CN105293909B - In-glaze decoration embossment bottom material, in-glaze decoration marble paper and its manufacture craft with its production - Google Patents
In-glaze decoration embossment bottom material, in-glaze decoration marble paper and its manufacture craft with its production Download PDFInfo
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Abstract
The present invention relates to a kind of in-glaze decoration embossment bottom material, with its production in-glaze decoration marble paper and its manufacture craft, belong to in-glaze decoration marble paper technical field, the method of the present invention includes, in-glaze decoration embossment bottom material, in-glaze decoration marble paper and its manufacture craft with its production, the production of the in-glaze decoration embossment bottom material includes: calcining, ball milling, dries, pulverizes four steps, and the method with in-glaze decoration embossment bottom material production in-glaze decoration marble paper includes: to roll four ink, printing, color printing, sealing steps.Method of the invention, applicable difference glaze and firing temperature, the toning range for increasing in-glaze decoration raised piece increases product corrosion stability and wear resistance, the dissolution of zero heavy metal, pigment is soluble high, stereoscopic effect is good, brightness is strong, simplifies printing technology process, realizes finished product rate height, it is indefectible, it is more attractive；And lead-indium alloy can reach American-European countries's standard.
Description
Technical field
The invention belongs to in-glaze decoration embossment printing technology fields, and in particular to a kind of production work of in-glaze decoration marble paper
Skill.
Background technique
With the raising of people's quality of life and the transformation of consumption idea, to wanting for the artistry and appreciation of ceramic
Ask higher and higher.In order to improve the artistry of ceramic, generally require using a variety of surface decorating methods, such as in-glaze decoration marble paper
(also known as high temperature rapid firing marble paper), a kind of another ceramic decoration printing technology skill extended on the basis of overglaze color decoration technology
Art, instead of traditional handicraft colored drawing technology.
Due to ceramic paint manufacturing enterprise at present provided by relief materials less varieties, i.e., transparent and two kinds of embossments of milky
Color demand needed for material is insufficient for pattern, it is poor with pigment congruent melting, if being printed on made of cadmium class and cobalt class
The phenomenon that snuff can be generated in color, lead-indium alloy severely exceed, and firing range amplitude is narrow, and temperature is difficult to control, serious shadow
Ring the effect in flower face and the requirement of client.
Due to the condition ceramics produced of the preparation and calcination equipment of the ceramic raw and auxiliary material of existing Production of Ceramics enterprise
The usual firing temperature of product firing time 16 ~ 20 hours, adds current high temperature rapid firing stains sheet in 1230 ~ 1250 DEG C of ranges
Product color difference caused by the ceramic product of body firing range narrow (20 DEG C of temperature difference) decoration is serious, and dim pattern is unclear, color is sent out
Black, obfuscation, flies the defects of color at discoloration.
Application No. is 200610037153.9 Chinese patent, a kind of in-glaze decoration decorative daily-use porcelain and its producer are disclosed
Method, blank raw material preferred ingredient by weight percentage include: Longyan clay raw ore 18%, weathered potash feldspar 11%%, Jiepai clay 12%, potassium
Feldspar 10% tempers aluminium oxide 9%, Guizhou clay 5%, Longyan clay suction mud 23%, quartz 12%, and blank-making technology is first to configure pug, through adding
Water for ball milling is crossed and screens out iron, filters pressing, thick refining, aging, refining, molding, dry；Production method includes first making green body, enamel and glaze
It prizes marble paper, then by green body glazing, through 1240 ~ 1260 DEG C of biscuitings 5-7 hours, decal paper, then through 1100 ~ 1150 DEG C of barbecue 3-
Become product within 5 hours.Although product strength made from the in-glaze decoration decorative daily-use porcelain and its production method is high, glaze surface intensity is big,
Transparency is fine with stability, is suitble to produce in enormous quantities, still, which is not suitable in other glaze and firing temperature and glaze
The toning of color raised piece is limited in scope, and the blank raw material component used is more, blank-making technology trivial operations, biscuiting temperature be high,
Time is not longer easy to operate.
