CN112314818A - Preparation method of phyllanthus emblica and corn stigma compound beverage - Google Patents
Preparation method of phyllanthus emblica and corn stigma compound beverage Download PDFInfo
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- CN112314818A CN112314818A CN202011185143.6A CN202011185143A CN112314818A CN 112314818 A CN112314818 A CN 112314818A CN 202011185143 A CN202011185143 A CN 202011185143A CN 112314818 A CN112314818 A CN 112314818A
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- corn stigma
- emblic leafflower
- leafflower fruit
- mulberry leaf
- water
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/04—Extraction of juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/42—Preservation of non-alcoholic beverages
- A23L2/46—Preservation of non-alcoholic beverages by heating
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/80—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by adsorption
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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Abstract
The invention discloses a preparation method of a phyllanthus emblica and corn stigma composite beverage, and relates to the technical field of foods. The preparation method of the phyllanthus emblica and corn stigma compound beverage comprises the following steps: (1) separating pulp and kernel of fresh fructus Phyllanthi, squeezing, and filtering to obtain residue and filtrate; extracting the filter residue and the fruit stones with water to obtain an extracting solution; mixing the extractive solution and the filtrate to obtain fructus Phyllanthi juice; (2) adding water into corn stigma and folium Mori, and extracting to obtain corn stigma-folium Mori extractive solution; (3) respectively adding clarifying agent into fructus Phyllanthi juice and stigma Maydis-folium Mori extractive solution, mixing, standing, and performing solid-liquid separation to obtain clarified fructus Phyllanthi juice and stigma Maydis-folium Mori extractive solution; (4) respectively concentrating the clarified phyllanthus emblica juice and the corn stigma-mulberry leaf extracting solution to obtain concentrated solutions; (5) mixing the concentrated solution with sweetener and adjuvants, homogenizing, sterilizing, and making into compound beverage.
Description
Technical Field
The invention relates to the technical field of food, in particular to a preparation method of an emblic leafflower fruit and corn stigma compound beverage.
Background
At present, a compound functional beverage with light fruit aroma, which takes fresh emblic leafflower fruits, corn stigma and mulberry leaves as raw materials, does not exist. The prior phyllanthus emblica is mostly prepared into dry fruits and then is used for decocting and extracting juice, but the method can greatly reduce the fruity flavor of the fresh phyllanthus emblica and also reduce the content of the effective component phyllanthus emblica polysaccharide. Therefore, the fresh phyllanthus emblica is squeezed to obtain juice, the pomace and the kernels are subjected to hot water extraction and juice concentration, the whole fresh fruit is fully utilized, and the utilization rate of the fresh phyllanthus emblica is improved.
Disclosure of Invention
Based on the above, the invention aims to overcome the defects of the prior art and provide a preparation method of an emblic leafflower fruit and corn stigma compound beverage which can provide various nutrients, provide various vitamins, amino acids, polysaccharides, mineral substances and various physiologically active substances for a human body and has various effects of resisting gout, reducing blood sugar, reducing blood fat, reducing blood pressure, delaying senility and the like.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows: a preparation method of an emblic leafflower fruit and corn stigma compound beverage comprises the following steps:
(1) separating pulp and kernel of fresh fructus Phyllanthi; juicing fructus Phyllanthi, and filtering to obtain filter residue and filtrate; extracting the filter residue and the emblic leafflower fruit kernel by adding water to obtain an extracting solution; mixing the extractive solution and the filtrate to obtain fructus Phyllanthi juice;
(2) mixing stigma Maydis and folium Mori, and extracting with water to obtain stigma Maydis-folium Mori extractive solution;
(3) respectively adding clarifying agents into the emblic leafflower fruit juice prepared in the step (1) and the corn stigma-mulberry leaf extracting solution prepared in the step (2), uniformly mixing, standing, and performing solid-liquid separation to obtain clarified emblic leafflower fruit juice and corn stigma-mulberry leaf extracting solution;
(4) respectively concentrating the clarified emblic leafflower fruit juice liquid and the corn stigma-mulberry leaf extracting solution prepared in the step (3) to obtain an emblic leafflower fruit juice concentrated solution and a corn stigma-mulberry leaf concentrated solution;
(5) and (4) mixing the concentrated phyllanthus emblica juice solution and the concentrated corn stigma-mulberry leaf solution obtained in the step (4) with a sweetening agent and auxiliary materials, homogenizing, packaging and sterilizing to prepare the phyllanthus emblica and corn stigma compound beverage.
The emblic leafflower fruit is a wild fruit, is rich in various vitamins, is edible, and can promote the production of body fluid to quench thirst, moisten lung to reduce phlegm, treat cough and laryngalgia, relieve blowfish poisoning and the like. It is sour and astringent in taste and sweet in flavor for a long time, so it is called "Yuganzi". The emblic leafflower fruit is the famous name of emblic leafflower fruit, is commonly called the emblic leafflower fruit by folk, and is especially produced in the two regions, Yunnan, Fujian, Sichuan and the like.
