CN112252027A - 一种负离子保健内衣的制备方法 - Google Patents
一种负离子保健内衣的制备方法 Download PDFInfo
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- CN112252027A CN112252027A CN202011177372.3A CN202011177372A CN112252027A CN 112252027 A CN112252027 A CN 112252027A CN 202011177372 A CN202011177372 A CN 202011177372A CN 112252027 A CN112252027 A CN 112252027A
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- VCJMYUPGQJHHFU-UHFFFAOYSA-N iron(3+);trinitrate Chemical compound [Fe+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O VCJMYUPGQJHHFU-UHFFFAOYSA-N 0.000 claims description 20
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- KBJMLQFLOWQJNF-UHFFFAOYSA-N nickel(ii) nitrate Chemical compound [Ni+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O KBJMLQFLOWQJNF-UHFFFAOYSA-N 0.000 claims description 10
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- 229910052911 sodium silicate Inorganic materials 0.000 claims description 7
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 7
- 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 claims description 7
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 7
- 229920002554 vinyl polymer Polymers 0.000 claims description 7
- XMPZTFVPEKAKFH-UHFFFAOYSA-P ceric ammonium nitrate Chemical compound [NH4+].[NH4+].[Ce+4].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O XMPZTFVPEKAKFH-UHFFFAOYSA-P 0.000 claims description 6
- PVLBXNICXUCXTA-UHFFFAOYSA-N [2-hydroxy-3-(3-triethoxysilylpropylamino)propyl] prop-2-enoate Chemical compound CCO[Si](OCC)(OCC)CCCNCC(O)COC(=O)C=C PVLBXNICXUCXTA-UHFFFAOYSA-N 0.000 claims description 5
- INJVFBCDVXYHGQ-UHFFFAOYSA-N n'-(3-triethoxysilylpropyl)ethane-1,2-diamine Chemical group CCO[Si](OCC)(OCC)CCCNCCN INJVFBCDVXYHGQ-UHFFFAOYSA-N 0.000 claims description 5
