CN111991253A - Sleep-aiding shower gel and preparation method thereof - Google Patents
Sleep-aiding shower gel and preparation method thereof Download PDFInfo
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- CN111991253A CN111991253A CN202010992909.5A CN202010992909A CN111991253A CN 111991253 A CN111991253 A CN 111991253A CN 202010992909 A CN202010992909 A CN 202010992909A CN 111991253 A CN111991253 A CN 111991253A
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- 238000002360 preparation method Methods 0.000 title abstract description 17
- 238000001879 gelation Methods 0.000 title description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 53
- 239000000284 extract Substances 0.000 claims abstract description 44
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 42
- 239000008367 deionised water Substances 0.000 claims abstract description 40
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 40
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims abstract description 38
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 36
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 claims abstract description 36
- 235000010254 Jasminum officinale Nutrition 0.000 claims abstract description 31
- 241000565359 Fraxinus chinensis Species 0.000 claims abstract description 24
- 239000000843 powder Substances 0.000 claims abstract description 24
- KWIUHFFTVRNATP-UHFFFAOYSA-N Betaine Natural products C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 claims abstract description 19
- KWIUHFFTVRNATP-UHFFFAOYSA-O N,N,N-trimethylglycinium Chemical compound C[N+](C)(C)CC(O)=O KWIUHFFTVRNATP-UHFFFAOYSA-O 0.000 claims abstract description 19
- 229960003237 betaine Drugs 0.000 claims abstract description 19
- GWTCIAGIKURVBJ-UHFFFAOYSA-L dipotassium;dodecyl phosphate Chemical compound [K+].[K+].CCCCCCCCCCCCOP([O-])([O-])=O GWTCIAGIKURVBJ-UHFFFAOYSA-L 0.000 claims abstract description 19
- ZUVCYFMOHFTGDM-UHFFFAOYSA-N hexadecyl dihydrogen phosphate Chemical compound CCCCCCCCCCCCCCCCOP(O)(O)=O ZUVCYFMOHFTGDM-UHFFFAOYSA-N 0.000 claims abstract description 19
- KRIXEEBVZRZHOS-UHFFFAOYSA-N tetradecyl dihydrogen phosphate Chemical compound CCCCCCCCCCCCCCOP(O)(O)=O KRIXEEBVZRZHOS-UHFFFAOYSA-N 0.000 claims abstract description 19
- 235000020767 valerian extract Nutrition 0.000 claims abstract description 19
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims abstract description 18
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims abstract description 18
- WOWHHFRSBJGXCM-UHFFFAOYSA-M cetyltrimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+](C)(C)C WOWHHFRSBJGXCM-UHFFFAOYSA-M 0.000 claims abstract description 18
- 229940041616 menthol Drugs 0.000 claims abstract description 18
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 18
- 229960004889 salicylic acid Drugs 0.000 claims abstract description 18
- 239000011780 sodium chloride Substances 0.000 claims abstract description 18
- 238000001035 drying Methods 0.000 claims abstract description 13
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 claims abstract description 12
- 238000003756 stirring Methods 0.000 claims description 66
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 36
- 241000207840 Jasminum Species 0.000 claims description 30
- 238000005303 weighing Methods 0.000 claims description 18
- TVACALAUIQMRDF-UHFFFAOYSA-N dodecyl dihydrogen phosphate Chemical group CCCCCCCCCCCCOP(O)(O)=O TVACALAUIQMRDF-UHFFFAOYSA-N 0.000 claims description 17
- 229960002668 sodium chloride Drugs 0.000 claims description 17
- 241000628997 Flos Species 0.000 claims description 12
- 239000000706 filtrate Substances 0.000 claims description 12
- 239000002244 precipitate Substances 0.000 claims description 12
- 230000001376 precipitating effect Effects 0.000 claims description 12
- 238000007873 sieving Methods 0.000 claims description 12
- 238000000967 suction filtration Methods 0.000 claims description 12
- 238000001291 vacuum drying Methods 0.000 claims description 12
- 238000005406 washing Methods 0.000 claims description 12
- TUNFSRHWOTWDNC-UHFFFAOYSA-N Myristic acid Natural products CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 claims description 7
- 244000178870 Lavandula angustifolia Species 0.000 claims description 6
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims description 6
- 244000126014 Valeriana officinalis Species 0.000 claims description 6
- 235000013832 Valeriana officinalis Nutrition 0.000 claims description 6
- 239000001102 lavandula vera Substances 0.000 claims description 6
- 235000018219 lavender Nutrition 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 235000016788 valerian Nutrition 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 5
- 239000006260 foam Substances 0.000 abstract description 11
- 230000000694 effects Effects 0.000 abstract description 10
- 239000005639 Lauric acid Substances 0.000 abstract description 4
