CN116942548A - Multifunctional cosmetic cream and preparation method thereof - Google Patents
Multifunctional cosmetic cream and preparation method thereof Download PDFInfo
- Publication number
- CN116942548A CN116942548A CN202310940907.5A CN202310940907A CN116942548A CN 116942548 A CN116942548 A CN 116942548A CN 202310940907 A CN202310940907 A CN 202310940907A CN 116942548 A CN116942548 A CN 116942548A
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- parts
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- cosmetic cream
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- multifunctional cosmetic
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- 239000008278 cosmetic cream Substances 0.000 title claims abstract description 124
- 238000002360 preparation method Methods 0.000 title abstract description 11
- 239000000516 sunscreening agent Substances 0.000 claims abstract description 65
- 239000000843 powder Substances 0.000 claims abstract description 62
- 239000002994 raw material Substances 0.000 claims abstract description 43
- 239000000126 substance Substances 0.000 claims abstract description 36
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 35
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 25
- 230000037072 sun protection Effects 0.000 claims abstract description 24
- 239000004519 grease Substances 0.000 claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000000839 emulsion Substances 0.000 claims abstract description 11
- 239000003906 humectant Substances 0.000 claims abstract description 10
- 239000003755 preservative agent Substances 0.000 claims abstract description 10
- 230000002335 preservative effect Effects 0.000 claims abstract description 10
- 239000003381 stabilizer Substances 0.000 claims abstract description 10
- 239000002562 thickening agent Substances 0.000 claims abstract description 10
- 239000003607 modifier Substances 0.000 claims abstract description 7
- -1 polydimethylsiloxane Polymers 0.000 claims description 67
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 64
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 64
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 64
- 238000002156 mixing Methods 0.000 claims description 30
- 239000007788 liquid Substances 0.000 claims description 28
- 239000000047 product Substances 0.000 claims description 27
- 239000000341 volatile oil Substances 0.000 claims description 27
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 18
- 238000012216 screening Methods 0.000 claims description 18
- GTJOHISYCKPIMT-UHFFFAOYSA-N 2-methylundecane Chemical compound CCCCCCCCCC(C)C GTJOHISYCKPIMT-UHFFFAOYSA-N 0.000 claims description 16
- SGVYKUFIHHTIFL-UHFFFAOYSA-N Isobutylhexyl Natural products CCCCCCCC(C)C SGVYKUFIHHTIFL-UHFFFAOYSA-N 0.000 claims description 16
- VKPSKYDESGTTFR-UHFFFAOYSA-N isododecane Natural products CC(C)(C)CC(C)CC(C)(C)C VKPSKYDESGTTFR-UHFFFAOYSA-N 0.000 claims description 16
- 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 14
- YBGZDTIWKVFICR-JLHYYAGUSA-N Octyl 4-methoxycinnamic acid Chemical compound CCCCC(CC)COC(=O)\C=C\C1=CC=C(OC)C=C1 YBGZDTIWKVFICR-JLHYYAGUSA-N 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 13
- YZUUTMGDONTGTN-UHFFFAOYSA-N nonaethylene glycol Chemical compound OCCOCCOCCOCCOCCOCCOCCOCCOCCO YZUUTMGDONTGTN-UHFFFAOYSA-N 0.000 claims description 13
- 229960001679 octinoxate Drugs 0.000 claims description 13
- FMRHJJZUHUTGKE-UHFFFAOYSA-N Ethylhexyl salicylate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1O FMRHJJZUHUTGKE-UHFFFAOYSA-N 0.000 claims description 12
- 229940068171 ethyl hexyl salicylate Drugs 0.000 claims description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 9
- 239000003921 oil Substances 0.000 claims description 9
- 239000013067 intermediate product Substances 0.000 claims description 8
- SHZIWNPUGXLXDT-UHFFFAOYSA-N caproic acid ethyl ester Natural products CCCCCC(=O)OCC SHZIWNPUGXLXDT-UHFFFAOYSA-N 0.000 claims description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- 229920001577 copolymer Polymers 0.000 claims description 6
- 229920002545 silicone oil Polymers 0.000 claims description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 4
- 150000002148 esters Chemical class 0.000 claims description 4
- 230000003472 neutralizing effect Effects 0.000 claims description 4
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 3
- ANZUDYZHSVGBRF-UHFFFAOYSA-N 3-ethylnonane-1,2,3-triol Chemical compound CCCCCCC(O)(CC)C(O)CO ANZUDYZHSVGBRF-UHFFFAOYSA-N 0.000 claims description 3
- PFHLGILELJGQSJ-UHFFFAOYSA-N 4-(2h-benzotriazol-4-ylmethyl)-2h-benzotriazole;2-butyl-3,4,5,6-tetramethylphenol Chemical compound CCCCC1=C(C)C(C)=C(C)C(C)=C1O.C=1C=CC=2NN=NC=2C=1CC1=CC=CC2=C1N=NN2 PFHLGILELJGQSJ-UHFFFAOYSA-N 0.000 claims description 3
- 229910002012 Aerosil® Inorganic materials 0.000 claims description 3
- CMBYOWLFQAFZCP-UHFFFAOYSA-N Hexyl dodecanoate Chemical compound CCCCCCCCCCCC(=O)OCCCCCC CMBYOWLFQAFZCP-UHFFFAOYSA-N 0.000 claims description 3
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 3
- CBTVGIZVANVGBH-UHFFFAOYSA-N aminomethyl propanol Chemical compound CC(C)(N)CO CBTVGIZVANVGBH-UHFFFAOYSA-N 0.000 claims description 3
- 239000000440 bentonite Substances 0.000 claims description 3
- 229910000278 bentonite Inorganic materials 0.000 claims description 3
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 3
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims description 3
- 229940008099 dimethicone Drugs 0.000 claims description 3
- PKPOVTYZGGYDIJ-UHFFFAOYSA-N dioctyl carbonate Chemical compound CCCCCCCCOC(=O)OCCCCCCCC PKPOVTYZGGYDIJ-UHFFFAOYSA-N 0.000 claims description 3
- UVCJGUGAGLDPAA-UHFFFAOYSA-N ensulizole Chemical compound N1C2=CC(S(=O)(=O)O)=CC=C2N=C1C1=CC=CC=C1 UVCJGUGAGLDPAA-UHFFFAOYSA-N 0.000 claims description 3
- 229960000655 ensulizole Drugs 0.000 claims description 3
- 235000011187 glycerol Nutrition 0.000 claims description 3
- 229940100463 hexyl laurate Drugs 0.000 claims description 3
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims description 3
- 235000019341 magnesium sulphate Nutrition 0.000 claims description 3
- 239000008204 material by function Substances 0.000 claims description 3
- 229960005323 phenoxyethanol Drugs 0.000 claims description 3
- 239000000377 silicon dioxide Substances 0.000 claims description 3
- 229920002379 silicone rubber Polymers 0.000 claims description 3
- 239000011780 sodium chloride Substances 0.000 claims description 3
- UUJLHYCIMQOUKC-UHFFFAOYSA-N trimethyl-[oxo(trimethylsilylperoxy)silyl]peroxysilane Chemical compound C[Si](C)(C)OO[Si](=O)OO[Si](C)(C)C UUJLHYCIMQOUKC-UHFFFAOYSA-N 0.000 claims description 3
