CN112194911A - Novel color aluminum tube pigment on ceramic glaze and preparation method thereof - Google Patents
Novel color aluminum tube pigment on ceramic glaze and preparation method thereof Download PDFInfo
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- CN112194911A CN112194911A CN201910610266.0A CN201910610266A CN112194911A CN 112194911 A CN112194911 A CN 112194911A CN 201910610266 A CN201910610266 A CN 201910610266A CN 112194911 A CN112194911 A CN 112194911A
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- aluminum tube
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/0009—Pigments for ceramics
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/08—Treatment with low-molecular-weight non-polymer organic compounds
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- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Abstract
The invention provides a new color aluminum tube pigment on ceramic glaze and a preparation method thereof, wherein the new color aluminum tube pigment is a product obtained by blending inorganic mineral pigment powder and oil material according to the proportion of 1:2, wherein the inorganic mineral pigment powder is prepared by mineral separation, crushing, grinding and grading of natural ores; the oil material is selected from mastic oil. The mastic oil is put into a stirrer to be stirred, and then the inorganic mineral pigment powder is slowly added to be blended and stirred until the mastic oil is saturated; filling the saturated cream-like mixture into an aluminum tube, sealing with a sealing machine, sealing, storing, and selling. The invention mixes and grinds the new color mineral pigment powder and the oil material on the ceramic glaze according to the corresponding proportion, and then the mixture is put into an aluminum tube for sealed sale, thereby reducing the resource waste caused by that the raw materials are dried and cracked and can not be used because of being placed outside for a long time.
Description
Technical Field
The invention belongs to the technical field of ceramic glazing, and particularly relates to a novel aluminum tube pigment on ceramic glazing and a preparation method thereof.
Background
The ceramic decorative pigment is rich, and has underglaze blue and white, high temperature colored glaze, and overglaze pink, ancient color and new color, especially new color pigment. The three categories of decoration, including overglaze decoration, underglaze decoration and in-glaze decoration, are technically described. The new color decoration of ceramics also draws high attention of people, and the application of the new color is gradually wide.
The new color is a glaze low-temperature pigment, and the new color decoration is a product obtained by drawing on a porcelain white body by using the low-temperature new color pigment and then placing the porcelain white body into a cellar for sintering at the temperature of about 700-. The low-temperature pigment is stable in ceramic technology, so that the ceramic glaze has rich colors and can basically meet the requirements of special painting. The new color is prepared with mainly powdered colorant and solvent, the colorant is mainly the mixture of various metal oxides, and the mixture is calcined into color-forming mineral matter, and the solvent is one kind of low temperature vitreous adhesive and is molten at 800 deg.c and 700 deg.c. The low-temperature pigment has rich colors and better stability than other colors, so that the picture color in color drawing can be expressed at will, like drawing on paper, the influence of color change after firing is not considered, so that the new color is more complete in variety than ancient colors, pink colors and other underglaze colors, and can be mutually blended to better meet the color requirement of the picture, and meanwhile, if a certain foundation is provided for the ceramic process, a plurality of colors can be repeatedly matched for a plurality of times to obtain more colors. Because of the rich color of the new color, the characteristics of fineness and elegance of the color material are increased, various modern decorative patterns and patterns can be drawn, and the new color can better represent various subject matters.
In the prior art, mineral pigments are obtained by directly grinding mineral substances into powder for sale, and have the disadvantages of easy waste, poor safety factor, environmental pollution and more time waste due to grinding materials.
The mastic oil is prepared by distilling mastic resin secreted by mastic tree of boswellia of Burseraceae with steam, and has relative density of 0.865-0.917, refractive index of 1.469-1.483, blooming luminosity of-15 to +35 (25 deg.C), acid value of less than =4.0, and main components including terpene, levogyration camphor, p-cymene, dipentene, etc. and can be used for preparation and food essence. The mastic oil is also one of main oil materials for color matching of the painted porcelain, has soft and moist property, certain viscosity and difficult drying, and does not influence the color generation of the pigment.
