KR20120053259A - Lip cosmetic composition containing water soluble silicon compound - Google Patents

Lip cosmetic composition containing water soluble silicon compound Download PDF

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Publication number
KR20120053259A
KR20120053259A KR1020100114437A KR20100114437A KR20120053259A KR 20120053259 A KR20120053259 A KR 20120053259A KR 1020100114437 A KR1020100114437 A KR 1020100114437A KR 20100114437 A KR20100114437 A KR 20100114437A KR 20120053259 A KR20120053259 A KR 20120053259A
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South Korea
Prior art keywords
cosmetic composition
water soluble
lip
lips
water
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KR1020100114437A
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Korean (ko)
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KR101780709B1 (en
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김세진
김은정
고승용
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(주)아모레퍼시픽
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89—Polysiloxanes
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0216—Solid or semisolid forms
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89—Polysiloxanes
    • A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • A61K8/892—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a hydroxy group, e.g. dimethiconol
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02—Preparations containing skin colorants, e.g. pigments
    • A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02—Preparations containing skin colorants, e.g. pigments
    • A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
    • A61Q1/06—Lipsticks

Abstract

PURPOSE: A cosmetic composition for lip makeup containing water soluble silicon compounds is provided to ensure excellent luster effect and high transparency and to moisturize lip. CONSTITUTION: A cosmetic composition for lip contains 10-20 wt% of water soluble silicon compounds of chemical formula 1. In chemical formula 1, X is polyethylene glycol(PEG), polypropyelen glycol(PPG), or a mixture of PEG and PPG. The water soluble silicon compounds is prepared by nucleophilic substitution of hydrophilic polymers with chlorine of chlorosilane using a zinc catalyst.

Description

수용성 실리콘 화합물을 함유하는 입술용 화장료 조성물{Lip cosmetic composition containing water soluble silicon compound}Lip cosmetic composition containing water soluble silicon compound

본 발명은 수용성 실리콘 화합물을 함유하는 입술용 화장료 조성물 에 관한 것으로, 보다 상세하게는 친수성 고분자단과 실리콘이 결합된 수용성 실리콘 화합물을 함유하여 고광택 및 고밀착감을 부여하고 보습 효과가 우수한 입술용 화장료 조성물에 관한 것이다.
The present invention relates to a cosmetic composition for lips containing a water-soluble silicone compound, and more particularly, to a cosmetic composition for lips containing a water-soluble silicone compound in which a hydrophilic polymer group and silicone are combined to give high gloss and high adhesion and excellent moisturizing effect. It is about.

화장료 조성물, 특히, 립스틱, 립글로스, 립밤 및 립펜슬 등과 같이 입술에 사용 가능한 모든 화장료인 립메이크업 조성물은 피부(특히, 입술; 이하 같다)에 색상을 부여하여 아름답고 건강하게 보이도록 함과 동시에 피부를 보호하기 위한 것으로서, 이는 동?식물성 왁스, 에스테르계 오일 등의 유성 물질에 피부에 유용한 각종 영양성분, 유기 및 무기 안료를 분산시켜 균일한 혼합물로 만든 것이다. 즉, 화장료 조성물은 통상적으로, 고형 성분이나, 액상 유상 성분, 색소 및 기타 영양 성분 등을 포함한다.Cosmetic compositions, especially lip makeup compositions, which are all cosmetics available on the lips, such as lipsticks, lip gloss, lip balms and lip pencils, give the skin (especially the lips; the same) color to protect the skin while making it look beautiful and healthy This is to disperse various nutrients, organic and inorganic pigments useful for the skin in oily substances such as animal and vegetable waxes, ester oils, etc., to make a uniform mixture. That is, a cosmetic composition usually contains a solid component, a liquid oil component, a pigment | dye, other nutritional components, etc.

상기 고형 성분으로는 칸데릴라납, 세레신, 카르나우바납, 파라핀, 목납, 경납, 밀납, 마이크로 크리스탈린납 및 폴리에틸렌 등이 있으며, 이는 경도를 상승시켜 화장료 조성물의 외관 형태를 유지시키고, 사용감을 매끄럽게 개선한다.The solid ingredients include candelillanab, ceresin, carnauba wax, paraffin, nap, braze, beeswax, microcrystalline lead and polyethylene, which increase the hardness to maintain the appearance of the cosmetic composition and smoothly improve the feeling of use. do.

