CN112022784A - Removable fragrant toner and preparation method thereof - Google Patents

Abstract

The invention discloses a removable fragrant toner and a preparation method thereof, wherein the removable fragrant toner is prepared from the following raw materials in parts by weight: 6-9 parts of biomass softening solubilization factors, 3-6 parts of skin-friendly surfactant, 7-10 parts of biomass moisturizing and air-permeable factors, 2.5-4.5 parts of natural nutrients, 3.5-4.5 parts of plant soothing essential oil and 146-158 parts of solvent. The makeup-removable fragrant toner takes various natural biological-based environment-friendly components as main raw materials, is mild and skin-friendly, can be quickly absorbed, is moisture-preserving, breathable and not stuffy, can not only endow a fragrant effect, but also play a role in makeup removal, and integrates the functions of the toner, perfume and makeup-removal water.

Description

Removable fragrant toner and preparation method thereof

Technical Field

The invention belongs to the technical field of toner, and particularly relates to removable fragrant toner and a preparation method thereof.

Background

The toner is one of skin care products, is applied to the working procedure of skin cleaning, and has the effects of deep cleaning, moisturizing, relieving and the like. With the improvement of living standard, people have higher and higher requirements on the quality and the function of the toner, and the basic effects of most toners, firming toners and smoothing toners are not met. The existing commercially available toner products have various varieties and large quality difference, and most of the products still contain additives such as alcohol, essence, preservative and other chemical synthetic components, so the products are not particularly friendly to skin health. Therefore, the development of skin toner has been progressed to multi-functionalization mainly based on non-alcoholic green components.

The deep cleaning with the toner is just one auxiliary cleaning, and more effects of the deep cleaning are water replenishing after cleaning, and the application of the toner as auxiliary cleaning before formal skin cleaning is not reported. If the perfume can be applied to the processes before skin cleaning such as makeup removal and the like, or has a fragrance function after skin cleaning, the application occasions of the toner can be expanded, so that the toner has a higher commodity added value.

Based on the above, the weak acid toner which takes the biomass softening solubilization factors, the biomass moisturizing air-permeable factors, the skin-friendly surfactant and the plant soothing essential oil as main components, is mild in moisturizing and air-permeable, can be used as makeup remover, has the fragrance releasing function, greatly expands the variety and application range of the toner and has wide market prospect.

Disclosure of Invention

The invention aims to provide removable fragrant toner and a preparation method thereof, which aim to solve the problems in the background art.

In order to achieve the purpose, the invention provides the following technical scheme:

a makeup-removable fragrant toner is characterized in that: the makeup-removing fragrant toner comprises the following raw materials in parts by weight: 6-9 parts of biomass softening solubilization factors, 3-6 parts of skin-friendly surfactant, 7-10 parts of biomass moisturizing and air-permeable factors, 2.5-4.5 parts of natural nutrients, 3.5-4.5 parts of plant soothing essential oil and 146-158 parts of solvent.

Further, the makeup removing fragrant toner is characterized in that the preparation method of the biomass softening solubilization factor comprises the following steps:

drying organisms containing softening and solubilizing factors in an oven at 27-32 ℃ for 3-5 hours in advance, adding the dried organisms containing the softening and solubilizing factors into a medicine crusher, fully crushing, soaking in 75-95% ethanol water solution, adding a small amount of baking soda, uniformly mixing the whole system, soaking for 24 hours, and filtering to obtain a primary extracting solution, wherein the mass ratio of the organisms containing the softening and solubilizing factors to the ethanol water solution to the baking soda is 1: 10-20: 0.1-0.2;

and (2) dialyzing and separating the primary extract obtained by filtering at room temperature by using a dialysis membrane with the molecular weight cutoff of 12000-16000 for 3-5 days, performing rotary evaporation and concentration treatment after dialysis, performing suction filtration by using filter paper with the pore diameter of 1-5 mu m, wherein the pump pressure is 0.02-0.06 MPa, freeze-drying the obtained filtrate, and performing ultrasonic dispersion on the filtrate in glycerol (the mass ratio of solid particles obtained after freeze-drying the filtrate to the glycerol is 1-2: 10) to obtain the biomass softening solubilization factor.

As a preferred scheme of the removable makeup fragrant toner of the invention: the organism containing softening and solubilizing factors is a composition of three or more of olive, sweet potato, grapefruit, iris, tomato and soybean.

As a preferred scheme of the removable makeup fragrant toner of the invention: the skin-friendly surfactant is a composition of isopropyl myristate, phytosterol, soapberry saponin and N-hydroxyethyl lauryl glucose amide.

