CN111840155A - Foaming composition, preparation method and application thereof - Google Patents
Foaming composition, preparation method and application thereof Download PDFInfo
- Publication number
- CN111840155A CN111840155A CN202010662125.6A CN202010662125A CN111840155A CN 111840155 A CN111840155 A CN 111840155A CN 202010662125 A CN202010662125 A CN 202010662125A CN 111840155 A CN111840155 A CN 111840155A
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- silk
- foam
- foaming
- soapberry extract
- foaming composition
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Abstract
The invention provides foaming compositions, methods of making and uses thereof. The foaming composition comprises soapberry extract, hydrolyzed silk and silk collagen. The foaming composition of the embodiment of the invention has at least the following beneficial effects: the unique amino acid structure of the hydrolyzed silk enables hydrogen bonds in the hydrolyzed silk to be adsorbed on a foam interface, so that the foam distance is shortened, the loss of water is slowed down, the foamability of the soapberry extract is enhanced, and a certain foam stabilizing effect is achieved. And the small molecular structure of the silk collagen can form compact interface accumulation in the foam channel, so that charge repulsion among foams is weakened, and the effect of increasing the bubbles is achieved. After the two are compounded with the soapberry extract, obvious synergistic effect is achieved on the foamability and foam stability of the soapberry extract, and the foam amount is increased and is durable.
Description
Technical Field
The invention relates to the technical field of daily necessities, in particular to a foaming composition and a preparation method and application thereof.
Background
In the field of daily cosmetics, products such as shampoos, facial cleansers, body washes, hand sanitizers, etc., generally use various surfactants as foaming agents, such as sodium laureth sulfate, cocamidopropyl betaine, lauryl glucoside, etc. Such surfactants have excellent lathering properties, but are generally more irritating and may cause skin dryness, redness, and itching during use. For this reason, production researchers have attempted to screen mild, non-irritating foaming agents from natural products. The soapberry extract is a natural mild foaming agent which is generally accepted at present, and can effectively avoid anaphylactic reaction and the like caused by an artificial synthetic foaming agent. However, in the formulation of washing products, in order to provide some conditioning effects to the products besides the washing effects, some effect additives such as grease, cationic high molecular polymer and the like are usually added to be compounded with the foaming agent to achieve the corresponding effects. These performance additives can severely affect the foam properties of the blowing agent, leading to reduced, broken or non-durable foam. Therefore, there is a need to provide foaming compositions with improved foaming properties.
Disclosure of Invention
The present invention is directed to solving at least one of the problems of the prior art. Therefore, the invention provides a foaming composition with better foaming performance, and a preparation method and application thereof.
In a first aspect, one embodiment of the present invention provides a foaming composition comprising soapberry extract, hydrolyzed silk and silk collagen.
The foaming composition of the embodiment of the invention has at least the following beneficial effects:
the unique amino acid structure of the hydrolyzed silk enables hydrogen bonds in the hydrolyzed silk to be adsorbed on a foam interface, so that the foam distance is shortened, the loss of water is slowed down, the foamability of the soapberry extract is enhanced, and a certain foam stabilizing effect is achieved. And the small molecular structure of the silk collagen can form compact interface accumulation in the foam channel, so that charge repulsion among foams is weakened, and the effect of increasing the bubbles is achieved. After the two are compounded with the soapberry extract, obvious synergistic effect is achieved on the foamability and foam stability of the soapberry extract, and the foam amount is increased and is durable.
According to some embodiments of the foaming composition of the present invention, the mass ratio of the soapberry extract, the hydrolyzed silk and the silk collagen is (10-30): (1-20): (3-30). The hydrolyzed silk and the silk collagen according to the proportion can effectively improve the running-out property and the foam stability of the soapberry extract.
According to some embodiments of the foaming composition of the present invention, the mass ratio of the soapberry extract, the hydrolyzed silk and the silk collagen is (20-30): (5-15): (5-25).
In a second aspect, one embodiment of the present invention provides the use of a foaming composition for the preparation of a cleaning article. The foaming composition can ensure that the washing care product obtains better foaming property and foam stability, thereby meeting the requirement of the washing care product on the cleaning function.
According to some embodiments of the invention, the cleaning and care product may be a daily use chemical requiring a certain foaming property, including any of detergents, cleaners, and cosmetics, for example, products such as facial cleanser, bath lotion, hand sanitizer, shampoo, soap, and the like.