Application No. is 201310389403.5 Chinese patents, disclose a kind of color-painting method of in-glaze decoration ceramics, including
Following steps: (1) taking china clay, prepares mud plate；(2) pen draws embossment；(3) base is mended, base is shone；(4) first time glazing: spraying ash glaze；
(5) it is burnt into for the first time；(6) kiln discharge；(7) colored drawing: one layer of water-soluble fixative liquor is sprayed on porcelain plate surface, then draws painting with colorant, is dried
It is dry；(8) it is burnt into for second；(9) second of glazing: dry granular glaze is applied using sieve sieve；(10) third time is burnt into；(11) kiln discharge, i.e.,
It can.Although in-glaze decoration ceramics made of the method are exquisitely carved, space multistory sense is strong, and reserve value is high, the technique is also uncomfortable
Other glaze are closed, and the toning of firing temperature and in-glaze decoration raised piece is limited in scope, mechanical resistant abrasion is low with corrosion resistance,
And process is many and diverse, needs repeatedly to be burnt into, and firing time is long, cannot achieve the effect that energy-saving.
Summary of the invention
The glaze that the purpose of the present invention is overcome the deficiencies of the prior art and provide a kind of in-glaze decoration embossment bottom material, make of it
It prizes marble paper and its manufacture craft, the applicable different glaze of this method and firing temperature increase the toning of in-glaze decoration raised piece
Range increases product corrosion stability and wear resistance, and zero heavy metal dissolves out.
The present invention is achieved by the following technical solutions:
In-glaze decoration embossment bottom material, including the following component according to mass fraction meter: 47 ~ 52 parts of sclerotin soil, aluminium oxide 1 ~ 5
Part, 15 ~ 19 parts of silica flour, 8 ~ 11 parts of feldspar powder, 17 ~ 25 parts of high temperature glaze.
The in-glaze decoration embossment bottom material, including the following component according to mass fraction meter: sclerotin soil 50 parts, aluminium oxide 3
Part, 17 parts of silica flour, 10 parts of feldspar powder, 20 parts of high temperature glaze.
With the method for in-glaze decoration embossment bottom material production in-glaze decoration marble paper, include the following steps:
Step 1: the production of in-glaze decoration embossment bottom material:
A. it calcines: according to the quality proportioning, the in-glaze decoration embossment bottom material each component being uniformly mixed and is placed in kiln
It is calcined at 1100 DEG C ~ 1150 DEG C, calcination time is 12 ~ 14 hours, after natural cooling, obtains mixture；
B. ball milling: by mixture obtained by step 1 a, ball milling 5 ~ 7 days, ball milling bottom material is obtained；
C. it dries: ball milling bottom material obtained by step b being dried at 50 DEG C ~ 60 DEG C, obtains blocky bottom material；
D. it rolles over broken: blocky bottom material obtained by step c is smashed it through into 350 meshes to get the in-glaze decoration embossment bottom material；
Step 2: the production of in-glaze decoration marble paper:
E. it rolls ink: ceramic paint in the in-glaze decoration embossment bottom material and glaze is mixed according to the ratio of mass ratio 3:1 ~ 5:1,
Up to in-glaze decoration embossment pigment, the ratio tune for being 10:7 ~ 10:8 according to mass ratio by the in-glaze decoration embossment pigment and varnish
It closes, by grinding up to ink-like in-glaze decoration embossment pigment；
F. it prints: to obtain the final product dry after dry by ink-like in-glaze decoration embossment color-printed obtained by step 2 e on transcription base stock
Dry in-glaze decoration embossment bottom material；
G. designed various in-glaze pigments color printing: are printed on to in-glaze decoration embossment bottom material dry obtained by step 2 f
On, up to required in-glaze decoration embossing pattern after drying；
H. sealing: cover glue is printed on in-glaze decoration embossing pattern obtained by step 2 g, is spent after dry up to in-glaze decoration
Paper.
Further, the method with in-glaze decoration embossment bottom material production in-glaze decoration marble paper, in glaze described in step 2 e
Ratio 3:1 ~ 4:1 of ceramic paint mass ratio, the quality of the in-glaze decoration embossment bottom material and varnish in color embossment bottom material and glaze
Than for 10:7 ~ 10:8, the number of grinding described in step 2 e is 3 ~ 4 times.
Further, the method with in-glaze decoration embossment bottom material production in-glaze decoration marble paper, prints described in step 2 f
Halftone made of 300 mesh silk screen of Shi Caiyong, the number of printing are 3 ~ 4 times, and the drying is 22 DEG C in temperature, humidity 60%,
It is 6 hours dry in environment.
Further, the method with in-glaze decoration embossment bottom material production in-glaze decoration marble paper, it is dry described in step 2 g
It is 22 DEG C in temperature, it is 4 hours dry in the environment that humidity is 60%.