As a preferred scheme of the removable makeup fragrant toner of the invention: the biomass moisturizing and air-permeable factor is a composition of ethylhexyl glycerol, hyaluronic acid and water-soluble fullerene.

As a preferred scheme of the removable makeup fragrant toner of the invention: the natural nutrient is a composition of mandelic acid, ellagic acid, vitamin E and vitamin C.

As a preferred scheme of the removable makeup fragrant toner of the invention: the plant soothing essential oil is a composition of tea tree oil, guaiac wood essential oil, sedge essential oil and sweet orange oil.

As a preferred scheme of the removable makeup fragrant toner of the invention: the solvent is a composition of deionized water, butanediol and squalene.

Further, the preparation method of the makeup-removing fragrant toner is characterized by comprising the following specific steps:

stirring 4.5-5.5 parts of butanediol, 1.5-2.5 parts of squalene, 0.75-1.5 parts of isopropyl myristate, 0.5-1 part of phytosterol, 0.75-1.5 parts of sapindus saponin, 1-2 parts of N-hydroxyethyl lauryl glucamide and 70-75 parts of deionized water at 380-420 rpm until uniform, stable and complete dissolution is achieved, sequentially adding 6-9 parts of biomass solubilizing factor, 2-3 parts of ethylhexyl glycerol, 4-5.5 parts of hyaluronic acid, 1-1.5 parts of water-soluble fullerene, 0.75-1 part of tea tree oil, 1-1.25 parts of guaiazuki essential oil, 1.25-1.5 parts of sedum essential oil, 0.5-0.75 part of sweet orange oil into a stirrer, stirring at 820-880 rpm for 17-23 min, adding 70-75 parts of deionized water, 0.5-1 part of nervonic acid, 0.5-1.5 parts of ellagic acid, 0.5-1.5 parts of tannic, 0.5-1.5 parts of vitamin E, 560-13-7 rpm, continuously stirring at 820-880 rpm, and (3) adjusting the pH value to be between 5.5 and 6.2 by using a small amount of baking soda to obtain uniform and transparent liquid, namely the makeup-removing fragrant toner.

Compared with the prior art, the invention has the beneficial effects that:

1. the makeup-removable fragrant toner disclosed by the invention adopts various natural biological-based environment-friendly components as main raw materials, is safe and mild, is skin-friendly and not irritant, is moisture-retaining and breathable without being stuffy, reduces the phenomena of skin dryness, skin peeling and acne, has a deep cleansing effect capable of removing makeup while releasing the fragrance, and has a pH value close to that of the skin of a human body, so that the functions of the toner, perfume and the makeup-removing toner are combined into a whole.

2. The makeup-removable fragrant toner has the moisturizing and ventilating effects derived from the comprehensive effects of the solvent, the biomass moisturizing and ventilating factors, the skin-friendly surfactant and the biomass softening and solubilizing factors: the solvent in reasonable proportion can provide sufficient moisture for skin and simultaneously slow down the evaporation of the moisture, and has the effect of absorbing the moisture in the air; the biomass moisturizing and air-permeable factor further strengthens the capability of retaining water on the skin, and simultaneously opens a channel for the respiration of skin pores, so that the skin pores are air-permeable and comfortable, and cutin is softened, so that the skin pores can be deeply cleaned; one end of each skin-friendly surfactant molecule is hydrophilic, and the other end of each skin-friendly surfactant molecule is hydrophobic, so that the skin-friendly surfactant molecules can deeply permeate into the epidermis layer, maintain the moisture required by the dermis layer of the skin after deep cleaning, contribute to the permeation and affinity of each effective component to the skin, and fully exert the moisture-retaining and water-locking effects of the effective components; the biomass softening and solubilizing factors can promote metabolism of skin cells, soften cutin and reduce water loss in skin. This fully explains the mechanism of the synergistic interaction of the four ingredients.

3. The solvent, the skin-friendly surfactant, the natural nutrient and the biomass softening solubilization factor of the makeup removable fragrant toner of the invention are added to endow the toner with a makeup removable function: the natural nutrients and the biomass softening and solubilizing factors can gently soften and remove part of the makeup powder and the cuticle, and the natural nutrients and the biomass softening and solubilizing factors are cooperated with the deep penetration cleaning effect of the skin-friendly surfactant and have the functions of strongly dissolving the makeup powder and separating the makeup powder from the skin by the solvent, so that the ideal makeup removing effect is achieved. This indicates that there is a synergistic effect between the four classes of ingredients.

