CN112106910A - Soda water health beverage containing cyclocarya paliurus flavone and preparation method thereof - Google Patents
Soda water health beverage containing cyclocarya paliurus flavone and preparation method thereof Download PDFInfo
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- CN112106910A CN112106910A CN202010777820.7A CN202010777820A CN112106910A CN 112106910 A CN112106910 A CN 112106910A CN 202010777820 A CN202010777820 A CN 202010777820A CN 112106910 A CN112106910 A CN 112106910A
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- CN
- China
- Prior art keywords
- flavone
- cyclocarya paliurus
- sodium bicarbonate
- solution
- water
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 241000233779 Cyclocarya paliurus Species 0.000 title claims abstract description 46
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 title claims abstract description 37
- 229930003944 flavone Natural products 0.000 title claims abstract description 37
- 150000002212 flavone derivatives Chemical class 0.000 title claims abstract description 37
- 235000011949 flavones Nutrition 0.000 title claims abstract description 37
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 title claims abstract description 37
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 27
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 title claims abstract description 18
- 235000013361 beverage Nutrition 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 28
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims abstract description 14
- 235000017557 sodium bicarbonate Nutrition 0.000 claims abstract description 14
- 238000002156 mixing Methods 0.000 claims abstract description 9
- 239000000287 crude extract Substances 0.000 claims abstract description 8
- 238000004108 freeze drying Methods 0.000 claims abstract description 8
- XHFLOLLMZOTPSM-UHFFFAOYSA-M sodium;hydrogen carbonate;hydrate Chemical compound [OH-].[Na+].OC(O)=O XHFLOLLMZOTPSM-UHFFFAOYSA-M 0.000 claims abstract description 8
- 230000001954 sterilising effect Effects 0.000 claims abstract description 6
- 239000008213 purified water Substances 0.000 claims abstract description 5
- 239000004952 Polyamide Substances 0.000 claims abstract description 4
- 238000000605 extraction Methods 0.000 claims abstract description 4
- 238000001914 filtration Methods 0.000 claims abstract description 4
- 229920002647 polyamide Polymers 0.000 claims abstract description 4
- 239000000843 powder Substances 0.000 claims abstract description 4
- 238000011049 filling Methods 0.000 claims abstract description 3
- 238000000034 method Methods 0.000 claims abstract description 3
- 239000000243 solution Substances 0.000 claims description 15
- 239000007864 aqueous solution Substances 0.000 claims description 7
- 238000012371 Aseptic Filling Methods 0.000 claims description 3
- 238000004659 sterilization and disinfection Methods 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 2
- 230000036772 blood pressure Effects 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000008280 blood Substances 0.000 description 3
- 210000004369 blood Anatomy 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 241001122767 Theaceae Species 0.000 description 2
- 239000006228 supernatant Substances 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- 241000758791 Juglandaceae Species 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 201000006549 dyspepsia Diseases 0.000 description 1
- 239000003480 eluent Substances 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- -1 flavonoids compounds Chemical class 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Botany (AREA)
- Mycology (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention provides a soda water health-care beverage containing cyclocarya paliurus flavone and a preparation method thereof, wherein the method comprises the following steps: s1, extracting the cyclocarya paliurus leaf powder twice by adopting an extraction method, combining supernate, concentrating and freeze-drying to obtain a cyclocarya paliurus flavone crude extract; s2, preparing the cyclocarya paliurus flavone crude extract into a solution, filtering the solution by using a polyamide chromatographic column, concentrating and freeze-drying the solution to obtain cyclocarya paliurus flavone; s3, dissolving sodium bicarbonate in purified water to obtain a sodium bicarbonate water solution for later use; s4, sterilizing the sodium bicarbonate water solution, mixing with cyclocarya paliurus flavone in an aseptic environment, and filling aseptically. The health-care beverage has the effects of soda water and blood pressure reduction, is made of natural materials, and is environment-friendly and healthy.
Description
Technical Field
The invention relates to the technical field of beverages, and particularly relates to a soda water health-care beverage containing cyclocarya paliurus flavone and a preparation method thereof.