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- ZXMGHDIOOHOAAE-UHFFFAOYSA-N 1,1,1-trifluoro-n-(trifluoromethylsulfonyl)methanesulfonamide Chemical compound FC(F)(F)S(=O)(=O)NS(=O)(=O)C(F)(F)F ZXMGHDIOOHOAAE-UHFFFAOYSA-N 0.000 description 4
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- ZATMQQFXKCSCSO-UHFFFAOYSA-N 2-(3-methylimidazol-3-ium-1-yl)acetate Chemical compound C[N+]=1C=CN(CC([O-])=O)C=1 ZATMQQFXKCSCSO-UHFFFAOYSA-N 0.000 description 2
- RZVHIXYEVGDQDX-UHFFFAOYSA-N 9,10-anthraquinone Chemical group C1=CC=C2C(=O)C3=CC=CC=C3C(=O)C2=C1 RZVHIXYEVGDQDX-UHFFFAOYSA-N 0.000 description 2
- RAXXELZNTBOGNW-UHFFFAOYSA-O Imidazolium Chemical compound C1=C[NH+]=CN1 RAXXELZNTBOGNW-UHFFFAOYSA-O 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 2
- 150000001408 amides Chemical class 0.000 description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
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- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 2
- 230000008054 signal transmission Effects 0.000 description 2
- 229910000077 silane Inorganic materials 0.000 description 2
- 238000004381 surface treatment Methods 0.000 description 2
- 229910052684 Cerium Inorganic materials 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 1
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
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- 230000003862 health status Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000002329 infrared spectrum Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 238000000554 physical therapy Methods 0.000 description 1
- FZHAPNGMFPVSLP-UHFFFAOYSA-N silanamine Chemical compound [SiH3]N FZHAPNGMFPVSLP-UHFFFAOYSA-N 0.000 description 1
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/80—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides
- D06M11/82—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides with boron oxides; with boric, meta- or perboric acids or their salts, e.g. with borax