In a third aspect, an embodiment of the present invention provides a cleaning article comprising the above-described foaming composition and an acceptable vehicle. The washing and caring product added with the foaming composition can obtain better foaming property and foam stability, thereby enhancing the cleaning effect. Obviously, other materials which do not significantly adversely affect the lather performance of the personal care product may be added to the personal care product, depending on the application. For example, humectants, thickeners, antioxidants, preservatives, colors, fragrances, and the like are added.
A cleaning product according to some embodiments of the present invention includes the above-described foaming composition, as well as a moisturizing agent, a skin conditioning agent, a pH adjusting agent, and a preservative.
The laundry care article according to some embodiments of the present invention comprises the following components, based on the total weight of the laundry care article:
a cleaning article according to some embodiments of the present invention is selected from any one of a detergent, a cleanser and a cosmetic.
In a fourth aspect, an embodiment of the present invention provides a method of preparing a foaming composition, the method comprising the steps of:
mixing deionized water, a humectant, a skin conditioner and a pH regulator, and heating and stirring at 80-85 ℃ to obtain a first mixture;
cooling the first mixture to 50-60 ℃, and adding the soapberry extract for mixing to form a second mixture;
and (3) cooling the second mixture to 40-48 ℃, adding hydrolyzed silk, silk collagen and a preservative, mixing to obtain a third mixture, filtering and discharging.
By the above-mentioned order of addition and mixing and control of temperature conditions, various raw materials are sufficiently mixed, so that the foaming properties of the composition can be better exerted.
Detailed Description
The concept and technical effects of the present invention will be clearly and completely described below in conjunction with the embodiments to fully understand the objects, features and effects of the present invention. It is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments, and those skilled in the art can obtain other embodiments without inventive effort based on the embodiments of the present invention, and all embodiments are within the protection scope of the present invention.
Example 1
This example provides a laundry composition, which comprises the following specific components in table 1:
TABLE 1 laundry care composition Components
| Raw materials | Content (wt%) |
| Deionized water | 34.555 |
| Sapindus mukurossi extract | 25 |
| Silk collagen | 20 |
| Hydrolyzed silk | 10 |
| Glycerol | 10 |
| Allantoin | 0.15 |
| EDTA disodium salt | 0.2 |
| Kathon | 0.095 |
The preparation method of the washing and caring product composition comprises the following steps:
(1) weighing deionized water, glycerol, allantoin and EDTA disodium according to the formula, adding the weighed materials into a reaction pot, starting heating equipment, slowly stirring, and controlling the temperature to be 80-85 ℃. And after the material body is completely dissolved, forming a first mixture, preserving the heat for 15min, and cooling.
(2) Maintaining the temperature when the first mixture is cooled to 55 deg.C, adding corresponding amount of fructus Sapindi Mukouossi extract according to the above formula, stirring for 15min to form a second mixture, cooling.
(3) And (3) when the second mixture is cooled to 45 ℃, maintaining the temperature, adding corresponding amounts of silk collagen, hydrolyzed silk and kasons according to the formula, and stirring for 15min to form a third mixture. Sampling and inspecting various indexes after stirring, and filtering and discharging the materials by using a 200-mesh filter screen after the indexes are inspected to be qualified.
Example 2
Foaming Performance testing of different foaming compositions
The corresponding foaming compositions were formulated with water and cason according to table 2, respectively, and tested for foaming power. The specific method comprises the following steps: the foaming power at 40. + -. 1 ℃ was measured by the Ross-Miles method. First, 50mL of the foaming composition was placed in a foam meter, then 200mL of the test solution was poured vertically from the top of the foam meter, foam was generated by hitting the solution inside the foam meter, and the initial foam height was recorded at the time of initial and 5min, respectively, the initial foam height being indicative of the foaming fa (mm), the foam stability fs (mm) at the time of 5min, and the average of 3 times was taken as the foaming force of the test solution.
TABLE 2 foaming composition component constitution
| Case(s) | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 |
| Deionized water | 74.905 | 69.905 | 72.905 | 72.905 | 74.405 | 69.905 | 69.905 | 64.905 |
| Sapindus mukurossi extract | 25 | 25 | 25 | 25 | 25 | 25 | 25 | 25 |
| White mineral oil | / | 5 | / | / | / | / | / | / |
| Hexadecyl trimethyl ammonium chloride | / | / | 2 | / | / | / | / | / |
| Emulsified silicone oil | / | / | / | 2 | / | / | / | / |
| Guar hydroxypropyl trimethyl ammonium chloride | / | / | / | / | 0.5 | / | / | / |
| Hydrolyzed silk | / | / | / | / | / | 5 | / | 5 |
| Silk collagen | / | / | / | / | / | / | 5 | 5 |
| Kathon | 0.095 | 0.095 | 0.095 | 0.095 | 0.095 | 0.095 | 0.095 | 0.095 |
TABLE 3 foaming force test results for different foaming compositions
The results of the foaming force test are shown in table 3:
the foaming composition of case 1 was a single soapberry extract, and it was seen that the composition had abundant and long lasting foam.