Further, the printing is printed using halftone made of 80 mesh silk screens, and the dry environment is 50 DEG C of perseverances
The drying shed of temperature, the time of the naturally dry are 2 ~ 4 hours, and the temperature range of the grilling is 1230 ~ 1280 DEG C.
Wherein, in-glaze decoration marble paper is made with the method for above-mentioned in-glaze decoration embossment bottom material production in-glaze decoration marble paper.
The beneficial effects of the present invention are embodied in: compared with prior art, manufacture craft of the invention, it is applicable difference glaze
Material and firing temperature increase the toning range of in-glaze decoration marble paper, improve the abrasion of product surface enamel mechanical resistant and corrosion resistance,
And it is suitable for glaze applied by existing each Production of Ceramics producer, and stereoscopic effect is good, brightness is strong, printing technology process is simplified,
Finished product rate height is realized, it is indefectible, it is more attractive；And lead-indium alloy can reach American-European countries's standard.
Specific embodiment
Raw material of the present invention is commercially available product.
Embodiment 1
The in-glaze decoration embossment bottom material, including the following component according to mass fraction meter: sclerotin soil 47 parts, 1 part of aluminium oxide,
15 parts of silica flour, 8 parts of feldspar powder, 17 parts of high temperature glaze；The high temperature glaze is the saturating of the rich production of Britain Zhuan Xinwan
Bright frit, feature are that transparency is high, good leveling property.
With the method for in-glaze decoration embossment bottom material production in-glaze decoration marble paper, include the following steps:
Step 1: the production of in-glaze decoration embossment bottom material:
A. it calcines: according to the quality proportioning, the in-glaze decoration embossment bottom material each component being uniformly mixed and is put by quartz
High-temperature resistant container made of sand is built in kiln and is calcined at 1100 DEG C, and calcination time is 12 hours, after natural cooling,
Obtain mixture；
B. ball milling: after evenly mixing according to mass ratio 1:1 by mixture described in step 1 a and dehydrated alcohol, it is with revolving speed
The ball mill grinding of 1200r/h 5 days, obtains ball milling material；
C. it dries: ball milling material obtained by step 1 b being uniformly packed into rustless steel container, is put into 50 DEG C of thermostatic drying chambers sufficiently
It is dried to blocky bottom material；
D. it rolles over broken: powdered bottom material is made in blocky bottom material obtained by step 1 c with the pulverizer equipped with 350 mesh filter screens,
Obtain in-glaze decoration embossment bottom material；
Step 2: the production of in-glaze decoration marble paper:
E. it rolls ink: ceramic paint in the in-glaze decoration embossment bottom material and glaze is mixed according to the ratio of mass parts ratio 3:1,
In-glaze decoration embossment pigment is obtained, the color embossment pigment and varnish are concocted according to the ratio that mass parts ratio is 10:7, by
Three roller ink grinding mills grind 3 times into ink-like in-glaze decoration embossment pigment；
F. it prints: ink-like in-glaze decoration embossment pigment obtained by step 2 e is fitted into the halftone made of 300 mesh silk screens,
The thickness according to required by product, with screen process press color-printed on transcription base stock, print pass be 3 times, wherein print
After brush is primary, after being spontaneously dried 6 hours under 22 DEG C of temperature, the isoperibol of humidity 60%, it just can be carried out and print next time
Brush is to get dry in-glaze decoration embossment bottom material；
G. color printing: step 2 f will be printed on according to the good various in-glaze pigments of decoration Pattern Design with the halftone of 200 mesh
It is 22 DEG C in temperature on the in-glaze decoration embossment bottom material of resulting drying, it is 6 hours dry under the constant-temperature constant-humidity environment that humidity is 60%,
Up to required in-glaze decoration embossing pattern；
H. sealing: the halftone made of 80 mesh silk screens brushes cover offset printing on in-glaze decoration embossing pattern obtained by step 2 g,
Freeze-day with constant temperature in 50 DEG C of drying shed is placed, up to in-glaze decoration marble paper after drying.
Tested with the in-glaze decoration marble paper pack, outbound, it is enterprising in ceramic semi-finished product with the in-glaze decoration marble paper
Row applique, naturally dry, grilling are to get in-glaze decoration embossment ceramic.
Wherein, during applique, the cleaning of ceramic surface is kept, and scrape reality with frictioning, removed between marble paper and ceramics
Moisture or bubble carry out grilling, the temperature of grilling after in-glaze decoration embossment ceramic semi-finished product are made within naturally dry 4 hours after applique
Degree is 1230 DEG C, and one hour of constant temperature grilling, carrying out furnace heating-up speed when grilling is 27 DEG C/h.