Phyllanthus emblica is used as both medicine and food, and can be used as medicine and food. The Chinese pharmacopoeia contains dried mature fruit of emblic leafflower fruit of Phyllanthus emblica L. Clear heat and cool blood, promote digestion and invigorate stomach, promote the production of body fluid and relieve cough. Can be used for treating blood heat and blood stasis, dyspepsia, abdominal distention, cough, laryngalgia, and xerostomia. Cool in nature, sweet, sour and astringent in taste. It enters lung and stomach meridians. Harvesting from winter to spring fruit, removing impurities, and drying. The dosage is 3-9 g.
The research reports of emblic leafflower fruit polysaccharide in-vitro hypoglycemic and antioxidant activity research, emblic leafflower fruit extract influence on blood sugar of diabetic mice and the like, the emblic leafflower fruit polysaccharide can obviously improve insulin resistance, has obvious hypoglycemic effect on mice caused by alloxan, can effectively inhibit activity of alpha-amylase and alpha-glucosidase, and shows that the emblic leafflower fruit polysaccharide has an effect on the process from starch enzymolysis to glucose generation, delays or inhibits the generation of glucose and is beneficial to relieving postprandial blood sugar peak values. In addition, the emblic leafflower fruit polysaccharide is p.OH, O2 -And DPPH have certain cleaning effect, so that the oxidative stress of the diabetic can be relieved, and the diabetic complications can be effectively prevented.
The method takes the phyllanthus emblica raw material as the fresh fruit, adds a proper amount of water to squeeze juice, and then adds water to decoct and extract filter residue and fruit stones, is different from the traditional method of decoct and extract by using dry fruits, can fully utilize the whole fresh fruit, and can improve the utilization rate of the fresh phyllanthus emblica and effectively improve the extraction rate of phyllanthus emblica polysaccharide.
Stigma Maydis, which is stigma and stigma of Zea mays L. Most of the plants are produced all over the country. Collecting the ripe summer and autumn fruits, and removing impurities. Unprocessed or unprocessed after dried in the sun. The Yunnan herbal medicine: wide intestine and descending qi. It is used to treat female nodules of breast, galactostasis, red swelling and pain, aversion to cold, fever, headache and physical difficulty. Lingnan herbal medicine collection book: and pork decoction for diabetes. It is also indicated for dribbling urine with stone and intolerable pain, and it is often taken after decocted. Folk herbal compilation for common use: can lower blood pressure, induce diuresis and relieve swelling. It is indicated for nosebleed and metrorrhagia. In the Chiense on Sichuan Chinese herbs (Yan Zhi): clear blood heat and promote urination.
The corn stigma can be used as both medicine and food, and can be used as medicine and food. Corn silk is also called dragon silk, and has a wide range of prevention and health care purposes, so it is said that one corn silk can be called two-golden. The stigma Maydis contains crude fiber, crude protein, polysaccharide and crude fat. Researches show that the water extract of the corn stigma has the effects of resisting gout, reducing blood sugar and reducing blood fat.
The folium Mori is dried leaf of Morus alba L of Moraceae. Collected after blooming, removed of impurities and dried in the sun, is a wind-heat dispersing medicine which can be taken orally or applied externally. It is cold in nature, sweet and bitter in taste, has effects of dispelling pathogenic wind and heat, clearing lung-heat, moistening dryness, removing liver fire, and improving eyesight, and can be used for treating wind-heat type common cold, lung heat type cough, dizziness, headache, conjunctival congestion, and dim eyesight.
The mulberry leaf can be used as both medicine and food, and can be used as medicine and food. The mulberry leaves contain abundant amino acids, cellulose, vitamins, mineral substances and various physiological active substances, and have various health-care effects of reducing blood sugar, blood pressure and blood fat, delaying senility and the like.
According to the invention, based on the principle of homologous medicinal and edible raw materials and scientific compatibility, concentrated phyllanthus emblica juice is extracted on the basis of fresh phyllanthus emblica fruits, and then the corn stigma-mulberry leaf concentrated solution is added, so that the corn stigma has the effects of clearing away blood heat, reducing blood pressure and promoting urination, and can expel in-vivo toxin out of a body by accelerating urination and enhance the effect of promoting microcirculation; the mulberry leaves have the functions of dispelling wind and heat, clearing away the lung-heat, moistening dryness and regulating qi activity, and can discharge toxins in the body out of the body through sweat, thereby further enhancing the function of promoting microcirculation. The emblic leafflower fruit, the corn stigma and the mulberry leaf are combined, and the effects of clearing heat, promoting diuresis, reducing blood sugar, reducing blood fat and reducing blood pressure can be achieved by promoting the microcirculation function of blood vessels, urethra and sweat glands, so that the beverage is particularly suitable for sub-health people with three high levels as a daily healthy beverage for body building and health.
