscosity test and the stability test were performed for the experimental examples and 4 comparative examples, and the test results are shown in the following table.
Figure BDA0002850353050000042
Figure BDA0002850353050000051
As can be seen from the table, in comparison with comparative examples 1 and 2, in comparative examples 1 and 2, the viscosity coefficient is greatly reduced by only slightly increasing the amount of one ingredient in the sunscreen agent, which indicates that the viscosity of the viscosity system is greatly influenced by the amount of the sunscreen agent; comparative examples 3 and 4 are where the addition of additional sunscreen agents, with the total amount of sunscreen agent being unchanged, also resulted in a substantial reduction in the viscosity of the system. Furthermore, comparative examples 1 to 4 all gave very rapid oil development after standing and very poor stability, whereas the viscosity dropped within a small range after one day of standing at various temperatures in the present experimental example. The types and compatibility relationship of the sunscreen agent and the thickening agent are obtained through repeated research, experiments and summarization, and the sunscreen agent and the thickening agent can ensure better stability under the condition of having enough high viscosity, so that the sunscreen agent and the thickening agent are not easy to produce oil when in use, and the skin feel is lighter and thinner.
The sun protection index of the experimental example is tested, and the sun protection index is as high as 24.6, which is enough for the sun protection requirement of the sun protection product.
In addition, the experimental examples of the invention are used and tested, and compared with the common makeup pre-emulsion, the cosmetic cream has a better function of hiding pores, is beneficial to makeup and has certain sun-screening capability. Compared with common oily sun block, the skin feel is lighter, and the mud rubbing phenomenon can not occur after the sun block is used for a period of time.

Claims (9)

1. A translucent cream cosmetic composition characterized by: the sunscreen agent comprises, by mass, 5-7.5 parts of ethylhexyl methoxycinnamate, 4-8 parts of homosalate, 2-6 parts of ethylhexyl salicylate, 2-6 parts of octocrylene and 1-3 parts of bis-ethylhexyloxyphenol methoxyphenyl triazine; the thickening agent comprises 1-2 parts of trihydroxystearin, 20-35 parts of PEG-10 polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and 10-20 parts of polydimethylsiloxane cross-linked polymer.
2. The translucent cream cosmetic composition of claim 1, wherein: the skin care product also comprises 40-48 parts of an emollient, 0.2-1 part of a skin conditioner, 25-40 parts of a suspension thickening agent, 0.5-6 parts of an active ingredient and 0.1-2 parts of a preservative by mass.
3. The translucent cream cosmetic composition of claim 2, wherein: the emollient includes isohexadecane, cyclopentadecyldimethicone, isododecane, phenyl polytrimethylsiloxane, dimethicone, and isononyl isononanoate; the mass ratio of the isohexadecane, the cyclopentadecyldimethylsiloxane, the isododecane, the phenyl polytriethylsiloxane, the polydimethylsiloxane and the isononyl isononanoate is 1: 3: 3: 1: 2: 2.5.
4. the translucent cream cosmetic composition of claim 2, wherein: the skin conditioner comprises ethylhexyl glycerin and octyl glycol, wherein the mass ratio of the ethylhexyl glycerin to the octyl glycol is 1: 1.
5. the translucent cream cosmetic composition of claim 2, wherein: the active ingredient is white Potentilla chinensis seed oil.
6. The translucent cream cosmetic composition of claim 2, wherein: the preservative is glyceryl caprylate.
7. Process for the preparation of a cosmetic composition in the form of a translucent cream according to any one of claims 2 to 6, characterized in that it comprises the following steps:
firstly, mixing and heating a sun-screening agent and a thickening agent, completely and uniformly mixing, and then cooling to room temperature to obtain a phase A;
② mixing the emollient, the skin conditioner, the active ingredient and the preservative evenly to obtain phase B.
And thirdly, putting the A phase product into the B phase, starting stirring, and homogenizing.
8. A process for the preparation of a cosmetic translucent cream composition according to claim 7, characterized in that: in the step I, the heating temperature is 100-160 ℃, and the heating time is 5-10 min.
9. A process for the preparation of a cosmetic translucent cream composition according to claim 7, characterized in that: in the third step, the stirring time is 2-5min, and the stirring speed is 2500 plus 3500 rpm/min; the homogenization time is 1-2min, and the homogenization speed is 1000-1200 rpm/min.
CN202011524369.4A 2020-12-22 2020-12-22 Semi-transparent cream-like cosmetic composition and preparation method thereof Pending CN112402297A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116942548A (en) * 2023-07-28 2023-10-27 上海绵花棠生物科技有限公司 Multifunctional cosmetic cream and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103037832A (en) * 2010-02-12 2013-04-10 拜尔斯道夫股份有限公司 Cosmetic preparation containing acyl arginine ester component
CN108464948A (en) * 2018-04-29 2018-08-31 佛山云裳化妆品有限公司 A kind of high spf value suncream of double gel rubber systems
CN110279605A (en) * 2019-07-29 2019-09-27 西安博和医疗科技有限公司 Sunscreen composition

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103037832A (en) * 2010-02-12 2013-04-10 拜尔斯道夫股份有限公司 Cosmetic preparation containing acyl arginine ester component
CN108464948A (en) * 2018-04-29 2018-08-31 佛山云裳化妆品有限公司 A kind of high spf value suncream of double gel rubber systems
CN110279605A (en) * 2019-07-29 2019-09-27 西安博和医疗科技有限公司 Sunscreen composition

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116942548A (en) * 2023-07-28 2023-10-27 上海绵花棠生物科技有限公司 Multifunctional cosmetic cream and preparation method thereof

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