- BYQPMKXSZDJZAW-UHFFFAOYSA-N 1-octanoyloxybutyl octanoate Chemical compound CCCCCCCC(=O)OC(CCC)OC(=O)CCCCCCC BYQPMKXSZDJZAW-UHFFFAOYSA-N 0.000 claims description 2
- UIVPNOBLHXUKDX-UHFFFAOYSA-N 3,5,5-trimethylhexyl 3,5,5-trimethylhexanoate Chemical compound CC(C)(C)CC(C)CCOC(=O)CC(C)CC(C)(C)C UIVPNOBLHXUKDX-UHFFFAOYSA-N 0.000 claims description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 2
- 239000007983 Tris buffer Substances 0.000 claims description 2
- DTPCFIHYWYONMD-UHFFFAOYSA-N decaethylene glycol Chemical compound OCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO DTPCFIHYWYONMD-UHFFFAOYSA-N 0.000 claims description 2
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 2
- 229940100554 isononyl isononanoate Drugs 0.000 claims description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 claims description 2
- GLZWNFNQMJAZGY-UHFFFAOYSA-N octaethylene glycol Chemical compound OCCOCCOCCOCCOCCOCCOCCOCCO GLZWNFNQMJAZGY-UHFFFAOYSA-N 0.000 claims description 2
- FMJSMJQBSVNSBF-UHFFFAOYSA-N octocrylene Chemical group C=1C=CC=CC=1C(=C(C#N)C(=O)OCC(CC)CCCC)C1=CC=CC=C1 FMJSMJQBSVNSBF-UHFFFAOYSA-N 0.000 claims description 2
- 229960000601 octocrylene Drugs 0.000 claims description 2
- UWJJYHHHVWZFEP-UHFFFAOYSA-N pentane-1,1-diol Chemical compound CCCCC(O)O UWJJYHHHVWZFEP-UHFFFAOYSA-N 0.000 claims description 2
- 229920003217 poly(methylsilsesquioxane) Polymers 0.000 claims description 2
- 229920001296 polysiloxane Polymers 0.000 claims description 2
- 239000011863 silicon-based powder Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 47
- 230000000475 sunscreen effect Effects 0.000 abstract description 23
- 238000005282 brightening Methods 0.000 abstract description 21
- 238000012360 testing method Methods 0.000 description 21
- 230000000875 corresponding effect Effects 0.000 description 11
- 230000000052 comparative effect Effects 0.000 description 9
- 239000002537 cosmetic Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- 230000009286 beneficial effect Effects 0.000 description 4
- 230000001815 facial effect Effects 0.000 description 4
- 239000006071 cream Substances 0.000 description 3
- 206010013786 Dry skin Diseases 0.000 description 2
- 230000037336 dry skin Effects 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 238000002203 pretreatment Methods 0.000 description 2
- 230000036555 skin type Effects 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 210000004243 sweat Anatomy 0.000 description 2
- 206010042496 Sunburn Diseases 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 229920006037 cross link polymer Polymers 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000007888 film coating Substances 0.000 description 1
- 238000009501 film coating Methods 0.000 description 1
- 230000003760 hair shine Effects 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 239000011858 nanopowder Substances 0.000 description 1
- OEIJHBUUFURJLI-UHFFFAOYSA-N octane-1,8-diol Chemical compound OCCCCCCCCO OEIJHBUUFURJLI-UHFFFAOYSA-N 0.000 description 1
- 229940061571 peg-9 dimethicone Drugs 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 229920003229 poly(methyl methacrylate) Polymers 0.000 description 1
- 239000004926 polymethyl methacrylate Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/894—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a polyoxyalkylene group, e.g. cetyl dimethicone copolyol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Inorganic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Dermatology (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The application relates to the technical field of cosmetic cream, and particularly discloses multifunctional cosmetic cream and a preparation method thereof. A multifunctional cosmetic cream is prepared from the following raw materials in parts by weight: 2.5-6.5 parts of emulsifying agent; 10-30 parts of volatile grease; 3-7 parts of moistening type grease; 2-12 parts of oily chemical sun-screening agent; 3-7 parts of skin feel modifier; 1-6 parts of film forming agent; 1-5 parts of functional raw materials; 0.1-2 parts of thickener; 3-8 parts of toner; 5-20 parts of sun-proof powder; 2-10 parts of humectant; 0.5-2 parts of emulsion stabilizer; 0.1-1 part of preservative; 2-8 parts of an aqueous sun-screening agent; 0.1-1 part of neutralizer; 20-30 parts of water; the color and sunscreen powders are pre-treated prior to use in the preparation of multifunctional cosmetic creams. The multifunctional cosmetic cream provided by the application belongs to a three-in-one product, has excellent compatibility in combination of sun protection, pre-makeup and corresponding brightening effects, is convenient to apply, does not generate a mud rubbing phenomenon that multiple products are sequentially applied, and has excellent consumer experience.
Description
Technical Field
The application relates to the technical field of cosmetic cream, in particular to multifunctional cosmetic cream and a preparation method thereof.
Background
With the pursuit of beauty, cosmetics are more and more kinds, and cosmetic creams are one of products with higher use frequency, and are mainly an emulsion composed of oil, fat, wax, water, emulsifying agent and the like.
Aiming at cosmetic cream, different types of products such as sun protection, pre-make-up, brightening and the like exist at present, and different products have different characteristics. Conventionally, sun protection products have high requirements on sun protection index, and require the addition of a relatively large amount of nanopowder; for the pre-makeup product, the product is used for helping the subsequent dressing to be applied; the effect of lightening and evening the skin color is mainly focused on lightening the product. Because of the differences between the sun protection product, the pre-make-up product, and the lightening product, consumers typically apply the sun protection product first, then the pre-make-up product, and then the lightening product.
For the above related art, the inventors consider that the application of three products, namely sun protection, pre-makeup and brightening, is complicated, and requires a lot of time to make up, and when the products are used one by one, a mud rubbing phenomenon is generated in the process of making up and stacking, so that the consumer experience is seriously affected, and therefore, a scheme is needed to solve the above technical problems.
Disclosure of Invention
In order to simultaneously meet the effect requirements of sun protection, pre-make-up and brightening cosmetic cream and overcome the defects of practical application of three products, and further improve consumer experience, the application provides multifunctional cosmetic cream and a preparation method thereof.