Through examining, as a result are as follows: 6000 turns of wearability, 4 grades；Capacitive lead content < 0.005 mg/kg；Capacitive cadmium content
< 0.05mg/kg, referring to table 1:
The performance detection data of 1 embodiment of table, 1 gained in-glaze decoration embossment ceramic
Embodiment 2
The in-glaze decoration embossment bottom material, including the following component according to mass fraction meter: sclerotin soil 50 parts, 3 parts of aluminium oxide,
17 parts of silica flour, 10 parts of feldspar powder, 20 parts of high temperature glaze；The high temperature glaze is the saturating of the rich production of Britain Zhuan Xinwan
Bright frit, feature are that transparency is high, and good leveling property is usually useful in medium temperature and sclerotin enamel raw material.
With the method for in-glaze decoration embossment bottom material production in-glaze decoration marble paper, include the following steps:
Step 1: the production of in-glaze decoration embossment bottom material:
A. it calcines: according to the quality proportioning, the in-glaze decoration embossment bottom material each component being uniformly mixed and is put by quartz
High-temperature resistant container made of sand is built in kiln and is calcined at 1125 DEG C, and calcination time is 13 hours, after natural cooling,
Obtain mixture；
B. ball milling: after evenly mixing according to mass ratio 1:1 by mixture described in step 1 a and dehydrated alcohol, it is with revolving speed
The ball mill grinding of 1200r/h 6 days, obtains ball milling material；
C drying: ball milling material obtained by step 1 b. is uniformly packed into rustless steel container, is put into 55 DEG C of thermostatic drying chambers sufficiently
It is dried to blocky bottom material；
D. it rolles over broken: powdered bottom material is made in blocky bottom material obtained by step 1 c with the pulverizer equipped with 350 mesh filter screens,
Obtain in-glaze decoration embossment bottom material；
Step 2: the production of in-glaze decoration marble paper:
E. it rolls ink: ceramic paint in the in-glaze decoration embossment bottom material and glaze is mixed according to the ratio of mass parts ratio 4:1,
In-glaze decoration embossment pigment is obtained, the color embossment pigment and varnish are concocted according to the ratio that mass parts ratio is 10:7.5, after
4 times are ground into ink-like in-glaze decoration embossment pigment through three roller ink grinding mills；
F. it prints: ink-like in-glaze decoration embossment pigment obtained by step 2 e is fitted into the halftone made of 300 mesh silk screens,
The thickness according to required by product, with screen process press color-printed on transcription base stock, print pass be 4 times, wherein print
After brush is primary, after being spontaneously dried 6 hours under 22 DEG C of temperature, the isoperibol of humidity 60%, it just can be carried out and print next time
Brush is to get dry in-glaze decoration embossment bottom material；
G. color printing: step 2 f will be printed on according to the good various in-glaze pigments of decoration Pattern Design with the halftone of 200 mesh
It is 22 DEG C in temperature on the in-glaze decoration embossment bottom material of resulting drying, it is 6 hours dry under the constant-temperature constant-humidity environment that humidity is 60%,
Up to required in-glaze decoration embossing pattern；
H. sealing: the halftone made of 80 mesh silk screens brushes cover offset printing on in-glaze decoration embossing pattern obtained by step 2 g,
Freeze-day with constant temperature in 50 DEG C of drying shed is placed, up to in-glaze decoration marble paper after drying.
Tested with the in-glaze decoration marble paper pack, outbound, it is enterprising in ceramic semi-finished product with the in-glaze decoration marble paper
Row applique, naturally dry, grilling are to get in-glaze decoration embossment ceramic.
Wherein, during applique, the cleaning of ceramic surface is kept, and scrape reality with frictioning, removed between marble paper and ceramics
Moisture or bubble carry out grilling, the temperature of grilling after in-glaze decoration embossment ceramic semi-finished product are made within naturally dry 4 hours after applique
Degree is 1230 DEG C, and one hour of constant temperature grilling, carrying out furnace heating-up speed when grilling is 27 DEG C/h.
Through examining, as a result are as follows: 6000 turns of wearability, 4 grades；Capacitive lead content < 0.005mg/L；Capacitive cadmium content <
0.005 mg/L, referring to table 2:
The performance detection data of 2 embodiment of table, 2 gained in-glaze decoration embossment ceramic
Embodiment 3
The in-glaze decoration embossment bottom material, including the following component according to mass fraction meter: sclerotin soil 52 parts, 5 parts of aluminium oxide,
19 parts of silica flour, 11 parts of feldspar powder, 25 parts of high temperature glaze；The high temperature glaze is the saturating of the rich production of Britain Zhuan Xinwan
Bright frit, feature are that transparency is high, and good leveling property is usually useful in medium temperature and sclerotin enamel raw material.