The addition of white mineral oil to the foaming composition of case 2 greatly affects the foaming properties of the soapberry extract, and after the addition, the foam is reduced to disappear. This is probably because, after the addition of white mineral oil, an oil-water interface is formed, and a large amount of the soapberry extract is adsorbed to the oil-water interface, so that the concentration of the soapberry extract in water is reduced and foaming is difficult.
Cetyl trimethyl ammonium chloride in the foaming composition of case 3 also had a great influence on the foaming properties of the soapberry extract, probably because cetyl trimethyl ammonium chloride, as a cationic surfactant, combined with soapberry extract in water, resulted in a significant reduction of foam.
The foaming composition of case 4 employed silicone emulsion in a similar manner to that of case 2, because the formation of an oil-water interface reduced the concentration of soapberry extract in water and the foam was greatly reduced.
The guar hydroxypropyl trimonium chloride added to the foaming composition of case 5 is a high molecular polymer, and molecular chains of the polymer form a three-dimensional network structure in water, so that the movement resistance between water molecules is increased, the water loss speed between foams is reduced, and the stability of a foam film is improved to a certain extent. Thus, the composition has a poor foamability but still has a certain foam stability.
The foaming composition of case 6 has hydrolyzed silk added separately, and the unique amino acid structure of the hydrolyzed silk makes the hydrogen bond adsorbed onto the foam interface, so as to shorten the foam interval and slow down the water loss, and thus reach the effect of increasing and stabilizing foam. Thus, it can be seen that both the foamability and foam stability were improved to some extent compared with case 1.
The foaming composition of case 7 is added with silk collagen alone, and the small molecular structure of the silk collagen can form close interface accumulation in foam channels, so that the charge repulsion between foams is weakened, and although the foaming performance of the composition is not greatly influenced, the foaming effect is more obvious.
The foaming composition of case 8 was formulated with hydrolyzed silk and silk collagen on the basis of the soapberry extract, and the foaming and foam stabilizing properties of the composition were significantly improved compared to the independent addition of these two components: adding hydrolyzed silk alone, increasing foaming FA by 15mm, and increasing foam stability FS by 28 mm; with the addition of fibroin alone, the foaming FA increased by 5mm and the foam stability FS increased by 15 mm. After the hydrolyzed silk and the silk collagen are added simultaneously, the foamability FA is increased by 45mm, and the foam stability FS is increased by 59mm, which is far larger than the sum of the two independently added materials.
From the above results, it can be seen that the combination of hydrolyzed silk, silk collagen and soapberry extract can provide excellent foaming properties to the composition.
Example 3
Conditioning efficacy testing of laundry care compositions
The conditioning effect means that after the product is used, skin and hair can become soft and smooth. Since the hair is more visually indicative of the conditioning properties of the cleaning composition. Thus, hair was selected as the subject of the study in this experiment. The test method is as follows:
tress combing force test: the reduction in combing power before and after use of the cleaning composition in the dry state was compared by subjecting the cleaning composition to a dry combing test. The testing instrument is an MTT175 micro tension tester, and the hair quality of the used hair bundle is tested to be damaged hair quality, the weight of the hair bundle is 16g, the length is 23.5cm, and the width is 5.5 cm. Firstly, testing the combing work of the dry comb before using the sample for each hair bundle, then uniformly coating 1.5g of the sample on the hair bundle, massaging for 10min, then washing the hair cleanly according to a normal procedure, naturally drying the washed hair bundle, and measuring the combing work of the dry comb. Calculating the smoothness lifting rate according to the following formula:
the smoothness increasing rate is (carding work before use-carding work after use)/carding work before use is multiplied by 100 percent
TABLE 4 different toiletry composition Components
The conditioning efficacy was tested with the respective detergent compositions in table 4 and the results are shown in table 5.