In a first aspect, the application provides a multifunctional cosmetic cream, which adopts the following technical scheme:
a multifunctional cosmetic cream is prepared from the following raw materials in parts by weight:
2.5-6.5 parts of emulsifying agent;
10-30 parts of volatile grease;
3-7 parts of moistening type grease;
2-12 parts of oily chemical sun-screening agent;
3-7 parts of skin feel modifier;
1-6 parts of film forming agent;
1-5 parts of functional raw materials;
0.1-2 parts of thickener;
3-8 parts of toner;
5-20 parts of sun-proof powder;
2-10 parts of humectant;
0.5-2 parts of emulsion stabilizer;
0.1-1 part of preservative;
2-8 parts of an aqueous sun-screening agent;
0.1-1 part of neutralizer;
20-30 parts of water;
the toner is subjected to pretreatment before being used for preparing multifunctional cosmetic cream, and specifically comprises the following steps:
uniformly mixing 1.5-3.5% of film forming agent and volatile oil with the same amount to obtain a treatment liquid A, uniformly mixing the toner and the treatment liquid A, and baking at 80-130 ℃ for 1-3 hours to obtain the toner;
the sun protection powder is subjected to pretreatment before being used for preparing multifunctional cosmetic cream, and specifically comprises the following steps:
taking 2.5-3.5% of oily chemical sun-screening agent by weight, adding 40-60% of volatile oil by weight of the oily chemical sun-screening agent, uniformly mixing to obtain a treatment liquid B, uniformly mixing sun-screening powder and the treatment liquid B, and baking at 80-100 ℃ for 1-2h to obtain the finished product.
By adopting the technical scheme, the multifunctional cosmetic cream can achieve the effects of sun protection, pre-make-up and brightening three corresponding products, can be used as sun protection cream for blocking ultraviolet rays, can be used as pre-make-up cream for helping follow-up dressing and pasting, can be used as brightening cream, realizes three-in-one, and has the advantages that only one make-up is needed in the application process, the time is less, and excellent consumer experience is realized.
In order to realize the combination of three different effects and exert excellent effects, the pretreatment of the toner is carried out before the toner is used for preparing the multifunctional cosmetic cream, and compared with the simple addition and mixing of the raw materials, the pretreatment toner has excellent covering and brightening effects, and has more excellent skin pasting property and durability; the sunscreen powder is subjected to pretreatment before being used for preparing multifunctional cosmetic cream, compared with the simple addition and mixing of the raw materials, the problem that pores are blocked by the sunscreen powder can be avoided to the greatest extent, the skin-friendly performance is better, and the sunscreen powder has excellent sunscreen capability. Meanwhile, the pretreatment toner and the pretreatment sun screen can show excellent compatibility and combination property when being mixed with other residual raw materials in the follow-up process, and further show excellent compatibility in combination of corresponding effects of sun screen, pre-makeup and brightening, so that the obtained multifunctional cosmetic cream has excellent application quality.
Preferably, the toner is composed of Ti-02 SG, YP-75SG, RP-29SG and BP-50SG, and the weight ratio of Ti-02 SG, YP-75SG, RP-29SG and BP-50SG is (45-55): (6-9): (1-2): 1.
Through adopting above-mentioned technical scheme, the toner that above-mentioned kind of raw materials was constituteed according to specific proportion scope, and it can overcome self reunion, blue light and the whitening problem through mutual complementation, and skin pasting nature and affinity are better in the application, can keep lasting stable nature in the makeup process, and then have excellent effect that shines, even complexion to have excellent compatibility with preventing sunburn powder, be favorable to guaranteeing the performance of the trinity efficiency of multi-functional cosmetic cream.
Preferably, the sun protection powder consists of Ti-Si1000 and ZN-AS 6800, and the weight ratio of the Ti-Si1000 to the ZN-AS 6800 is 1 (1.2-1.8).
By adopting the technical scheme, the sun-proof powder composed of the Ti-Si1000 and the ZN-AS 6800 according to the specific proportion range can achieve the sun-proof purpose by reflecting, scattering and absorbing part of ultraviolet rays, has excellent stable sun-proof performance and excellent compatibility with toner, and is beneficial to ensuring the exertion of the three-in-one effect of multifunctional cosmetic cream.
Preferably, the film forming agent is one or more of acrylic acid (ester) copolymer/polydimethylsiloxane, trimethylsiloxysilicate, acrylic acid (ester) copolymer/polydimethylsiloxane methacrylate copolymer and polymethylsilsesquioxane;
the volatile oil is one or a combination of a plurality of cyclopentadimethicone, isododecane, methyl trimethyl silicone and dimethicone;
the oily chemical sun-screening agent is one or a combination of more of ethylhexyl methoxycinnamate, octocrylene, ethylhexyl salicylate and polysiloxane-15.
By adopting the technical scheme, the film forming agent of the type can stably act on the surface of the toner in the pretreatment of the toner, fully act in the subsequent mixing of the raw materials of the components, and exert excellent film forming effect; the volatile oil of the type can not only make skin feel more water and fresh, but also assist the film forming agent and the oily chemical sun screening agent to fully play roles; the oily chemical sun-screening agent can stably act on the surface of sun-screening powder in pretreatment of the sun-screening powder, fully act in the subsequent mixing of the raw materials of the components and play an excellent sun-screening effect.
Preferably, the volatile oil consists of cyclopentadimethicone and isododecane, and the weight ratio of the cyclopentadimethicone to the isododecane is (2.5-3.5): 1.
By adopting the technical scheme, the cyclopentadimethicone has excellent smoothness and smoothness, can form a layer of smooth and slippery film on the surface of the skin, and is beneficial to improving the texture of the skin and enhancing the glossiness and softness of the skin; the isododecane has strong volatility and is beneficial to enhancing the film coating feel and the refreshing feel of the product; when the volatile grease is formed by the cyclopentadimethicone and the isododecane according to the proportion, the excellent effects are exerted, and besides the excellent effects, the film forming agent and the oily chemical sunscreen agent can be matched to better act on the surfaces of the toner and the sun screen respectively, so that the obtained multifunctional cosmetic cream shows excellent compatibility in sun protection, pre-make-up and brightening, and the corresponding effects are also excellent.
Preferably, the oily chemical sun-screening agent consists of ethylhexyl methoxycinnamate, polysiloxane-15 and ethylhexyl salicylate, and the weight ratio of the ethylhexyl methoxycinnamate, the polysiloxane-15 and the ethylhexyl salicylate is (1.6-2.4): (0.8-1.2): 1.