With the method for in-glaze decoration embossment bottom material production in-glaze decoration marble paper, include the following steps:
Step 1: the production of in-glaze decoration embossment bottom material:
A. it calcines: according to the quality proportioning, the in-glaze decoration embossment bottom material each component being uniformly mixed and is put by quartz
High-temperature resistant container made of sand is built in kiln and is calcined at 1150 DEG C, and calcination time is 14 hours, after natural cooling,
Obtain mixture；
B. ball milling: after evenly mixing according to mass ratio 1:1 by mixture described in step 1 a and dehydrated alcohol, it is with revolving speed
The ball mill grinding of 1200r/h 5 days, obtains ball milling material；
C. it dries: ball milling material obtained by step 1 b being uniformly packed into rustless steel container, is put into 50 DEG C of thermostatic drying chambers sufficiently
It is dried to blocky bottom material；
D. it rolles over broken: powdered bottom material is made in blocky bottom material obtained by step 1 c with the pulverizer equipped with 350 mesh filter screens,
Obtain in-glaze decoration embossment bottom material；
Step 2: the production of in-glaze decoration marble paper:
E. it rolls ink: ceramic paint in the in-glaze decoration embossment bottom material and glaze is mixed according to the ratio of mass parts ratio 5:1,
In-glaze decoration embossment pigment is obtained, the color embossment pigment and varnish are concocted according to the ratio that mass parts ratio is 10:8, by
Three roller ink grinding mills grind 4 times into ink-like in-glaze decoration embossment pigment；
F printing: ink-like in-glaze decoration embossment pigment obtained by step 2 e is fitted into the halftone made of 300 mesh silk screens, root
According to thickness required by product, with screen process press color-printed on transcription base stock, a brush number is 4 times, wherein printing
After primary, after spontaneously drying 6 hours under 22 DEG C of temperature, the isoperibol of humidity 60%, it just can be carried out subsequent printings,
Up to dry in-glaze decoration embossment bottom material；
G. color printing: step 2 f will be printed on according to the good various in-glaze pigments of decoration Pattern Design with the halftone of 200 mesh
It is 20 DEG C in temperature on the in-glaze decoration embossment bottom material of resulting drying, it is 6 hours dry under the constant-temperature constant-humidity environment that humidity is 60%,
Up to required in-glaze decoration embossing pattern；
H. sealing: the halftone made of 80 mesh silk screens brushes cover offset printing on in-glaze decoration embossing pattern obtained by step 2 g,
Freeze-day with constant temperature in 50 DEG C of drying shed is placed, up to in-glaze decoration marble paper after drying.
Tested with the in-glaze decoration marble paper pack, outbound, it is enterprising in ceramic semi-finished product with the in-glaze decoration marble paper
Row applique, naturally dry, grilling are to get in-glaze decoration embossment ceramic.
Wherein, during applique, the cleaning of ceramic surface is kept, and scrape reality with frictioning, removed between marble paper and ceramics
Moisture or bubble carry out grilling, the temperature of grilling after in-glaze decoration embossment ceramic semi-finished product are made within naturally dry 4 hours after applique
Degree is 1230 DEG C, and one hour of constant temperature grilling, carrying out furnace heating-up speed when grilling is 27 DEG C/h.
Through examining, as a result are as follows: 6000 turns of wearability, 4 grades；Capacitive lead content < 0.005 mg/L；Capacitive cadmium content <
0.005 mg/L, referring to table 3:
The performance detection data of 3 embodiment of table, 3 gained in-glaze decoration embossment ceramic
The above is a preferred embodiment of the present invention, it is noted that for those skilled in the art
For, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also considered as
Protection scope of the present invention.
Claims (7)
1. in-glaze decoration embossment bottom material, it is characterised in that: including the following component according to mass fraction meter: sclerotin soil 47 ~ 52
Part, 1 ~ 5 part of aluminium oxide, 15 ~ 19 parts of silica flour, 8 ~ 11 parts of feldspar powder, 17 ~ 25 parts of high temperature glaze.