- 230000002378 acidificating effect Effects 0.000 abstract description 2
- 239000006071 cream Substances 0.000 abstract description 2
- 230000007794 irritation Effects 0.000 abstract description 2
- 230000007774 longterm Effects 0.000 abstract description 2
- 240000005385 Jasminum sambac Species 0.000 abstract 1
- 210000003491 skin Anatomy 0.000 description 15
- 235000011187 glycerol Nutrition 0.000 description 14
- 238000004140 cleaning Methods 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 6
- 239000000047 product Substances 0.000 description 5
- 230000002195 synergetic effect Effects 0.000 description 3
- 238000010998 test method Methods 0.000 description 3
- 206010013786 Dry skin Diseases 0.000 description 2
- 230000006978 adaptation Effects 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000003385 bacteriostatic effect Effects 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 230000037336 dry skin Effects 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 238000011010 flushing procedure Methods 0.000 description 2
- 150000002632 lipids Chemical class 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000003860 sleep quality Effects 0.000 description 2
- 239000000344 soap Substances 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- TWJNQYPJQDRXPH-UHFFFAOYSA-N 2-cyanobenzohydrazide Chemical compound NNC(=O)C1=CC=CC=C1C#N TWJNQYPJQDRXPH-UHFFFAOYSA-N 0.000 description 1
- 235000021360 Myristic acid Nutrition 0.000 description 1
- 206010052428 Wound Diseases 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 238000003287 bathing Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 230000035876 healing Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- -1 monododecyl Chemical compound 0.000 description 1
- 230000008447 perception Effects 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 230000004622 sleep time Effects 0.000 description 1
- 210000000434 stratum corneum Anatomy 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P25/00—Drugs for disorders of the nervous system
- A61P25/20—Hypnotics; Sedatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
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- A61Q19/00—Preparations for care of the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Abstract
The invention discloses sleep-aiding shower gel and a preparation method thereof, wherein the sleep-aiding shower gel comprises the following raw materials in parts by weight: 200-235 parts of lauric acid, 60-68 parts of myristic acid, 100-118 parts of potassium monododecyl phosphate, 20-25 parts of hexadecyl phosphate betaine, monododecyl, 35-42 parts of tetradecyl phosphate, 10-15 parts of glycerol, 12-18 parts of hexadecyl trimethyl ammonium chloride, 5-7 parts of sodium chloride, 1-3 parts of jasmine flower extract, 1-3 parts of valerian extract, 1.5-2 parts of essence, 1-3 parts of fraxinus chinensis bark powder, 2.5-3.5 parts of menthol, 2-2.5 parts of salicylic acid and 550-650 parts of deionized water. The sleep-aiding shower gel has a good sleep-aiding effect; the skin care cream is acidic, mild, low in irritation, easy to wash, rich in foam, strong in foam texture, free of drying and peeling of the skin, and capable of protecting the skin after long-term use.
Description
Technical Field
The invention relates to the field of bath products, and particularly relates to sleep-aiding shower gel and a preparation method thereof.
Background
The shower gel is a common cleaning product for modern people, and the shower gel is mainly invented to replace the touch and efficacy of the traditional cleaning soap. With the continuous improvement of living standards, the demands and requirements of people on body bath products are higher and higher, the formula of the shower gel is also improved continuously, people not only need the shower gel to have rich foam, but also need the shower gel to have good cleaning capability and high mildness, the people have fresh and non-greasy skin feeling after bathing, and the shower gel also needs to have different efficacies, such as moisturizing, whitening, exfoliating and the like.
However, the currently used body wash has the following problems:
1. the currently used shower gel is alkaline, can destroy a skin lipid membrane with weak acidity on the surface of the skin while cleaning, can destroy the horny layer, can dry and peel the skin, and can cause wrinkles after being used for a long time;
2. has no sleep-aiding effect or has pungent smell causing discomfort;
3. the cleaning ability for removing stains is weaker, the foam is less, the foam texture is poor, and the skin care effect is avoided;
namely, the existing shower gel has poor comprehensive use performance.
Disclosure of Invention
Based on the situation, the invention aims to provide the sleep-aiding shower gel and the preparation method thereof, which can effectively solve the problems.