Preferably, in the step (1), when the emblic leafflower fruit is juiced, the mass ratio of the emblic leafflower fruit pulp to the water is as follows: emblic leafflower fruit flesh: water 1: 1-3; when the filter residue and the emblic leafflower fruit kernel are extracted by adding water, the mass ratio of the filter residue, the fruit kernel and the water is as follows: filtering residues and kernels: water 1: 8-12, and the extraction time is 1-2 h.
Preferably, in the step (2), the weight ratio of the corn silk to the mulberry leaf is: corn silk: and (3) mulberry leaf is 64-82: 18 to 36; the extraction times are two; in the first extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1: 10-25; during the second extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1: 6 to 12.
Mixing the two extractive solutions, adding adsorptive colloid for clarification, fine filtering, and removing precipitate to obtain stigma Maydis-folium Mori extractive solution.
Preferably, in the step (3), the clarifying agent is a compound of bentonite, sodium alginate, chitosan, xanthan gum and pectin.
Preferably, in the step (4), the clarified phyllanthus emblica juice is concentrated by using a microwave vacuum biological drying device; wherein the vacuum degree is-0.1 to-0.04 Kpa, the microwave power is 1.0 to 1.6KW, the concentration temperature is 60 to 70 ℃, and the concentration time is 1 to 2 hours.
The microwave vacuum biological drying equipment is adopted for concentration, so that the effective components and flavor characteristics in the phyllanthus emblica juice are greatly retained.
Preferably, in the step (4), the clarified corn stigma-mulberry leaf extracting solution is subjected to reduced pressure concentration, the vacuum degree is-0.06-0.04 Mpa, and the concentration time is 1.5-2.5 h.
When the clear corn stigma-mulberry leaf extracting solution is subjected to reduced pressure concentration, stirring is not required in the concentration process, and partial substances are prevented from being coked.
Preferably, in the step (5), a pasteurization method is adopted, wherein the pasteurization temperature is 60-80 ℃, and the pasteurization time is 20-60 min.
In addition, the invention also provides the emblic leafflower fruit and corn stigma compound beverage prepared by the preparation method.
Preferably, the phyllanthus emblica and corn stigma compound beverage comprises the following components in parts by weight: 20-25 parts of phyllanthus emblica juice concentrated solution, 20-25 parts of corn stigma-mulberry leaf concentrated solution, 15-25 parts of sweetening agent and 3-8 parts of auxiliary materials; wherein the sweetening agent is non-starch fructose, and the auxiliary material is a compound of pectin and carboxymethyl cellulose; wherein the weight ratio of pectin to carboxymethyl cellulose is as follows: pectin: carboxymethyl cellulose 2-5: 1 to 3.
Further preferably, the emblic leafflower fruit and corn stigma compound beverage comprises the following components in parts by weight: 20 parts of emblic leafflower fruit juice concentrated solution, 25 parts of corn stigma-mulberry leaf concentrated solution, 15 parts of sweetening agent and 5 parts of auxiliary material; wherein the weight ratio of pectin to carboxymethyl cellulose is as follows: pectin: carboxymethyl cellulose ═ 4: 1.
the phyllanthus emblica and corn stigma composite beverage is packaged in bottles or bags, and the mass of each bottle/bag is 10-100 g.
In addition, the non-starch fructose sweetening agent is added for seasoning, and the auxiliary materials such as pectin and carboxymethyl cellulose are added for mixing and blending, so that the defect of strong sour and astringent taste of the phyllanthus emblica fruit is overcome, the edible flavor and nutrient substances can be improved, and the phyllanthus emblica fruit is more suitable for daily eating.
Compared with the prior art, the invention has the beneficial effects that:
(1) the emblic leafflower fruit and corn stigma compound beverage prepared by the method has various health-care effects of reducing blood sugar, blood fat and blood pressure, and has obvious fruity flavor, obviously improved integral flavor, more suitability for daily eating and higher consumer acceptance degree compared with other products prepared by taking dried emblic leafflower fruits as raw materials and adopting the method.
(2) The method takes fresh phyllanthus emblica fruits as raw materials, adds a proper amount of water for juicing, and then adds water for decocting and extracting filter residues and fruit stones.
(3) The invention can well play a role in improving effective components of the emblic leafflower fruit, enhancing nutrition, keeping flavor and expanding the acceptance range of people, and provides the emblic leafflower fruit and corn stigma compound beverage with higher nutritive value. The method is controllable, stable and reliable.
Drawings
Fig. 1 is a process flow chart of preparing the emblic leafflower fruit and corn stigma compound beverage.