2. the in-glaze decoration embossment bottom material according to claim 1, it is characterised in that: including according to mass fraction meter as
Under
Component: sclerotin soil 50 parts, 3 parts of aluminium oxide, 17 parts of silica flour, 10 parts of feldspar powder, high temperature glaze 20
Part.
3. the method for the production in-glaze decoration marble paper of the in-glaze decoration embossment bottom material described in claim 1, which is characterized in that including such as
Lower step:
Step 1: the production of in-glaze decoration embossment bottom material
A. calcine: according to the quality proportioning, the in-glaze decoration embossment bottom material each component is uniformly mixed be placed in kiln in
It is calcined at 1100 DEG C ~ 1150 DEG C, calcination time is 12 ~ 14 hours, after natural cooling, obtains mixture；
B. ball milling: by mixture obtained by step 1 a, ball milling 5 ~ 7 days, ball milling bottom material is obtained；
C. it dries: ball milling bottom material obtained by step 1 b being dried at 50 DEG C ~ 60 DEG C, obtains blocky bottom material；
D. it rolles over broken: blocky bottom material obtained by step 1 c is smashed it through into 350 meshes to get the in-glaze decoration embossment bottom material
；Step 2: the production of in-glaze decoration marble paper:
E. it rolls ink: ceramic paint in gained in-glaze decoration embossment bottom material and glaze is mixed according to the ratio of mass ratio 3:1 ~ 5:1,
Up to in-glaze decoration embossment pigment, the ratio for being 10:7 ~ 10:8 according to mass ratio by the in-glaze decoration embossment pigment and varnish
Blending, by grinding up to ink-like in-glaze decoration embossment pigment；
F. it prints: to obtain the final product dry after dry by ink-like in-glaze decoration embossment color-printed obtained by step 2 e on transcription base stock
Dry in-glaze decoration embossment bottom material；
G. color printing: designed in-glaze pigment being printed on in-glaze decoration embossment bottom material dry obtained by step 2 f, is done
Up to required in-glaze decoration embossing pattern after dry；
H. sealing: cover glue is printed on in-glaze decoration embossing pattern obtained by step 2 g, it is dry after through test package, go out
Library is up to in-glaze decoration marble paper.
4. with the method for in-glaze decoration embossment bottom material production in-glaze decoration marble paper according to claim 3, which is characterized in that step
In in-glaze decoration embossment bottom material described in rapid two e and glaze the mass ratio of ceramic paint be 4:1, the in-glaze decoration embossment pigment and
The mass ratio of varnish is 10:7.5, and the number of grinding described in step 2 e is 3 ~ 4 times.
5. with the method for in-glaze decoration embossment bottom material production in-glaze decoration marble paper according to claim 3, which is characterized in that
Using halftone made of 300 mesh when printing described in step 2 f, the number of printing is 3 ~ 4 times, and the drying is in temperature
It is 22 DEG C, it is 6 hours dry in the environment that humidity is 60%.
6. with the method for in-glaze decoration embossment bottom material production in-glaze decoration marble paper according to claim 3, which is characterized in that step
Being dried described in rapid two g in temperature is 22 DEG C, and humidity is 4 hours dry in the environment of being 60%.
7. the in-glaze decoration marble paper of the method production of the production in-glaze decoration marble paper of the in-glaze decoration embossment bottom material described in claim 3.
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| CN103183528A (en) * | 2013-03-29 | 2013-07-03 | 深圳市永丰源瓷业有限公司 | Shaping glaze and firing technology of bone china containing high-permeability pigment |
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| CN101613204A (en) * | 2008-06-26 | 2009-12-30 | 庄助民 | In-glaze decoration sclerotin porcelain production technique |
| CN101665347A (en) * | 2009-09-22 | 2010-03-10 | 景德镇陶瓷学院 | Daily-used fine porcelain with high property and preparation method thereof |
| CN102166899A (en) * | 2010-12-28 | 2011-08-31 | 宗海燕 | Applique non-removal paper one-time sintered ceramic in-glaze color flower paper |
| CN103183528A (en) * | 2013-03-29 | 2013-07-03 | 深圳市永丰源瓷业有限公司 | Shaping glaze and firing technology of bone china containing high-permeability pigment |
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Denomination of invention: Underglaze color relief base material, underglaze color flower paper made with it and its manufacturing technology Effective date of registration: 20210726 Granted publication date: 20190329 Pledgee: Industrial Commercial Bank of China Ltd. Dehua branch Pledgor: FUJIAN PROVINCE DEHUA MINGFENG JINHUA PAPER Co.,Ltd. Registration number: Y2021980006760 |