By adopting the technical scheme, the oily flower Xie Fangshai agent prepared from the raw materials in a specific weight ratio range can fully act on the surface of the sun-screening powder in the pretreatment process of the sun-screening powder, can be stably matched with other component raw materials in the subsequent process, shows excellent skin adhesion, further enables the multifunctional cosmetic cream to show excellent sun-screening effect, and can give consideration to excellent exertion of corresponding effects of pre-dressing and brightening.
Preferably, the emulsifier consists of a silicone oil emulsifier and a grease emulsifier, and the weight ratio of the silicone oil emulsifier to the grease emulsifier is 1 (2-4);
the silicone oil emulsifier is one or a combination of more of PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane, PEG/PPG-18/18 polydimethylsiloxane and PEG-10 polydimethylsiloxane;
the oil emulsifier is one or more of lauryl polyglycerol-3 polydimethylsiloxane ethyl polydimethylsiloxane, cetyl PEG/PPG-10/1 polydimethylsiloxane, lauryl PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane and lauryl PEG-10 tris (trimethylsiloxy) silyl ethyl polydimethylsiloxane.
Through adopting above-mentioned technical scheme, above-mentioned two types of emulsifiers can play excellent dispersion and equilibrium effect to each component raw materials when mutually supporting to make whole mixed system keep excellent stability, especially to the cooperation between preliminary treatment back toner, sun-proof powder and other component raw materials, play excellent supplementary cooperation effect, and then guarantee that multi-functional cosmetic cream can exert excellent sun-proof, make up the preceding and the corresponding efficiency of brightening, improve consumer's good experience through trinity.
Preferably, the emulsifier consists of PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane and cetyl PEG/PPG-10/1 polydimethylsiloxane in a weight ratio of 1:3.
By adopting the technical scheme, the PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane and cetyl PEG/PPG-10/1 polydimethylsiloxane in the weight ratio have excellent mutual matching effect, so that the emulsifier is required for the corresponding effects of sun protection, pre-make-up and brightening, the auxiliary compatibility is outstanding, and the obtained multifunctional cosmetic cream has better quality.
Preferably, the moistening grease is one or a combination of more of dioctyl carbonate, cetyl ethyl caproate, hexyl laurate, neopentyl glycol di (ethyl caproate), isononyl isononanoate and butanediol dicaprylate/dicaprate;
the functional raw material is one or a combination of more of silicon elastomer, silica and organic silicon powder;
the thickener is one or a combination of a plurality of bentonite and aerosil;
the humectant is one or more of glycerin, butanediol, propylene glycol and pentanediol;
the emulsion stabilizer is one or a combination of a plurality of sodium chloride and magnesium sulfate;
the preservative is one or a combination of more of phenoxyethanol, octaethylene glycol and ethylhexyl glycerol;
the water-based sun-screening agent is one or a combination of more of phenylbenzimidazole sulfonic acid and methylene bis-benzotriazole tetramethylbutylphenol;
the neutralizing agent is one or a combination of more of aminomethyl propanol, sodium hydroxide and triethanolamine.
Through adopting above-mentioned technical scheme, above-mentioned kind of raw materials are all applicable to multi-functional cosmetic cream, and the dispersibility and the cohesiveness of each other are preferred to can fully volatilize self effect in mixed system, and then guarantee that the multi-functional cosmetic cream that obtains has stable excellent quality.
In a second aspect, the application provides a preparation method of multifunctional cosmetic cream, which adopts the following technical scheme:
a preparation method of multifunctional cosmetic cream comprises the following steps:
(1) Preparing raw materials comprising A phase, B phase, C phase, D phase, E phase and F phase according to a proportion, wherein the A phase comprises an emulsifier, a film forming agent, volatile grease, an oily chemical sunscreen agent, a skin feel modifier and moist grease; phase B includes a thickener; phase C includes toner; phase D comprises sun-proof powder; the E phase comprises water, a humectant, an emulsion stabilizer, an aqueous sun-screening agent, a preservative and a neutralizer; phase F includes functional materials;
(2) Uniformly mixing 1.5-3.5% of film forming agent and volatile oil with the same amount to obtain a treatment liquid A, uniformly mixing C-phase toner and the treatment liquid A, and baking at 80-130 ℃ for 1-3 hours to obtain pretreated toner; taking 2.5-3.5% by weight of oily chemical sun-screening agent, adding 40-60% by weight of volatile oil of the oily chemical sun-screening agent, uniformly mixing to obtain treatment liquid B, uniformly mixing D-phase sun-screening powder and the treatment liquid B, and baking at 80-100 ℃ for 1-2h to obtain pretreatment sun-screening powder;
(3) Uniformly mixing the other raw materials except the raw materials used in the step (2), adding the raw materials of the phase B and the phase F, uniformly dispersing, then homogenizing, continuously adding pretreatment toner for homogenizing, and then adding pretreatment sun-proof powder for homogenizing to obtain an intermediate product; (4) And (3) after uniformly mixing the raw materials in the E phase, adding the mixture into the intermediate product obtained in the step (3), continuously homogenizing in the process, and continuously homogenizing after the addition is finished, thus obtaining the multifunctional cosmetic cream.
By adopting the technical scheme, the preparation method is simple to operate and convenient for large-scale production, after pretreatment toner and pretreatment sun powder are obtained, the pretreatment toner and the pretreatment sun powder are mixed with the mixture of the residual A phase, B phase and F phase to obtain a uniform oil phase intermediate product, and the water phase obtained after the raw materials in the E phase are mixed is added into the intermediate product, so that the multifunctional cosmetic cream with excellent and stable quality can be obtained.
In summary, the application has the following beneficial effects:
1. because the application carries out pretreatment on the toner and the sun-proof powder before being used for preparing the multifunctional cosmetic cream, the toner and the sun-proof powder can show excellent compatibility and combination with each other when being mixed with other residual raw materials in the subsequent period, and can show excellent compatibility in combination of corresponding effects of sun protection, pre-makeup and brightening; the multifunctional cosmetic cream belongs to a three-in-one product, is convenient to apply, does not generate the mud rubbing phenomenon that a plurality of products are sequentially applied, and has excellent consumer experience;
2. when the cyclopentadimethicone and isododecane are formed into volatile grease according to a specific proportion range, the volatile grease can be matched with a film forming agent and an oily chemical sun screening agent to better act on the surfaces of the toner and the sun screening powder respectively, so that the obtained multifunctional cosmetic cream shows better compatibility in sun screening, pre-make-up and brightening, and the corresponding efficacy is exerted more prominently;
3. the emulsifier composed of PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane and cetyl PEG/PPG-10/1 polydimethylsiloxane according to a specific proportion range is adopted, so that excellent dispersing and balancing effects can be achieved on raw materials of each component, auxiliary compatibility is outstanding, and the multifunctional cosmetic cream can be ensured to exert excellent corresponding effects of sun protection, pre-make-up and brightening.