Background
Soda water is a flavored water beverage containing sodium bicarbonate and no sugar, is weakly alkaline, and is helpful for nourishing stomach, and relieving dyspepsia and constipation. Due to their unique taste and function, soda water is enjoyed by more and more health-seeking consumers. However, in the prior art, most of the research and preparation of soda water is added with edible essence for blending or added with trace nutrient elements, so that the taste and the function are single, and the requirements of consumers are difficult to meet.
Cyclocarya paliurus is a unique juglandaceae plant in China, belongs to deciduous trees, is also called cyclocarya paliurus, cyclocarya paliurus and the like, and is widely distributed in southern areas of China. Cyclocarya paliurus has various effects of clearing away summer-heat, reducing blood sugar, resisting fatigue and the like, has been used as tea in China for thousands of years, and is called blood sugar-reducing nerve tea. The flavonoids compounds are important active ingredients in the cyclocarya paliurus leaves, are not only natural and nontoxic antioxidants, but also have various physiological activities of reducing blood sugar, inhibiting bacteria, regulating intestinal flora and the like.
Disclosure of Invention
In order to solve the defects and shortcomings of the prior art, the invention aims to provide a soda water health-care beverage containing cyclocarya paliurus flavone and a preparation method thereof.
The purpose of the invention is realized by the following technical scheme:
a preparation method of soda water health beverage containing cyclocarya paliurus flavone comprises the following steps:
s1, extracting the cyclocarya paliurus leaf powder twice by adopting an extraction method, combining supernate, concentrating and freeze-drying to obtain a cyclocarya paliurus flavone crude extract;
s2, preparing the cyclocarya paliurus flavone crude extract into a solution, filtering the solution by using a polyamide chromatographic column, concentrating and freeze-drying the solution to obtain cyclocarya paliurus flavone;
s3, dissolving sodium bicarbonate in purified water to obtain a sodium bicarbonate water solution for later use;
s4, sterilizing the sodium bicarbonate water solution, mixing with cyclocarya paliurus flavone in an aseptic environment, and filling aseptically.
In the S3, the ratio of the sodium bicarbonate to the purified water is (20-80) mg: 100 g.
The S4 specifically includes: placing the sodium bicarbonate aqueous solution at 105 ℃ for sterilization treatment for 4 minutes, adding cyclocarya paliurus flavone into the sodium bicarbonate aqueous solution in an aseptic environment, mixing, and carrying out aseptic filling.
In the S4, the mass ratio of the cyclocarya paliurus flavone to the sodium bicarbonate water solution is (0.05-0.1): 100.
a soda water health beverage containing cyclocarya paliurus flavone is prepared by dissolving cyclocarya paliurus flavone in soda water.
Preferably, the mass ratio of the cyclocarya paliurus flavone to the sodium bicarbonate aqueous solution is (0.05-0.1): 100.
compared with the prior art, the invention has the advantages that:
the soda water added with the cyclocarya paliurus flavone is clear in appearance and light yellow, has the special faint scent and taste of the soda water containing the cyclocarya paliurus flavone, and does not need to be added with food additives such as essence, sweetener and the like.
Detailed Description
The embodiment provides a preparation method of a soda water health-care beverage containing cyclocarya paliurus flavone, which comprises the following steps:
1. weighing an appropriate amount of pulverized cyclocarya paliurus powder, adding hot water (within the range of 55-60 ℃) according to the material-to-liquid ratio of 1:20, performing oscillation extraction for 40min in a constant temperature oscillator at 60 ℃, centrifuging for 15min at 6000r/min to obtain a supernatant, leaching residues again by the same method, combining the two supernatants, concentrating and freeze-drying to obtain a cyclocarya paliurus flavone crude extract;
2. preparing the cyclocarya paliurus flavone crude extract into a solution with the mass percentage concentration of 2%, filtering the solution by using a filter membrane with the pore diameter of 0.45 mu m, and then putting the filtered solution on a polyamide chromatographic column (30cm multiplied by 1.6 cm); firstly, washing off water-soluble impurities by using water, wherein the elution flow rate is 2.0mL/min, after eluting for 2BV (BV is the volume of a column bed), eluting by using 80% ethanol, collecting eluent (10 mL/tube) by using an automatic part collector, concentrating and freeze-drying to obtain a cyclocarya paliurus flavone sample;
3. sodium bicarbonate was added at room temperature in the following ratio (20-80) mg: dissolving 100g of the mixture in purified water, and uniformly mixing;
4. placing sodium bicarbonate water solution at 105 deg.C for sterilizing for 4min, and mixing with cyclocarya paliurus flavone sample (0.05-0.1 g): mixing 100g of the components in a mass ratio, and performing aseptic filling.