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- D01F1/00—General methods for the manufacture of artificial filaments or the like
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- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
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Abstract
本发明涉及纺织品制备领域,具体关于一种负离子保健内衣的制备方法;包括:基础面料的制备,浸扎处理,负离子负载和裁剪制衣等步骤;本发明有多种复合面料制备的基础面料具有弹性好,柔软性好的有限,是一种适合用在内衣上的面料,本发明的内衣具有优异的负离子保健功能,且耐水洗,负离子功能经过多次水洗也不会明显下降。
Description
技术领域
本发明涉及纺织品制备领域,尤其是一种负离子保健内衣的制备方法。
背景技术
随着消费者生活水平的不断提高,内衣作为直接接触皮肤的衣物,气功能性和舒适性越来越受到人们的关注。
CN110678091A公开了一种功能型内衣(1)具有包括左胸部覆盖部(111)和右胸部覆盖部(112)的胸部覆盖部(11)和包括左背部覆盖部(21)和右背部覆盖部(22)的背部覆盖部。左胸部覆盖部(111)覆盖从穿着者的左侧的乳房的下缘至左肩的区域,且由能够在连接该穿着者的心窝和左肩的方向上伸缩的伸缩材料形成,右胸部覆盖部(112)覆盖从穿着者的右侧的乳房的下缘至右肩的区域,且由能够在连接该穿着者的心窝和右肩的方向上伸缩的伸缩材料形成。左背部覆盖部(21)隔着穿着者的上半身与所述左胸部覆盖部(111)相对,且由能够在与该左胸部覆盖部(111)的能够伸缩的方向相同的方向上伸缩的伸缩材料形成,右背部覆盖部(22)隔着穿着者的上半身与右胸部覆盖部(112)相对,且由能够在与该右胸部覆盖部(112)的能够伸缩的方向相同的方向上伸缩的伸缩材料形成。左胸部覆盖部(111)和右胸部覆盖部(112)在下部重叠,左背部覆盖部(21)和右背部覆盖部(22)在下部重叠。
CN111358063A公开了一种多功能内衣,包括内衣本体,所述内衣本体设有内层和外层,所述内层布置心音检测模块和肺音检测模块,所述心音检测模块的检测触点位于内层贴合心脏处,所述肺音检测模块的检测触点分别位于内层的前后侧,所述心音检测模块的检测触点、所述肺音检测模块的检测触点均与信号采集模块连接,所述信号采集模块与信号传输模块连接;同时所述心音检测模块的检测触点、所述肺音检测模块的检测触点均与用于将心音和肺音放大的扩音模块连接,所述扩音模块的输出端与振动发电模块的能量收集端连接,所述振动发电模块的输出与供电单元连接,所述信号采集模块和信号传输模块均与所述供电单元连接。该发明方便、快捷地监测人体健康状态、使用方便。
CN101653293B提供一种功能型内衣,所有体型的人都可以完全适合个人的体型并且舒适地穿着。本发明的功能性内衣,其特征在于:由具备左右罩杯部的胸衣部、正面部、后背部构成,整体由具有伸缩性的材料构成,胸衣部具有自左右各罩杯部的下缘的周围向下方延伸设计的伸缩部,正面部的上缘形成为沿着罩杯部的下缘的形状,正面部的上部重叠于伸缩部之上,正面部的上缘的、沿各罩杯部的下缘部分的两端处与各罩杯部的下缘的对应的端部结合而形成。
负离子能够增强新陈代谢和免疫力负离子可提高人体氧气转化能力,加速新陈代谢,使人心情舒畅,产生理疗作用,可增强多种酶的活性,提高免疫力等多重保健功能,目前市场上也有一些具有负离子保健功能的内衣上市,但是其耐久性差,往往经过几次洗涤后就失去了负离子功能,起到的保健作用有限。
发明内容
为了解决上述问题,本发明提供了一种负离子保健内衣的制备方法。
一种负离子保健内衣的制备方法,其制备步骤为:
步骤一,基础面料的制备:按照质量份数,将0.2-0.6份的锦纶纤维、0.1-0.4份的复合弹性纤维、0.05-0.3份的羊绒纤维、0.4-0.9份的聚酯纤维经过混纺得到基础面料;所述的复合弹性纤维中的组分包括65%-75%的丁烯/乙烯/苯乙烯共聚物,10%-14%的低密度聚乙烯,5%-10%的乙烯基聚二甲基硅氧烷和添加剂;