Detailed Description
The present application will be described in further detail with reference to examples.
The raw materials used in the preparation examples and examples of the present application are all commercially available except for the specific descriptions: ti-02 SG, YP-75SG, RP-29SG, BP-50SG, ti-Si1000 and ZN-AS 6300 were purchased from Shanghai Korotkoku Biotech Co.
Examples
Example 1
The multifunctional cosmetic cream is prepared from the following raw materials in parts by weight as shown in table 1:
(1) Preparing raw materials comprising A phase, B phase, C phase, D phase, E phase and F phase according to a proportion, wherein the A phase comprises an emulsifier, a film forming agent, volatile grease, an oily chemical sunscreen agent, a skin feel modifier and moist grease; phase B includes a thickener; phase C includes toner; phase D comprises sun-proof powder; the E phase comprises water, a humectant, an emulsion stabilizer, an aqueous sun-screening agent, a preservative and a neutralizer; phase F includes functional materials;
(2) Uniformly mixing 2.5% by weight of film forming agent and the same amount of volatile oil to obtain a treatment liquid A, uniformly mixing C-phase toner and the treatment liquid A, and baking at 105 ℃ for 2 hours to obtain pretreated toner; adding 3% by weight of oily chemical sun-screening agent, adding 50% by weight of volatile oil of the oily chemical sun-screening agent, uniformly mixing to obtain a treatment liquid B, uniformly mixing D-phase sun-screening powder and the treatment liquid B, and baking at 90 ℃ for 1.5 hours to obtain pretreatment sun-screening powder;
(3) Uniformly mixing the other raw materials except the raw materials used in the step (2) in the phase A, stirring for 3min at 500rpm, adding the raw materials of the phase B and the phase F, uniformly dispersing, stirring for 2min at 500rpm, homogenizing for 3min at 5000rpm, continuously adding pretreated toner for homogenizing for 3min at 5000rpm, adding pretreated sun-proof powder for homogenizing, and homogenizing for 2min at 6000rpm to obtain an intermediate product;
(4) And (3) after uniformly mixing the raw materials in the E phase, adding the mixture into the intermediate product obtained in the step (3), continuously homogenizing at 5000rpm in the process after 3min dropwise addition, and continuously homogenizing at 6000rpm for 3min after addition, thereby obtaining the multifunctional cosmetic cream.
Note that: in the above steps, the toner consists of Ti-02 SG, YP-75SG, RP-29SG and BP-50 SG; the sun protection powder consists of Ti-Si1000 and ZN-AS 6800; the oily chemical sun-screening agent consists of ethylhexyl methoxycinnamate, polysiloxane-15 and ethylhexyl salicylate; the volatile oil consists of cyclopentadimethicone and isododecane; the emulsifier consists of PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane and cetyl PEG/PPG-10/1 polydimethylsiloxane; the film forming agent is trimethylsiloxysilicate; the functional raw material is silica; the thickener is bentonite; the humectant is butanediol; the emulsion stabilizer is sodium chloride; the preservative consists of phenoxyethanol and octanediol; the water-based sun-screening agent is phenylbenzimidazole sulfonic acid; the neutralizing agent is triethanolamine; the skin feel modifier is polydimethylsiloxane/vinyl polydimethylsiloxane crosslinked polymer; the moistening oil is cetyl ethyl caproate.
Examples 2 to 4
A multifunctional cosmetic cream is different from example 1 in that the raw materials of each component and the corresponding weights thereof are shown in Table 1.
Table 1 raw materials for each component in examples 1 to 3 and parts by weight (kg/part)
Example 5
A multifunctional cosmetic cream is different from example 1 in that 1.5% by weight of a film forming agent and an equivalent amount of volatile oil are uniformly mixed to obtain a treatment liquid A, and a C-phase toner and the treatment liquid A are uniformly mixed and baked at 130 ℃ for 1 hour to obtain a pretreatment toner.
Example 6
A multifunctional cosmetic cream is different from example 1 in that 3.5% by weight of a film forming agent and an equivalent amount of volatile oil are uniformly mixed to obtain a treatment liquid A, and a C-phase toner and the treatment liquid A are uniformly mixed and baked for 3 hours at 80-DEG C to obtain a pretreatment toner.
Example 7
A multifunctional cosmetic cream is different from example 1 in that 2.5% by weight of oily chemical sunscreen agent is taken, 40% by weight of volatile oil of the oily chemical sunscreen agent is added and mixed uniformly to obtain treatment liquid B, D-phase sunscreen powder and treatment liquid B are mixed uniformly, and the pretreatment sunscreen powder is obtained after baking at 100 ℃ for 1 h.
Example 8
A multifunctional cosmetic cream is different from example 1 in that 3.5% by weight of oily chemical sunscreen agent is taken, 60% by weight of volatile oil of the oily chemical sunscreen agent is added and mixed uniformly to obtain treatment liquid B, D-phase sunscreen powder and treatment liquid B are mixed uniformly, and the pretreatment sunscreen powder is obtained after baking at 80 ℃ for 2 hours.
Example 9
A multifunctional cosmetic cream differs from example 1 in that the total weight of the toner is unchanged, and the weight ratio of Ti-02 SG, YP-75SG, RP-29SG and BP-50SG is adjusted to 45:6:1:1.
Example 10
A multifunctional cosmetic cream differs from example 1 in that the total weight of the toner is unchanged, and the weight ratio of Ti-02 SG, YP-75SG, RP-29SG and BP-50SG is adjusted to 55:9:2:1.
Example 11
A multifunctional cosmetic cream is different from example 1 in that the total weight of the toner is unchanged, and the multifunctional cosmetic cream consists of Ti-02 SG and YP-75SG in a weight ratio of 50:7.5.
Example 12
A multifunctional cosmetic cream is different from example 1 in that the total weight of the toner is unchanged, and the cosmetic cream consists of RP-29SG and BP-50SG according to a weight ratio of 1.5:1.
Example 13
A multifunctional cosmetic cream differs from example 1 in that the total weight of the toner is unchanged, and the weight ratio of Ti-02 SG, YP-75SG, RP-29SG and BP-50SG is adjusted to 40:5:0.8:1.
Example 14
A multifunctional cosmetic cream differs from example 1 in that the total weight of the toner is unchanged, and the weight ratio of Ti-02 SG, YP-75SG, RP-29SG and BP-50SG is adjusted to 60:10:2.2:1.
Example 15
A multifunctional cosmetic cream is different from example 1 in that the total weight of the sun powder is unchanged, and the cosmetic cream consists of Ti-Si1000 and ZN-AS 6800 in a weight ratio of 1:1.2.