In order to solve the technical problems, the technical scheme provided by the invention is as follows:
the sleep-aiding shower gel comprises the following raw materials in parts by weight:
200-235 parts of dodecanoic acid,
60-68 parts of myristic acid,
100-118 parts of potassium monododecyl phosphate,
20-25 parts of hexadecyl phosphate betaine,
35 to 42 parts of monododecyl and tetradecyl phosphate,
10-15 parts of glycerol,
12-18 parts of hexadecyl trimethyl ammonium chloride,
5-7 parts of sodium chloride,
1-3 parts of jasmine flower extract,
1-3 parts of valerian extract,
1.5-2 parts of essence,
1-3 parts of fraxinus chinensis bark powder,
2.5 to 3.5 parts of menthol,
2-2.5 parts of salicylic acid,
550-650 parts of deionized water.
Preferably, the sleep-aiding shower gel comprises the following raw materials in parts by weight:
218 portions of dodecanoic acid,
64 parts of myristic acid,
109 parts of potassium monododecyl phosphate,
22.5 parts of hexadecyl phosphate betaine,
38.5 parts of monododecyl and tetradecyl phosphate,
12.5 parts of glycerol,
15 portions of hexadecyl trimethyl ammonium chloride,
6 portions of sodium chloride,
2 parts of jasmine flower extract,
2 parts of valerian extract,
1.75 parts of essence,
2 portions of Chinese ash bark powder,
3 portions of menthol,
2.25 portions of salicylic acid,
600 parts of deionized water.
Preferably, the preparation method of the jasmine flower extract comprises the following steps: weighing jasmine flowers, drying, crushing, sieving with a 100-mesh sieve, adding deionized water with the weight of 20-25 times that of the jasmine flowers, extracting for 2 hours at 74 ℃ under an ultrasonic condition, carrying out suction filtration, repeating for 3-5 times, and combining filtrates to obtain an extracting solution; slowly adding anhydrous ethanol into the extractive solution, slowly stirring to make ethanol concentration reach 82%, standing for 10h, centrifuging at 5000r/min for 10 min, precipitating to obtain centrifugal precipitate, centrifuging and washing for several times, and vacuum drying to obtain flos Jasmini sambac extract.
Preferably, the preparation method of the valerian extract comprises the following steps: weighing valerian, drying, crushing, sieving with a 100-mesh sieve, adding deionized water of 20-25 times, extracting at 76 ℃ for 2 hours, carrying out suction filtration, repeating for 3-5 times, and combining filtrates to obtain an extracting solution; slowly adding anhydrous ethanol into the extractive solution, slowly stirring to make ethanol concentration reach 78%, standing for 10 hr, centrifuging at 5000r/min for 10 min, precipitating to obtain centrifugal precipitate, centrifuging, washing for several times, and vacuum drying to obtain the rhizoma et radix Valerianae extract.
Preferably, the granularity of the fraxinus chinensis bark powder is 300-500 meshes.
Preferably, the essence is lavender essence.
The invention also provides a preparation method of the sleep-aiding shower gel, which comprises the following steps:
A. weighing the raw materials of the sleep-aiding shower gel according to parts by weight for later use;
B. firstly, putting dodecanoic acid, tetradecanoic acid, potassium monododecyl phosphate, hexadecyl phosphate betaine, monododecyl phosphate and tetradecyl phosphate into a stirring container, adding 4/5 deionized water, stirring and dispersing uniformly, adding glycerol, and continuing stirring until the viscosity is stable; adding flos Jasmini sambac extract, rhizoma et radix Valerianae extract and essence into another stirring container, adding 1/10 deionized water, stirring and dispersing; putting hexadecyl trimethyl ammonium chloride into another stirring container, adding 1/10 deionized water, and stirring and dispersing uniformly;
C. then mixing the three dispersed mixtures obtained in the step B, and stirring and dispersing uniformly;
D. and then sequentially adding the fraxinus chinensis bark powder, sodium chloride, menthol and salicylic acid, continuously stirring and uniformly dispersing to obtain the sleep-aiding shower gel.
Compared with the prior art, the invention has the following advantages and beneficial effects:
the sleep-aiding shower gel disclosed by the invention is prepared by selecting raw materials, optimizing the content of each raw material, and selecting lauric acid, myristic acid, potassium monododecyl phosphate, hexadecyl phosphate betaine, monododecyl, tetradecyl phosphate, glycerol, hexadecyl trimethyl ammonium chloride, sodium chloride, a jasmine flower extract, a valerian extract, essence, Chinese ash bark powder, menthol, salicylic acid and the like in a proper proportion, so that the advantages of the components are fully exerted, the components are mutually supplemented and mutually promoted, the prepared sleep-aiding shower gel has a good sleep-aiding effect, after a consumer uses the sleep-aiding shower gel, the sleep-aiding shower gel can shorten the sleep time and improve the sleep quality, and no irritating odor causing discomfort exists; the skin care cream is acidic, mild, low in irritation, easy to wash, good in stain removing capacity, rich in foam, strong in foam texture, free of damage to a skin lipid film with weak acidity on the surface of the skin and stratum corneum and dry and peeling of the skin when used for a long time, and can also play a skin care role.
