CN111792969A - Harmless treatment process of efficient organic fertilizer based on pig manure and chicken manure - Google Patents

Harmless treatment process of efficient organic fertilizer based on pig manure and chicken manure Download PDF

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Publication number
CN111792969A
CN111792969A CN202010541794.8A CN202010541794A CN111792969A CN 111792969 A CN111792969 A CN 111792969A CN 202010541794 A CN202010541794 A CN 202010541794A CN 111792969 A CN111792969 A CN 111792969A
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CN
China
Prior art keywords
organic fertilizer
treatment process
manure
mixture
product obtained
Prior art date
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Pending
Application number
CN202010541794.8A
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Chinese (zh)
Inventor
余成蛟
林萌萌
牛乾
刘玉
何小龙
董爱云
何文江
庞海龙
王小辉
范小龙
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Tianshui Maiji District Animal Husbandry And Veterinary Service Center
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Tianshui Maiji District Animal Husbandry And Veterinary Service Center
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Publication date
Application filed by Tianshui Maiji District Animal Husbandry And Veterinary Service Center filed Critical Tianshui Maiji District Animal Husbandry And Veterinary Service Center
Priority to CN202010541794.8A priority Critical patent/CN111792969A/en
Publication of CN111792969A publication Critical patent/CN111792969A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00Other inorganic fertilisers
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01GHORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G22/00Cultivation of specific crops or plants not otherwise provided for
    • A01G22/20Cereals
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • C05F17/20Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation using specific microorganisms or substances, e.g. enzymes, for activating or stimulating the treatment
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • C05F17/50Treatments combining two or more different biological or biochemical treatments, e.g. anaerobic and aerobic treatment or vermicomposting and aerobic treatment
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F3/00Fertilisers from human or animal excrements, e.g. manure
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/10Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
    • Y02A40/20Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

Abstract

The invention provides a harmless treatment process of a high-efficiency organic fertilizer based on pig manure and chicken manure. The invention obtains the technical effects of innocent treatment of pig manure and chicken manure and preparation of high-efficiency organic fertilizer by two-stage fermentation process. The harmless treatment process is simple and convenient to implement, the obtained organic fertilizer has excellent fertilizer efficiency, and is particularly suitable for cultivation of corn, the yield per mu of the corn is as high as 1200kg, and the utilization rate of nitrogen is 51-52%.