步骤二,浸扎处理:将基础面料放入浸扎液中进行浸扎处理,所述的浸扎液内含有0.8-1.6g/L的硅酸钠,0.01-0.08g/L的硫酸氢钾,0.3-0.7g/L石油磺酸钠;控温75-85℃下浸扎处理,一浸一扎处理之后通过烘箱在110-120℃下烘干;
步骤三,负离子负载:将浸扎好的基础面料放入到负离子负载剂中,控温60-80℃,处理10-30min,然后在80-100℃下烘干,即可得到负载负离子面料;
步骤四,裁剪制衣,将得到负载负离子面料经过设计裁剪后制成内衣,即可得到所述的一种负离子保健内衣。
所述的负离子负载剂为一种改性电气石粉体分散液,其制备方法如下:
步骤一:按照质量份数,将25-38份的电气石粉体分散到150-180份的金属盐溶液中,所述的金属盐溶液中含有0.1-0.3份的硝酸铁,0.05-0.2份的硝酸镍,0.01-0.08份的硝酸铈铵和0.05-0.15份的硝酸铜,混合均匀后加热到80-100℃,在搅拌下将溶液蒸干,得到的固体在400-600℃煅烧60-180min,然后冷却到室温后将得到的固体和0.5-1.4份的偶联剂混合后控温60-80℃研磨5-10h,完成后用乙醇洗涤粉末,然后干燥后将粉末分散到分散到200-500份的乙醇中,
步骤二:在氮气保护下升温到60-70℃,将0.02-0.08份的1-羧甲基-3-甲基咪唑双(三氟甲烷磺酰)亚胺盐,2-6份的蒽醌-2-甲酸加入到反应釜中,保温回流反应90-180min,完成后过滤,乙醇洗涤后将得到的固体分散到去离子水中,控制固含量为2.8%-5.4%,并加入质量百分比浓度0.1%-0.5%分散剂三聚磷酸钠,搅拌混合均匀后即可得到所述的一种改性电气石粉体分散液。
所述的偶联剂为N-氨乙基-3-氨丙基三乙氧基硅烷或N-(3-丙烯酰氧基-2-羟丙基)-3-氨丙基三乙氧基硅烷。
所述的添加剂为三聚氰胺氰尿酸盐辐照敏化剂和2,8-二叔丁基-4-甲基苯酚抗氧化剂,其质量之比为1:1-1.5。
所述的添加剂的用量为0.5%-1.8%。
所述改性电气石粉体分散液,使用电气石粉体负载硝酸铁,硝酸镍,硝酸铈铵和硝酸铜,煅烧后为含有铁,镍,铈和铜的氧化物的复合材料。
经N-氨乙基-3-氨丙基三乙氧基硅烷或N-(3-丙烯酰氧基-2-羟丙基)-3-氨丙基三乙氧基硅烷表面处理,生成带有氨基的硅烷改性电气石粉体复合材料;
与1-羧甲基-3-甲基咪唑双(三氟甲烷磺酰)亚胺盐,蒽醌-2-甲酸的羧基生成酰胺,将咪唑双(三氟甲烷磺酰)亚胺盐,蒽醌官能团引入复到复合材料表面。其部分反应机理示意为:
所述的复合弹性纤维的制备方法是将各个组份混合均匀后挤出造粒得到母粒,然后在熔融纺丝机中纺成原丝纤维,然后将纤维在100-150kGy的辐照剂量下辐照处理。
所述的熔融纺丝法的纺丝温度为150-280℃。
本发明的一种负离子保健内衣的制备方法,本发明有多种复合面料制备的基础面料具有弹性好,柔软性好的有限,是一种适合用在内衣上的面料,本发明在面料经过在改性电气石粉体分散液浸渍后具备了优异的负离子功能,所述改性电气石粉体分散液,使用电气石粉体负载硝酸铁,硝酸镍,硝酸铈铵和硝酸铜,煅烧后为含有铁,镍,铈和铜的氧化物的复合材料。经氨基硅烷表面处理,生成带有氨基的硅烷改性电气石粉体复合材料;与1-羧甲基-3-甲基咪唑双(三氟甲烷磺酰)亚胺盐,蒽醌-2-甲酸的羧基生成酰胺,将咪唑双(三氟甲烷磺酰)亚胺盐,蒽醌官能团引入复到复合材料表面。能提供良好的负离子保健功能;本发明提供的改性电气石粉体分散液中的电气石粉经过金属氧化物的修饰后具有了更强的负离子功能,再经辐照改性的复合弹性纤维接枝,能牢牢的将电气石粉固定在织物上,起到耐水洗的作用;本发明的内衣具有优异的负离子保健功能,且耐水洗,负离子功能经过多次水洗也不会明显下降。
附图说明
图1为实施例3制备的改性电气石粉体分散液的付利叶红外光谱图;
在3385/1625cm-1附近存在水的吸收峰,说明水参与了反应;在925cm-1附近存在硅酸根离子的吸收峰,说明电气石粉体参与了反应;在1359/832cm-1附近存在硝酸根离子的反对称伸缩/面外弯曲吸收峰,说明硝酸铁、硝酸镍、硝酸铈铵、硝酸铜参与了反应;在3023/1408cm-1附近存在铵根离子的对称伸缩/不对称变角吸收峰,说明硝酸铈铵参与了反应;在1500cm-1附近存在苯环的吸收峰,在1752cm-1附近存在羰基的伸缩吸收峰,说明蒽醌-2-甲酸参与了反应。