Disclosure of Invention
Aiming at the defects in the prior art, the invention provides a novel color aluminum tube pigment on ceramic glaze and a preparation method thereof.
In order to achieve the purpose, the technical scheme of the invention is as follows:
a new color aluminum tube pigment on ceramic glaze is a product obtained by blending inorganic mineral pigment powder and oil according to the proportion of 1:2, wherein the inorganic mineral pigment powder is prepared by mineral separation, crushing, grinding and grading of natural ores; the oil material is selected from mastic oil.
Further, the varieties of the inorganic mineral pigment powder comprise: yellow red, black red, verdant, verdigris, red lead, white lead, black lead and the like.
The invention also provides a preparation method of the novel color aluminum tube pigment on the ceramic glaze, which comprises the following steps:
(1) selecting natural ore with heavy color and high grade, feeding the natural ore into a crusher, continuously crushing the natural ore into mineral particles with the diameter of 0.1-0.3 mm, feeding the mineral particles into a ball mill, wherein ball mills are zirconia grinding balls with the diameter of 1-5 mm, the mass ratio of ball materials is 30-40: 1, the rotating speed of the ball mill is 200-350 r/min, and the ball milling time is 10-48 hours, so as to obtain fine powder; classifying to obtain 20-35 micron fine powder, and drying the classified fine powder at 80-150 ℃ for 5-8 hours to obtain inorganic mineral pigment powder;
(2) weighing inorganic mineral pigment powder and mastic oil according to the proportion of 1:2, placing mastic oil into a stirrer, stirring, slowly adding the inorganic mineral pigment powder obtained in the step (1), blending and stirring to obtain a saturated cream-shaped mixture;
(3) and (3) filling the saturated cream mixture obtained in the step (2) into an aluminum tube, sealing the aluminum tube by using a sealing machine, sealing, storing and selling.
Has the advantages that: the invention mixes and grinds the new color mineral pigment powder and the oil material on the ceramic glaze according to the corresponding proportion, and then the mixture is put into an aluminum tube for sealed sale, thereby reducing the resource waste caused by that the raw materials are dried and cracked and can not be used because of being placed outside for a long time.
Detailed Description
The invention is illustrated below with reference to specific examples. It will be understood by those skilled in the art that these examples are for illustrative purposes only and are not intended to limit the scope of the present invention in any way.
Example 1
A new color aluminum tube pigment on ceramic glaze is a product obtained by blending inorganic mineral pigment powder and oil according to the proportion of 1:2, wherein the inorganic mineral pigment powder is prepared by mineral separation, crushing, grinding and grading of natural ores; the oil material is selected from mastic oil; the inorganic mineral pigment powder comprises the following varieties: yellow red, black red, verdant, verdigris, red lead, white lead, black lead and the like.
Example 2
A preparation method of a new color aluminum tube pigment on ceramic glaze comprises the following steps:
(1) selecting natural ore with heavy color and high grade, sending the natural ore into a crusher, continuously crushing the natural ore into mineral particles with the diameter of 0.2 mm, sending the mineral particles into a ball mill, wherein ball grinders are zirconia grinding balls with the diameter of 1-5 mm, the mass ratio of ball materials is 35:1, the rotating speed of the ball mill is 300 r/min, and the ball milling time is 30 hours, so as to obtain fine powder; classifying to obtain fine powder of 20-35 microns, and drying the classified fine powder for 6 hours at the temperature of 100 ℃ to obtain inorganic mineral pigment powder;
(2) weighing inorganic mineral pigment powder and mastic oil according to the proportion of 1:2, placing mastic oil into a stirrer, stirring, slowly adding the inorganic mineral pigment powder obtained in the step (1), blending and stirring to obtain a saturated cream-shaped mixture;
(3) and (3) filling the saturated cream mixture obtained in the step (2) into an aluminum tube, sealing the aluminum tube by using a sealing machine, sealing, storing and selling.