It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.
Claims (6)
1. A preparation method of a soda water health-care beverage containing cyclocarya paliurus flavone is characterized by comprising the following steps:
s1, extracting the cyclocarya paliurus leaf powder twice by adopting an extraction method, combining supernate, concentrating and freeze-drying to obtain a cyclocarya paliurus flavone crude extract;
s2, preparing the cyclocarya paliurus flavone crude extract into a solution, filtering the solution by using a polyamide chromatographic column, concentrating and freeze-drying the solution to obtain cyclocarya paliurus flavone;
s3, dissolving sodium bicarbonate in purified water to obtain a sodium bicarbonate water solution for later use;
s4, sterilizing the sodium bicarbonate water solution, mixing with cyclocarya paliurus flavone in an aseptic environment, and filling aseptically.
2. The method according to claim 1, wherein in the S3, the sodium bicarbonate is added in a ratio of (20-80) mg: 100 g.
3. The preparation method according to claim 1, wherein the S4 specifically comprises: placing the sodium bicarbonate aqueous solution at 105 ℃ for sterilization treatment for 4 minutes, adding cyclocarya paliurus flavone into the sodium bicarbonate aqueous solution in an aseptic environment, mixing, and carrying out aseptic filling.
4. The preparation method according to claim 2, wherein in the step S4, the mass ratio of the cyclocarya paliurus flavone to the sodium bicarbonate aqueous solution is (0.05-0.1): 100.
5. a soda water health beverage containing cyclocarya paliurus flavone is characterized in that the cyclocarya paliurus flavone is prepared by dissolving cyclocarya paliurus flavone in soda water.
6. A carbonated water health-care beverage as claimed in claim 5, wherein the mass ratio of cyclocarya paliurus flavone to the sodium bicarbonate aqueous solution is (0.05-0.1): 100.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010777820.7A CN112106910A (en) | 2020-08-05 | 2020-08-05 | Soda water health beverage containing cyclocarya paliurus flavone and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010777820.7A CN112106910A (en) | 2020-08-05 | 2020-08-05 | Soda water health beverage containing cyclocarya paliurus flavone and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112106910A true CN112106910A (en) | 2020-12-22 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010777820.7A Pending CN112106910A (en) | 2020-08-05 | 2020-08-05 | Soda water health beverage containing cyclocarya paliurus flavone and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN112106910A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104013669A (en) * | 2014-06-24 | 2014-09-03 | 南京中医药大学 | Method for preparing cyclocarya paliurus total flavonoid with effect of reducing blood glucose |
| CN107362146A (en) * | 2017-02-15 | 2017-11-21 | 南昌大学 | A kind of blue or green money willow polysaccharide effervescence tablet with antioxidation activity and preparation method thereof |
| CN110917240A (en) * | 2019-12-11 | 2020-03-27 | 湖南华诚生物资源股份有限公司 | Continuous method for separating multiple effective components from cyclocarya paliurus |
-
2020
- 2020-08-05 CN CN202010777820.7A patent/CN112106910A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104013669A (en) * | 2014-06-24 | 2014-09-03 | 南京中医药大学 | Method for preparing cyclocarya paliurus total flavonoid with effect of reducing blood glucose |
| CN107362146A (en) * | 2017-02-15 | 2017-11-21 | 南昌大学 | A kind of blue or green money willow polysaccharide effervescence tablet with antioxidation activity and preparation method thereof |
| CN110917240A (en) * | 2019-12-11 | 2020-03-27 | 湖南华诚生物资源股份有限公司 | Continuous method for separating multiple effective components from cyclocarya paliurus |
Non-Patent Citations (2)
| Title |
|---|
| 赵宝丰: "《茶饮料制品607例》", 31 December 2003, 科学技术文献出版社 * |
| 陈玉慧: "青钱柳黄酮及三萜调节人体肠道菌群作用研究", 《中国野生植物资源》 * |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20201222 |
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| RJ01 | Rejection of invention patent application after publication |