상기 액상 유상 성분으로는 피마자유, 호호바유, 스쿠알란, 라놀린 오일, 라놀린 유도체, 동?식물에서 추출된 오일과 합성에스테르 오일 및 기타 오일 등이 있다.The liquid oil phase components include castor oil, jojoba oil, squalane, lanolin oil, lanolin derivatives, oils extracted from animals and plants, synthetic ester oils, and other oils.

그 밖에, 화장료 조성물에는 유기 및 무기 색소로 이루어지는 색소성분이 포함되고, 또한, 산화방지제, 방부제, 향 성분 및 영양성분 등 기타 성분이 첨가된다.In addition, the cosmetic composition contains a pigment component consisting of organic and inorganic pigments, and other components such as antioxidants, preservatives, fragrance components, and nutritional components are added.

립메이크업 화장료에서 입술에의 도포 시 광택을 향상시키기 위한 방법으로는 일반적으로 고광택의 오일 성분을 다량 함유하여 도포 광택을 향상시키는 방법이 널리 이용되고 있다. 그러나, 고광택의 오일 성분들은 지속성이 낮아 입술 위에서 오래 지속되지 못하고 입술로 흡수되거나 입술 바깥으로 흐른다는 단점이 있다.
As a method for improving the glossiness when applying to the lips in the lip makeup cosmetics, a method of improving the application gloss by containing a large amount of a high gloss oil component is widely used. However, high gloss oils have a disadvantage of low persistence, which does not last long on the lips and is absorbed by the lips or flows out of the lips.

이에, 본 발명자들은 상기와 같은 종래 입술용 화장료 조성물의 문제점을 해결하고자 노력한 결과, 친수성 고분자단과 실리콘이 결합된 수용성 실리콘 화합물을 함유하면 내용물의 투명도를 더해 우수한 광택 효과를 보이고, 점증효과도 좋아 입술에 편안한 밀착감을 제공할 뿐만 아니라 보습효과를 줄 수 있음을 발견하고, 본 발명을 완성하였다.Thus, the present inventors have tried to solve the problems of the conventional cosmetic composition for lips as described above, when containing a water-soluble silicone compound combined with a hydrophilic polymer group and silicone shows an excellent gloss effect by adding the transparency of the contents, the lips also have good gradual effect The present invention was found to be able to provide a moisturizing effect as well as to provide a comfortable fit.

따라서, 본 발명의 목적은 입술에서의 고광택 효과 및 밀착감과 보습 효과가 우수하며 입술에 부드럽게 도포되는 입술용 화장료 조성물을 제공하는 것이다.
Accordingly, an object of the present invention is to provide a cosmetic composition for lips that is excellent in the high gloss effect and adhesion and moisturizing effect on the lips and gently applied to the lips.

상기 목적을 달성하기 위하여, 본 발명에서는 친수성 고분자단과 실리콘이 결합된 구조를 갖는 수용성 실리콘 화합물을 함유하는 입술용 화장료 조성물을 제공한다.
In order to achieve the above object, the present invention provides a cosmetic composition for lips containing a water-soluble silicone compound having a structure in which the hydrophilic polymer group and the silicon is bonded.

본 발명에 따른 입술용 화장료 조성물은 실리콘과 친수성 고분자가 결합된 실리콘화합물을 함유함으로써 내용물의 투명도를 더해 우수한 광택 효과를 보이고, 점증 효과도 좋아 입술에 편안한 밀착감을 제공할 뿐만 아니라, 우수한 보습 효과를 제공하며 입술에 부드럽게 도포되는 입술용 화장료 조성물을 제공한다. 본 발명에 따르면 고광택 및 고밀착감을 부여하면서 입술 보습 효과가 뛰어난 립메이크업 또는 입술 케어용 화장료 조성물을 제공할 수 있다.
The cosmetic composition for lips according to the present invention contains a silicone compound combined with silicone and a hydrophilic polymer to show the excellent gloss effect by adding the transparency of the contents, and also has a thickening effect, providing a comfortable fit to the lips, as well as excellent moisturizing effect. It provides and provides a cosmetic composition for lips that is gently applied to the lips. According to the present invention, it is possible to provide a lip makeup or lip care cosmetic composition having excellent lip moisturizing effect while providing high gloss and high adhesion.