The sleep-aiding shower gel disclosed by the invention is added with lauric acid, myristic acid, potassium monododecyl phosphate, hexadecyl phosphate betaine, monododecyl phosphate and tetradecyl phosphate in a proper proportion, wherein the lauric acid and the myristic acid are soap bases, and the potassium monododecyl phosphate, the hexadecyl phosphate betaine, the monododecyl phosphate and the tetradecyl phosphate are surfactants, so that the five surfactants are matched with each other to play a good synergistic effect.
The glycerin with a proper proportion is added into the sleep-aiding shower gel and is matched with other components of the sleep-aiding shower gel, so that the sleep-aiding shower gel has a good thickening effect.
The hexadecyl trimethyl ammonium chloride with a proper proportion is added into the sleep-aiding shower gel, and is matched with other components of the sleep-aiding shower gel to play a good synergistic effect, so that the sleep-aiding shower gel has a good conditioning effect, and the comprehensive use performance of the sleep-aiding shower gel is further improved.
The sleep-aiding shower gel disclosed by the invention is added with sodium chloride in a proper proportion, and is matched with menthol and salicylic acid in a proper proportion, so that the sleep-aiding shower gel is mutually matched to play a good antibacterial and bacteriostatic role, and the antibacterial and bacteriostatic performance of the sleep-aiding shower gel is improved.
The special jasmine flower extract, the special valerian extract and the essence are added in the sleep-aiding shower gel in a proper proportion, and the special jasmine flower extract, the special valerian extract and the essence are matched with each other to play a good synergistic effect, so that the sleep-aiding shower gel has a good sleep-aiding effect, can shorten the sleep-aiding time of a consumer after being used, improves the sleep quality, and does not have pungent smell causing discomfort.
The Chinese ash bark powder with a proper proportion is added into the sleep-aiding shower gel, so that the sleep-aiding shower gel has good foaming performance, is easy to disperse quickly and stably, can increase the friction effect with skin moderately, further improves the decontamination and cleaning capability of the sleep-aiding shower gel, has a good skin-care effect, can promote the healing of small wounds of the skin, and further improves the skin-care effect of the sleep-aiding shower gel for long-term use.
The preparation method has simple process and simple and convenient operation, and saves manpower and equipment cost.
Detailed Description
In order that those skilled in the art will better understand the technical solutions of the present invention, the following description of the preferred embodiments of the present invention is provided in connection with specific examples, which should not be construed as limiting the present patent.
The test methods or test methods described in the following examples are conventional methods unless otherwise specified; the reagents and materials, unless otherwise indicated, are conventionally obtained commercially or prepared by conventional methods.
Example 1:
the sleep-aiding shower gel comprises the following raw materials in parts by weight:
200-235 parts of dodecanoic acid,
60-68 parts of myristic acid,
100-118 parts of potassium monododecyl phosphate,
20-25 parts of hexadecyl phosphate betaine,
35 to 42 parts of monododecyl and tetradecyl phosphate,
10-15 parts of glycerol,
12-18 parts of hexadecyl trimethyl ammonium chloride,
5-7 parts of sodium chloride,
1-3 parts of jasmine flower extract,
1-3 parts of valerian extract,
1.5-2 parts of essence,
1-3 parts of fraxinus chinensis bark powder,
2.5 to 3.5 parts of menthol,
2-2.5 parts of salicylic acid,
550-650 parts of deionized water.
In this embodiment, the sleep-aiding shower gel preferably, but not limited to, comprises the following raw materials in parts by weight:
218 portions of dodecanoic acid,
64 parts of myristic acid,
109 parts of potassium monododecyl phosphate,
22.5 parts of hexadecyl phosphate betaine,
38.5 parts of monododecyl and tetradecyl phosphate,
12.5 parts of glycerol,
15 portions of hexadecyl trimethyl ammonium chloride,
6 portions of sodium chloride,
2 parts of jasmine flower extract,
2 parts of valerian extract,
1.75 parts of essence,
2 portions of Chinese ash bark powder,
3 portions of menthol,
2.25 portions of salicylic acid,
600 parts of deionized water.