Detailed Description
To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to the accompanying drawings and specific embodiments.
Example 1
In an embodiment of the present invention, a preparation flow process diagram is shown in fig. 1, and a preparation method of the emblic leafflower fruit and corn stigma composite beverage in the specific embodiment includes the following steps:
(1) separating pulp and kernel of fresh fructus Phyllanthi; juicing the pulp of the emblic leafflower fruit, wherein the mass ratio of the pulp of the emblic leafflower fruit to water is as follows: emblic leafflower fruit flesh: water 1:1, filtering to obtain filter residue and filtrate; adding water into the filter residue and the emblic leafflower fruit stone for extraction, wherein when the filter residue and the emblic leafflower fruit stone are extracted by adding water, the mass ratio of the filter residue to the fruit stone to the water is as follows: filtering residues and kernels: water 1:8, extracting for 1h to obtain an extracting solution; mixing the extractive solution and the filtrate to obtain fructus Phyllanthi juice;
(2) mixing corn silk and mulberry leaves, wherein the weight ratio of the corn silk to the mulberry leaves is as follows: corn silk: and (4) mulberry leaf 64: 18; adding water for extraction twice; in the first extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1: 10; during the second extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1: 6, combining the two extracting solutions to obtain a corn stigma-mulberry leaf extracting solution;
(3) respectively adding clarifying agents into the emblic leafflower fruit juice prepared in the step (1) and the corn stigma-mulberry leaf extracting solution prepared in the step (2), uniformly mixing, standing, and performing solid-liquid separation to obtain clarified emblic leafflower fruit juice and corn stigma-mulberry leaf extracting solution;
(4) respectively concentrating the clarified phyllanthus emblica juice liquid and the corn stigma-mulberry leaf extracting solution prepared in the step (3), and concentrating the clarified phyllanthus emblica juice by adopting microwave vacuum biological drying equipment; wherein the vacuum degree is-0.1 Kpa, the microwave power is 1.0KW, the concentration temperature is 60 ℃, and the concentration time is 1 h; carrying out reduced pressure concentration on the clear corn stigma-mulberry leaf extracting solution, wherein the vacuum degree is-0.06 to-0.04 Mpa, and the concentration time is 1.5h, so as to obtain an emblic leafflower fruit juice concentrated solution and a corn stigma-mulberry leaf concentrated solution;
(5) mixing the phyllanthus emblica juice concentrated solution and the corn stigma-mulberry leaf concentrated solution obtained in the step (4) with a sweetening agent and auxiliary materials in parts by weight: 25 parts of emblic leafflower fruit juice concentrated solution, 20 parts of corn stigma-mulberry leaf concentrated solution, 25 parts of non-starch fructose, 2 parts of pectin and 1 part of carboxymethyl cellulose, and mixing, homogenizing, sterilizing and preparing the emblic leafflower fruit and corn stigma composite beverage.
Example 2
In an embodiment of the present invention, a preparation flow process diagram is shown in fig. 1, and a preparation method of the emblic leafflower fruit and corn stigma composite beverage in the specific embodiment includes the following steps:
(1) separating pulp and kernel of fresh fructus Phyllanthi; juicing the pulp of the emblic leafflower fruit, wherein the mass ratio of the pulp of the emblic leafflower fruit to water is as follows: emblic leafflower fruit flesh: water 1: 2, filtering to obtain filter residue and filtrate; adding water into the filter residue and the emblic leafflower fruit stone for extraction, wherein when the filter residue and the emblic leafflower fruit stone are extracted by adding water, the mass ratio of the filter residue to the fruit stone to the water is as follows: filtering residues and kernels: water 1:10, extracting for 1.5 hours to obtain an extracting solution; mixing the extractive solution and the filtrate to obtain fructus Phyllanthi juice;
(2) mixing corn silk and mulberry leaves, wherein the weight ratio of the corn silk to the mulberry leaves is as follows: corn silk: 70 parts of mulberry leaves: 27; adding water for extraction twice; in the first extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1: 15; during the second extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1:10, mixing the two extracting solutions to obtain a corn stigma-mulberry leaf extracting solution;
(3) respectively adding clarifying agents into the emblic leafflower fruit juice prepared in the step (1) and the corn stigma-mulberry leaf extracting solution prepared in the step (2), uniformly mixing, standing, and performing solid-liquid separation to obtain clarified emblic leafflower fruit juice and corn stigma-mulberry leaf extracting solution;
(4) respectively concentrating the clarified phyllanthus emblica juice liquid and the corn stigma-mulberry leaf extracting solution prepared in the step (3), and concentrating the clarified phyllanthus emblica juice by adopting microwave vacuum biological drying equipment; wherein the vacuum degree is-0.08 Kpa, the microwave power is 1.3KW, the concentration temperature is 65 ℃, and the concentration time is 1.5 h; carrying out reduced pressure concentration on the clear corn stigma-mulberry leaf extracting solution, wherein the vacuum degree is-0.06 to-0.04 Mpa, and the concentration time is 2 hours, so as to obtain an emblic leafflower fruit juice concentrated solution and a corn stigma-mulberry leaf concentrated solution;
(5) mixing the phyllanthus emblica juice concentrated solution and the corn stigma-mulberry leaf concentrated solution obtained in the step (4) with a sweetening agent and auxiliary materials in parts by weight: 20 parts of emblic leafflower fruit juice concentrated solution, 25 parts of corn stigma-mulberry leaf concentrated solution, 15 parts of non-starch fructose, 4 parts of pectin and 1 part of carboxymethyl cellulose, and mixing, homogenizing, sterilizing and preparing the emblic leafflower fruit and corn stigma composite beverage.