4. According to the detachable fragrant toner, the addition of the biomass softening solubilization factor, the plant soothing essential oil and the skin-friendly surfactant endows the toner with a fragrance releasing effect: the biomass softening solubilization factor may contain certain essential oil components, a pleasant fragrance is obtained by the proper proportion of the biomass softening solubilization factor and the plant soothing essential oil, and the skin-friendly surfactant may have the function of fixing fragrance and delay the release speed of the fragrance, so that the three components also have a synergistic effect.

5. According to the detachable fragrant toner, deionized water is added twice during preparation, and a skin-friendly surfactant is added in the early stage, and experiments prove that only through the addition sequence and the proportion, the finally obtained toner has the emulsion type of oil-in-water, and only through the type of the detachable fragrant toner can the finally obtained toner be more stable, various functions can be fully exerted, otherwise, the effect is greatly reduced.

Test method

Basic performance test: according to subjective feeling evaluation of each person before and after the face use, basic performances (comprehensive feeling of moisture retention and air permeability) are divided into 5 grades, wherein the grade 1 is the worst, the grade 5 is the best, and more than 10 persons (dry, dry mixed, neutral, oil mixed and oily persons are equal in number) are evaluated by averaging, and the using amount is 2 g/person.

Fragrance release performance test: according to subjective feeling evaluation of each person before and after face use, the fragrance releasing performance is divided into 5 grades, wherein the grade 1 is the worst, the grade 5 is the best, and more than 10 persons (dry, neutral, oily and oily persons are equal in number) are subjected to average value taking, and the using amount is 2 g/person.

And (3) makeup removal performance test: according to subjective feeling evaluation before and after each person uses the face, the makeup removing performance (comprehensive evaluation of the removal degree of the makeup powder and the undamaged degree of the skin) is divided into 5 grades, the worst grade is 1 grade, the best grade is 5 grade, and the average value of more than 10 persons (the dry, neutral, oil and oily persons are equal in number) is taken by an evaluation group, and the using amount is 2 g/person.

Detailed description of the preferred embodiment

In order to make the aforementioned objects, features and advantages of the present invention comprehensible, embodiments accompanied with examples are described in detail below.

In the following description, numerous specific details are set forth in order to provide a thorough understanding of the present invention, but the present invention may be practiced in other ways than those specifically described and will be readily apparent to those of ordinary skill in the art without departing from the spirit of the present invention, and therefore the present invention is not limited to the specific embodiments disclosed below.

Furthermore, reference herein to "one embodiment" or "an embodiment" means that a particular feature, structure, or characteristic described in connection with the embodiment is included in at least one implementation of the invention. The appearances of the phrase "in one embodiment" in various places in the specification are not necessarily all referring to the same embodiment, nor are separate or alternative embodiments mutually exclusive of other embodiments.

Example 1

Drying olive, sweet potato, tomato and soybean (the mass ratio is 1.2:1:0.8:1) in an oven at 27-32 ℃ for 4 hours in advance, fully crushing in a medicine crusher, soaking in 75-95% ethanol water solution, adding a small amount of baking soda, the mass ratio of organisms containing softening solubilization factors, the ethanol water solution and the baking soda is 1:15:0.15, uniformly mixing the whole system, soaking for 24 hours, and filtering to obtain a primary extracting solution;

dialyzing and separating the primary extract obtained by filtering at room temperature by using a dialysis membrane with the molecular weight cutoff of 12000-16000 for 3-5 days, performing rotary evaporation and concentration treatment after dialysis, performing suction filtration by using filter paper with the aperture of 1-5 mu m, wherein the pump pressure is 0.02-0.06 MPa, freeze-drying the obtained filtrate, and performing ultrasonic dispersion on the filtrate in glycerol (the mass ratio of solid particles obtained after freeze-drying the filtrate to the glycerol is 1.5:10) to obtain a biomass softening solubilization factor;

stirring 5 parts of butanediol, 2 parts of squalene, 1.125 parts of isopropyl myristate, 0.75 part of phytosterol, 1.125 parts of soapberry saponin, 1.5 parts of N-hydroxyethyl lauryl glucamide and 72.5 parts of deionized water at the speed of 400rpm until the mixture is uniform, stable and completely dissolved, then adding 7.5 parts of biomass softening solubilization factor, 2.5 parts of ethylhexyl glycerin, 4.75 parts of hyaluronic acid, 1.25 parts of water-soluble fullerene, 0.875 part of tea tree oil, 1.125 parts of guaiacum essential oil, 1.375 parts of nutgrass flatsedge essential oil and 0.625 parts of sweet orange oil into the mixture in turn, stirring for 20min at 850rpm with a high speed stirrer, adding 72.5 parts deionized water, 0.75 part mandelic acid, 0.75 part ellagic acid, 0.75 part vitamin E, and 1.25 parts vitamin C, and continuously stirring at 540rpm for 10min, and adjusting the pH value to 5.5-6.2 with a small amount of baking soda to obtain a uniform and transparent liquid, namely the makeup-removing fragrant toner.