In this embodiment, the preparation method of the jasmine extract is preferably, but not limited to, as follows: weighing jasmine flowers, drying, crushing, sieving with a 100-mesh sieve, adding deionized water with the weight of 20-25 times that of the jasmine flowers, extracting for 2 hours at 74 ℃ under an ultrasonic condition, carrying out suction filtration, repeating for 3-5 times, and combining filtrates to obtain an extracting solution; slowly adding anhydrous ethanol into the extractive solution, slowly stirring to make ethanol concentration reach 82%, standing for 10h, centrifuging at 5000r/min for 10 min, precipitating to obtain centrifugal precipitate, centrifuging and washing for several times, and vacuum drying to obtain flos Jasmini sambac extract.
In this embodiment, the valerian extracts are preferably prepared by, but not limited to, the following methods: weighing valerian, drying, crushing, sieving with a 100-mesh sieve, adding deionized water of 20-25 times, extracting at 76 ℃ for 2 hours, carrying out suction filtration, repeating for 3-5 times, and combining filtrates to obtain an extracting solution; slowly adding anhydrous ethanol into the extractive solution, slowly stirring to make ethanol concentration reach 78%, standing for 10 hr, centrifuging at 5000r/min for 10 min, precipitating to obtain centrifugal precipitate, centrifuging, washing for several times, and vacuum drying to obtain the rhizoma et radix Valerianae extract.
In this embodiment, the particle size of the fraxinus chinensis bark powder is preferably, but not limited to, 300 to 500 mesh.
In this embodiment, the essence is preferably, but not limited to, lavender essence.
The embodiment also provides a preparation method of the sleep-aiding shower gel, which comprises the following steps:
A. weighing the raw materials of the sleep-aiding shower gel according to parts by weight for later use;
B. firstly, putting dodecanoic acid, tetradecanoic acid, potassium monododecyl phosphate, hexadecyl phosphate betaine, monododecyl phosphate and tetradecyl phosphate into a stirring container, adding 4/5 deionized water, stirring and dispersing uniformly, adding glycerol, and continuing stirring until the viscosity is stable; adding flos Jasmini sambac extract, rhizoma et radix Valerianae extract and essence into another stirring container, adding 1/10 deionized water, stirring and dispersing; putting hexadecyl trimethyl ammonium chloride into another stirring container, adding 1/10 deionized water, and stirring and dispersing uniformly;
C. then mixing the three dispersed mixtures obtained in the step B, and stirring and dispersing uniformly;
D. and then sequentially adding the fraxinus chinensis bark powder, sodium chloride, menthol and salicylic acid, continuously stirring and uniformly dispersing to obtain the sleep-aiding shower gel.
Example 2:
the sleep-aiding shower gel comprises the following raw materials in parts by weight:
200 portions of dodecanoic acid,
60 parts of myristic acid,
100 portions of potassium monododecyl phosphate,
20 portions of hexadecyl phosphate betaine,
35 parts of monododecyl and tetradecyl phosphate,
10 portions of glycerol,
12 parts of hexadecyl trimethyl ammonium chloride,
5 parts of sodium chloride,
1 part of jasmine extract,
1 part of valerian extract,
1.5 parts of essence,
1 part of fraxinus chinensis bark powder,
2.5 portions of menthol,
2 portions of salicylic acid,
And 550 parts of deionized water.
In this example, the preparation method of the jasmine extract is as follows: weighing jasmine flowers, drying, crushing, sieving with a 100-mesh sieve, adding deionized water 20 times of the weight of the jasmine flowers, extracting for 2h at 74 ℃ under an ultrasonic condition, carrying out suction filtration, repeating for 5 times, and combining filtrates to obtain an extracting solution; slowly adding anhydrous ethanol into the extractive solution, slowly stirring to make ethanol concentration reach 82%, standing for 10h, centrifuging at 5000r/min for 10 min, precipitating to obtain centrifugal precipitate, centrifuging and washing for several times, and vacuum drying to obtain flos Jasmini sambac extract.
In this example, the valerian extracts were prepared as follows: weighing valerian, drying, crushing, sieving with a 100-mesh sieve, adding 20 times of deionized water, extracting at 76 ℃ for 2h, carrying out suction filtration, repeating for 5 times, and combining filtrates to obtain an extract; slowly adding anhydrous ethanol into the extractive solution, slowly stirring to make ethanol concentration reach 78%, standing for 10 hr, centrifuging at 5000r/min for 10 min, precipitating to obtain centrifugal precipitate, centrifuging, washing for several times, and vacuum drying to obtain the rhizoma et radix Valerianae extract.
In this embodiment, the particle size of the fraxinus chinensis bark powder is 300 mesh.
In this embodiment, the essence is lavender essence.