Example 3
In an embodiment of the present invention, a preparation flow process diagram is shown in fig. 1, and a preparation method of the emblic leafflower fruit and corn stigma composite beverage in the specific embodiment includes the following steps:
(1) separating pulp and kernel of fructus Phyllanthi; juicing the pulp of the emblic leafflower fruit, wherein the mass ratio of the pulp of the emblic leafflower fruit to water is as follows: emblic leafflower fruit flesh: water 1: 3, filtering to obtain filter residue and filtrate; adding water into the filter residue and the emblic leafflower fruit stone for extraction, wherein when the filter residue and the emblic leafflower fruit stone are extracted by adding water, the mass ratio of the filter residue to the fruit stone to the water is as follows: filtering residues and kernels: water 1: 12, extracting for 2 hours to obtain an extracting solution; mixing the extractive solution and the filtrate to obtain fructus Phyllanthi juice;
(2) mixing corn silk and mulberry leaves, wherein the weight ratio of the corn silk to the mulberry leaves is as follows: corn silk: and (2) mulberry leaf, namely 82: 36; adding water for extraction twice; in the first extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1: 25; during the second extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1: 12, combining the two extracting solutions to obtain corn stigma-mulberry leaf extracting solution;
(3) respectively adding clarifying agents into the emblic leafflower fruit juice prepared in the step (1) and the corn stigma-mulberry leaf extracting solution prepared in the step (2), uniformly mixing, standing, and performing solid-liquid separation to obtain clarified emblic leafflower fruit juice and corn stigma-mulberry leaf extracting solution;
(4) respectively concentrating the clarified phyllanthus emblica juice liquid and the corn stigma-mulberry leaf extracting solution prepared in the step (3), and concentrating the clarified phyllanthus emblica juice by adopting microwave vacuum biological drying equipment; wherein the vacuum degree is-0.04 Kpa, the microwave power is 1.6KW, the concentration temperature is 70 ℃, and the concentration time is 2 h; carrying out reduced pressure concentration on the clear corn stigma-mulberry leaf extracting solution, wherein the vacuum degree is-0.06 to-0.04 Mpa, and the concentration time is 2.5h, so as to obtain an emblic leafflower fruit juice concentrated solution and a corn stigma-mulberry leaf concentrated solution;
(5) mixing the phyllanthus emblica juice concentrated solution and the corn stigma-mulberry leaf concentrated solution obtained in the step (4) with a sweetening agent and auxiliary materials in parts by weight: 25 parts of emblic leafflower fruit juice concentrated solution, 25 parts of corn stigma-mulberry leaf concentrated solution, 25 parts of non-starch fructose, 5 parts of pectin and 3 parts of carboxymethyl cellulose, and mixing, homogenizing, sterilizing and preparing the emblic leafflower fruit and corn stigma composite beverage.
Comparative example 1
The specific preparation method of the emblic leafflower fruit and corn stigma compound beverage in the comparative example comprises the following steps:
(1) weighing the same batch and weight of fresh phyllanthus emblica fruits as in example 1, cleaning, draining, cutting into two halves, spreading on a shelf, and placing in a hot air drying oven. And (3) drying at the temperature of 55-60 ℃ for 6-8 hours to obtain the dried phyllanthus emblica fruits.
(2) Adding water into dried emblic leafflower fruits for first extraction, wherein the mass ratio of the dried emblic leafflower fruits to the water is 1:10, and the extraction time is 1.5 h; adding water into the dried emblic leafflower fruits for secondary extraction, wherein the mass ratio of the dried emblic leafflower fruits to the water is 1:8, and the extraction time is 1.0h, so as to finally obtain the dried emblic leafflower fruit extracting solution.