And (3) testing results: the obtained makeup-removing fragrant toner is uniform, transparent and stable; basic performance is grade 5; the fragrance releasing performance is 4.9 grades; the makeup removal performance was grade 4.9.

Comparative example 1

Drying olive, sweet potato, tomato and soybean (the mass ratio is 1.2:1:0.8:1) in an oven at 27-32 ℃ for 4 hours in advance, fully crushing in a medicine crusher, soaking in 75-95% ethanol water solution, adding a small amount of baking soda, the mass ratio of organisms containing softening solubilization factors, the ethanol water solution and the baking soda is 1:15:0.15, uniformly mixing the whole system, soaking for 24 hours, and filtering to obtain a primary extracting solution;

dialyzing and separating the primary extract obtained by filtering at room temperature by using a dialysis membrane with the molecular weight cutoff of 12000-16000 for 3-5 days, performing rotary evaporation and concentration treatment after dialysis, performing suction filtration by using filter paper with the aperture of 1-5 mu m, wherein the pump pressure is 0.02-0.06 MPa, freeze-drying the obtained filtrate, and performing ultrasonic dispersion on the filtrate in glycerol (the mass ratio of solid particles obtained after freeze-drying the filtrate to the glycerol is 1.5:10) to obtain a biomass softening solubilization factor;

stirring 5 parts of butanediol, 2 parts of squalene, 1.125 parts of isopropyl myristate, 0.75 part of phytosterol, 1.125 parts of soapberry saponin, 1.5 parts of N-hydroxyethyl lauryl glucamide and 72.5 parts of deionized water at the speed of 400rpm until the mixture is uniform, stable and completely dissolved, then adding 7.5 parts of biomass softening solubilization factor, 0.875 part of tea tree oil, 1.125 parts of guaiac wood essential oil, 1.375 parts of sedge essential oil and 0.625 part of sweet orange oil into the mixture in turn, stirring for 20min at 850rpm with a high speed stirrer, adding 72.5 parts deionized water, 0.75 part mandelic acid, 0.75 part ellagic acid, 0.75 part vitamin E, and 1.25 parts vitamin C, and continuously stirring at 540rpm for 10min, and adjusting the pH value to 5.5-6.2 with a small amount of baking soda to obtain a uniform and transparent liquid, namely the makeup-removing fragrant toner (compared with the toner obtained in example 1, no biomass moisturizing and ventilating factor is added).

And (3) testing results: the obtained makeup-removing fragrant toner is uniform, transparent and stable; basic performance is grade 2.0; the fragrance releasing performance is 4.6 grades; the makeup removal performance was grade 4.5.

Comparative example 2

Drying olive, sweet potato, tomato and soybean (the mass ratio is 1.2:1:0.8:1) in an oven at 27-32 ℃ for 4 hours in advance, fully crushing in a medicine crusher, soaking in 75-95% ethanol water solution, adding a small amount of baking soda, the mass ratio of organisms containing softening solubilization factors, the ethanol water solution and the baking soda is 1:15:0.15, uniformly mixing the whole system, soaking for 24 hours, and filtering to obtain a primary extracting solution;

dialyzing and separating the primary extract obtained by filtering at room temperature by using a dialysis membrane with the molecular weight cutoff of 12000-16000 for 3-5 days, performing rotary evaporation and concentration treatment after dialysis, performing suction filtration by using filter paper with the aperture of 1-5 mu m, wherein the pump pressure is 0.02-0.06 MPa, freeze-drying the obtained filtrate, and performing ultrasonic dispersion on the filtrate in glycerol (the mass ratio of solid particles obtained after freeze-drying the filtrate to the glycerol is 1.5:10) to obtain a biomass softening solubilization factor;