Description

Harmless treatment process of efficient organic fertilizer based on pig manure and chicken manure
Technical Field
The invention belongs to the technical field of agricultural waste treatment and organic fertilizer preparation, and particularly relates to a pig manure and chicken manure based harmless treatment process, an efficient organic fertilizer prepared by the process and application of the organic fertilizer in corn planting.
Background
In a large-scale farm, pigs and chickens are common raised animals, a large amount of excrement produced by the pigs and the chickens is an important problem troubling the farm owner, and if the pig and the chickens are not treated well, the pig and the chickens easily pollute the environment, breed germs and are not beneficial to the health of people and livestock.
At present, in the aspect of harmless treatment technology of pig manure and chicken manure, the harmless treatment technology is mostly carried out through processes of solid-liquid separation, anaerobic digestion, ammonia nitrogen removal and the like, such as Chinese patent CN 201210513731.7. In the biological treatment, specific microorganisms are usually used, and for example, CN200810058576.8 discloses a method for detoxifying human feces mainly by fermenting a mixture of water plants of water hyacinth and blue algae, and soil plants of straw plants by using yeasts, Bacillus subtilis and Lactobacillus of Candida species.
In the field of biological treatment, many techniques are currently available to achieve the detoxification of feces, but the resulting treated products have little or low utility. Therefore, if efficient organic fertilizers can be obtained through harmless treatment, the value of pig manure and chicken manure can be maximized.
Disclosure of Invention
Aiming at the defects and social requirements of the prior art, one of the purposes of the invention is to provide a harmless treatment process of a high-efficiency organic fertilizer based on pig manure and chicken manure, wherein the harmless treatment process comprises the following steps:
(1) collecting and mixing fresh pig manure and fresh chicken manure to obtain a mixture A, and performing filtrate operation and drying operation on the mixed manure; when filtrate operation is carried out, the collected excrement is suspended, the aperture of the used filter cloth or filter plate is based on that the solid excrement does not flow out but only liquid flows out, and the operation time is based on that no liquid drops drop after suspension is carried out for at least 3 minutes; the drying operation is carried out after the filtrate operation is carried out, and drying is carried out at the temperature of 50-80 ℃ until the moisture content is not more than 10%;
(2) culturing bacillus subtilis B9601-Y2, collecting thallus, and suspending in PBS buffer solution to make the thallus concentration be 1-2 × 103CFU/mL to obtain a treatment solution A, and uniformly spraying the treatment solution in the product obtained in the step (1) to enable the water content to reach 30-40%; the bacillus subtilis B9601-Y2 is preserved in the China general microbiological culture Collection center of the China Committee for culture Collection of microorganisms, and the preservation number is CGMCC NO. 0954;
(3) performing sealed fermentation on the product obtained in the step (2) at 25-30 ℃ for 3-5 days;
(4) collecting and mixing additional fresh pig manure and fresh chicken manure to obtain a mixture B, and adding the product obtained in the step (3), the crushed corn straw and kaolin into the mixture B and mixing; wherein the weight ratio of the product obtained in the step (3), the crushed corn straw, the kaolin and the mixture B is 1: 3-5: 25-35, and the mixture B is subjected to stack retting fermentation at the temperature of 20-30 ℃ for 12-15 days and is inoculated during fermentation.
Preferably, in the step (4), the weight ratio of the product obtained in the step (3), the crushed corn straw, the kaolin and the mixture B is 1:4:3: 35.
The invention also aims at the high-efficiency organic fertilizer obtained by the harmless treatment process.
Preferably, when the organic fertilizer is prepared by a harmless treatment process, humic acid is further added after the step (4); wherein the weight of the humic acid is 0.5-1.0% of the weight of the product obtained in the step (4).
In the research process, the invention discovers that when Bacillus subtilis ACCC03120 is used as a fermentation strain, the fertilizer efficiency of the obtained organic fertilizer is poor. Meanwhile, the inventor also finds that when kaolin is not adopted, the fermentation time is very long and reaches more than 20 days. Through a large amount of grope, the fact that a small amount of kaolin is added to be matched with the crushed corn straws is discovered accidentally, the fermentation time can be well shortened, and meanwhile, the obtained organic fertilizer is high in fertilizer efficiency and particularly suitable for planting of corn.
The invention has the beneficial effects that:
1. the harmless treatment process is simple and convenient to implement;
2. the organic fertilizer obtained by the invention has excellent fertilizer efficiency, is particularly suitable for the cultivation of corn, the yield per mu of the corn is as high as 1200kg, and the utilization rate of nitrogen is 51-52%.
Detailed Description
The present invention is described in detail below by way of examples, and it should be noted that the following examples are only for illustrating the present invention and should not be construed as limiting the scope of the present invention.
In the following examples, the term "fresh" means that the discharge is less than 1 day.
Both Bacillus subtilis ACCC03120 and Bacillus subtilis B9601-Y2 of the present invention are commercially available, and the two strains of bacteria were not screened by the present invention.
Example 1
(1) Collecting and mixing fresh pig manure and fresh chicken manure to obtain a mixture A, and performing filtrate operation and drying operation on the mixed manure; when filtrate operation is carried out, the collected excrement is suspended, the aperture of the used filter cloth or filter plate is based on that the solid excrement does not flow out but only liquid flows out, and the operation time is based on that no liquid drops drop after suspension is carried out for at least 3 minutes; the drying operation is carried out after the filtrate operation is carried out, and drying is carried out at the temperature of 50-80 ℃ until the moisture content is not more than 10%;
(2) culturing witheredBacillus subtilis B9601-Y2, collecting thallus, and suspending in PBS buffer solution to make thallus concentration 1-2 × 103CFU/mL to obtain a treatment solution A, and uniformly spraying the treatment solution in the product obtained in the step (1) to enable the water content to reach 30-40%; the bacillus subtilis B9601-Y2 is preserved in the China general microbiological culture Collection center of the China Committee for culture Collection of microorganisms, and the preservation number is CGMCC NO. 0954;
(3) performing sealed fermentation on the product obtained in the step (2) at 25-30 ℃ for 3-5 days;
(4) collecting and mixing additional fresh pig manure and fresh chicken manure to obtain a mixture B, and adding the product obtained in the step (3), the crushed corn straw and kaolin into the mixture B and mixing; wherein the weight ratio of the product obtained in the step (3), the crushed corn straw, the kaolin and the mixture B is 1:4:3:35, and the mixture B is subjected to stack retting fermentation for 12-15 days at the temperature of 20-30 ℃ and inoculated during fermentation.
(5) Humic acid is also added after the step (4); the weight of humic acid was 0.5% of the weight of the product obtained in step (4).
The obtained product is used as an organic fertilizer for planting corn, the fertilizing amount is 50 kg/mu, the yield reaches 1229 kg/mu, and the utilization rate of nitrogen is 51.7%.
Comparative example 1
For comparison, the organic fertilizer is prepared according to the method of example 1, only the Bacillus subtilis B9601-Y2 is replaced by Bacillus subtilis ACCC03120, the organic fertilizer is also used for planting corn, the fertilizing amount is 50 kg/mu, but the yield is only 924 kg/mu.
Comparative example 2
In contrast, the organic fertilizer prepared according to the method of example 1, only lacking kaolin, takes 24 days for fermentation to fully mature and produce an effect that can be used for corn planting. The effect of corn planting is that the yield per mu reaches over 800kg after the fertilizer is used.