具体实施方式
下面通过具体实施例对该发明作进一步说明:
在实施例和对比例中,本实验采用AIC-200离子测试仪,参照《空气离子测量仪通用规范》进行测试,每个试样测量50次求得平均值,并考查水洗10次后对织物的负离子释放量的影响。为防止空气流动对负离子测试准确性的影响,实验中搭建防风实验平台。
所述1-羧甲基-3-甲基咪唑双(三氟甲烷磺酰)亚胺盐,CAS号,671793-16-1。
实施例1
一种负离子保健内衣的制备方法,其制备步骤为:
步骤一,基础面料的制备:将0.2kg锦纶纤维、0.1kg复合弹性纤维、0.05kg羊绒纤维、0.4kg聚酯纤维经过混纺得到基础面料;所述的复合弹性纤维中的组分包括65%的丁烯/乙烯/苯乙烯共聚物,10%的低密度聚乙烯,5%的乙烯基聚二甲基硅氧烷和添加剂;
步骤二,浸扎处理:将基础面料放入浸扎液中进行浸扎处理,所述的浸扎液内含有0.8g/L的硅酸钠,0.01g/L的硫酸氢钾,0.3g/L石油磺酸钠;控温80℃下浸扎处理,一浸一扎处理之后通过烘箱在115℃下烘干;
步骤三,负离子负载:将浸扎好的基础面料放入到负离子负载剂中,控温70℃,处理20min,然后在90℃下烘干,即可得到负载负离子面料;
步骤四,裁剪制衣,将得到负载负离子面料经过设计裁剪后制成内衣,即可得到所述的一种负离子保健内衣。
所述的负离子负载剂为一种改性电气石粉体分散液,其制备方法如下:
步骤一:将25kg的电气石粉体分散到150kg的金属盐溶液中,所述的金属盐溶液中含有0.1kg的硝酸铁,0.05kg的硝酸镍,0.01kg的硝酸铈铵和0.05kg的硝酸铜,混合均匀后加热到80℃,在搅拌下将溶液蒸干,得到的固体在400℃煅烧60min,然后冷却到室温后将得到的固体和0.5kg的偶联剂混合后控温60℃研磨5h,完成后用乙醇洗涤粉末,然后干燥后将粉末分散到分散到200kg的乙醇中,
步骤二:在氮气保护下升温到60℃,将0.02kg的1-羧甲基-3-甲基咪唑双(三氟甲烷磺酰)亚胺盐,2kg的蒽醌-2-甲酸加入到反应釜中,保温回流反应90min,完成后过滤,乙醇洗涤后将得到的固体分散到去离子水中,控制固含量为2.8%,并加入质量百分比浓度0.1%分散剂三聚磷酸钠,搅拌混合均匀后即可得到所述的一种改性电气石粉体分散液。
所述的偶联剂为N-氨乙基-3-氨丙基三乙氧基硅烷。
所述的添加剂为三聚氰胺氰尿酸盐辐照敏化剂和2,8-二叔丁基-4-甲基苯酚抗氧化剂,其质量之比为1:1。
所述的添加剂的用量为0.5%。
所述的复合弹性纤维的制备方法是将各个组份混合均匀后挤出造粒得到母粒,然后在熔融纺丝机中纺成原丝纤维,然后将纤维在100kGy的辐照剂量下辐照处理。
所述的熔融纺丝法的纺丝温度为150℃。
实施例2
一种负离子保健内衣的制备方法,其制备步骤为:
步骤一,基础面料的制备:将0.4kg锦纶纤维、0.3kg复合弹性纤维、0.12kg羊绒纤维、0.6kg聚酯纤维经过混纺得到基础面料;所述的复合弹性纤维中的组分包括70%的丁烯/乙烯/苯乙烯共聚物,12%的低密度聚乙烯,8%的乙烯基聚二甲基硅氧烷和添加剂;
步骤二,浸扎处理:将基础面料放入浸扎液中进行浸扎处理,所述的浸扎液内含有1.2g/L的硅酸钠,0.04g/L的硫酸氢钾,0.5g/L石油磺酸钠;控温70℃下浸扎处理,一浸一扎处理之后通过烘箱在115℃下烘干;
步骤三,负离子负载:将浸扎好的基础面料放入到负离子负载剂中,控温70℃,处理20min,然后在90℃下烘干,即可得到负载负离子面料;
步骤四,裁剪制衣,将得到负载负离子面料经过设计裁剪后制成内衣,即可得到所述的一种负离子保健内衣。
所述的负离子负载剂为一种改性电气石粉体分散液,其制备方法如下:
步骤一:将27kg的电气石粉体分散到160kg的金属盐溶液中,所述的金属盐溶液中含有0.2kg的硝酸铁,0.07kg的硝酸镍,0.03kg的硝酸铈铵和0.1kg的硝酸铜,混合均匀后加热到85℃,在搅拌下将溶液蒸干,得到的固体在460℃煅烧80min,然后冷却到室温后将得到的固体和0.7kg的偶联剂混合后控温65℃研磨7h,完成后用乙醇洗涤粉末,然后干燥后将粉末分散到分散到300kg的乙醇中,