본 발명은 하기 화학식 1의 구조를 갖는 수용성 실리콘 화합물을 함유하는 입술용 화장료 조성물을 제공한다.The present invention provides a cosmetic composition for lips containing a water-soluble silicone compound having a structure of formula (1).

Figure pat00001
Figure pat00001

상기 식에서, X는 폴리에틸렌글리콜(PEG), 폴리프로필렌글리콜(PPG) 또는 PEG와 PPG의 혼합이고, n은 10~20 사이의 정수이다. R1 및 R2는 각각 메틸기 또는 에틸기이다.Wherein X is polyethylene glycol (PEG), polypropylene glycol (PPG) or a mixture of PEG and PPG, and n is an integer between 10 and 20. R 1 and R 2 are each a methyl group or an ethyl group.

이하, 본 발명을 보다 상세히 설명한다.
Hereinafter, the present invention will be described in more detail.

본 발명의 유효성분인 수용성 실리콘 화합물은 친수성 고분자단과 실리콘이 결합된 구조를 갖는다.The water-soluble silicone compound which is an active ingredient of the present invention has a structure in which a hydrophilic polymer group and silicon are bonded.

본 발명의 수용성 실리콘 화합물은 상기 구조로 인해 실온에서는 왁스와 같은 성상을 가지고 있으며, 물과의 상용성이 매우 훌륭하며 물을 점증시켜 입술에 밀착감을 높여주는 역할을 한다. 또한, 높은 굴절률로 기존의 화장료 조성물에 비해 높은 광택 효과를 제공한다.The water-soluble silicone compound of the present invention has a wax-like property at room temperature due to the above structure, and has excellent compatibility with water and increases water to increase adhesion to lips. In addition, the high refractive index provides a high gloss effect compared to conventional cosmetic compositions.

본 발명의 수용성 실리콘 화합물은 클로로실란(R1, R2가 결합된 상태)에서 아연 촉매를 이용하여 친수성 고분자단을 클로로실란의 염소와 자리를 바꾸는 친핵성(Nucleophilic) 치환 반응을 실시하여 제조할 수 있다.The water-soluble silicone compound of the present invention may be prepared by performing a nucleophilic substitution reaction in which a hydrophilic polymer group is replaced with chlorine of chlorosilane by using a zinc catalyst in chlorosilane (R 1 and R 2 bonded). Can be.

본 발명의 수용성 실리콘 화합물은 조성물 총 중량에 대하여 10 내지 20 중량%로 함유될 수 있다. 이는 10 중량% 미만이면 밀착감이나 광택이 떨어지고, 20 중량% 초과하면 광택도도 저하되고 과한 쓴맛으로 사용하기 어렵다.The water-soluble silicone compound of the present invention may be contained in 10 to 20% by weight based on the total weight of the composition. If it is less than 10% by weight, the adhesion or gloss is inferior, and if it exceeds 20% by weight, the gloss is also lowered and it is difficult to use with excessive bitter taste.

본 발명의 립메이크업 조성물은 유효성분 이외에 본 발명의 효과를 손상시키지 않는 범위 내에서 왁스, 오일, 파우더, 안료, 영양성분, 휘발성 용해제, 산화방지제, 방부제 및 향 등과 같은 통상의 립메이크업 조성물에 함유되는 성분(이하 "기타 성분"이라고 한다)을 포함할 수 있다.The lip makeup composition of the present invention is contained in conventional lip makeup compositions such as waxes, oils, powders, pigments, nutrients, volatile solubilizers, antioxidants, preservatives and fragrances within the range of not impairing the effects of the present invention other than the active ingredient. It may include a component (hereinafter referred to as "other components").