Example 16
A multifunctional cosmetic cream is different from example 1 in that the total weight of the sun powder is unchanged, and the cosmetic cream consists of Ti-Si1000 and ZN-AS 6800 in a weight ratio of 1:1.8.
Example 17
A multifunctional cosmetic cream differs from example 1 in that the total weight of the sun powder is unchanged and contains only Ti-Si1000.
Example 18
A multifunctional cosmetic cream differs from example 1 in that the total weight of the sun powder is unchanged, and only ZN-AS 6800 is contained.
Example 19
A multifunctional cosmetic cream is different from example 1 in that the total weight of the sun powder is unchanged, and the cosmetic cream consists of Ti-Si1000 and ZN-AS 6800 in a weight ratio of 1:1.
Example 20
A multifunctional cosmetic cream is different from example 1 in that the total weight of the sun powder is unchanged, and the cosmetic cream consists of Ti-Si1000 and ZN-AS 6800 in a weight ratio of 1:2.
Example 21
A multifunctional cosmetic cream is different from example 1 in that the total weight of volatile oil is unchanged, and the multifunctional cosmetic cream consists of cyclopentadimethicone and isododecane according to a weight ratio of 2.5:1.
Example 22
A multifunctional cosmetic cream is different from example 1 in that the total weight of volatile oil is unchanged, and the multifunctional cosmetic cream consists of cyclopentadimethicone and isododecane according to the weight ratio of 3.5:1.
Example 23
A multifunctional cosmetic cream differs from example 1 in that the total weight of volatile oil is unchanged, and only cyclopentadimethicone is contained.
Example 24
A multifunctional cosmetic cream differs from example 1 in that the total weight of volatile oil is unchanged and only isododecane is contained.
Example 25
A multifunctional cosmetic cream is different from example 1 in that the total weight of volatile oil is unchanged, and the multifunctional cosmetic cream consists of cyclopentadimethicone and isododecane according to a weight ratio of 2:1.
Example 26
A multifunctional cosmetic cream is different from example 1 in that the total weight of volatile oil is unchanged, and the multifunctional cosmetic cream consists of cyclopentadimethicone and isododecane according to a weight ratio of 4:1.
Example 27
A multifunctional cosmetic cream is different from example 1 in that the total weight of the oily chemical sunscreen agent is unchanged, and the multifunctional cosmetic cream consists of ethylhexyl methoxycinnamate, polysiloxane-15 and ethylhexyl salicylate according to a weight ratio of 1.6:0.8:1.
Example 28
A multifunctional cosmetic cream is different from example 1 in that the total weight of the oily chemical sunscreen agent is unchanged, and the multifunctional cosmetic cream consists of ethylhexyl methoxycinnamate, polysiloxane-15 and ethylhexyl salicylate according to a weight ratio of 2.4:1.2:1.
Example 29
A multifunctional cosmetic cream is different from example 1 in that the total weight of the oily chemical sunscreen agent is unchanged, and the weight ratio of ethylhexyl methoxycinnamate to polysiloxane-15 is 2:1.
Example 30
A multifunctional cosmetic cream differs from example 1 in that the total weight of the oily chemical sunscreen is unchanged, containing only polysiloxane-15.
Example 31
A multifunctional cosmetic cream is different from example 1 in that the total weight of the oily chemical sunscreen agent is unchanged, and the multifunctional cosmetic cream consists of ethylhexyl methoxycinnamate, polysiloxane-15 and ethylhexyl salicylate according to a weight ratio of 1.5:0.7:1.
Example 32
A multifunctional cosmetic cream is different from example 1 in that the total weight of the oily chemical sunscreen agent is unchanged, and the multifunctional cosmetic cream consists of ethylhexyl methoxycinnamate, polysiloxane-15 and ethylhexyl salicylate according to a weight ratio of 2.5:1.3:1.
Example 33
A multifunctional cosmetic cream is different from example 1 in that the emulsifier consists of PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane and cetyl PEG/PPG-10/1 polydimethylsiloxane in a weight ratio of 1:2.
Example 34
A multifunctional cosmetic cream is different from example 1 in that the emulsifier consists of PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane and cetyl PEG/PPG-10/1 polydimethylsiloxane in a weight ratio of 1:4.
Example 35
A multifunctional cosmetic cream differs from example 1 in that the emulsifier is PEG-9 dimethicone ethyl dimethicone.
Example 36
A multifunctional cosmetic cream differs from example 1 in that the emulsifier is cetyl PEG/PPG-10/1 polydimethylsiloxane.
Example 37
A multifunctional cosmetic cream is different from example 1 in that the emulsifier consists of PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane and cetyl PEG/PPG-10/1 polydimethylsiloxane in a weight ratio of 1:1.5.
Example 38
A multifunctional cosmetic cream differs from example 1 in that the emulsifier consists of PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane and cetyl PEG/PPG-10/1 polydimethylsiloxane in a weight ratio of 1:4.5.
Example 39
A multifunctional cosmetic cream differs from example 1 in that the film former is an acrylic/polydimethylsiloxane copolymer.
Example 40
A multifunctional cosmetic cream is different from example 1 in that the moisturizing grease is a composition of dioctyl carbonate and hexyl laurate in a weight ratio of 1:1.
Example 41
A multifunctional cosmetic cream differs from example 1 in that the functional raw material is a silicon elastomer.
Example 42
A multifunctional cosmetic cream differs from example 1 in that the thickener is aerosil.
Example 43
A multifunctional cosmetic cream differs from example 1 in that the humectant is glycerin.
Example 44
A multifunctional cosmetic cream differs from example 1 in that the emulsion stabilizer is magnesium sulfate.
Example 45
A multifunctional cosmetic cream differs from example 1 in that the preservative is ethylhexyl glycerol.
Example 46
A multifunctional cosmetic cream differs from example 1 in that the aqueous sunscreen is methylenebis-benzotriazole tetramethylbutylphenol.
Example 47
A multifunctional cosmetic cream differs from example 1 in that the neutralizing agent is aminomethylpropanol.
Comparative example
Comparative example 1
A multifunctional cosmetic cream differs from example 1 in that the toner is not subjected to pretreatment.
Comparative example 2
A multifunctional cosmetic cream differs from example 1 in that the sun powder is not pre-treated.
Comparative example 3
A multifunctional cosmetic cream differs from example 1 in that neither the toner nor the sun powder is subjected to pretreatment.
Performance test samples: the multifunctional cosmetic cream obtained in examples 1 to 47 was used as test samples 1 to 47, and the multifunctional cosmetic cream obtained in comparative examples 1 to 3 was used as control samples 1 to 3.
The test method comprises the following steps:
(1) Sun protection efficacy test: 0.05 g of the sample is uniformly smeared on a PMMA plate, stored for 15 minutes in a dark place, then placed on SPF-290AS equipment, 8-point sampling test is selected, 1 plate is tested for each sample, and test results are recorded in Table 2; wherein SPF value represents UVB protection capability, PA value represents UVA protection capability, wherein PA value is expressed in "+" quantity, and the more quantity, the better effect.