步骤二:在氮气保护下升温到63℃,将0.03kg的1-羧甲基-3-甲基咪唑双(三氟甲烷磺酰)亚胺盐,3kg的蒽醌-2-甲酸加入到反应釜中,保温回流反应110min,完成后过滤,乙醇洗涤后将得到的固体分散到去离子水中,控制固含量为3.1%,并加入质量百分比浓度0.2%分散剂三聚磷酸钠,搅拌混合均匀后即可得到所述的一种改性电气石粉体分散液。
所述的偶联剂为N-(3-丙烯酰氧基-2-羟丙基)-3-氨丙基三乙氧基硅烷。
所述的添加剂为三聚氰胺氰尿酸盐辐照敏化剂和2,8-二叔丁基-4-甲基苯酚抗氧化剂,其质量之比为1:1.2。
所述的添加剂的用量为1.2%。
所述的复合弹性纤维的制备方法是将各个组份混合均匀后挤出造粒得到母粒,然后在熔融纺丝机中纺成原丝纤维,然后将纤维在120kGy的辐照剂量下辐照处理。
所述的熔融纺丝法的纺丝温度为220℃。
实施例3
一种负离子保健内衣的制备方法,其制备步骤为:
步骤一,基础面料的制备:将0.6kg锦纶纤维、0.4kg复合弹性纤维、0.3kg羊绒纤维、0.9kg聚酯纤维经过混纺得到基础面料;所述的复合弹性纤维中的组分包括75%的丁烯/乙烯/苯乙烯共聚物,14%的低密度聚乙烯,10%的乙烯基聚二甲基硅氧烷和添加剂;
步骤二,浸扎处理:将基础面料放入浸扎液中进行浸扎处理,所述的浸扎液内含有1.6g/L的硅酸钠,0.08g/L的硫酸氢钾,0.7g/L石油磺酸钠;控温85℃下浸扎处理,一浸一扎处理之后通过烘箱在120℃下烘干;
步骤三,负离子负载:将浸扎好的基础面料放入到负离子负载剂中,控温80℃,处理30min,然后在100℃下烘干,即可得到负载负离子面料;
步骤四,裁剪制衣,将得到负载负离子面料经过设计裁剪后制成内衣,即可得到所述的一种负离子保健内衣。
所述的负离子负载剂为一种改性电气石粉体分散液,其制备方法如下:
步骤一:将31kg的电气石粉体分散到170kg的金属盐溶液中,所述的金属盐溶液中含有0.22kg的硝酸铁,0.13kg的硝酸镍,0.07kg的硝酸铈铵和0.11kg的硝酸铜,混合均匀后加热到100℃,在搅拌下将溶液蒸干,得到的固体在500℃煅烧160min,然后冷却到室温后将得到的固体和0.9kg的偶联剂混合后控温70℃研磨9h,完成后用乙醇洗涤粉末,然后干燥后将粉末分散到分散到400kg的乙醇中,
步骤二:在氮气保护下升温到68℃,将0.07kg的1-羧甲基-3-甲基咪唑双(三氟甲烷磺酰)亚胺盐,5kg的蒽醌-2-甲酸加入到反应釜中,保温回流反应170min,完成后过滤,乙醇洗涤后将得到的固体分散到去离子水中,控制固含量为5.1%,并加入质量百分比浓度0.4%分散剂三聚磷酸钠,搅拌混合均匀后即可得到所述的一种改性电气石粉体分散液。
所述的偶联剂为N-(3-丙烯酰氧基-2-羟丙基)-3-氨丙基三乙氧基硅烷。
所述的添加剂为三聚氰胺氰尿酸盐辐照敏化剂和2,8-二叔丁基-4-甲基苯酚抗氧化剂,其质量之比为1:1.5。
所述的添加剂的用量为1.8%。
所述的复合弹性纤维的制备方法是将各个组份混合均匀后挤出造粒得到母粒,然后在熔融纺丝机中纺成原丝纤维,然后将纤维在150kGy的辐照剂量下辐照处理。
所述的熔融纺丝法的纺丝温度为280℃。
实施例4
一种负离子保健内衣的制备方法,其制备步骤为:
步骤一,基础面料的制备:将0.6kg锦纶纤维、0.4kg复合弹性纤维、0.3kg羊绒纤维、0.9kg聚酯纤维经过混纺得到基础面料;所述的复合弹性纤维中的组分包括75%的丁烯/乙烯/苯乙烯共聚物,14%的低密度聚乙烯,10%的乙烯基聚二甲基硅氧烷和添加剂;
步骤二,浸扎处理:将基础面料放入浸扎液中进行浸扎处理,所述的浸扎液内含有1.6g/L的硅酸钠,0.08g/L的硫酸氢钾,0.7g/L石油磺酸钠;控温85℃下浸扎处理,一浸一扎处理之后通过烘箱在120℃下烘干;
步骤三,负离子负载:将浸扎好的基础面料放入到负离子负载剂中,控温80℃,处理30min,然后在100℃下烘干,即可得到负载负离子面料;
步骤四,裁剪制衣,将得到负载负离子面料经过设计裁剪后制成内衣,即可得到所述的一种负离子保健内衣。
所述的负离子负载剂为一种改性电气石粉体分散液,其制备方法如下:
步骤一:将38kg的电气石粉体分散到180kg的金属盐溶液中,所述的金属盐溶液中含有0.3kg的硝酸铁,0.2kg的硝酸镍,0.08kg的硝酸铈铵和0.15kg的硝酸铜,混合均匀后加热到100℃,在搅拌下将溶液蒸干,得到的固体在600℃煅烧180min,然后冷却到室温后将得到的固体和1.4kg的偶联剂混合后控温80℃研磨10h,完成后用乙醇洗涤粉末,然后干燥后将粉末分散到分散到500kg的乙醇中,
步骤二:在氮气保护下升温到70℃,将0.08kg的1-羧甲基-3-甲基咪唑双(三氟甲烷磺酰)亚胺盐,6kg的蒽醌-2-甲酸加入到反应釜中,保温回流反应180min,完成后过滤,乙醇洗涤后将得到的固体分散到去离子水中,控制固含量为5.4%,并加入质量百分比浓度0.5%分散剂三聚磷酸钠,搅拌混合均匀后即可得到所述的一种改性电气石粉体分散液。
所述的偶联剂为N-氨乙基-3-氨丙基三乙氧基硅烷。
所述的添加剂为三聚氰胺氰尿酸盐辐照敏化剂和2,8-二叔丁基-4-甲基苯酚抗氧化剂,其质量之比为1:1。
所述的添加剂的用量为0.5%。
所述的复合弹性纤维的制备方法是将各个组份混合均匀后挤出造粒得到母粒,然后在熔融纺丝机中纺成原丝纤维,然后将纤维在100kGy的辐照剂量下辐照处理。
所述的熔融纺丝法的纺丝温度为150℃。
以上实施例制备的织物的负离子浓度和水洗后负离子下降率,其结果统计结果如下:
编号 | 负离子浓度(个/cm<sup>3</sup>) | 负离子下降率(%) |
实施例1 | 3421 | 2.61 |
实施例2 | 3627 | 1.25 |
实施例3 | 3728 | 0.57 |
实施例4 | 3596 | 0.93 |
对比例1
所述的负离子负载剂为一种改性电气石粉体分散液,其制备方法如下:
步骤一:将25kg的电气石粉体分散到150kg的金属盐溶液中,所述的金属盐溶液中含有0.1kg的硝酸铁,0.05kg的硝酸镍,0.01kg的硝酸铈铵和0.05kg的硝酸铜,混合均匀后加热到80℃,在搅拌下将溶液蒸干,得到的固体在400℃煅烧60min,然后冷却到室温后将得到的固体和0.5kg的偶联剂混合后控温60℃研磨5h,完成后用乙醇洗涤粉末,然后干燥后将粉末分散到分散到200kg的乙醇中,
步骤二:在氮气保护下升温到60℃,2kg的蒽醌-2-甲酸加入到反应釜中,保温回流反应90min,完成后过滤,乙醇洗涤后将得到的固体分散到去离子水中,控制固含量为2.8%,并加入质量百分比浓度0.1%分散剂三聚磷酸钠,搅拌混合均匀后即可得到所述的一种改性电气石粉体分散液。
其它技术方案与实施例1相同。
对比例2
所述的负离子负载剂为一种改性电气石粉体分散液,其制备方法如下:
步骤一:将25kg的电气石粉体分散到150kg的金属盐溶液中,所述的金属盐溶液中含有0.1kg的硝酸铁,0.05kg的硝酸镍,0.01kg的硝酸铈铵和0.05kg的硝酸铜,混合均匀后加热到80℃,在搅拌下将溶液蒸干,得到的固体在400℃煅烧60min,然后冷却到室温后将得到的固体和0.5kg的偶联剂混合后控温60℃研磨5h,完成后用乙醇洗涤粉末,然后干燥后将粉末分散到分散到200kg的乙醇中,
步骤二:在氮气保护下升温到60℃,将0.02kg的1-羧甲基-3-甲基咪唑双(三氟甲烷磺酰)亚胺盐加入到反应釜中,保温回流反应90min,完成后过滤,乙醇洗涤后将得到的固体分散到去离子水中,控制固含量为2.8%,并加入质量百分比浓度0.1%分散剂三聚磷酸钠,搅拌混合均匀后即可得到所述的一种改性电气石粉体分散液。
其它技术方案与实施例1相同。
对比例3
一种负离子保健内衣的制备方法,其制备步骤为:
步骤一,基础面料的制备:将0.2kg锦纶纤维、0.1kg复合弹性纤维、0.05kg羊绒纤维、0.4kg聚酯纤维经过混纺得到基础面料;所述的复合弹性纤维中的组分包括65%的丁烯/乙烯/苯乙烯共聚物,10%的低密度聚乙烯,5%的乙烯基聚二甲基硅氧烷和添加剂;
步骤二,浸扎处理:将基础面料放入浸扎液中进行浸扎处理,所述的浸扎液内含有0.8g/L的硅酸钠,0.01g/L的硫酸氢钾,0.3g/L石油磺酸钠;控温80℃下浸扎处理,一浸一扎处理之后通过烘箱在115℃下烘干;
步骤三,裁剪制衣,将得到负载负离子面料经过设计裁剪后制成内衣,即可得到所述的一种负离子保健内衣。
所述的添加剂为三聚氰胺氰尿酸盐辐照敏化剂和2,8-二叔丁基-4-甲基苯酚抗氧化剂,其质量之比为1:1。
所述的添加剂的用量为0.5%。