5 parts of butanediol, 2 parts of squalene, 0.5 part of N-hydroxyethyl laurylglucamide and 72.5 parts of deionized water are stirred at the speed of 400rpm until uniform and stable and complete dissolution is achieved, then 7.5 parts of biomass softening solubilization factor, 2.5 parts of ethylhexyl glycerol, 4.75 parts of hyaluronic acid, 1.25 parts of water-soluble fullerene, 0.875 part of tea tree oil, 1.125 parts of guaiacum essential oil, 1.375 parts of nutgrass flatsedge essential oil and 0.625 part of sweet orange oil are sequentially added into the mixture, a high-speed stirrer is used for stirring at 850rpm for 20min at the same time, at the moment, 72.5 parts of deionized water, 0.75 part of mandelic acid, 0.75 part of ellagic acid, 0.75 part of vitamin E and 1.25 parts of vitamin C are added, stirring is continued for 10min at 540rpm, a small amount of baking soda is used for regulating the pH value to be between 5.5 and 6.2, and then uniform transparent liquid, namely the makeup removing perfume toner (compared with the skin-friendly surfactant N-hydroxyethyl laurylglucamide used in example 1, and the amount added is reduced).

And (3) testing results: the obtained makeup-removing fragrant toner is uniform, transparent and stable; basic performance is grade 2.8; the fragrance releasing performance is 3.4 grade; the makeup removal performance was grade 2.3.

Comparative example 3

Drying olive, sweet potato, tomato and soybean (the mass ratio is 1.2:1:0.8:1) in an oven at 27-32 ℃ for 4 hours in advance, fully crushing in a medicine crusher, soaking in 75-95% ethanol water solution, adding a small amount of baking soda, the mass ratio of organisms containing softening solubilization factors, the ethanol water solution and the baking soda is 1:15:0.15, uniformly mixing the whole system, soaking for 24 hours, and filtering to obtain a primary extracting solution;

dialyzing and separating the primary extract obtained by filtering at room temperature by using a dialysis membrane with the molecular weight cutoff of 12000-16000 for 3-5 days, performing rotary evaporation and concentration treatment after dialysis, performing suction filtration by using filter paper with the aperture of 1-5 mu m, wherein the pump pressure is 0.02-0.06 MPa, freeze-drying the obtained filtrate, and performing ultrasonic dispersion on the filtrate in glycerol (the mass ratio of solid particles obtained after freeze-drying the filtrate to the glycerol is 1.5:10) to obtain a biomass softening solubilization factor;

stirring 5 parts of butanediol, 2 parts of squalene, 1.125 parts of isopropyl myristate, 0.75 part of phytosterol, 1.125 parts of soapberry saponin, 1.5 parts of N-hydroxyethyl lauryl glucamide and 72.5 parts of deionized water at the speed of 400rpm until the mixture is uniform, stable and completely dissolved, then adding 1.5 parts of biomass softening solubilization factor, 2.5 parts of ethylhexyl glycerin, 4.75 parts of hyaluronic acid, 1.25 parts of water-soluble fullerene, 0.875 part of tea tree oil, 1.125 parts of guaiacum essential oil, 1.375 parts of nutgrass flatsedge essential oil and 0.625 parts of sweet orange oil into the mixture in turn, stirring for 20min at 850rpm with a high speed stirrer, adding 72.5 parts deionized water, 0.75 part mandelic acid, 0.75 part ellagic acid, 0.75 part vitamin E, and 1.25 parts vitamin C, and continuously stirring at 540rpm for 10min, and adjusting the pH value to 5.5-6.2 with a small amount of baking soda to obtain a uniform and transparent liquid, namely the makeup-removing fragrant toner (compared with the example 1, the addition amount of the biomass softening solubilization factor is reduced).

And (3) testing results: the obtained makeup-removing fragrant toner is uniform, transparent and stable; basic performance was grade 3.2; the fragrance releasing performance is 3.9 grades; the makeup removal performance was grade 2.7.

Comparative example 4

Drying olive, sweet potato, tomato and soybean (the mass ratio is 1.2:1:0.8:1) in an oven at 27-32 ℃ for 4 hours in advance, fully crushing in a medicine crusher, soaking in 75-95% ethanol water solution, adding a small amount of baking soda, the mass ratio of organisms containing softening solubilization factors, the ethanol water solution and the baking soda is 1:15:0.15, uniformly mixing the whole system, soaking for 24 hours, and filtering to obtain a primary extracting solution;

dialyzing and separating the primary extract obtained by filtering at room temperature by using a dialysis membrane with the molecular weight cutoff of 12000-16000 for 3-5 days, performing rotary evaporation and concentration treatment after dialysis, performing suction filtration by using filter paper with the aperture of 1-5 mu m, wherein the pump pressure is 0.02-0.06 MPa, freeze-drying the obtained filtrate, and performing ultrasonic dispersion on the filtrate in glycerol (the mass ratio of solid particles obtained after freeze-drying the filtrate to the glycerol is 1.5:10) to obtain a biomass softening solubilization factor;