Claims (6)

1. A harmless treatment process of a high-efficiency organic fertilizer based on pig manure and chicken manure is characterized by comprising the following steps:
(1) collecting and mixing fresh pig manure and fresh chicken manure to obtain a mixture A, and performing filtrate operation and drying operation on the mixed manure; when filtrate operation is carried out, the collected excrement is suspended, the aperture of the used filter cloth or filter plate is based on that the solid excrement does not flow out but only liquid flows out, and the operation time is based on that no liquid drops drop after suspension is carried out for at least 3 minutes; the drying operation is carried out after the filtrate operation is carried out, and drying is carried out at the temperature of 50-80 ℃ until the moisture content is not more than 10%;
(2) culturing bacillus subtilis B9601-Y2, collecting thallus, and suspending in PBS buffer solution to make the thallus concentration be 1-2 × 103CFU/mL to obtain a treatment solution A, and uniformly spraying the treatment solution in the product obtained in the step (1) to enable the water content to reach 30-40%; the bacillus subtilis B9601-Y2 is preserved in the China general microbiological culture Collection center of the China Committee for culture Collection of microorganisms, and the preservation number is CGMCC NO. 0954;
(3) performing sealed fermentation on the product obtained in the step (2) at 25-30 ℃ for 3-5 days;
(4) collecting and mixing additional fresh pig manure and fresh chicken manure to obtain a mixture B, and adding the product obtained in the step (3), the crushed corn straw and kaolin into the mixture B and mixing; wherein the weight ratio of the product obtained in the step (3), the crushed corn straw, the kaolin and the mixture B is 1: 3-5: 25-35, and the mixture B is subjected to stack retting fermentation at the temperature of 20-30 ℃ for 12-15 days and is inoculated during fermentation.
2. The innocent treatment process according to claim 1, wherein in the step (4), the weight ratio of the product obtained in the step (3), the crushed corn stalks, the kaolin and the mixture B is 1:4:3: 35.
3. A high-efficiency organic fertilizer obtained by the innocent treatment process of claim 1 or 2.
4. The organic fertilizer according to claim 3, wherein when the organic fertilizer is prepared by a harmless treatment process, humic acid is further added after step (4); wherein the weight of the humic acid is 0.5-1.0% of the weight of the product obtained in the step (4).
5. The application of the high-efficiency organic fertilizer obtained by the harmless treatment process of claim 3 in the aspect of planting corn.
6. The application of the high-efficiency organic fertilizer obtained by the harmless treatment process of claim 4 in the aspect of planting corn.
CN202010541794.8A 2020-06-15 2020-06-15 Harmless treatment process of efficient organic fertilizer based on pig manure and chicken manure Pending CN111792969A (en)

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CN202010541794.8A CN111792969A (en) 2020-06-15 2020-06-15 Harmless treatment process of efficient organic fertilizer based on pig manure and chicken manure

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Application Number Priority Date Filing Date Title
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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1554744A (en) * 2003-12-28 2004-12-15 何月秋 Bacillus subtilis strain
CN105110833A (en) * 2015-09-22 2015-12-02 宋春刚 Harm-less fast fermented bio-organic fertilizer and preparation method thereof
CN106431742A (en) * 2016-08-28 2017-02-22 天长市天兴园林绿化工程有限公司 High-yield green traditional Chinese medicine additive organic fertilizer used for lawn planting
CN107935721A (en) * 2017-12-12 2018-04-20 沈平瑞 A kind of preparation method of the selenium-enriched organic fertilizer of refuse reclamation
CN111115840A (en) * 2019-10-18 2020-05-08 河南省科学院生物研究所有限责任公司 Method for harmless treatment and resource recycling of waste of live pig farm

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1554744A (en) * 2003-12-28 2004-12-15 何月秋 Bacillus subtilis strain
CN105110833A (en) * 2015-09-22 2015-12-02 宋春刚 Harm-less fast fermented bio-organic fertilizer and preparation method thereof
CN106431742A (en) * 2016-08-28 2017-02-22 天长市天兴园林绿化工程有限公司 High-yield green traditional Chinese medicine additive organic fertilizer used for lawn planting
CN107935721A (en) * 2017-12-12 2018-04-20 沈平瑞 A kind of preparation method of the selenium-enriched organic fertilizer of refuse reclamation
CN111115840A (en) * 2019-10-18 2020-05-08 河南省科学院生物研究所有限责任公司 Method for harmless treatment and resource recycling of waste of live pig farm

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