상기 고상의 왁스로는 마이크로크리스탈린왁스, 오조케라이트, 밀납, 칸데릴라왁스, 카나우바왁스, 세레신, 파라핀, 몬탄왁스, 저팬왁스, 코코아버터 및 합성왁스 등이 있으며, 이들에만 한정되는 것은 아니다.The solid waxes include microcrystalline wax, ozokerite, beeswax, candelilla wax, carnauba wax, ceresin, paraffin, montan wax, Japan wax, cocoa butter and synthetic wax, but are not limited thereto. .

상기 오일 성분으로는 리퀴드 파라핀과 같은 광물성 오일; 스쿠알렌 및 하이드로 스쿠알렌 등의 동물성 오일; 팜오일, 아보카도 오일, 호호바오일, 세사미오일, 올리브오일 및 피마자유 등의 식물성 오일; 부틸 미리스테이트, 이소프로필 미리스테이트, 세틸 미리스테이트, 이소프로필팔미테이트, 부틸스테아레이트, 폴리부텐, 폴리이소부텐, 수첨폴리이소부텐, 각종 폴리올, 트리-2-에틸헥실산 글리세린, 트리글리세라이드계 오일, 젖산 미리스틸, 옥틸 도데칸올 및 디이소스테아릴 말레이트 등의 합성 오일이 있으며, 이들에만 한정되는 것은 아니다.The oil component may be a mineral oil such as liquid paraffin; Animal oils such as squalene and hydro squalene; Vegetable oils such as palm oil, avocado oil, jojoba oil, sesame oil, olive oil and castor oil; Butyl myristate, isopropyl myristate, cetyl myristate, isopropyl palmitate, butyl stearate, polybutene, polyisobutene, hydrogenated polyisobutene, various polyols, tri-2-ethylhexyl glycerol, triglyceride oil Synthetic oils such as lactic acid myristyl, octyl dodecanol, and diisostearyl maleate, but are not limited thereto.

상기 파우더 성분으로는 통상적으로 화장료에 사용되는 안료, 예를 들면 백운모, 합성운모, 견운모, 카올린, 이산화티탄, 산화티탄피복 운모, 알루미늄 파우더, 황산화철, 흑산화철, 카본블랙, 황산바륨, 실리카 및 제올라이트 등의 무기 파우더; 및 나일론, PMMA, 폴리스틸렌 파우더, 폴리에틸렌 파우더 및 셀룰로오스 파우더 등의 유기 파우더가 있으며, 이들에만 한정되는 것은 아니다.As the powder component, pigments commonly used in cosmetics, for example, mica, synthetic mica, mica, kaolin, titanium dioxide, titanium oxide coated mica, aluminum powder, iron sulfate, black iron oxide, carbon black, barium sulfate, silica, and Inorganic powders such as zeolites; And organic powders such as nylon, PMMA, polystyrene powder, polyethylene powder, and cellulose powder, but are not limited thereto.

상기 안료로는 황색 203호, 황색 4호, 황색 5호, 황색 201호, 황색 204호, 적색 103호, 적색 201호, 적색 202호, 적색 218호, 적색 220호, 적색 223호, 적색 226호, 적색 227호, 청색 1호, 청색 2호 등의 바륨 또는 알루미늄 레이크의 유기 안료 및 진주 안료 등이 있으며, 이들에만 한정되는 것은 아니다.As the pigment, yellow 203, yellow 4, yellow 5, yellow 201, yellow 204, red 103, red 201, red 202, red 218, red 220, red 223, red 226 Organic pigments and pearl pigments of barium or aluminum lakes such as No. 1, Red No. 227, Blue No. 1 and Blue No. 2, and the like, and the like.

본 발명의 립메이크업 조성물은 통상의 제조방법에 의하여 가열, 혼합 및 교반 등의 처리를 거침으로써 립스틱, 액상루즈 또는 립글로즈 등으로 제형화될 수 있다.The lip makeup composition of the present invention may be formulated into a lipstick, a liquid rouge or a lip gloss by undergoing a treatment such as heating, mixing and stirring by a conventional manufacturing method.

이하, 실시예 및 시험예를 들어 본 발명을 보다 구체적으로 설명하지만, 본 발명이 이에만 한정되는 것은 아니다.
Hereinafter, although an Example and a test example are given and this invention is demonstrated more concretely, this invention is not limited only to this.