5 parts of butanediol, 2 parts of squalene, 1.125 parts of isopropyl myristate, 0.75 part of phytosterol, 1.125 parts of soapnut saponin, 1.5 parts of N-hydroxyethyl lauryl glucamide and 72.5 parts of deionized water are stirred at the speed of 400rpm until the components are uniform, stable and completely dissolved, then 7.5 parts of biomass softening solubilization factor, 2.5 parts of ethylhexyl glycerol, 4.75 parts of hyaluronic acid, 1.25 parts of water-soluble fullerene, 0.875 part of tea tree oil, 1.125 parts of guaiacum essential oil, 1.375 parts of sedum essential oil and 0.625 part of sweet orange oil are sequentially added into the mixture, and simultaneously a high-speed stirrer is used for stirring at 850rpm for 20min, then 72.5 parts of deionized water is added, the mixture is continuously stirred at 540rpm for 10min, and a small amount of sodium bicarbonate is used for regulating the pH value to be between 5.5 and 6.2, so as to obtain uniform transparent liquid, namely the makeup removing perfume toner (compared with example 1, natural nutrients are not added).

And (3) testing results: the obtained makeup-removing fragrant toner is uniform, transparent and stable; basic performance was grade 4.3; the fragrance releasing performance is 4.2 grade; the makeup removal performance was grade 3.1.

Comparative example 5

Drying olive, sweet potato, tomato and soybean (the mass ratio is 1.2:1:0.8:1) in an oven at 27-32 ℃ for 4 hours in advance, fully crushing in a medicine crusher, soaking in 75-95% ethanol water solution, adding a small amount of baking soda, the mass ratio of organisms containing softening solubilization factors, the ethanol water solution and the baking soda is 1:15:0.15, uniformly mixing the whole system, soaking for 24 hours, and filtering to obtain a primary extracting solution;

dialyzing and separating the primary extract obtained by filtering at room temperature by using a dialysis membrane with the molecular weight cutoff of 12000-16000 for 3-5 days, performing rotary evaporation and concentration treatment after dialysis, performing suction filtration by using filter paper with the aperture of 1-5 mu m, wherein the pump pressure is 0.02-0.06 MPa, freeze-drying the obtained filtrate, and performing ultrasonic dispersion on the filtrate in glycerol (the mass ratio of solid particles obtained after freeze-drying the filtrate to the glycerol is 1.5:10) to obtain a biomass softening solubilization factor;

5 parts of butanediol, 2 parts of squalene, 1.125 parts of isopropyl myristate, 0.75 part of phytosterol, 1.125 parts of soapnut saponin, 1.5 parts of N-hydroxyethyl lauryl glucamide and 72.5 parts of deionized water are stirred at the speed of 400rpm until the mixture is uniform and stable and is completely dissolved, then 7.5 parts of biomass softening solubilization factor, 2.5 parts of ethylhexyl glycerol, 4.75 parts of hyaluronic acid and 1.25 parts of water-soluble fullerene are sequentially added into the mixture, a high-speed stirrer is used for stirring at 850rpm for 20min, at the moment, 72.5 parts of deionized water, 0.75 part of mandelic acid, 0.75 part of ellagic acid, 0.75 part of vitamin E and 1.25 parts of vitamin C are added, the mixture is continuously stirred at 540rpm for 10min, and a small amount of baking soda is used for adjusting the pH value to be between 5.5 and 6.2, so as to obtain transparent liquid, namely the uniform makeup-removing perfume water (compared with the plant soothing essential oil not added in the example 1).

And (3) testing results: the obtained makeup-removing fragrant toner is uniform, transparent and stable; basic performance is class 4.4; the fragrance releasing performance is 1.7 grade; the makeup removal performance was grade 4.5.

Comparative example 6

Drying olive, sweet potato, tomato and soybean (the mass ratio is 1.2:1:0.8:1) in an oven at 27-32 ℃ for 4 hours in advance, fully crushing in a medicine crusher, soaking in 75-95% ethanol water solution, adding a small amount of baking soda, the mass ratio of organisms containing softening solubilization factors, the ethanol water solution and the baking soda is 1:15:0.15, uniformly mixing the whole system, soaking for 24 hours, and filtering to obtain a primary extracting solution;

dialyzing and separating the primary extract obtained by filtering at room temperature by using a dialysis membrane with the molecular weight cutoff of 12000-16000 for 3-5 days, performing rotary evaporation and concentration treatment after dialysis, performing suction filtration by using filter paper with the aperture of 1-5 mu m, wherein the pump pressure is 0.02-0.06 MPa, freeze-drying the obtained filtrate, and performing ultrasonic dispersion on the filtrate in glycerol (the mass ratio of solid particles obtained after freeze-drying the filtrate to the glycerol is 1.5:10) to obtain a biomass softening solubilization factor;