(3) Mixing corn silk and mulberry leaves, wherein the weight ratio of the corn silk to the mulberry leaves is as follows: corn silk: and (4) mulberry leaf 64: 18; adding water for extraction twice; in the first extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1: 10; during the second extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1: 6, combining the two extracting solutions to obtain a corn stigma-mulberry leaf extracting solution;
(4) respectively adding a clarifying agent into the dried emblic leafflower fruit extracting solution prepared in the step (2) and the corn stigma-mulberry leaf extracting solution prepared in the step (3), uniformly mixing, standing, and performing solid-liquid separation to obtain clarified dried emblic leafflower fruit extracting solution and corn stigma-mulberry leaf extracting solution;
(5) and (4) respectively carrying out reduced pressure concentration on the clear dried emblic leafflower fruit extract and the corn stigma-mulberry leaf extract prepared in the step (4). Wherein the concentration vacuum degree of the extracting solution of the dried emblic leafflower fruit is-0.06 Mpa to-0.04 Mpa, and the concentration time is 1.0 h; the vacuum degree of the corn stigma-mulberry leaf extracting solution is reduced to-0.06 MPa to-0.04 MPa, and the concentration time is 1.5 h.
(6) Mixing the dried emblic leafflower fruit concentrated solution and the corn stigma-mulberry leaf concentrated solution obtained in the step (5) with a sweetening agent and auxiliary materials in parts by weight: 25 parts of dry emblic leafflower fruit concentrated solution, 20 parts of corn stigma-mulberry leaf concentrated solution, 25 parts of non-starch fructose, 2 parts of pectin and 1 part of carboxymethyl cellulose, and mixing, homogenizing, sterilizing and preparing the emblic leafflower fruit and corn stigma composite beverage.
Comparative example 2
The specific preparation method of the emblic leafflower fruit and corn stigma compound beverage in the comparative example comprises the following steps:
(1) weighing the same batch and weight of fresh phyllanthus emblica fruits as in example 2, cleaning, draining, cutting into two halves, spreading on a shelf, and placing in a hot air drying oven. And (3) drying at the temperature of 55-60 ℃ for 6-8 hours to obtain the dried phyllanthus emblica fruits.
(2) Adding water into dried emblic leafflower fruits for first extraction, wherein the mass ratio of the dried emblic leafflower fruits to the water is 1:10, and the extraction time is 1.5 h; adding water into the dried emblic leafflower fruits for secondary extraction, wherein the mass ratio of the dried emblic leafflower fruits to the water is 1:8, and the extraction time is 1.0h, so as to finally obtain the dried emblic leafflower fruit extracting solution.
(3) Mixing corn silk and mulberry leaves, wherein the weight ratio of the corn silk to the mulberry leaves is as follows: corn silk: 70 parts of mulberry leaves: 27; adding water for extraction twice; in the first extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1: 15; during the second extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1:10, mixing the two extracting solutions to obtain a corn stigma-mulberry leaf extracting solution;
(4) respectively adding a clarifying agent into the dried emblic leafflower fruit extracting solution prepared in the step (2) and the corn stigma-mulberry leaf extracting solution prepared in the step (3), uniformly mixing, standing, and performing solid-liquid separation to obtain clarified dried emblic leafflower fruit extracting solution and corn stigma-mulberry leaf extracting solution;
(5) and (4) respectively carrying out reduced pressure concentration on the clear dried emblic leafflower fruit extract and the corn stigma-mulberry leaf extract prepared in the step (4). Wherein the concentration vacuum degree of the extracting solution of the dried emblic leafflower fruit is-0.06 Mpa to-0.04 Mpa, and the concentration time is 1.0 h; the vacuum degree of the corn stigma-mulberry leaf extracting solution is reduced to-0.06 MPa to-0.04 MPa, and the concentration time is 2.0 h.
(6) Mixing the dried emblic leafflower fruit concentrated solution and the corn stigma-mulberry leaf concentrated solution obtained in the step (5) with a sweetening agent and auxiliary materials in parts by weight: 20 parts of dry emblic leafflower fruit concentrated solution, 25 parts of corn stigma-mulberry leaf concentrated solution, 15 parts of non-starch fructose, 4 parts of pectin and 1 part of carboxymethyl cellulose, and mixing, homogenizing, sterilizing and preparing the emblic leafflower fruit and corn stigma composite beverage.
Test example 1 comparison of polysaccharide content in concentrated solution of fresh Phyllanthus emblica fruit and concentrated solution of dried Phyllanthus emblica fruit
(1) Preparation of concentrated solution of fresh emblic leafflower fruit
Collecting 3 batches of fresh phyllanthus emblica fruits (fresh fruit I, fresh fruit II and fresh fruit III) with different production places.
A proper amount of fresh fruit I, fresh fruit II and fresh fruit III was respectively taken, and concentrated solutions of fresh emblic leafflower fruit were prepared according to the corresponding methods in example 1.