[실시예 1~3 및 비교예 1~5][Examples 1-3 and Comparative Examples 1-5]

하기 표 1의 조성으로 립스틱 제형의 실시예 1~3 및 비교예 1~5를 제조하였다(단위: 중량%). 본 발명에 따른 실시예 1~3은 수용성 실리콘 화합물을 조성물 총 중량에 대하여 각각 10, 15, 20중량%로 함유하는 반면, 비교예 4~5는 수용성 실리콘 화합물을 본 발명의 바람직한 함량 범위를 벗어난 9, 21중량%로 함유하도록 제조하였다. 비교예 1~3은 수용성 실리콘 화합물이 아닌 루브라젤 CG 및 스트럭쳐 2001을 함유하도록 제조하였다. To the compositions of Table 1, Examples 1 to 3 and Comparative Examples 1 to 5 of the lipstick formulation were prepared (unit: wt%). Examples 1 to 3 according to the present invention contain 10, 15 and 20% by weight, respectively, of the water-soluble silicone compound based on the total weight of the composition, while Comparative Examples 4 to 5 contained the water-soluble silicone compound outside the preferred content range of the present invention. Prepared to contain 9, 21% by weight. Comparative Examples 1 to 3 were prepared to contain Lubragel CG and Structure 2001, not water-soluble silicone compounds.

실험에 사용된 루브라젤 CG는 글리세린(Glycerin), 글리세릴 아크릴레이트/아크릴산 코폴리머(Glyceryl Acrylate/Acrylic Acid Copolymer) 및 폴리필렌 글리콜(Propylene Glycol)의 혼합물이고, 스트럭쳐 2001은 아크릴레이트/스테아레쓰-20 이타코네이트 코폴리머(Acrylates/Steareth-20 Itaconate Copolymer)이며, 수용성 실리콘 화합물로는 비스-PEG-18 메틸 에테르 디메틸 실란(Grant Industries, Inc.)을 사용하였다.Lubragel CG used in the experiment is a mixture of Glycerin, Glyceryl Acrylate / Acrylic Acid Copolymer and Propylene Glycol, and Structure 2001 is an acrylate / steare Tsu-20 itaconate copolymer (Acrylates / Steareth-20 Itaconate Copolymer), and a water-soluble silicone compound was used as bis-PEG-18 methyl ether dimethyl silane (Grant Industries, Inc.).

성분명Ingredients 비교예 1Comparative Example 1 비교예 2Comparative Example 2 비교예 3Comparative Example 3 비교예 4Comparative Example 4 비교예 5Comparative Example 5 실시예 1Example 1 실시예 2Example 2 실시예 3Example 3 1. 물1. Water 73.973.9 73.973.9 73.973.9 73.973.9 73.973.9 73.973.9 73.973.9 73.973.9 2. 글리세린2. Glycerin 66 66 66 66 66 66 66 66 3. 루브라젤 CG3. Rubrazel CG 1515 -- 7.57.5 -- -- -- -- -- 4. 스트럭쳐 20014. Structure 2001 -- 1515 7.57.5 -- -- -- -- -- 5. 수용성실리콘화합물5. Water Soluble Silicone Compound -- -- -- 99 2121 1010 1515 2020 6. 적색227호6. Red No. 227 0.090.09 0.090.09 0.090.09 0.090.09 0.090.09 0.090.09 0.090.09 0.090.09 7. 황색 4호7. Yellow No. 4 0.010.01 0.010.01 0.010.01 0.010.01 0.010.01 0.010.01 0.010.01 0.010.01 8. 에탄올 95%8. Ethanol 95% 55 55 55 55 55 55 55 55

<실시예 1~3 및 비교예 1~5의 제조방법><The manufacturing method of Examples 1-3 and Comparative Examples 1-5>

1) 상기 성분 1~5를 50℃로 가열하여 용해시켰다.1) The said components 1-5 were heated and dissolved at 50 degreeC.

2) 상기 1) 단계의 용해물에 상기 성분 6~7을 첨가하여 50℃로 가열한 상태에서 호모 믹서(homo mixer)로 분산시켰다.2) The components 6-7 were added to the melt of step 1) and dispersed in a homo mixer while heated to 50 ° C.