stirring 5 parts of butanediol, 2 parts of squalene and 145 parts of deionized water at the speed of 400rpm until the components are uniform and stable and are completely dissolved, sequentially adding 7.5 parts of biomass softening solubilization factor, 2.5 parts of ethylhexylglycerin, 4.75 parts of hyaluronic acid, 1.25 parts of water-soluble fullerene, 0.875 part of tea tree oil, 1.125 parts of guaiacum essential oil, 1.375 parts of sedum essential oil and 0.625 part of sweet orange oil into the mixture, stirring the mixture at 850rpm by using a high-speed stirrer for 20min, then adding 1.125 parts of isopropyl myristate, 0.75 part of phytosterol, 1.125 parts of sapindoside, 1.5 parts of N-hydroxyethyl lauryl glucamide, 0.75 part of mandelic acid, 0.75 part of ellagic acid, 0.75 part of vitamin E and 1.25 parts of vitamin C, continuously stirring the mixture at 540rpm for 10min, adjusting the pH value to be between 5.5 and 6.2 by using a small amount of sodium bicarbonate, and obtaining a uniform transparent cosmetic liquid (compared with the example of deionized water after 1,one-time of deionized water is added, and the order of addition of the skin-friendly surfactant is delayed).

And (3) testing results: the obtained makeup-removing fragrant toner is uniform, transparent and stable; the basic performance is grade 3.8; the fragrance releasing performance is 3.6 grade; the makeup removal performance was grade 3.9.

In conclusion, the removable fragrant toner adopts various natural biological-based environment-friendly components as main raw materials, is safe and mild, is skin-friendly and non-irritating, is moisture-retaining and breathable without being stuffy, reduces the phenomena of skin dryness, skin peeling and acne, has a deep cleaning effect of removing makeup while releasing fragrance, and combines the functions of the toner, perfume and the makeup remover into a whole, and the pH value of the toner is weak acid and close to that of human skin.

The makeup-removable fragrant toner has the moisturizing and ventilating effects derived from the comprehensive effects of the solvent, the biomass moisturizing and ventilating factors, the skin-friendly surfactant and the biomass softening and solubilizing factors: the solvent in reasonable proportion can provide sufficient moisture for skin and simultaneously slow down the evaporation of the moisture, and has the effect of absorbing the moisture in the air; the biomass moisturizing and air-permeable factor further strengthens the capability of retaining water on the skin, and simultaneously opens a channel for the respiration of skin pores, so that the skin pores are air-permeable and comfortable, and cutin is softened, so that the skin pores can be deeply cleaned; one end of each skin-friendly surfactant molecule is hydrophilic, and the other end of each skin-friendly surfactant molecule is hydrophobic, so that the skin-friendly surfactant molecules can deeply permeate into the epidermis layer, maintain the moisture required by the dermis layer of the skin after deep cleaning, contribute to the permeation and affinity of each effective component to the skin, and fully exert the moisture-retaining and water-locking effects of the effective components; the biomass softening and solubilizing factors can promote metabolism of skin cells, soften cutin and reduce water loss in skin. This fully explains the mechanism of the synergistic interaction of the four ingredients.

The solvent, the skin-friendly surfactant, the natural nutrient and the biomass softening solubilization factor of the makeup removable fragrant toner of the invention are added to endow the toner with a makeup removable function: the natural nutrients and the biomass softening and solubilizing factors can gently soften and remove part of the makeup powder and the cuticle, and the natural nutrients and the biomass softening and solubilizing factors are cooperated with the deep penetration cleaning effect of the skin-friendly surfactant and have the functions of strongly dissolving the makeup powder and separating the makeup powder from the skin by the solvent, so that the ideal makeup removing effect is achieved. This indicates that there is a synergistic effect between the four classes of ingredients.

According to the detachable fragrant toner, the addition of the biomass softening solubilization factor, the plant soothing essential oil and the skin-friendly surfactant endows the toner with a fragrance releasing effect: the biomass softening solubilization factor may contain certain essential oil components, a pleasant fragrance is obtained by the proper proportion of the biomass softening solubilization factor and the plant soothing essential oil, and the skin-friendly surfactant may have the function of fixing fragrance and delay the release speed of the fragrance, so that the three components also have a synergistic effect.