In this embodiment, the preparation method of the sleep-aiding shower gel comprises the following steps:
A. weighing the raw materials of the sleep-aiding shower gel according to parts by weight for later use;
B. firstly, putting dodecanoic acid, tetradecanoic acid, potassium monododecyl phosphate, hexadecyl phosphate betaine, monododecyl phosphate and tetradecyl phosphate into a stirring container, adding 4/5 deionized water, stirring and dispersing uniformly, adding glycerol, and continuing stirring until the viscosity is stable; adding flos Jasmini sambac extract, rhizoma et radix Valerianae extract and essence into another stirring container, adding 1/10 deionized water, stirring and dispersing; putting hexadecyl trimethyl ammonium chloride into another stirring container, adding 1/10 deionized water, and stirring and dispersing uniformly;
C. then mixing the three dispersed mixtures obtained in the step B, and stirring and dispersing uniformly;
D. and then sequentially adding the fraxinus chinensis bark powder, sodium chloride, menthol and salicylic acid, continuously stirring and uniformly dispersing to obtain the sleep-aiding shower gel.
Example 3:
the sleep-aiding shower gel comprises the following raw materials in parts by weight:
235 portions of dodecanoic acid,
68 parts of myristic acid,
118 parts of potassium monododecyl phosphate,
25 parts of hexadecyl phosphate betaine,
42 parts of monododecyl and tetradecyl phosphate,
15 portions of glycerol,
18 parts of hexadecyl trimethyl ammonium chloride,
7 parts of sodium chloride,
3 parts of jasmine flower extract,
Valerian extract 3 parts,
2 parts of essence,
3 portions of Chinese ash bark powder,
3.5 portions of menthol,
2.5 portions of salicylic acid,
650 parts of deionized water.
In this example, the preparation method of the jasmine extract is as follows: weighing jasmine flowers, drying, crushing, sieving with a 100-mesh sieve, adding deionized water 25 times of the weight of the jasmine flowers, extracting for 2 hours at 74 ℃ under an ultrasonic condition, carrying out suction filtration, repeating for 3 times, and combining filtrates to obtain an extracting solution; slowly adding anhydrous ethanol into the extractive solution, slowly stirring to make ethanol concentration reach 82%, standing for 10h, centrifuging at 5000r/min for 10 min, precipitating to obtain centrifugal precipitate, centrifuging and washing for several times, and vacuum drying to obtain flos Jasmini sambac extract.
In this example, the valerian extracts were prepared as follows: weighing valerian, drying, crushing, sieving with a 100-mesh sieve, adding 25 times of deionized water, extracting at 76 ℃ for 2h, carrying out suction filtration, repeating for 3 times, and combining filtrates to obtain an extracting solution; slowly adding anhydrous ethanol into the extractive solution, slowly stirring to make ethanol concentration reach 78%, standing for 10 hr, centrifuging at 5000r/min for 10 min, precipitating to obtain centrifugal precipitate, centrifuging, washing for several times, and vacuum drying to obtain the rhizoma et radix Valerianae extract.
In this embodiment, the particle size of the fraxinus chinensis bark powder is 500 mesh.
In this embodiment, the essence is lavender essence.
In this embodiment, the preparation method of the sleep-aiding shower gel comprises the following steps:
A. weighing the raw materials of the sleep-aiding shower gel according to parts by weight for later use;
B. firstly, putting dodecanoic acid, tetradecanoic acid, potassium monododecyl phosphate, hexadecyl phosphate betaine, monododecyl phosphate and tetradecyl phosphate into a stirring container, adding 4/5 deionized water, stirring and dispersing uniformly, adding glycerol, and continuing stirring until the viscosity is stable; adding flos Jasmini sambac extract, rhizoma et radix Valerianae extract and essence into another stirring container, adding 1/10 deionized water, stirring and dispersing; putting hexadecyl trimethyl ammonium chloride into another stirring container, adding 1/10 deionized water, and stirring and dispersing uniformly;
C. then mixing the three dispersed mixtures obtained in the step B, and stirring and dispersing uniformly;
D. and then sequentially adding the fraxinus chinensis bark powder, sodium chloride, menthol and salicylic acid, continuously stirring and uniformly dispersing to obtain the sleep-aiding shower gel.