(2) Preparation of concentrated solution of dried emblic leafflower fruit
Taking the fresh fruit I with the same weight as the fresh fruit I in the step, cleaning, draining, cutting the fresh fruit I into halves, laying the cut fruits on a shelf, placing the cut fruits in a hot air drying box, and drying the cut fruits for 6 to 8 hours at the temperature of 55 to 60 ℃ to obtain the dried emblic leafflower fruit (dried fruit I). Adding water into the dry fruit I for primary extraction, wherein the mass ratio of the dry fruit I to the water is 1:10, and the extraction time is 1.5 h; adding water into the dry fruit I for secondary extraction, wherein the mass ratio of the dry fruit I to the water is 1:8, and the extraction time is 1.0h, so as to finally obtain an extracting solution of the dry fruit I of the emblic leafflower fruit; adding a clarifying agent, uniformly mixing, standing, and performing solid-liquid separation to obtain a clarified dried emblic leafflower fruit I extracting solution. And carrying out reduced pressure concentration on the extracting solution, wherein the concentration vacuum degree is-0.06 Mpa to-0.04 Mpa, and the concentration time is 1.0h, thus finally obtaining the concentrated solution of the dried emblic leafflower fruit I.
Preparing concentrated solution II and III from fructus Phyllanthi by the same method.
(3) Determination of polysaccharide content
The content of polysaccharide in the concentrated solution of the fresh emblic leafflower fruit and the concentrated solution of the dry emblic leafflower fruit is measured by adopting a phenol-sulfuric acid colorimetric method (reference document: Wangrui. research on polysaccharide of emblic leafflower fruit for reducing blood sugar and resisting oxidation activity in vitro [ J ] research and development of food, 2018,39(17):189-192,224.).
(4) Results and analysis
The results are shown in table 1:
TABLE 1 measurement results of polysaccharide content in concentrated phyllanthus emblica liquid
Fresh fruit concentrated solution | Polysaccharide content (mg/ml) | Dried fruit concentrated solution | Polysaccharide content (mg/ml) |
Fresh fruit I | 0.066 | Dried fruit I | 0.043 |
Fresh fruit II | 0.070 | Dried fruit II | 0.048 |
Fresh fruit III | 0.066 | Dried fruit III | 0.042 |
As can be seen from table 1, the polysaccharide content of each batch of the fresh emblic concentrated solution is greater than that of the corresponding batch of the dry fruit concentrated solution.
Test example 2 comparison of flavor of a Phyllanthus emblica and corn stigma composite beverage prepared from fresh Phyllanthus emblica and dried Phyllanthus emblica fruits, respectively
And (3) carrying out sensory evaluation test on the preference degrees of 60 consumers on the four samples by referring to GB/T12315-2008 sensory analysis methodology sorting method. The samples of sample numbers 311 and 904 are the emblic leafflower fruit and corn stigma compound beverages prepared by the preparation methods of example 1 and example 2 using fresh emblic leafflower fruit, respectively. The samples of sample No. 883 and sample No. 671 are emblic leafflower fruit and corn stigma composite beverages prepared by the preparation methods of comparative example 1 and comparative example 2 using dried emblic leafflower fruit, respectively.
The results are shown in tables 2 and 3, by statistical analysis:
TABLE 2 organoleptic evaluation test results of the Compound beverages
TABLE 3 multiple comparative analysis results of composite beverage sensory evaluation LSD
Of the four samples, the average consumer preference score and the average rank score for sample number 904 were all highest, indicating that the flavor of sample number 904 was the best of the four samples; the next is sample number 311. In addition, the P value is 6.1975E-23 < 0.05, which indicates that the four samples have significant difference. Therefore, LSD multiple comparisons are required, and the data shown in table 3 indicate that the significance P values of the sample number 311 and the three other samples are all less than 0.01, i.e. the sample number 311 and the three other samples have significance differences between each other; similarly, sample number 904 is significantly different from the other three samples in pairs. Thus, number 904 can be derived, i.e., the sample of example 2 is most popular with consumers, followed by the sample of example 1. Example 3 similar to examples 1 and 2, a concentrated juice of fresh emblic leafflower fruit is used, which is not repeated herein. That is, the concentrated juice of fresh emblic leafflower fruit is obviously different from the concentrated juice of dry emblic leafflower fruit for the consumers. Therefore, the extraction of fresh phyllanthus emblica fruits can obviously improve the overall flavor of the product and is more popular with consumers.