(2) Pre-cosmetic efficacy test: the volunteers select 5 female volunteers (specific below) with different skin types, the product is uniformly smeared on the face, 2 milligrams per square centimeter is obtained, before and after the product is used, the product is respectively photographed and analyzed by a Visia facial analysis instrument to obtain facial speckle percentiles, and the facial speckle percentiles are respectively marked as A and B; obtaining a facial speckle percentile by the same method after using the product for 8 hours, and marking as C1; spraying artificial sweat, denoted C2, after use of the product; then, the base retention rate of the artificial sweat sprayed after 8 hours was calculated, wherein the base retention rate= (C-se:Sub>A)/(B-se:Sub>A) ×100%, and C in the formulse:Sub>A may be C1 or C2.
| Age of | Skin type | |
| Subject 1 | 32 | Dry skin |
| Subject 2 | 32 | Mixed dry skin |
| Subject 3 | 22 | Oil skin |
| Subject 4 | 22 | Mixed oil skin |
| Subject 5 | 32 | Mixed oil skin |
(3) Brightness enhancement efficacy test: testing whiteness and hiding power by using a color difference meter, wherein whiteness refers to the degree of increase or decrease of skin color whiteness after using a test article; the hiding power test is to uniformly coat the paste on black and white cardboard.
Test results of Table test samples 1-47 and control samples 1-3
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As can be seen from the combination of examples 1 to 8 and comparative examples 1 to 3 and the combination of table 2, the present application can make the obtained multifunctional cosmetic cream exhibit excellent sunscreen, pre-make-up and lightening effects by pre-treating the toner, the sunscreen powder before use in the preparation of the multifunctional cosmetic cream. Comparative example 3 the toner, the sunproof powder were used directly without pretreatment, and the test results of the sun-proof effect, the pre-make-up effect and the lightening effect were poor; however, in comparative example 1, when the toner was used only by pretreatment, it was found that the sunscreen effect was inferior in the test, and the pre-makeup effect and the lightening effect were greatly improved, but there was still a significant difference from example 1; however, in comparative example 2, when the sunscreen powder was used only by pretreatment, it was found that the pre-makeup efficacy and the lightening efficacy were poor, and the test of the sunscreen efficacy was greatly improved, but there was still a significant difference from example 1; therefore, the pretreatment of the toner or the sunscreen powder alone can lead to poor combination and compatibility with the other party, thereby affecting the exertion of the corresponding effects.
As can be seen from the combination of example 1 and examples 9 to 14 and Table 2, the toner composed of Ti-02 SG, YP-75SG, RP-29SG and BP-50SG in the weight ratio of (45-55): 6-9): 1-2): 1 was capable of exerting a superior effect after pretreatment. Any two of the materials are selected as the toner, or are combined outside the proportion range, so that the test results of the pre-makeup and the brightening effects are greatly lost, and meanwhile, the multifunctional cosmetic cream is found to have the loss of the sun protection effect, which means that the obtained pre-treatment toner can be stably matched with the pre-treatment sun protection powder only when the four materials are combined and applied in the proportion range, and further the excellent and stable effect is exerted.
As can be seen from the combination of examples 1 and 15-20 and Table 2, the sunscreen powder, which consists of Ti-Si1000 and ZN-AS 6800 in a weight ratio of 1 (1.2-1.8), exhibits excellent efficacy after pretreatment. Any one of the materials is selected as the sun-proof powder, or the sun-proof powder obtained by combining the materials in the proportion range can be used for placing the test result of the sun-proof effect to be greatly reduced, and meanwhile, the test result of the pre-makeup and brightening effects of the multifunctional cosmetic cream can be found to be reduced, so that the obtained pretreatment sun-proof powder can be stably matched with the pretreatment toner only when the two materials are combined and applied in the proportion range, and further, the excellent and stable effects can be exerted.
It can be seen from the combination of examples 1 and 21 to 26 and the combination of Table 2 that the volatile oil composed of cyclopentamethyl siloxane and isododecane in a weight ratio of (2.5 to 3.5): 1 can exhibit more excellent effects in the pretreatment process of toner and suntan powder, and further the obtained multifunctional cosmetic cream has excellent sun protection, pre-make-up and lightening effects. And any one of the cosmetic creams is selected to be used singly or combined beyond the proportion range, so that the multifunctional cosmetic cream has obvious reduction in the testing results of sun protection effect, pre-cosmetic effect and brightening effect.
It can be seen from the combination of example 1 and examples 27 to 32 and the combination of Table 2 that the oily chemical sunscreen agent consisting of ethylhexyl methoxycinnamate, polysiloxane-15 and ethylhexyl salicylate in a weight ratio of (1.6-2.4): (0.8-1.2): 1 has more excellent pretreatment effect on the sunscreen powder during application, and ensures the compromise and excellent exertion of the sunscreen effect, pre-cosmetic effect and lightening effect. And any one of the cosmetic creams is selected to be used independently or is combined beyond the proportion range, so that the multifunctional cosmetic cream is obviously reduced in the test result of the sun protection effect, and simultaneously, the test results of the pre-cosmetic effect and the brightening effect are also reduced, which means that the combination of the pre-cosmetic effect and the brightening effect is poor, and the effect is damaged.
As can be seen from the combination of examples 1 and 33-38 and the combination of Table 2, the emulsifier consists of PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane and cetyl PEG/PPG-10/1 polydimethylsiloxane in a weight ratio of 1 (2-3), and can play a superior auxiliary role in the combination and efficacy of the pretreatment toner and the pretreatment suntan powder. And when any one of PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane and cetyl PEG/PPG-10/1 polydimethylsiloxane is used as an emulsifier or is combined and used outside the range of the proportion, the testing results of sun-screening efficacy, pre-makeup efficacy and brightening efficacy are obviously reduced.
The present embodiment is only for explanation of the present application and is not to be construed as limiting the present application, and modifications to the present embodiment, which may not creatively contribute to the present application as required by those skilled in the art after reading the present specification, are all protected by patent laws within the scope of claims of the present application.