3) 상기 2) 단계의 분산액에 상기 성분 8을 넣은 후, 향을 첨가하고 용기에 담아 립스틱을 제조하였다.
3) After the ingredient 8 was added to the dispersion of step 2), the perfume was added and put in a container to prepare a lipstick.

[시험예 1] 광택도 측정Test Example 1 Glossiness Measurement

상기 비교예 1~5 및 실시예 1~3에 의한 립메이크업 조성물의 도포 광택을 광택계(glossmeter)를 이용하여 테스트하였다.Coating gloss of the lip makeup compositions according to Comparative Examples 1 to 5 and Examples 1 to 3 was tested using a glossmeter.

측정 방법은 광택측정지에 비교예 1~5 및 실시예 1~3에 의한 립스틱 조성물을 일정한 힘으로 3회 왕복 도포한 후, 광택계(Gardner사)를 이용하여 60도 각도에서의 반사 각도로 도포면에 빛을 쏘았을 때의 반사량을 측정하여 광택도를 측정하고, 그 결과를 하기 표 2에 나타내었다(5회 측정 후 평균값). 하기 표 2의 결과에 나타낸 수치가 클수록 광택도가 우수한 것을 의미한다.The measurement method was applied to the gloss measurement paper by reciprocating the lipstick composition according to Comparative Examples 1 to 5 and Examples 1 to 3 three times with a constant force, and then coated surface at a reflection angle at an angle of 60 degrees using a glossmeter (Gardner). Glossiness was measured by measuring the amount of reflection when light was emitted, and the results are shown in Table 2 below (average value after five measurements). The larger the numerical value shown in the results of Table 2 below, the better the glossiness.

구분division 비교예 1Comparative Example 1 비교예 2Comparative Example 2 비교예 3Comparative Example 3 비교예 4Comparative Example 4 비교예 5Comparative Example 5 실시예 1Example 1 실시예 2Example 2 실시예 3Example 3 광택도Glossiness 28.128.1 22.622.6 25.925.9 22.322.3 20.520.5 30.430.4 36.336.3 31.731.7

상기 표 2의 결과에서 볼 수 있듯이, 본 발명에 따라 수용성 실리콘 화합물을 조성물 총 중량에 대하여 10 내지 20중량%로 함유한 립메이크업 조성물(실시예 1~3)은 수용성 실리콘 화합물을 함유하지 않고 루브라젤 CG 및 스트럭쳐 2001을 함유하는 비교예 1~3에 비해 광택도가 우수한 것을 확인할 수 있었다. 또한, 수용성 실리콘 화합물을 각각 9, 21중량%로 함유한 립메이크업 조성물(비교예 4~5)는 광택도가 급격히 저하됨을 확인할 수 있었다.
As can be seen from the results in Table 2, the lip makeup composition (Examples 1 to 3) containing the water-soluble silicone compound in an amount of 10 to 20% by weight based on the total weight of the composition according to the present invention does not contain a water-soluble silicone compound and It was confirmed that glossiness was superior to Comparative Examples 1 to 3 containing Brazel CG and Structure 2001. In addition, it was confirmed that the lip makeup compositions (Comparative Examples 4 to 5) each containing 9 and 21% by weight of a water-soluble silicone compound decreased sharply.

[시험예 2] 보습력 및 밀착감 평가[Test Example 2] Evaluation of moisturizing power and adhesion

상기 비교예 1~5 및 실시예 1~3의 립메이크업 조성물의 보습력, 밀착감(사용 시 입술에 접착되는 정도)을 평가하였다. The moisturizing power and adhesiveness of the lip makeup compositions of Comparative Examples 1 to 5 and Examples 1 to 3 were evaluated.

평가 대상은 24~35세 미혼 및 기혼 여성으로서 화장 경력이 최소 2년 이상이며, 일주일에 최소 5회 이상 지속적으로 립 제품을 사용하는 여성인 전문 패널 30명이 항목별 5점 만점으로 비교 평가하였다.The subjects of this study were unmarried and married women aged 24 to 35 years who had at least two years of makeup experience.