Example 3
A preparation method of a new color aluminum tube pigment on ceramic glaze comprises the following steps:
(1) selecting natural ore with heavy color and high grade, sending the natural ore into a crusher, continuously crushing the natural ore into mineral particles with the diameter of 0.1 mm, sending the mineral particles into a ball mill, wherein ball grinders are zirconia grinding balls with the diameter of 1-5 mm, the mass ratio of ball materials is 30:1, the rotating speed of the ball mill is 350 r/min, and the ball milling time is 10 hours, so as to obtain fine powder; classifying to obtain fine powder of 20-35 microns, and drying the classified fine powder for 5 hours at the temperature of 100 ℃ to obtain inorganic mineral pigment powder;
(2) weighing inorganic mineral pigment powder and mastic oil according to the proportion of 1:2, placing mastic oil into a stirrer, stirring, slowly adding the inorganic mineral pigment powder obtained in the step (1), blending and stirring to obtain a saturated cream-shaped mixture;
(3) and (3) filling the saturated cream mixture obtained in the step (2) into an aluminum tube, sealing the aluminum tube by using a sealing machine, sealing, storing and selling.
Example 4
A preparation method of a new color aluminum tube pigment on ceramic glaze comprises the following steps:
(1) selecting natural ore with heavy color and high grade, sending the natural ore into a crusher, continuously crushing the natural ore into mineral particles with the diameter of 0.3 mm, sending the mineral particles into a ball mill, wherein ball grinders are zirconia grinding balls with the diameter of 1-5 mm, the mass ratio of ball materials is 40:1, the rotating speed of the ball mill is 200 r/min, and the ball milling time is 48 hours, so that fine powder is obtained; classifying to obtain fine powder of 20-35 microns, and drying the classified fine powder for 8 hours at the temperature of 100 ℃ to obtain inorganic mineral pigment powder;
(2) weighing inorganic mineral pigment powder and mastic oil according to the proportion of 1:2, placing mastic oil into a stirrer, stirring, slowly adding the inorganic mineral pigment powder obtained in the step (1), blending and stirring to obtain a saturated cream-shaped mixture;
(3) and (3) filling the saturated cream mixture obtained in the step (2) into an aluminum tube, sealing the aluminum tube by using a sealing machine, sealing, storing and selling.
Claims (3)
1. A new color aluminum tube pigment on ceramic glaze is characterized in that: the product is obtained by blending inorganic mineral pigment powder and oil material which are obtained by mineral separation, crushing, grinding and grading of natural ore according to the proportion of 1: 2; the oil material is selected from mastic oil.
2. The ceramic over-glaze new color aluminum tube pigment of claim 1, wherein: the inorganic mineral pigment powder comprises the following varieties: yellow red, black red, verdant, verdigris, red lead, white lead, black lead and the like.