According to the detachable fragrant toner, deionized water is added twice during preparation, and a skin-friendly surfactant is added in the early stage, and experiments prove that only through the addition sequence and the proportion, the finally obtained toner has the emulsion type of oil-in-water, and only through the type of the detachable fragrant toner can the finally obtained toner be more stable, various functions can be fully exerted, otherwise, the effect is greatly reduced.

It should be noted that the above-mentioned embodiments are only for illustrating the technical solutions of the present invention and not for limiting, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions may be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention, which should be covered by the claims of the present invention.

Claims (9)

1. A makeup-removable fragrant toner is characterized in that: the makeup-removing fragrant toner comprises the following raw materials in parts by weight: 6-9 parts of biomass softening solubilization factors, 3-6 parts of skin-friendly surfactant, 7-10 parts of biomass moisturizing and air-permeable factors, 2.5-4.5 parts of natural nutrients, 3.5-4.5 parts of plant soothing essential oil and 146-158 parts of solvent.

2. The removable fragrant toner according to claim 1, wherein the biomass softening solubilization factor is prepared by:

drying organisms containing softening and solubilizing factors in an oven at 27-32 ℃ for 3-5 hours in advance, adding the dried organisms containing the softening and solubilizing factors into a medicine crusher, fully crushing, soaking in 75-95% ethanol water solution, adding a small amount of baking soda, uniformly mixing the whole system, soaking for 24 hours, and filtering to obtain a primary extracting solution, wherein the mass ratio of the organisms containing the softening and solubilizing factors to the ethanol water solution to the baking soda is 1: 10-20: 0.1-0.2;

and (2) dialyzing and separating the primary extract obtained by filtering at room temperature by using a dialysis membrane with the molecular weight cutoff of 12000-16000 for 3-5 days, performing rotary evaporation and concentration treatment after dialysis, performing suction filtration by using filter paper with the pore diameter of 1-5 mu m, wherein the pump pressure is 0.02-0.06 MPa, freeze-drying the obtained filtrate, and performing ultrasonic dispersion on the filtrate in glycerol (the mass ratio of solid particles obtained after freeze-drying the filtrate to the glycerol is 1-2: 10) to obtain the biomass softening solubilization factor.

3. The method for preparing biomass softening solubilization factors according to claim 2, characterized in that: the organism containing softening and solubilizing factors is a composition of three or more of olive, sweet potato, grapefruit, iris, tomato and soybean.

4. The removable fragrance toner of claim 1, wherein: the skin-friendly surfactant is a composition of isopropyl myristate, phytosterol, soapberry saponin and N-hydroxyethyl lauryl glucose amide.

5. The removable fragrance toner of claim 1, wherein: the biomass moisturizing and air-permeable factor is a composition of ethylhexyl glycerol, hyaluronic acid and water-soluble fullerene.

6. The removable fragrance toner of claim 1, wherein: the natural nutrient is a composition of mandelic acid, ellagic acid, vitamin E and vitamin C.

7. The removable fragrance toner of claim 1, wherein: the plant soothing essential oil is a composition of tea tree oil, guaiac wood essential oil, sedge essential oil and sweet orange oil.

8. The removable fragrance toner of claim 1, wherein: the solvent is a composition of deionized water, butanediol and squalene.

9. The preparation method of the removable fragrant toner according to any one of claims 1 to 9, characterized by comprising the following steps:

stirring 4.5-5.5 parts of butanediol, 1.5-2.5 parts of squalene, 0.75-1.5 parts of isopropyl myristate, 0.5-1 part of phytosterol, 0.75-1.5 parts of sapindus saponin, 1-2 parts of N-hydroxyethyl lauryl glucamide and 70-75 parts of deionized water at 380-420 rpm until uniform, stable and complete dissolution is achieved, sequentially adding 6-9 parts of biomass solubilizing factor, 2-3 parts of ethylhexyl glycerol, 4-5.5 parts of hyaluronic acid, 1-1.5 parts of water-soluble fullerene, 0.75-1 part of tea tree oil, 1-1.25 parts of guaiazuki essential oil, 1.25-1.5 parts of sedum essential oil, 0.5-0.75 part of sweet orange oil into a stirrer, stirring at 820-880 rpm for 17-23 min, adding 70-75 parts of deionized water, 0.5-1 part of nervonic acid, 0.5-1.5 parts of ellagic acid, 0.5-1.5 parts of tannic, 0.5-1.5 parts of vitamin E, 560-13-7 rpm, continuously stirring at 820-880 rpm, and (3) adjusting the pH value to be between 5.5 and 6.2 by using a small amount of baking soda to obtain uniform and transparent liquid, namely the makeup-removing fragrant toner.