Claims (10)
1. The multifunctional cosmetic cream is characterized by being prepared from the following raw materials in parts by weight:
2.5-6.5 parts of emulsifying agent;
10-30 parts of volatile grease;
3-7 parts of moistening type grease;
2-12 parts of oily chemical sun-screening agent;
3-7 parts of skin feel modifier;
1-6 parts of film forming agent;
1-5 parts of functional raw materials;
0.1-2 parts of thickener;
3-8 parts of toner;
5-20 parts of sun-proof powder;
2-10 parts of humectant;
0.5-2 parts of emulsion stabilizer;
0.1-1 part of preservative;
2-8 parts of water-based sun-screening agent;
0.1-1 part of neutralizer;
20-30 parts of water;
the toner is subjected to pretreatment before being used for preparing multifunctional cosmetic cream, and specifically comprises the following steps:
uniformly mixing 1.5-3.5% of film forming agent and volatile oil with the same amount to obtain a treatment liquid A, uniformly mixing the toner and the treatment liquid A, and baking at 80-130 ℃ for 1-3 hours to obtain the toner;
the sun protection powder is subjected to pretreatment before being used for preparing multifunctional cosmetic cream, and specifically comprises the following steps:
taking 2.5-3.5% of oily chemical sun-screening agent by weight, adding 40-60% of volatile oil by weight of the oily chemical sun-screening agent, uniformly mixing to obtain a treatment liquid B, uniformly mixing sun-screening powder and the treatment liquid B, and baking at 80-100 ℃ for 1-2h to obtain the finished product.
2. The multifunctional cosmetic cream of claim 1, wherein: the toner consists of Ti-02 SG, YP-75SG, RP-29SG and BP-50SG, and the weight ratio of the Ti-02 SG, the YP-75SG, the RP-29SG and the BP-50SG is (45-55): (6-9): (1-2): 1.
3. The multifunctional cosmetic cream of claim 1, wherein: the sun-screening powder consists of Ti-Si1000 and ZN-AS 6800, and the weight ratio of the Ti-Si1000 to the ZN-AS 6800 is 1 (1.2-1.8).
4. The multifunctional cosmetic cream of claim 1, wherein: the film forming agent is one or a combination of more than one of acrylic acid (ester) copolymer/polydimethylsiloxane, trimethylsiloxysilicate, acrylic acid (ester) copolymer/polydimethylsiloxane methacrylate copolymer and polymethylsilsesquioxane;
the volatile oil is one or a combination of a plurality of cyclopentadimethicone, isododecane, methyl trimethyl silicone and dimethicone;
the oily chemical sun-screening agent is one or a combination of more of ethylhexyl methoxycinnamate, octocrylene, ethylhexyl salicylate and polysiloxane-15.
5. The multifunctional cosmetic cream of claim 4, wherein: the volatile oil consists of cyclopentadimethicone and isododecane, and the weight ratio of the cyclopentadimethicone to the isododecane is (2.5-3.5): 1.
6. The multifunctional cosmetic cream of claim 4, wherein: the oily chemical sun-screening agent consists of ethylhexyl methoxycinnamate, polysiloxane-15 and ethylhexyl salicylate, and the weight ratio of the ethylhexyl methoxycinnamate to the polysiloxane-15 to the ethylhexyl salicylate is (1.6-2.4): (0.8-1.2): 1.
7. The multifunctional cosmetic cream of claim 1, wherein: the emulsifying agent consists of a silicone oil emulsifying agent and a grease emulsifying agent, and the weight ratio of the silicone oil emulsifying agent to the grease emulsifying agent is 1 (2-4);
the silicone oil emulsifier is one or a combination of more of PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane, PEG/PPG-18/18 polydimethylsiloxane and PEG-10 polydimethylsiloxane;
the oil emulsifier is one or more of lauryl polyglycerol-3 polydimethylsiloxane ethyl polydimethylsiloxane, cetyl PEG/PPG-10/1 polydimethylsiloxane, lauryl PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane and lauryl PEG-10 tris (trimethylsiloxy) silyl ethyl polydimethylsiloxane.
8. The multifunctional cosmetic cream of claim 7, wherein: the emulsifier consists of PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane and cetyl PEG/PPG-10/1 polydimethylsiloxane according to the weight ratio of 1:3.
9. The multifunctional cosmetic cream of claim 1, wherein: the moistening oil is one or more of dioctyl carbonate, cetyl ethyl caproate, hexyl laurate, neopentyl glycol di (ethyl caproate), isononyl isononanoate and butanediol dicaprylate/dicaprate;
the functional raw material is one or a combination of more of silicon elastomer, silica and organic silicon powder;
the thickener is one or a combination of a plurality of bentonite and aerosil;
the humectant is one or more of glycerin, butanediol, propylene glycol and pentanediol;
the emulsion stabilizer is one or a combination of a plurality of sodium chloride and magnesium sulfate;
the preservative is one or a combination of more of phenoxyethanol, octaethylene glycol and ethylhexyl glycerol;
the water-based sun-screening agent is one or a combination of more of phenylbenzimidazole sulfonic acid and methylene bis-benzotriazole tetramethylbutylphenol;
the neutralizing agent is one or a combination of more of aminomethyl propanol, sodium hydroxide and triethanolamine.
10. The method for preparing a multifunctional cosmetic cream according to claim 1, characterized in that: the method comprises the following steps:
(1) Preparing raw materials comprising A phase, B phase, C phase, D phase, E phase and F phase according to a proportion, wherein the A phase comprises an emulsifier, a film forming agent, volatile grease, an oily chemical sunscreen agent, a skin feel modifier and moist grease; phase B includes a thickener; phase C includes toner; phase D comprises sun-proof powder; the E phase comprises water, a humectant, an emulsion stabilizer, an aqueous sun-screening agent, a preservative and a neutralizer; phase F includes functional materials;
(2) Uniformly mixing 1.5-3.5% of film forming agent and volatile oil with the same amount to obtain a treatment liquid A, uniformly mixing C-phase toner and the treatment liquid A, and baking at 80-130 ℃ for 1-3 hours to obtain pretreated toner; taking 2.5-3.5% by weight of oily chemical sun-screening agent, adding 40-60% by weight of volatile oil of the oily chemical sun-screening agent, uniformly mixing to obtain treatment liquid B, uniformly mixing D-phase sun-screening powder and the treatment liquid B, and baking at 80-100 ℃ for 1-2h to obtain pretreatment sun-screening powder;
(3) Uniformly mixing the other raw materials except the raw materials used in the step (2), adding the raw materials of the phase B and the phase F, uniformly dispersing, then homogenizing, continuously adding pretreatment toner for homogenizing, and then adding pretreatment sun-proof powder for homogenizing to obtain an intermediate product;
(4) And (3) after uniformly mixing the raw materials in the E phase, adding the mixture into the intermediate product obtained in the step (3), continuously homogenizing in the process, and continuously homogenizing after the addition is finished, thus obtaining the multifunctional cosmetic cream.
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| CN202310940907.5A CN116942548A (en) | 2023-07-28 | 2023-07-28 | Multifunctional cosmetic cream and preparation method thereof |
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| CN202310940907.5A CN116942548A (en) | 2023-07-28 | 2023-07-28 | Multifunctional cosmetic cream and preparation method thereof |
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