3. A method for preparing a new color aluminum tube pigment on ceramic glaze according to any one of claims 1 or 2, characterized in that: the method comprises the following steps:
(1) selecting natural ore with heavy color and high grade, feeding the natural ore into a crusher, continuously crushing the natural ore into mineral particles with the diameter of 0.1-0.3 mm, feeding the mineral particles into a ball mill, wherein ball mills are zirconia grinding balls with the diameter of 1-5 mm, the mass ratio of ball materials is 30-40: 1, the rotating speed of the ball mill is 200-350 r/min, and the ball milling time is 10-48 hours, so as to obtain fine powder; classifying to obtain 20-35 micron fine powder, and drying the classified fine powder at 80-150 ℃ for 5-8 hours to obtain inorganic mineral pigment powder;
(2) weighing inorganic mineral pigment powder and mastic oil according to the proportion of 1:2, placing mastic oil into a stirrer, stirring, slowly adding the inorganic mineral pigment powder obtained in the step (1), blending and stirring to obtain a saturated cream-shaped mixture;
(3) and (3) filling the saturated cream mixture obtained in the step (2) into an aluminum tube, sealing the aluminum tube by using a sealing machine, sealing, storing and selling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201910610266.0A CN112194911A (en) | 2019-07-08 | 2019-07-08 | Novel color aluminum tube pigment on ceramic glaze and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910610266.0A CN112194911A (en) | 2019-07-08 | 2019-07-08 | Novel color aluminum tube pigment on ceramic glaze and preparation method thereof |
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| CN112194911A true CN112194911A (en) | 2021-01-08 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112903400A (en) * | 2021-01-13 | 2021-06-04 | 河南中博生物塑化科技有限公司 | Method for dyeing blood vessels and nerves of human plasticized specimen |
Citations (8)
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|---|---|---|---|---|
| CN88100123A (en) * | 1988-01-16 | 1988-10-12 | 江西省科学院能源研究所 | Cheap solar energy vacuum heat-collecting tube and manufacture method thereof |
| CN2037452U (en) * | 1988-09-30 | 1989-05-10 | 江西省科学院能源研究所 | Effective vacuum tuber solar water heater |
| CN1091763A (en) * | 1994-02-22 | 1994-09-07 | 蒋采苹 | A kind of pigment paste of the usefulness of painting and piece and working method thereof |
| CN103242062A (en) * | 2013-04-25 | 2013-08-14 | 湖南醴陵元诏瓷业有限公司 | Technological process for decoration and repair of paint with five colors under glaze |
| CN104446344A (en) * | 2014-11-01 | 2015-03-25 | 景德镇景浮宫陶瓷文化有限公司 | Preparation method of slim mirror-plane artistic porcelain painting and product prepared by preparation method |
| CN105753465A (en) * | 2016-01-24 | 2016-07-13 | 伍剑峰 | Method of making ceramic super-flat mirror art mural and product made thereby |
| CN107523096A (en) * | 2017-08-16 | 2017-12-29 | 醴陵市精陶瓷业有限公司 | A kind of ceramics etching frosted color artistic decorative pigment |
| CN108546081A (en) * | 2018-04-27 | 2018-09-18 | 孙劲松 | A kind of method for cooking of enamel painting on porcelain |
-
2019
- 2019-07-08 CN CN201910610266.0A patent/CN112194911A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN88100123A (en) * | 1988-01-16 | 1988-10-12 | 江西省科学院能源研究所 | Cheap solar energy vacuum heat-collecting tube and manufacture method thereof |
| CN2037452U (en) * | 1988-09-30 | 1989-05-10 | 江西省科学院能源研究所 | Effective vacuum tuber solar water heater |
| CN1091763A (en) * | 1994-02-22 | 1994-09-07 | 蒋采苹 | A kind of pigment paste of the usefulness of painting and piece and working method thereof |
| CN103242062A (en) * | 2013-04-25 | 2013-08-14 | 湖南醴陵元诏瓷业有限公司 | Technological process for decoration and repair of paint with five colors under glaze |
| CN104446344A (en) * | 2014-11-01 | 2015-03-25 | 景德镇景浮宫陶瓷文化有限公司 | Preparation method of slim mirror-plane artistic porcelain painting and product prepared by preparation method |
| CN105753465A (en) * | 2016-01-24 | 2016-07-13 | 伍剑峰 | Method of making ceramic super-flat mirror art mural and product made thereby |
| CN107523096A (en) * | 2017-08-16 | 2017-12-29 | 醴陵市精陶瓷业有限公司 | A kind of ceramics etching frosted color artistic decorative pigment |
| CN108546081A (en) * | 2018-04-27 | 2018-09-18 | 孙劲松 | A kind of method for cooking of enamel painting on porcelain |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112903400A (en) * | 2021-01-13 | 2021-06-04 | 河南中博生物塑化科技有限公司 | Method for dyeing blood vessels and nerves of human plasticized specimen |
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Application publication date: 20210108 |