所述的复合弹性纤维的制备方法是将各个组份混合均匀后挤出造粒得到母粒,然后在熔融纺丝机中纺成原丝纤维,然后将纤维在100kGy的辐照剂量下辐照处理。
所述的熔融纺丝法的纺丝温度为150℃。
以上对比例制备的织物的负离子浓度和水洗后负离子下降率,其结果统计结果如下:
编号 | 负离子浓度(个/cm<sup>3</sup>) | 负离子下降率(%) |
对比例1 | 2847 | 7.84 |
对比例2 | 2657 | 8.36 |
对比例3 | 1175 | 22.73 |
Claims (7)
1.一种负离子保健内衣的制备方法,其制备步骤为:
步骤一,基础面料的制备:按照质量份数,将0.2-0.6份的锦纶纤维、0.1-0.4份的复合弹性纤维、0.05-0.3份的羊绒纤维、0.4-0.9份的聚酯纤维经过混纺得到基础面料;所述的复合弹性纤维中的组分包括65%-75%的丁烯/乙烯/苯乙烯共聚物,10%-14%的低密度聚乙烯,5%-10%的乙烯基聚二甲基硅氧烷和添加剂;
步骤二,浸扎处理:将基础面料放入浸扎液中进行浸扎处理,所述的浸扎液内含有0.8-1.6g/L的硅酸钠,0.01-0.08g/L的硫酸氢钾,0.3-0.7g/L石油磺酸钠;控温75-85℃下浸扎处理,一浸一扎处理之后通过烘箱在110-120℃下烘干;
步骤三,负离子负载:将浸扎好的基础面料放入到负离子负载剂中,控温60-80℃,处理10-30min,然后在80-100℃下烘干,即可得到负载负离子面料;
步骤四,裁剪制衣,将得到负载负离子面料经过设计裁剪后制成内衣,即可得到所述的一种负离子保健内衣。
2.根据权利要求1所述的一种负离子保健内衣的制备方法,其特征在于:所述的负离子负载剂为一种改性电气石粉体分散液,其制备方法如下:
步骤一:按照质量份数,将25-38份的电气石粉体分散到150-180份的金属盐溶液中,所述的金属盐溶液中含有0.1-0.3份的硝酸铁,0.05-0.2份的硝酸镍,0.01-0.08份的硝酸铈铵和0.05-0.15份的硝酸铜,混合均匀后加热到80-100℃,在搅拌下将溶液蒸干,得到的固体在400-600℃煅烧60-180min,然后冷却到室温后将得到的固体和0.5-1.4份的偶联剂混合后控温60-80℃研磨5-10h,完成后用乙醇洗涤粉末,然后干燥后将粉末分散到分散到200-500份的乙醇中,
步骤二:在氮气保护下升温到60-70℃,将0.02-0.08份的1-羧甲基-3-甲基咪唑双(三氟甲烷磺酰)亚胺盐,2-6份的蒽醌-2-甲酸加入到反应釜中,保温回流反应90-180min,完成后过滤,乙醇洗涤后将得到的固体分散到去离子水中,控制固含量为2.8%-5.4%,并加入质量百分比浓度0.1%-0.5%分散剂三聚磷酸钠,搅拌混合均匀后即可得到所述的一种改性电气石粉体分散液。
3.根据权利要求2所述的一种负离子保健内衣的制备方法,其特征在于:所述的偶联剂为N-氨乙基-3-氨丙基三乙氧基硅烷或N-(3-丙烯酰氧基-2-羟丙基)-3-氨丙基三乙氧基硅烷。
4.根据权利要求1所述的一种负离子保健内衣的制备方法,其特征在于:所述的添加剂为三聚氰胺氰尿酸盐辐照敏化剂和2,8-二叔丁基-4-甲基苯酚抗氧化剂,其质量之比为1:1-1.5。
5.根据权利要求1所述的一种负离子保健内衣的制备方法,其特征在于:所述的添加剂的用量为0.5%-1.8%。
6.根据权利要求1所述的一种负离子保健内衣的制备方法,其特征在于:所述的复合弹性纤维的制备方法是将各个组份混合均匀后挤出造粒得到母粒,然后在熔融纺丝机中纺成原丝纤维,然后将纤维在100-150kGy的辐照剂量下辐照处理。
7.根据权利要求1所述的一种负离子保健内衣的制备方法,其特征在于:所述的熔融纺丝法的纺丝温度为150-280℃。
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CN115073146A (zh) * | 2022-06-10 | 2022-09-20 | 贵州群华九九特种陶瓷科技有限公司 | 一种可释放负氧离子的陶瓷及其制备方法、茶具 |
CN115073146B (zh) * | 2022-06-10 | 2023-08-22 | 贵州群华九九特种陶瓷科技有限公司 | 一种可释放负氧离子的陶瓷及其制备方法、茶具 |
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