Example 4:
the sleep-aiding shower gel comprises the following raw materials in parts by weight:
218 portions of dodecanoic acid,
64 parts of myristic acid,
109 parts of potassium monododecyl phosphate,
22.5 parts of hexadecyl phosphate betaine,
38.5 parts of monododecyl and tetradecyl phosphate,
12.5 parts of glycerol,
15 portions of hexadecyl trimethyl ammonium chloride,
6 portions of sodium chloride,
2 parts of jasmine flower extract,
2 parts of valerian extract,
1.75 parts of essence,
2 portions of Chinese ash bark powder,
3 portions of menthol,
2.25 portions of salicylic acid,
600 parts of deionized water.
In this example, the preparation method of the jasmine extract is as follows: weighing jasmine flowers, drying, crushing, sieving with a 100-mesh sieve, adding deionized water 23 times of the weight of the jasmine flowers, extracting for 2 hours at 74 ℃ under an ultrasonic condition, carrying out suction filtration, repeating for 4 times, and combining filtrates to obtain an extracting solution; slowly adding anhydrous ethanol into the extractive solution, slowly stirring to make ethanol concentration reach 82%, standing for 10h, centrifuging at 5000r/min for 10 min, precipitating to obtain centrifugal precipitate, centrifuging and washing for several times, and vacuum drying to obtain flos Jasmini sambac extract.
In this example, the valerian extracts were prepared as follows: weighing valerian, drying, crushing, sieving with a 100-mesh sieve, adding 23 times of deionized water, extracting at 76 ℃ for 2h, carrying out suction filtration, repeating for 4 times, and combining filtrates to obtain an extracting solution; slowly adding anhydrous ethanol into the extractive solution, slowly stirring to make ethanol concentration reach 78%, standing for 10 hr, centrifuging at 5000r/min for 10 min, precipitating to obtain centrifugal precipitate, centrifuging, washing for several times, and vacuum drying to obtain the rhizoma et radix Valerianae extract.
In this embodiment, the particle size of the fraxinus chinensis bark powder is 400 mesh.
In this embodiment, the essence is lavender essence.
In this embodiment, the preparation method of the sleep-aiding shower gel comprises the following steps:
A. weighing the raw materials of the sleep-aiding shower gel according to parts by weight for later use;
B. firstly, putting dodecanoic acid, tetradecanoic acid, potassium monododecyl phosphate, hexadecyl phosphate betaine, monododecyl phosphate and tetradecyl phosphate into a stirring container, adding 4/5 deionized water, stirring and dispersing uniformly, adding glycerol, and continuing stirring until the viscosity is stable; adding flos Jasmini sambac extract, rhizoma et radix Valerianae extract and essence into another stirring container, adding 1/10 deionized water, stirring and dispersing; putting hexadecyl trimethyl ammonium chloride into another stirring container, adding 1/10 deionized water, and stirring and dispersing uniformly;
C. then mixing the three dispersed mixtures obtained in the step B, and stirring and dispersing uniformly;
D. and then sequentially adding the fraxinus chinensis bark powder, sodium chloride, menthol and salicylic acid, continuously stirring and uniformly dispersing to obtain the sleep-aiding shower gel.
Comparative example:
chinese patent application publication No. CN 110897931A.
The sleeping aid shower gel obtained in examples 2 to 4 of the present invention and the comparative example were subjected to performance tests, and the test results are shown in table 1.
The test method comprises the following steps: carrying out use feeling, microorganism index and sensory index detection, wherein the evaluation method of the use feeling comprises the following steps: 100 testers (equal male and female, age range 18-65 years) are selected, 25 testers are extracted from each example and comparative example respectively, and blind tests are carried out on the examples and comparative examples. Each example and comparative example were measured in parallel 3 times. The testers evaluate the product according to the use feeling of the testers, and the product mainly comprises six directions of mildness, spreadability, rich foam, foam texture, water flushing skin feeling and dry skin feeling. The evaluation result is the average score of all testers, the higher the average score is, the better the effect is, the comprehensive scoring standard adopts 10 scores, 1 score is the worst, and 10 score is the best. The using method comprises the following steps: wetting the body; 20 g of the sample is put on one wet hand, the hands are soft, the body skin is coated evenly and bubbles are formed, and finally the body is washed clean by clear water and wiped dry.
TABLE 1
| Usage perception scoring | Example 2 | Example 3 | Example 4 | Comparative example |
| Mildness property | 9.4 | 9.7 | 9.6 | 9.3 |
| Spreadability | 9.3 | 9.6 | 9.5 | 9.5 |
| Rich foam feeling | 9.4 | 9.6 | 9.7 | 9.6 |
| Foam texture | 9.2 | 9.6 | 9.7 | 9.1 |
| Skin feel by flushing | 9.1 | 9.5 | 9.4 | 9.1 |
| Dry skin feel | 8.9 | 9.3 | 9.2 | 8.5 |
The above is only a preferred embodiment of the present invention, and it should be noted that the above preferred embodiment should not be considered as limiting the present invention, and the protection scope of the present invention should be subject to the scope defined by the claims. It will be apparent to those skilled in the art that various modifications and adaptations can be made without departing from the spirit and scope of the invention, and these modifications and adaptations should be considered within the scope of the invention.