구체적인 평가 방법은 입술에 각각 비교예 1~5 및 실시예 1~3의 립스틱 조성물을 번갈아가며 2주 동안 사용해본 후 평가하였고, 그 결과를 하기 표 3에 나타내었다.Specific evaluation method was evaluated after using the lipstick composition of Comparative Examples 1 to 5 and Examples 1 to 3 alternately on the lips for 2 weeks, and the results are shown in Table 3 below.

구분division 비교예 1Comparative Example 1 비교예 2Comparative Example 2 비교예 3Comparative Example 3 비교예 4Comparative Example 4 비교예 5Comparative Example 5 실시예 1Example 1 실시예 2Example 2 실시예 3Example 3 보습력Moisturizing 2.332.33 2.572.57 3.33.3 3.43.4 3.73.7 3.93.9 4.14.1 4.44.4 밀착감A sense of closeness 1.121.12 2.22.2 1.541.54 2.62.6 2.92.9 3.23.2 3.43.4 3.73.7 평점grade 1.71.7 2.42.4 2.42.4 33 3.33.3 3.63.6 3.73.7 44

상기 표 3에서 알 수 있듯이, 본 발명에 따라 수용성 실리콘 화합물을 함유하는 입술용 화장료 조성물(실시예 1~3)은 비교예 1~5보다 보습력 및 밀착감 항목에서 우수한 만족감을 나타냈으며, 전체적인 평점도 유의하게 높았다.
As can be seen in Table 3, the cosmetic composition for lips containing a water-soluble silicone compound (Examples 1 to 3) according to the present invention showed excellent satisfaction in the moisturizing power and adhesion feeling items than Comparative Examples 1 to 5, the overall rating Significantly higher.

Claims (2)

하기 화학식 1의 구조를 갖는 수용성 실리콘 화합물을 함유하는 입술용 화장료 조성물.
[화학식 1]
Figure pat00002

상기 식에서, X는 폴리에틸렌글리콜(PEG), 폴리프로필렌글리콜(PPG) 또는 PEG와 PPG의 혼합이고, n은 10~20 사이의 정수이다. R1 및 R2는 각각 메틸기 또는 에틸기이다.A cosmetic composition for lips containing a water-soluble silicone compound having the structure of Formula 1.
[Formula 1]
Figure pat00002

Wherein X is polyethylene glycol (PEG), polypropylene glycol (PPG) or a mixture of PEG and PPG, and n is an integer between 10 and 20. R 1 and R 2 are each a methyl group or an ethyl group. 제 1항에 있어서, 상기 수용성 실리콘 화합물이 조성물 총 중량에 대하여 10 내지 20 중량 %로 함유되는 것을 특징으로 하는 입술용 화장료 조성물.
The cosmetic composition for the lips according to claim 1, wherein the water-soluble silicone compound is contained in an amount of 10 to 20% by weight based on the total weight of the composition.
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KR20170001268A (en) * 2015-06-26 2017-01-04 (주)아모레퍼시픽 Lip cosmetic composition emulisified as water-in-oil type comprising a water-soluble polymer
KR20230045939A (en) 2021-09-29 2023-04-05 코스맥스 주식회사 An oil-dispersion cosmetic composition containing a water-soluble dye and polyol, and method for preparing the same

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US5885559A (en) 1996-09-06 1999-03-23 Colgate Palmolive Company Solid cosmetic composition containing hexanediol-behenyl beeswax as gelling agent
EP1928399A1 (en) 2005-09-26 2008-06-11 L'Oréal Composition and process for treating keratinous substrates with at least two immiscible cosmetic compositions
EP2394703B1 (en) 2010-06-14 2015-12-23 Symrise AG Cooling mixture with reinforced cooling effect of 5-methyl-2-(propan-2-yl)cyclohexyl-N-ethyloxamate

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20170001268A (en) * 2015-06-26 2017-01-04 (주)아모레퍼시픽 Lip cosmetic composition emulisified as water-in-oil type comprising a water-soluble polymer
KR20230045939A (en) 2021-09-29 2023-04-05 코스맥스 주식회사 An oil-dispersion cosmetic composition containing a water-soluble dye and polyol, and method for preparing the same

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