The tests prove that the extraction by using the fresh phyllanthus emblica fruits can not only improve the utilization rate of the fresh phyllanthus emblica fruits, but also effectively improve the extraction rate of phyllanthus emblica polysaccharide, and can improve the overall flavor of the product, so that the phyllanthus emblica polysaccharide is more popular with consumers.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (10)
1. The preparation method of the phyllanthus emblica and corn stigma composite beverage is characterized by comprising the following steps of:
(1) separating pulp and kernel of fresh fructus Phyllanthi; juicing fructus Phyllanthi, and filtering to obtain filter residue and filtrate; extracting the filter residue and the emblic leafflower fruit kernel by adding water to obtain an extracting solution; mixing the extractive solution and the filtrate to obtain fructus Phyllanthi juice;
(2) mixing stigma Maydis and folium Mori, and extracting with water to obtain stigma Maydis-folium Mori extractive solution;
(3) respectively adding clarifying agents into the emblic leafflower fruit juice prepared in the step (1) and the corn stigma-mulberry leaf extracting solution prepared in the step (2), uniformly mixing, standing, and performing solid-liquid separation to obtain clarified emblic leafflower fruit juice and corn stigma-mulberry leaf extracting solution;
(4) respectively concentrating the clarified emblic leafflower fruit juice liquid and the corn stigma-mulberry leaf extracting solution prepared in the step (3) to obtain an emblic leafflower fruit juice concentrated solution and a corn stigma-mulberry leaf concentrated solution;
(5) and (4) mixing the concentrated phyllanthus emblica juice solution and the concentrated corn stigma-mulberry leaf solution obtained in the step (4) with a sweetening agent and auxiliary materials, homogenizing, packaging and sterilizing to prepare the phyllanthus emblica and corn stigma compound beverage.
2. The preparation method of the emblic leafflower fruit and corn stigma compound beverage according to claim 1, wherein in the step (1), when the emblic leafflower fruit is juiced, the mass ratio of the emblic leafflower fruit pulp to water is as follows: emblic leafflower fruit flesh: water 1: 1-3; when the filter residue and the emblic leafflower fruit kernel are extracted by adding water, the mass ratio of the filter residue, the fruit kernel and the water is as follows: filtering residues and kernels: water 1: 8-12, and the extraction time is 1-2 h.
3. The preparation method of the emblic leafflower fruit and corn stigma compound beverage according to claim 1, wherein in the step (2), the weight ratio of the corn stigma to the mulberry leaf is as follows: corn silk: and (3) mulberry leaf is 64-82: 18 to 36; the extraction times are two; in the first extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1: 10-25; during the second extraction, the mass ratio of the corn stigma to the mulberry leaves to the water is as follows: corn silk-mulberry leaf: water 1: 6 to 12.
4. The preparation method of the emblic leafflower fruit and corn stigma compound beverage according to claim 1, wherein in the step (3), the clarifying agent is a compound of bentonite, sodium alginate, chitosan, xanthan gum and pectin.
5. The preparation method of the emblic leafflower fruit and corn stigma compound beverage according to claim 1, wherein in the step (4), the clarified emblic leafflower fruit juice is concentrated by using a microwave vacuum biological drying device; wherein the vacuum degree is-0.1 to-0.04 Kpa, the microwave power is 1.0 to 1.6KW, the concentration temperature is 60 to 70 ℃, and the concentration time is 1 to 2 hours.
6. The preparation method of the emblic leafflower fruit and corn stigma compound beverage according to claim 1, wherein in the step (4), the clarified corn stigma-mulberry leaf extracting solution is concentrated under reduced pressure, the vacuum degree is-0.06-0.04 MPa, and the concentration time is 1.5-2.5 h.
7. The preparation method of the emblic leafflower fruit and corn stigma compound beverage according to claim 1, wherein in the step (5), a pasteurization method is adopted, wherein the pasteurization temperature is 60-80 ℃, and the pasteurization time is 20-60 min.
8. The emblic leafflower fruit and corn stigma compound beverage prepared by the preparation method of any one of claims 1 to 7.
9. The emblic leafflower fruit and corn stigma compound beverage as claimed in claim 8, is characterized by comprising the following components in parts by weight: 20-25 parts of phyllanthus emblica juice concentrated solution, 20-25 parts of corn stigma-mulberry leaf concentrated solution, 15-25 parts of sweetening agent and 3-8 parts of auxiliary materials; the sweetening agent is non-starch fructose, and the auxiliary material is a compound of pectin and carboxymethyl cellulose; wherein the weight ratio of pectin to carboxymethyl cellulose is as follows: pectin: carboxymethyl cellulose 2-5: 1 to 3.
10. The emblic leafflower fruit and corn stigma compound beverage as claimed in claim 9, is characterized by comprising the following components in parts by weight: 20 parts of emblic leafflower fruit juice concentrated solution, 25 parts of corn stigma-mulberry leaf concentrated solution, 15 parts of sweetening agent and 5 parts of auxiliary material; wherein the weight ratio of pectin to carboxymethyl cellulose is as follows: pectin: carboxymethyl cellulose ═ 4: 1.
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