Claims (7)
1. The sleep-aiding shower gel is characterized by comprising the following raw materials in parts by weight:
200-235 parts of dodecanoic acid,
60-68 parts of myristic acid,
100-118 parts of potassium monododecyl phosphate,
20-25 parts of hexadecyl phosphate betaine,
35 to 42 parts of monododecyl and tetradecyl phosphate,
10-15 parts of glycerol,
12-18 parts of hexadecyl trimethyl ammonium chloride,
5-7 parts of sodium chloride,
1-3 parts of jasmine flower extract,
1-3 parts of valerian extract,
1.5-2 parts of essence,
1-3 parts of fraxinus chinensis bark powder,
2.5 to 3.5 parts of menthol,
2-2.5 parts of salicylic acid,
550-650 parts of deionized water.
2. The sleep-aiding shower gel as claimed in claim 1, which is characterized by comprising the following raw materials in parts by weight:
218 portions of dodecanoic acid,
64 parts of myristic acid,
109 parts of potassium monododecyl phosphate,
22.5 parts of hexadecyl phosphate betaine,
38.5 parts of monododecyl and tetradecyl phosphate,
12.5 parts of glycerol,
15 portions of hexadecyl trimethyl ammonium chloride,
6 portions of sodium chloride,
2 parts of jasmine flower extract,
2 parts of valerian extract,
1.75 parts of essence,
2 portions of Chinese ash bark powder,
3 portions of menthol,
2.25 portions of salicylic acid,
600 parts of deionized water.
3. The sleep-aiding shower gel as claimed in claim 1, wherein the jasmine flower extract is prepared by the following method: weighing jasmine flowers, drying, crushing, sieving with a 100-mesh sieve, adding deionized water with the weight of 20-25 times that of the jasmine flowers, extracting for 2 hours at 74 ℃ under an ultrasonic condition, carrying out suction filtration, repeating for 3-5 times, and combining filtrates to obtain an extracting solution; slowly adding anhydrous ethanol into the extractive solution, slowly stirring to make ethanol concentration reach 82%, standing for 10h, centrifuging at 5000r/min for 10 min, precipitating to obtain centrifugal precipitate, centrifuging and washing for several times, and vacuum drying to obtain flos Jasmini sambac extract.
4. The sleep-aiding shower gel according to claim 1, wherein the valerian extract is prepared by the following method: weighing valerian, drying, crushing, sieving with a 100-mesh sieve, adding deionized water of 20-25 times, extracting at 76 ℃ for 2 hours, carrying out suction filtration, repeating for 3-5 times, and combining filtrates to obtain an extracting solution; slowly adding anhydrous ethanol into the extractive solution, slowly stirring to make ethanol concentration reach 78%, standing for 10 hr, centrifuging at 5000r/min for 10 min, precipitating to obtain centrifugal precipitate, centrifuging, washing for several times, and vacuum drying to obtain the rhizoma et radix Valerianae extract.
5. The sleep-aiding shower gel as claimed in claim 1, wherein the particle size of the fraxinus chinensis bark powder is 300-500 meshes.
6. The sleep-aiding shower gel according to claim 1, wherein the essence is lavender essence.
7. A method of preparing a sleep aid shower gel as claimed in any one of claims 1 to 6 comprising the steps of:
A. weighing the raw materials of the sleep-aiding shower gel according to parts by weight for later use;
B. firstly, putting dodecanoic acid, tetradecanoic acid, potassium monododecyl phosphate, hexadecyl phosphate betaine, monododecyl phosphate and tetradecyl phosphate into a stirring container, adding 4/5 deionized water, stirring and dispersing uniformly, adding glycerol, and continuing stirring until the viscosity is stable; adding flos Jasmini sambac extract, rhizoma et radix Valerianae extract and essence into another stirring container, adding 1/10 deionized water, stirring and dispersing; putting hexadecyl trimethyl ammonium chloride into another stirring container, adding 1/10 deionized water, and stirring and dispersing uniformly;
C. then mixing the three dispersed mixtures obtained in the step B, and stirring and dispersing uniformly;
D. and then sequentially adding the fraxinus chinensis bark powder, sodium chloride, menthol and salicylic acid, continuously stirring and uniformly dispersing to obtain the sleep-aiding shower gel.
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