TABLE 5 Conditioning efficacy test results
As can be seen from table 5, formula 1, as a placebo formula, had only weak conditioning efficacy on hair. While formulas 2-6 have certain conditioning effect on hair after other components are added. The conditioning effect of the washing composition prepared by compounding the hydrolyzed silk, the silk collagen and the soapberry extract is obviously superior to that of the combination of white mineral oil, hexadecyl trimethyl ammonium chloride, emulsified silicone oil, guar gum and the soapberry extract. The hydrolyzed silk and the silk collagen are proteins formed by various amino acids, are similar to the amino acid structure of hair keratin, and can be well combined and supplemented with hair according to the similar compatibility principle, so that damaged hair scales can be repaired, and hair roots and hair are nourished, thereby having excellent conditioning effect.
Example 4
Service test of different products
The foaming composition (soapberry extract: silk collagen: hydrolyzed silk mass ratio of 25: 20: 10) in the cleaning and care product composition of example 1 was mixed to prepare four different types of washing products, namely shampoo, facial cleanser, shower gel and hand sanitizer, according to the mixture ratio of table 6. Volunteers (50 persons in 18-38 years old and 50 persons in 38-58 years old) in different age groups are respectively selected as trial objects, the trial objects are used for washing hair, face, bath and hands once every two days for one month continuously, a test table is filled after trial, and each effect is graded from high to low according to 5-1 points.
TABLE 6 formulation of different detergent products
| Component (wt%)) | Shampoo liquid | Facial cleanser | Shower gel | Hand sanitizer |
| Deionized water | 54.605 | 59.605 | 76.605 | 84.605 |
| Foaming composition | 45 | 40 | 23 | 15 |
| Kathon | 0.095 | 0.095 | 0.095 | 0.095 |
| Essence | 0.3 | 0.3 | 0.3 | 0.3 |
TABLE 7 scoring results for different laundry products
The results of the various uses of the different detergent products are shown in table 7. As can be seen from the table, various washing products prepared from the foaming composition provided by the embodiment of the invention have rich foaming property, are mild and non-irritant, and have excellent conditioning and moisturizing effects. Therefore, the foaming composition can be processed into different washing and caring products, such as facial cleanser, shower gel, hand sanitizer, shampoo and the like, and the thorough cleaning of a target area is realized through excellent foaming property and foam stability.
The present invention has been described in detail with reference to the embodiments, but the present invention is not limited to the embodiments described above, and various changes can be made within the knowledge of those skilled in the art without departing from the gist of the present invention. Furthermore, the embodiments of the present invention and the features of the embodiments may be combined with each other without conflict.
Claims (10)
1. Foaming composition characterized by comprising soapberry extract, hydrolyzed silk and silk collagen.
2. The foaming composition according to claim 1, wherein the mass ratio of the soapberry extract, the hydrolyzed silk and the silk collagen is (10-30): (1-20): (3-30).
3. The foaming composition according to claim 1, wherein the mass ratio of the soapberry extract, the hydrolyzed silk and the silk collagen is (20-30): (5-15): (5-25).
4. Use of a foaming composition according to any one of claims 1 to 3 for the preparation of a cleaning composition.
5. Use according to claim 4, wherein the laundry article is selected from any of a detergent, a cleanser and a cosmetic.
6. A cleaning article characterized by comprising the foaming composition of any one of claims 1 to 3 and an acceptable excipient.
7. The cleaning product of claim 6 wherein said adjuvants include moisturizers, skin conditioners, pH modifiers and preservatives.
8. The toiletry product according to claim 6, comprising the following components, based on the total weight of the toiletry product:
9. the cleaning article according to any one of claims 6 to 8, wherein said cleaning article is selected from any one of a detergent, a cleanser and a cosmetic.
10. A process for the preparation of a cleaning article according to any of claims 6 to 9, comprising the steps of:
mixing deionized water, a humectant, a skin conditioner and a pH regulator, and heating and stirring at 80-85 ℃ to obtain a first mixture;
cooling the first mixture to 50-60 ℃, and adding the soapberry extract for mixing to form a second mixture;
and (3) cooling the second mixture to 40-48 ℃, adding hydrolyzed silk, silk collagen and a preservative, mixing to obtain a third mixture, filtering and discharging.
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| CN202010662125.6A CN111840155A (en) | 2020-07-10 | 2020-07-10 | Foaming composition, preparation method and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010662125.6A CN111840155A (en) | 2020-07-10 | 2020-07-10 | Foaming composition, preparation method and application thereof |
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2020
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